CN107022112B - 一种炭黑表面石墨烯化的方法 - Google Patents
一种炭黑表面石墨烯化的方法 Download PDFInfo
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- CN107022112B CN107022112B CN201710330443.0A CN201710330443A CN107022112B CN 107022112 B CN107022112 B CN 107022112B CN 201710330443 A CN201710330443 A CN 201710330443A CN 107022112 B CN107022112 B CN 107022112B
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- Prior art keywords
- carbon black
- carbon
- black
- nitric acid
- blacksurface
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 229910002804 graphite Inorganic materials 0.000 title claims abstract description 29
- 239000010439 graphite Substances 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims abstract description 21
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 20
- 239000006229 carbon black Substances 0.000 claims abstract description 76
- 150000001721 carbon Chemical class 0.000 claims abstract description 27
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229910017604 nitric acid Inorganic materials 0.000 claims abstract description 15
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 239000003610 charcoal Substances 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 2
- 238000007254 oxidation reaction Methods 0.000 claims description 2
- 238000002604 ultrasonography Methods 0.000 claims description 2
- 229920001971 elastomer Polymers 0.000 abstract description 23
- 239000002131 composite material Substances 0.000 abstract description 20
- 238000006722 reduction reaction Methods 0.000 abstract description 11
- 239000013081 microcrystal Substances 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 4
- 241000872198 Serjania polyphylla Species 0.000 abstract 1
- 235000019241 carbon black Nutrition 0.000 description 66
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 34
- 239000008096 xylene Substances 0.000 description 16
- 238000002156 mixing Methods 0.000 description 9
- 238000001035 drying Methods 0.000 description 8
- 238000002360 preparation method Methods 0.000 description 8
- 230000009467 reduction Effects 0.000 description 8
- 244000043261 Hevea brasiliensis Species 0.000 description 7
- 239000007788 liquid Substances 0.000 description 7
- 229920003052 natural elastomer Polymers 0.000 description 7
- 229920001194 natural rubber Polymers 0.000 description 7
- 206010001497 Agitation Diseases 0.000 description 5
- 238000013019 agitation Methods 0.000 description 5
- 238000001704 evaporation Methods 0.000 description 5
- 230000008020 evaporation Effects 0.000 description 5
- 239000000945 filler Substances 0.000 description 5
- 239000006185 dispersion Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000011521 glass Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 229910052573 porcelain Inorganic materials 0.000 description 4
- 230000003014 reinforcing effect Effects 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 125000000524 functional group Chemical group 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 241000446313 Lamella Species 0.000 description 1
- 238000005411 Van der Waals force Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229910021389 graphene Inorganic materials 0.000 description 1
- 229910021385 hard carbon Inorganic materials 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/02—Ingredients treated with inorganic substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/04—Carbon
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/44—Carbon
- C09C1/48—Carbon black
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/06—Treatment with inorganic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710330443.0A CN107022112B (zh) | 2017-05-11 | 2017-05-11 | 一种炭黑表面石墨烯化的方法 |
Applications Claiming Priority (1)
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CN201710330443.0A CN107022112B (zh) | 2017-05-11 | 2017-05-11 | 一种炭黑表面石墨烯化的方法 |
Publications (2)
Publication Number | Publication Date |
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CN107022112A CN107022112A (zh) | 2017-08-08 |
CN107022112B true CN107022112B (zh) | 2018-10-09 |
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Family Applications (1)
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CN201710330443.0A Active CN107022112B (zh) | 2017-05-11 | 2017-05-11 | 一种炭黑表面石墨烯化的方法 |
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CN (1) | CN107022112B (zh) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109250707B (zh) * | 2018-11-30 | 2020-05-05 | 浙江农林大学 | 一种利用废旧轮胎制备的石墨烯材料及制备方法 |
CN109880237A (zh) * | 2019-01-28 | 2019-06-14 | 芜湖航天特种电缆厂股份有限公司 | 耐高温高韧性电缆及其制备方法 |
US11653646B2 (en) | 2019-04-01 | 2023-05-23 | Vulpes Agricultural Corp. | Bifunctional plant promoter and preparation thereof |
CN113150579A (zh) * | 2021-03-24 | 2021-07-23 | 茂名环星新材料股份有限公司 | 一种去除炭黑中杂质的方法及其应用 |
CN113307523A (zh) * | 2021-06-01 | 2021-08-27 | 安徽德瑞新材料科技有限公司 | 一种制备溶水性炭黑的方法、溶水性炭黑及其应用 |
CN114591645B (zh) * | 2022-03-04 | 2023-02-17 | 中国人民解放军火箭军工程大学 | 碳基吸波涂料、其制备方法和蜂窝夹层结构复合吸波材料 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3226244A (en) * | 1961-12-15 | 1965-12-28 | Cabot Corp | Process for making high color carbon black pigments |
US3306761A (en) * | 1963-04-26 | 1967-02-28 | Phillips Petroleum Co | Controlled partial oxidation of carbon black with ammonium nitrate, preferably in the presence of ammonium, alkali metal, and alkaline earth metal halides |
JP2004168898A (ja) * | 2002-11-20 | 2004-06-17 | Mitsubishi Chemicals Corp | カーボンブラックの表面処理方法 |
JP2005120223A (ja) * | 2003-10-16 | 2005-05-12 | Mitsubishi Chemicals Corp | カーボンブラック |
CN104151877A (zh) * | 2014-08-08 | 2014-11-19 | 四川理工学院 | 一种普通炭黑改性为色素炭黑的方法 |
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2017
- 2017-05-11 CN CN201710330443.0A patent/CN107022112B/zh active Active
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Effective date of registration: 20240112 Address after: Room 602, Unit D, Building B3, Fenglu Xintiandi, Nanchang Economic and Technological Development Zone, Nanchang City, Jiangxi Province, 330000 Patentee after: Jiangxi Liangben Information Technology Co.,Ltd. Address before: 643000 Huidong learning street 180, Zigong, Sichuan Patentee before: Sichuan University of Light Chemical Technology |
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