CN107007726A - A kind of hemorrhoids hemostasia liniment and preparation method thereof - Google Patents
A kind of hemorrhoids hemostasia liniment and preparation method thereof Download PDFInfo
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- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/80—Scrophulariaceae (Figwort family)
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- A61K2236/30—Extraction of the material
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- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A61K2236/30—Extraction of the material
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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Abstract
The invention discloses a kind of hemorrhoids hemostasia liniment, the raw material composition per 100mL hemorrhoids hemostasia liniments is as follows：The 83mL of d-Bomeol liquid 79, the 5mL of turpentine oil 4, the 5g of natural borneol 4, remaining is auxiliary agent；The auxiliary agent is made up of the raw material below according to parts by weight：11 14 parts of prepared rhizome of rehmannia, 59 parts of paris polyphylla.The invention also discloses the preparation method of the hemorrhoids hemostasia liniment.Hemorrhoids hemostasia liniment prepared by the present invention has the effects such as detumescence, analgesic, hemostasis, can effectively treat hemorrhoid hemorrhage, because for externally applied liniment, can go directly focus, and therapeutic effect is good, easy to use.
Description
Technical field
The present invention relates to technical field of traditional Chinese medicines, specifically a kind of hemorrhoids hemostasia liniment and preparation method thereof.
Background technology
Hemorrhoid are clinical common frdquently encountered diseases, and the incidence of disease of hemorrhoid accounts for 87.3% in whole anorectal disease, and is mainly in into
Year people, brings great pain, especially hemorrhagic hemorrhoid, harm to the human body is larger, and severe patient can be caused to many patients
Severe blood loss anemia, unhealthful and work.Therefore, the effective formula and drug for finding treatment hemorrhoid is preventing and treating anorectal disease
One important topic.
Clinically the medicine of conventional treatment hemorrhoid has a lot, there is tablet, capsule, granule, powder, suppository etc., these
Medicine generally existing curative effect is unsatisfactory, and prescription is complicated, or expensive defect, influences clinical practice.
The content of the invention
It is an object of the invention to provide a kind of hemorrhoids hemostasia liniment and preparation method thereof, to solve in above-mentioned background technology
The problem of proposition.
To achieve the above object, the present invention provides following technical scheme：
A kind of hemorrhoids hemostasia liniment, the raw material composition per 100mL hemorrhoids hemostasia liniments is as follows：D-Bomeol liquid 79-83mL,
Turpentine oil 4-5mL, natural borneol 4-5g, remaining is auxiliary agent；The auxiliary agent is made up of the raw material below according to parts by weight：Prepared rhizome of rehmannia
11-14 parts, 5-9 parts of paris polyphylla.
It is used as further scheme of the invention：Raw material composition per 100mL hemorrhoids hemostasia liniments is as follows：D-Bomeol liquid
81mL, turpentine oil 4.5mL, natural borneol 4.5g, remaining is auxiliary agent；The auxiliary agent is made up of the raw material below according to parts by weight：
13 parts of prepared rhizome of rehmannia, 7 parts of paris polyphylla.
It is used as further scheme of the invention：The d-Bomeol liquid is passed through using the fresh branches and leaves of canella borneol camphor tree
Extraction is processed into.
The preparation method of the hemorrhoids hemostasia liniment, step is as follows：
1) paris polyphylla is weighed, is cleaned, drying is ground, and adds vinegar, after stirring, and is stood 1-2h, is placed into sand
In pot, slow fire is heated to vinegar and is evaporated, and stops heating, and cooling obtains paris polyphylla powder；
2) prepared rhizome of rehmannia is weighed, is cleaned, is dried, is crushed, 30-50 mesh sieves are crossed, paris polyphylla powder is then added, is well mixed
Afterwards, mixture is obtained；
3) mixture is put into container, adds the alcoholic solution of 10-12 times of weight, soak 2-3h, heating and refluxing extraction
1-2h, obtains an extract solution and once extracts residue, collect an extract solution, will once extract residue and add 2-5 times again
The alcoholic solution of weight, soaks 1-2h, ultrasonic wave extraction 50-60min, obtains secondary raffinate and second extraction residue, collects
Secondary raffinate, an extract solution and secondary raffinate is merged, filtering, is obtained and is extracted total liquid, standby；
4) will extract total liquid and be concentrated by evaporation is relative density is 1.27-1.30 at 60 DEG C lotion, and lotion is added into 3 times
In the alcoholic solution of weight, stir evenly, stand 24-30h, filtration takes filtrate, you can obtain auxiliary agent；
5) d-Bomeol liquid, turpentine oil, natural borneol and auxiliary agent are taken according to formula, be well mixed, produce hemorrhoids hemostasia wiping
Agent.
It is used as further scheme of the invention：Step 1) in, the addition of the vinegar and the weight phase of paris polyphylla
Together.
It is used as further scheme of the invention：The alcoholic solution is the alcohol water blend of volumetric concentration 80%.
It is used as further scheme of the invention：Step 3) in, the ultrasonic wave extraction power is 1100W.
Compared with prior art, the beneficial effects of the invention are as follows：
Hemorrhoids hemostasia liniment prepared by the present invention has the effects such as detumescence, analgesic, hemostasis, can effectively treat hemorrhoid and go out
Blood, because for externally applied liniment, can go directly focus, and therapeutic effect is good, easy to use；Hemorrhoids hemostasia liniment prepared by the present invention,
Formula is simple, with low cost, can promote the use of on a large scale.
Embodiment
Technical scheme is described in more detail with reference to embodiment.
Embodiment 1
A kind of hemorrhoids hemostasia liniment, the raw material composition per 100mL hemorrhoids hemostasia liniments is as follows：D-Bomeol liquid 79mL, pine
Fuel-economizing 5mL, natural borneol 5g, remaining is auxiliary agent；The auxiliary agent is made up of the raw material below according to parts by weight：11 parts of prepared rhizome of rehmannia,
5 parts of paris polyphylla.Wherein, the d-Bomeol liquid uses the fresh branches and leaves of canella borneol camphor tree are extracted to be processed into.
In the present embodiment, the preparation method of the hemorrhoids hemostasia liniment, step is as follows：
1) paris polyphylla is weighed, is cleaned, drying is ground, and adds vinegar, after stirring, and is stood 1h, is placed into marmite
In, slow fire is heated to vinegar and is evaporated, stop heating, cooling, obtain paris polyphylla powder, wherein, the addition of the vinegar with
The weight of paris polyphylla is identical；
2) prepared rhizome of rehmannia is weighed, is cleaned, is dried, is crushed, 30 mesh sieves are crossed, paris polyphylla powder is then added, after being well mixed,
Obtain mixture；
3) mixture is put into container, adds the alcoholic solution of 10 times of weight, soaked 2h, heating and refluxing extraction 1h, obtain
Obtain an extract solution and once extract residue, collect an extract solution, will once extract the alcohol that residue adds 2 times of weight again
Solution, soaks 1h, ultrasonic wave extraction 50min, obtains secondary raffinate and second extraction residue, secondary raffinate is collected, by one
Secondary extract solution and secondary raffinate merge, filtering, obtain and extract total liquid, standby, wherein, the ultrasonic wave extraction power is
1100W；
4) will extract total liquid and be concentrated by evaporation is relative density is 1.27 at 60 DEG C lotion, and lotion is added into 3 times of weight
Alcoholic solution in, stir evenly, stand 24h, filtration, take filtrate, you can obtain auxiliary agent；
5) d-Bomeol liquid, turpentine oil, natural borneol and auxiliary agent are taken according to formula, be well mixed, produce hemorrhoids hemostasia wiping
Agent.
Above-mentioned alcoholic solution is the alcohol water blend of volumetric concentration 80%.
Embodiment 2
A kind of hemorrhoids hemostasia liniment, the raw material composition per 100mL hemorrhoids hemostasia liniments is as follows：D-Bomeol liquid 83mL, pine
Fuel-economizing 4mL, natural borneol 4g, remaining is auxiliary agent；The auxiliary agent is made up of the raw material below according to parts by weight：12 parts of prepared rhizome of rehmannia,
6 parts of paris polyphylla.Wherein, the d-Bomeol liquid uses the fresh branches and leaves of canella borneol camphor tree are extracted to be processed into.
In the present embodiment, the preparation method of the hemorrhoids hemostasia liniment, step is as follows：
1) paris polyphylla is weighed, is cleaned, drying is ground, and adds vinegar, after stirring, and is stood 1.5h, is placed into sand
In pot, slow fire is heated to vinegar and is evaporated, and stops heating, and cooling obtains paris polyphylla powder, wherein, the addition of the vinegar
It is identical with the weight of paris polyphylla；
2) prepared rhizome of rehmannia is weighed, is cleaned, is dried, is crushed, 35 mesh sieves are crossed, paris polyphylla powder is then added, after being well mixed,
Obtain mixture；
3) mixture is put into container, adds the alcoholic solution of 10 times of weight, soak 2.5h, heating and refluxing extraction 1h,
Obtain an extract solution and once extract residue, collect an extract solution, will once extract the wine that residue adds 3 times of weight again
Smart solution, soaks 1.5h, ultrasonic wave extraction 52min, obtains secondary raffinate and second extraction residue, collects secondary raffinate,
Extract solution and secondary raffinate are merged, filtering, obtain and extract total liquid, it is standby, wherein, the ultrasonic wave extraction power is
1100W；
4) will extract total liquid and be concentrated by evaporation is relative density is 1.28 at 60 DEG C lotion, and lotion is added into 3 times of weight
Alcoholic solution in, stir evenly, stand 25h, filtration, take filtrate, you can obtain auxiliary agent；
5) d-Bomeol liquid, turpentine oil, natural borneol and auxiliary agent are taken according to formula, be well mixed, produce hemorrhoids hemostasia wiping
Agent.
Above-mentioned alcoholic solution is the alcohol water blend of volumetric concentration 80%.
Embodiment 3
A kind of hemorrhoids hemostasia liniment, the raw material composition per 100mL hemorrhoids hemostasia liniments is as follows：D-Bomeol liquid 81mL, pine
Fuel-economizing 4.5mL, natural borneol 4.5g, remaining is auxiliary agent；The auxiliary agent is made up of the raw material below according to parts by weight：Prepared rhizome of rehmannia 13
Part, 7 parts of paris polyphylla.Wherein, the d-Bomeol liquid is made using the extracted processing of fresh branches and leaves of canella borneol camphor tree
Into.
In the present embodiment, the preparation method of the hemorrhoids hemostasia liniment, step is as follows：
1) paris polyphylla is weighed, is cleaned, drying is ground, and adds vinegar, after stirring, and is stood 1.5h, is placed into sand
In pot, slow fire is heated to vinegar and is evaporated, and stops heating, and cooling obtains paris polyphylla powder, wherein, the addition of the vinegar
It is identical with the weight of paris polyphylla；
2) prepared rhizome of rehmannia is weighed, is cleaned, is dried, is crushed, 40 mesh sieves are crossed, paris polyphylla powder is then added, after being well mixed,
Obtain mixture；
3) mixture is put into container, adds the alcoholic solution of 11 times of weight, soak 2.5h, heating and refluxing extraction
1.5h, obtains an extract solution and once extracts residue, collect an extract solution, will once extract residue and add 4 times of weights again
The alcoholic solution of amount, soaks 1.5h, ultrasonic wave extraction 55min, obtains secondary raffinate and second extraction residue, collects secondary carry
Liquid is taken, an extract solution and secondary raffinate are merged, filtering, obtains and extracts total liquid, it is standby, wherein, the ultrasonic wave extraction
Power is 1100W；
4) will extract total liquid and be concentrated by evaporation is relative density is 1.28 at 60 DEG C lotion, and lotion is added into 3 times of weight
Alcoholic solution in, stir evenly, stand 28h, filtration, take filtrate, you can obtain auxiliary agent；
5) d-Bomeol liquid, turpentine oil, natural borneol and auxiliary agent are taken according to formula, be well mixed, produce hemorrhoids hemostasia wiping
Agent.
Above-mentioned alcoholic solution is the alcohol water blend of volumetric concentration 80%.
Embodiment 4
A kind of hemorrhoids hemostasia liniment, the raw material composition per 100mL hemorrhoids hemostasia liniments is as follows：D-Bomeol liquid 80mL, pine
Fuel-economizing 4mL, natural borneol 5g, remaining is auxiliary agent；The auxiliary agent is made up of the raw material below according to parts by weight：13 parts of prepared rhizome of rehmannia,
7 parts of paris polyphylla.Wherein, the d-Bomeol liquid uses the fresh branches and leaves of canella borneol camphor tree are extracted to be processed into.
In the present embodiment, the preparation method of the hemorrhoids hemostasia liniment, step is as follows：
1) paris polyphylla is weighed, is cleaned, drying is ground, and adds vinegar, after stirring, and is stood 2h, is placed into marmite
In, slow fire is heated to vinegar and is evaporated, stop heating, cooling, obtain paris polyphylla powder, wherein, the addition of the vinegar with
The weight of paris polyphylla is identical；
2) prepared rhizome of rehmannia is weighed, is cleaned, is dried, is crushed, 45 mesh sieves are crossed, paris polyphylla powder is then added, after being well mixed,
Obtain mixture；
3) mixture is put into container, adds the alcoholic solution of 12 times of weight, soak 2.5h, heating and refluxing extraction 2h,
Obtain an extract solution and once extract residue, collect an extract solution, will once extract the wine that residue adds 4 times of weight again
Smart solution, soaks 2h, ultrasonic wave extraction 55min, obtains secondary raffinate and second extraction residue, collects secondary raffinate, will
Extract solution and secondary raffinate merge, filtering, obtain and extract total liquid, standby, wherein, the ultrasonic wave extraction power is
1100W；
4) will extract total liquid and be concentrated by evaporation is relative density is 1.29 at 60 DEG C lotion, and lotion is added into 3 times of weight
Alcoholic solution in, stir evenly, stand 28h, filtration, take filtrate, you can obtain auxiliary agent；
5) d-Bomeol liquid, turpentine oil, natural borneol and auxiliary agent are taken according to formula, be well mixed, produce hemorrhoids hemostasia wiping
Agent.
Above-mentioned alcoholic solution is the alcohol water blend of volumetric concentration 80%.
Embodiment 5
A kind of hemorrhoids hemostasia liniment, the raw material composition per 100mL hemorrhoids hemostasia liniments is as follows：D-Bomeol liquid 82mL, pine
Fuel-economizing 4.5mL, natural borneol 4.5g, remaining is auxiliary agent；The auxiliary agent is made up of the raw material below according to parts by weight：Prepared rhizome of rehmannia 14
Part, 9 parts of paris polyphylla.Wherein, the d-Bomeol liquid is made using the extracted processing of fresh branches and leaves of canella borneol camphor tree
Into.
In the present embodiment, the preparation method of the hemorrhoids hemostasia liniment, step is as follows：
1) paris polyphylla is weighed, is cleaned, drying is ground, and adds vinegar, after stirring, and is stood 2h, is placed into marmite
In, slow fire is heated to vinegar and is evaporated, stop heating, cooling, obtain paris polyphylla powder, wherein, the addition of the vinegar with
The weight of paris polyphylla is identical；
2) prepared rhizome of rehmannia is weighed, is cleaned, is dried, is crushed, 50 mesh sieves are crossed, paris polyphylla powder is then added, after being well mixed,
Obtain mixture；
3) mixture is put into container, adds the alcoholic solution of 12 times of weight, soaked 3h, heating and refluxing extraction 2h, obtain
Obtain an extract solution and once extract residue, collect an extract solution, will once extract the alcohol that residue adds 5 times of weight again
Solution, soaks 2h, ultrasonic wave extraction 60min, obtains secondary raffinate and second extraction residue, secondary raffinate is collected, by one
Secondary extract solution and secondary raffinate merge, filtering, obtain and extract total liquid, standby, wherein, the ultrasonic wave extraction power is
1100W；
4) will extract total liquid and be concentrated by evaporation is relative density is 1.30 at 60 DEG C lotion, and lotion is added into 3 times of weight
Alcoholic solution in, stir evenly, stand 30h, filtration, take filtrate, you can obtain auxiliary agent；
5) d-Bomeol liquid, turpentine oil, natural borneol and auxiliary agent are taken according to formula, be well mixed, produce hemorrhoids hemostasia wiping
Agent.
Above-mentioned alcoholic solution is the alcohol water blend of volumetric concentration 80%.
The hemorrhoids hemostasia liniment using d-Bomeol liquid as major ingredient, containing 28 kinds of active ingredients in d-Bomeol liquid,
Can anti-inflammatory, analgesic, detumescence, promoting blood circulation and removing blood stasis, penetration is strong, and auxiliary material, turpentine oil are used as using turpentine oil, natural borneol and auxiliary agent
Capillary can be permeated, anti-inflammatory, qualcomm meridian, blood-activating analgetic, natural borneol, its effect resuscitation with aromatics, analgesic antiphlogistic, compatibility is right
Rotation borneol liquid pins down reinforcement infiltration dynamics, and auxiliary agent can strengthen haemostatic effect of the externally applied liniment to hemorrhoid.
Hemorrhoids hemostasia liniment prepared by the present invention has the effects such as detumescence, analgesic, hemostasis, can effectively treat hemorrhoid and go out
Blood, because for externally applied liniment, can go directly focus, and therapeutic effect is good, easy to use；Hemorrhoids hemostasia liniment prepared by the present invention,
Formula is simple, with low cost, can promote the use of on a large scale.
The better embodiment to the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
, can also be on the premise of present inventive concept not be departed from formula, the knowledge that one skilled in the relevant art possesses
Various changes can be made.
Claims (7)
1. a kind of hemorrhoids hemostasia liniment, it is characterised in that the raw material composition per 100mL hemorrhoids hemostasia liniments is as follows：D-Bomeol
Liquid 79-83mL, turpentine oil 4-5mL, natural borneol 4-5g, remaining is auxiliary agent；The auxiliary agent is by below according to the raw material of parts by weight
It is made：11-14 parts of prepared rhizome of rehmannia, 5-9 parts of paris polyphylla.
2. hemorrhoids hemostasia liniment according to claim 1, it is characterised in that per the raw material group of 100mL hemorrhoids hemostasia liniments
Into as follows：D-Bomeol liquid 81mL, turpentine oil 4.5mL, natural borneol 4.5g, remaining is auxiliary agent；The auxiliary agent by below according to
The raw material of parts by weight is made：13 parts of prepared rhizome of rehmannia, 7 parts of paris polyphylla.
3. hemorrhoids hemostasia liniment according to claim 1, it is characterised in that the d-Bomeol liquid is using canella dragon
The fresh branches and leaves of brain camphor tree are extracted to be processed into.
4. the preparation method of a kind of hemorrhoids hemostasia liniment as described in claim 1-2 is any, it is characterised in that step is as follows：
1) paris polyphylla is weighed, is cleaned, drying is ground, and adds vinegar, after stirring, and is stood 1-2h, is placed into marmite
In, slow fire is heated to vinegar and is evaporated, and stops heating, and cooling obtains paris polyphylla powder；
2) prepared rhizome of rehmannia is weighed, is cleaned, is dried, is crushed, 30-50 mesh sieves are crossed, paris polyphylla powder is then added, after being well mixed,
Obtain mixture；
3) mixture is put into container, adds the alcoholic solution of 10-12 times of weight, soak 2-3h, heating and refluxing extraction 1-2h,
Obtain an extract solution and once extract residue, collect an extract solution, once extraction residue is added into 2-5 times of weight again
Alcoholic solution, soaks 1-2h, ultrasonic wave extraction 50-60min, obtains secondary raffinate and second extraction residue, collects secondary carry
Liquid is taken, an extract solution and secondary raffinate are merged, filtering, obtains and extracts total liquid, it is standby；
4) will extract total liquid and be concentrated by evaporation is relative density is 1.27-1.30 at 60 DEG C lotion, and lotion is added into 3 times of weight
Alcoholic solution in, stir evenly, stand 24-30h, filtration, take filtrate, you can obtain auxiliary agent；
5) d-Bomeol liquid, turpentine oil, natural borneol and auxiliary agent are taken according to formula, is well mixed, produces hemorrhoids hemostasia liniment.
5. the preparation method of hemorrhoids hemostasia liniment according to claim 3, it is characterised in that step 1) in, the vinegar
Addition it is identical with the weight of paris polyphylla.
6. the preparation method of hemorrhoids hemostasia liniment according to claim 3, it is characterised in that the alcoholic solution is volume
The alcohol water blend of concentration 80%.
7. the preparation method of hemorrhoids hemostasia liniment according to claim 3, it is characterised in that step 3) in, the ultrasound
It is 1100W that ripple, which extracts power,.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107668567A (en) * | 2017-10-11 | 2018-02-09 | 烟台宇诚企业管理咨询有限公司 | A kind of rheum officinale canned fish for improving sleep quality and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103463272A (en) * | 2013-09-17 | 2013-12-25 | 勘剑 | Medicine for completely treating haemorrhoids |
| CN103494937A (en) * | 2013-09-10 | 2014-01-08 | 姚自功 | Medicament for treating hemorrhoid |
-
2017
- 2017-05-25 CN CN201710380044.5A patent/CN107007726A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103494937A (en) * | 2013-09-10 | 2014-01-08 | 姚自功 | Medicament for treating hemorrhoid |
| CN103463272A (en) * | 2013-09-17 | 2013-12-25 | 勘剑 | Medicine for completely treating haemorrhoids |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107668567A (en) * | 2017-10-11 | 2018-02-09 | 烟台宇诚企业管理咨询有限公司 | A kind of rheum officinale canned fish for improving sleep quality and preparation method thereof |
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