CN107006533A - One planting fruit-trees efficient pesticides and its preparation method and application - Google Patents
One planting fruit-trees efficient pesticides and its preparation method and application Download PDFInfo
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- CN107006533A CN107006533A CN201710311396.5A CN201710311396A CN107006533A CN 107006533 A CN107006533 A CN 107006533A CN 201710311396 A CN201710311396 A CN 201710311396A CN 107006533 A CN107006533 A CN 107006533A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/14—Celastraceae [Staff-tree or Bittersweet family], e.g. spindle tree, bittersweet or thunder god vine
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/26—Meliaceae [Chinaberry or Mahogany family], e.g. mahogany, langsat or neem
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/30—Polygonaceae [Buckwheat family], e.g. red-knees or rhubarb
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/32—Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
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- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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Abstract
The invention discloses planting fruit-trees efficient pesticides and its preparation method and application, belong to fruit tree insecticide field, the insecticide includes following raw material by weight：Print 15 35 parts of chinaberry, 15 35 parts of Celastrus angulatus, 10 30 parts of five-leaved chaste tree seed, 5 25 parts of Kadsura Root-bark, 5 25 parts of monkshood, 5 25 parts of polygonum flaccidum, 5 15 parts of frutus cnidii, 5 15 parts of the seed of feather cockscomb, 4 12 parts of plants essential oil, 2 10 parts of propylene Ethyl formate, 15 parts of solubilizer, 15 parts of emulsifying agent, 15 parts of bleeding agent, 15 parts of antioxidant.Preparation method is will first to print after the plant materials such as chinaberry distinguish size-reduced, sieving to mix, and obtains compound, afterwards by second extraction, obtains effective ingredients in plant extract solution, is finally added thereto remaining auxiliary material, mixing.The fruit tree insecticide green non-pollution of the present invention, will not make the various insect germs on fruit tree develop immunity to drugs, consumption is few, and prevention effect is the organic fruit industry of development, the preferable agricultural chemicals of promotion fruits industry sustainable development significantly.
Description
Technical field
The invention belongs to fruit tree insecticide field, and in particular to planting fruit-trees efficient pesticides and preparation method thereof and should
With.
Background technology
At present, during planting fruit trees, to prevent insect germ from suppressing growing for fruit tree, usually used being
Agricultural chemical insecticide is learned, but the problem of environmental pollution that can be largely effectively caused using chemical pesticide is on the rise.Meanwhile, using change
Learn various phytopathogen strains during agricultural chemical insecticide and produce drug resistance, the resistance to the action of a drug, add the difficulty of preventing and treating, or even cause to prevent
Control failure.In addition, chemical pesticide will also result in threat because it is without selectivity to beneficial biology.Moreover, many chemistry agricultures
Medicine is non-degradable or is difficult to degraded, and the enrichment of thing is easily accumulated and polluted on fruit tree and fruit, water is not only influenceed
The sale of fruit, and be more likely detrimental to health in edible fruits.
With requirement more and more higher of the public to " pollution-free food ", " pollution-free food ", market to it is pollution-free, can drop naturally
The ecological insecticide demand of solution also gradually increases.From the point of view of the development of pesticide science, " returned certainly using upper in pesticide manufacturing
So " and agricultural chemicals " Harmless ", be the inexorable trend of society and Development of Natural Science, therefore new and effective non-harmful fruit tree
Insecticide has wide development prospect.
The content of the invention
The problem of existing for prior art, the invention provides planting fruit-trees efficient pesticides and preparation method thereof and should
With this kind of insecticide green non-pollution will not make the various insect germs on fruit tree develop immunity to drugs, consumption is few, prevention effect
Significantly.
In order to achieve the above object, the present invention is achieved through the following technical solutions：
One planting fruit-trees efficient pesticides, including following raw material by weight：Print 15-35 parts of chinaberry, 15-35 parts of Celastrus angulatus, Huang
10-30 parts of chaste tree seed, 5-25 parts of Kadsura Root-bark, 5-25 parts of monkshood, 5-25 parts of polygonum flaccidum, 5-15 parts of frutus cnidii, 5-15 parts of the seed of feather cockscomb, plant
4-12 parts of thing essential oil, 2-10 parts of propylene Ethyl formate, 1-5 parts of solubilizer, 1-5 parts of emulsifying agent, 1-5 parts of bleeding agent, antioxidant 1-5
Part.
Further, the insecticide includes following raw material by weight：Print 20-30 parts of chinaberry, Celastrus angulatus 20-30
Part, 15-25 parts of five-leaved chaste tree seed, 10-20 parts of Kadsura Root-bark, 10-20 parts of monkshood, 10-20 parts of polygonum flaccidum, 8-12 parts of frutus cnidii, the seed of feather cockscomb
8-12 parts, 6-10 parts of plants essential oil, 4-8 parts of propylene Ethyl formate, 2-4 parts of solubilizer, 2-4 parts of emulsifying agent, 2-4 parts of bleeding agent,
2-4 parts of antioxidant.
Further, the insecticide includes following raw material by weight：Print 25 parts of chinaberry, 25 parts of Celastrus angulatus, Huang
20 parts of chaste tree seed, 15 parts of Kadsura Root-bark, 15 parts of monkshood, 15 parts of polygonum flaccidum, 10 parts of frutus cnidii, 10 parts of the seed of feather cockscomb, 8 parts of plants essential oil, third
6 parts of zinecarboxylic acid ethyl ester, 3 parts of solubilizer, 3 parts of emulsifying agent, 3 parts of bleeding agent, 3 parts of antioxidant.
Preferably, the plants essential oil is wintergreen, camphor tree oil, caryophyllus oil, peppermint oil, eucalyptus oil, citronella oil or tea tree
One or more in oil.
Preferably, the solubilizer is neopelex, Potassium dodecylbenzenesulfonate, polysorbate, poly- second two
One or more in alcohol or sorbierite polyoxy ether.
Preferably, the emulsifying agent be mass concentration ratio be 75% polyoxyethylene sorbitan fatty acid ester, 85%
Castor oil polyoxyethylene ether, 55% polyoxyethylene fatty acid ester or sodium lignin sulfonate in one or more.
Preferably, the bleeding agent be mass concentration ratio be 75% azone, 65% AEO or suitable
One or more in butene dioic acid di-sec-octyl sodium sulfonate.
Preferably, the antioxidant is times in tocopherol, sodium sulfite or the ascorbic acid that mass concentration ratio is 85%
It is a kind of.
The preparation method of a described planting fruit-trees efficient pesticides, is followed the steps below：
（1）Raw material is weighed by above-mentioned parts by weight；
（2）Chinaberry, Celastrus angulatus, five-leaved chaste tree seed, Kadsura Root-bark, monkshood, polygonum flaccidum will be printed, frutus cnidii, the seed of feather cockscomb are distinguished after size-reduced, sieving
Mix, obtain compound；
（3）The 4-6 times of 70-90% measured ethanol water is added mixture into, 50-70 DEG C of decoction 2-4h is heated to, filters, filter
Liquid is collected, and filter residue adds the 4-6 times of 70-90% measured ethanol water, is heated to 60-80 DEG C of decoction 3-5h, and filtering, filtrate is received
Collection, merges above-mentioned whole filtrates, obtains plant extraction liquid；
（4）Solubilizer, emulsifying agent, bleeding agent, antioxidant are added in the plant extraction liquid while stirring successively, mixed
Afterwards, plants essential oil and propylene Ethyl formate, mixing are eventually adding.
The application of an above-mentioned planting fruit-trees efficient pesticides, i.e., add water in the insecticide under stirring at normal temperature,
Make it be diluted to after stoste accounts for 10-30wt% concentration to be spray applied.
The present invention has the advantages that：
（1）Extensively, cheap, preparation technology is simple and convenient, and cost is low for the fruit tree insecticide raw material sources of the present invention；
（2）The fruit tree insecticide consumption of the present invention is few, and prevention effect is good, Cercospora Sojina Hara that can be common to fruit tree, rest fungus, caterpillar
Many insect germs such as class, heart-eating worm, aphid kill preventing and treating, and the insecticide action speed is fast, efficiency time
It is long；
（3）Print chinaberry, Celastrus angulatus, five-leaved chaste tree seed that the fruit tree insecticide raw material of the present invention is selected etc., its extract solution active ingredient ring
Border compatibility is good, degradable, compared to chemical pesticide type insecticide safety and reliability, and its active ingredient have to disease pest bacterium food refusal,
The effects such as interference is laid eggs, tagged, is difficult to make disease pest bacterium develop immunity to drugs, improves the utilization rate of insecticide, green non-pollution is
Develop organic fruit industry, promote the preferable agricultural chemicals of fruits industry sustainable development.
Embodiment
The embodiment of the present invention is further described with reference to embodiment, following examples are only used for more
Technical scheme is clearly demonstrated, and can not be limited the scope of the invention with this.
Embodiment 1
One planting fruit-trees efficient pesticides, weigh following raw material：Print chinaberry 15kg, Celastrus angulatus 15kg, five-leaved chaste tree seed 10kg, Kadsura Root-bark
5kg, monkshood 5kg, polygonum flaccidum 5kg, frutus cnidii 5kg, seed of feather cockscomb 5kg, plants essential oil 4kg, propylene Ethyl formate 2kg, solubilizer
1kg, emulsifying agent 1kg, bleeding agent 1kg, antioxidant 1kg.
Wherein, above-mentioned plants essential oil uses wintergreen, three kinds of quality between mixture, and three of caryophyllus oil and peppermint oil
Than for 1:1:2；
Solubilizer uses two kinds of mixtures of neopelex and polyethylene glycol, and mass ratio between the two is 1:2；
Emulsifying agent use mass concentration ratio for 75% polyoxyethylene sorbitan fatty acid ester；
Bleeding agent use mass concentration ratio for 75% two kinds of mixtures of azone and disecoctylmaleate sodium sulfonate, and two
Mass ratio between person is 1:1；
Antioxidant use mass concentration ratio for 85% tocopherol.
The preparation method of an above-mentioned planting fruit-trees efficient pesticides, is followed the steps below：
（1）Raw material is weighed by above-mentioned ormal weight；
（2）Chinaberry, Celastrus angulatus, five-leaved chaste tree seed, Kadsura Root-bark, monkshood, polygonum flaccidum will be printed, frutus cnidii, the seed of feather cockscomb are distinguished after size-reduced, sieving
Mix, obtain compound；
（3）70% ethanol water of 4 times of amounts is added mixture into, 50 DEG C of decoction 2h are heated to, filtering, filtrate is collected, filter
Slag adds 70% ethanol water of 4 times of amounts, is heated to 60 DEG C of decoction 3h, and filtering, filtrate is collected, and merges above-mentioned all filters
Liquid, obtains plant extraction liquid；
（4）Solubilizer, emulsifying agent, bleeding agent, antioxidant are added in the plant extraction liquid while stirring successively, mixed
Afterwards, plants essential oil and propylene Ethyl formate are eventually adding, the fruit tree efficient pesticides for producing the present invention are mixed.
Embodiment 2
One planting fruit-trees efficient pesticides, weigh following raw material：Print chinaberry 20kg, Celastrus angulatus 20kg, five-leaved chaste tree seed 15kg, Kadsura Root-bark
10kg, monkshood 10kg, polygonum flaccidum 10kg, frutus cnidii 8kg, seed of feather cockscomb 8kg, plants essential oil 6kg, propylene Ethyl formate 4kg, solubilizer
2kg, emulsifying agent 2kg, bleeding agent 2kg, antioxidant 2kg.
Wherein, above-mentioned plants essential oil uses peppermint oil, eucalyptus oil, citronella oil and a variety of mixtures of tea oil, and each composition
Between mass ratio be 2:1:2:1；
Solubilizer uses polysorbate, polyethylene glycol and sorbierite polyoxy three kinds of mass ratioes between mixture, and three of ether
For 1:1:1；
Emulsifying agent use mass concentration ratio for 55% two kinds of mixtures of polyoxyethylene fatty acid ester and sodium lignin sulfonate, and two
Mass ratio between person is 2:1；
Bleeding agent use mass concentration ratio for 75% two kinds of mixtures of azone and disecoctylmaleate sodium sulfonate, and two
Mass ratio between person is 1:1；
Antioxidant uses sodium sulfite.
The preparation method of an above-mentioned planting fruit-trees efficient pesticides, is followed the steps below：
（1）Raw material is weighed by above-mentioned ormal weight；
（2）Chinaberry, Celastrus angulatus, five-leaved chaste tree seed, Kadsura Root-bark, monkshood, polygonum flaccidum will be printed, frutus cnidii, the seed of feather cockscomb are distinguished after size-reduced, sieving
Mix, obtain compound；
（3）75% ethanol water of 4 times of amounts is added mixture into, 55 DEG C of decoction 2h are heated to, filtering, filtrate is collected, filter
Slag adds 75% ethanol water of 4 times of amounts, is heated to 65 DEG C of decoction 3h, and filtering, filtrate is collected, and merges above-mentioned all filters
Liquid, obtains plant extraction liquid；
（4）Solubilizer, emulsifying agent, bleeding agent, antioxidant are added in the plant extraction liquid while stirring successively, mixed
Afterwards, plants essential oil and propylene Ethyl formate are eventually adding, the fruit tree efficient pesticides for producing the present invention are mixed.
Embodiment 3
One planting fruit-trees efficient pesticides, weigh following raw material：Print chinaberry 25kg, Celastrus angulatus 25kg, five-leaved chaste tree seed 20kg, Kadsura Root-bark
15kg, monkshood 15kg, polygonum flaccidum 15kg, frutus cnidii 10kg, seed of feather cockscomb 10kg, plants essential oil 8kg, propylene Ethyl formate 6kg, solubilising
Agent 3kg, emulsifying agent 3kg, bleeding agent 3kg, antioxidant 3kg.
Wherein, above-mentioned plants essential oil uses wintergreen, caryophyllus oil, citronella oil and a variety of mixtures of tea oil, and each composition
Between mass ratio be 1:1:1:1；
Solubilizer uses neopelex, three kinds of quality between mixture, and three of polysorbate and polyethylene glycol
Than for 1:1:1；
Emulsifying agent uses polyoxyethylene sorbitan fatty acid ester of the mass concentration ratio for 75%, 55% Polyoxyethylene fatty
Three kinds of mass ratioes between mixture, and three of acid esters and sodium lignin sulfonate are 1:1:2；
Bleeding agent use mass concentration ratio for 75% azone and 65% two kinds of mixtures of AEO, and both
Between mass ratio be 1:1；
Antioxidant uses ascorbic acid.
The preparation method of an above-mentioned planting fruit-trees efficient pesticides, is followed the steps below：
（1）Raw material is weighed by above-mentioned ormal weight；
（2）Chinaberry, Celastrus angulatus, five-leaved chaste tree seed, Kadsura Root-bark, monkshood, polygonum flaccidum will be printed, frutus cnidii, the seed of feather cockscomb are distinguished after size-reduced, sieving
Mix, obtain compound；
（3）80% ethanol water of 5 times of amounts is added mixture into, 60 DEG C of decoction 3h are heated to, filtering, filtrate is collected, filter
Slag adds 80% ethanol water of 5 times of amounts, is heated to 70 DEG C of decoction 4h, and filtering, filtrate is collected, and merges above-mentioned all filters
Liquid, obtains plant extraction liquid；
（4）Solubilizer, emulsifying agent, bleeding agent, antioxidant are added in the plant extraction liquid while stirring successively, mixed
Afterwards, plants essential oil and propylene Ethyl formate are eventually adding, the fruit tree efficient pesticides for producing the present invention are mixed.
Embodiment 4
One planting fruit-trees efficient pesticides, weigh following raw material：Print 30 parts of chinaberry, 30 parts of Celastrus angulatus, 25 parts of five-leaved chaste tree seed, Kadsura Root-bark 20
Part, 20 parts of monkshood, 20 parts of polygonum flaccidum, 12 parts of frutus cnidii, 12 parts of the seed of feather cockscomb, 10 parts of plants essential oil, 8 parts of propylene Ethyl formate, solubilising
4 parts of agent, 4 parts of emulsifying agent, 4 parts of bleeding agent, 4 parts of antioxidant.
Wherein, above-mentioned plants essential oil uses peppermint oil；
Solubilizer is using three kinds of Potassium dodecylbenzenesulfonate, polyethylene glycol and sorbierite polyoxy ether between mixture, and three
Mass ratio be 1:1:1；
Emulsifying agent uses mass concentration ratio for 85% castor oil polyoxyethylene ether, 55% polyoxyethylene fatty acid ester and wooden
Plain three kinds of mass ratioes between mixture, and three of sodium sulfonate are 1:1:1；
Bleeding agent use mass concentration ratio for 75% azone；
Antioxidant use mass concentration ratio for 85% tocopherol.
The preparation method of an above-mentioned planting fruit-trees efficient pesticides, is followed the steps below：
（1）Raw material is weighed by above-mentioned ormal weight；
（2）Chinaberry, Celastrus angulatus, five-leaved chaste tree seed, Kadsura Root-bark, monkshood, polygonum flaccidum will be printed, frutus cnidii, the seed of feather cockscomb are distinguished after size-reduced, sieving
Mix, obtain compound；
（3）85% ethanol water of 6 times of amounts is added mixture into, 65 DEG C of decoction 4h are heated to, filtering, filtrate is collected, filter
Slag adds 85% ethanol water of 6 times of amounts, is heated to 75 DEG C of decoction 5h, and filtering, filtrate is collected, and merges above-mentioned all filters
Liquid, obtains plant extraction liquid；
（4）Solubilizer, emulsifying agent, bleeding agent, antioxidant are added in the plant extraction liquid while stirring successively, mixed
Afterwards, plants essential oil and propylene Ethyl formate are eventually adding, the fruit tree efficient pesticides for producing the present invention are mixed.
Embodiment 5
One planting fruit-trees efficient pesticides, weigh following raw material：Print chinaberry 35kg, Celastrus angulatus 35kg, five-leaved chaste tree seed 30kg, Kadsura Root-bark
25kg, monkshood 25kg, polygonum flaccidum 25kg, frutus cnidii 15kg, seed of feather cockscomb 15kg, plants essential oil 12kg, propylene Ethyl formate 10kg, increasing
Solvent 5kg, emulsifying agent 5kg, bleeding agent 5kg, antioxidant 5kg.
Wherein, above-mentioned plants essential oil uses camphor tree oil, caryophyllus oil, eucalyptus oil and a variety of mixtures of citronella oil, and each composition
Between between mass ratio be 1:1:2:1；
Solubilizer uses neopelex；
Emulsifying agent use mass concentration ratio for 85% two kinds of mixtures of castor oil polyoxyethylene ether and sodium lignin sulfonate, and two
Mass ratio between person is 1:1；
Bleeding agent use mass concentration ratio for 75% azone and 65% two kinds of mixtures of AEO, and both
Between mass ratio be 1:1；
Antioxidant uses ascorbic acid.
The preparation method of an above-mentioned planting fruit-trees efficient pesticides, is followed the steps below：
（1）Raw material is weighed by above-mentioned ormal weight；
（2）Chinaberry, Celastrus angulatus, five-leaved chaste tree seed, Kadsura Root-bark, monkshood, polygonum flaccidum will be printed, frutus cnidii, the seed of feather cockscomb are distinguished after size-reduced, sieving
Mix, obtain compound；
（3）90% ethanol water of 6 times of amounts is added mixture into, 70 DEG C of decoction 4h are heated to, filtering, filtrate is collected, filter
Slag adds 90% ethanol water of 6 times of amounts, is heated to 80 DEG C of decoction 5h, and filtering, filtrate is collected, and merges above-mentioned all filters
Liquid, obtains plant extraction liquid；
（4）Solubilizer, emulsifying agent, bleeding agent, antioxidant are added in the plant extraction liquid while stirring successively, mixed
Afterwards, plants essential oil and propylene Ethyl formate are eventually adding, the fruit tree efficient pesticides for producing the present invention are mixed.
The fruit tree efficient pesticides that above-described embodiment 1-5 is prepared in actual applications, can add water under stirring at normal temperature
Enter into the insecticide, it is diluted to stoste and account for just sprayable after 10-30wt% concentration apply.
Control effect testing
Preventive effect place：The bright Dongxiang in Anhui Province Mingguang City.
The preventive effect time：September -20 days on the 3rd in 2014.
Preventive effect object：Tangerine.
Preventive effect instrument：Fruit tree efficient pesticides and comparative example prepared by embodiment 1-5（5% 3000 times of Frontline liquid）.
Preventive effect method：6 mu of soils are chosen, fruit tree efficient pesticides and 5% sharp strength of comparative example prepared by embodiment 1 to 5
Special 3000 times of liquid are sprayed in tangerine trunk periphery according to 5 kilograms every mu of consumption, and above-described embodiment and comparative example remove insecticide
Difference, other geographical, environment and moisture condition are all identical, the disease pest bacterium of tangerine after observing 2 days respectively, after 7 days and after 15 days
Evil situation, and every group of disease pest bacterium existence rate of statistic record is in table 1 below.
Table 1
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, although with reference to the foregoing embodiments
The present invention is described in detail, for those skilled in the art, it still can be to foregoing embodiments institute
The technical scheme of record is modified, or carries out equivalent substitution to which part technical characteristic.It is all the present invention spirit and
Within principle, any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.
Claims (10)
1. a planting fruit-trees efficient pesticides, it is characterised in that including following raw material by weight：Print 15-35 parts of chinaberry, bitter skin
15-35 parts of rattan, 10-30 parts of five-leaved chaste tree seed, 5-25 parts of Kadsura Root-bark, 5-25 parts of monkshood, 5-25 parts of polygonum flaccidum, 5-15 parts of frutus cnidii, green grass or young crops
5-15 parts of feather cockscomb, 4-12 parts of plants essential oil, 2-10 parts of propylene Ethyl formate, 1-5 parts of solubilizer, 1-5 parts of emulsifying agent, bleeding agent 1-
5 parts, 1-5 parts of antioxidant.
2. planting fruit-trees efficient pesticides according to claim 1, it is characterised in that including following original by weight
Material：Print 20-30 parts of chinaberry, 20-30 parts of Celastrus angulatus, 15-25 parts of five-leaved chaste tree seed, 10-20 parts of Kadsura Root-bark, 10-20 parts of monkshood, polygonum flaccidum
10-20 parts, 8-12 parts of frutus cnidii, 8-12 parts of the seed of feather cockscomb, 6-10 parts of plants essential oil, 4-8 parts of propylene Ethyl formate, solubilizer 2-4
Part, 2-4 parts of emulsifying agent, 2-4 parts of bleeding agent, 2-4 parts of antioxidant.
3. planting fruit-trees efficient pesticides according to claim 1, it is characterised in that including following original by weight
Material：25 parts of chinaberry of print, 25 parts of Celastrus angulatus, 20 parts of five-leaved chaste tree seed, 15 parts of Kadsura Root-bark, 15 parts of monkshood, 15 parts of polygonum flaccidum, 10 parts of frutus cnidii,
10 parts of the seed of feather cockscomb, 8 parts of plants essential oil, 6 parts of propylene Ethyl formate, 3 parts of solubilizer, 3 parts of emulsifying agent, 3 parts of bleeding agent, antioxidant 3
Part.
4. planting fruit-trees efficient pesticides according to claim 1, it is characterised in that the plants essential oil be wintergreen,
One or more in camphor tree oil, caryophyllus oil, peppermint oil, eucalyptus oil, citronella oil or tea oil.
5. planting fruit-trees efficient pesticides according to claim 1, it is characterised in that the solubilizer is detergent alkylate
One or more in sodium sulfonate, Potassium dodecylbenzenesulfonate, polysorbate, polyethylene glycol or sorbierite polyoxy ether.
6. planting fruit-trees efficient pesticides according to claim 1, it is characterised in that the emulsifying agent is mass concentration ratio
For 75% polyoxyethylene sorbitan fatty acid ester, 85% castor oil polyoxyethylene ether, 55% Polyoxyethylene fatty
One or more in acid esters or sodium lignin sulfonate.
7. planting fruit-trees efficient pesticides according to claim 1, it is characterised in that the bleeding agent is mass concentration ratio
For the one or more in 75% azone, 65% AEO or disecoctylmaleate sodium sulfonate.
8. planting fruit-trees efficient pesticides according to claim 1, it is characterised in that the antioxidant is mass concentration ratio
For 85% any of tocopherol, sodium sulfite or ascorbic acid.
9. a kind of preparation method of fruit tree efficient pesticides according to described in any one of claim 1-8, it is characterised in that bag
Include following steps：
（1）Raw material is weighed by above-mentioned parts by weight；
（2）Chinaberry, Celastrus angulatus, five-leaved chaste tree seed, Kadsura Root-bark, monkshood, polygonum flaccidum will be printed, frutus cnidii, the seed of feather cockscomb are distinguished after size-reduced, sieving
Mix, obtain compound；
（3）The 4-6 times of 70-90% measured ethanol water is added mixture into, 50-70 DEG C of decoction 2-4h is heated to, filters, filter
Liquid is collected, and filter residue adds the 4-6 times of 70-90% measured ethanol water, is heated to 60-80 DEG C of decoction 3-5h, and filtering, filtrate is received
Collection, merges above-mentioned whole filtrates, obtains plant extraction liquid；
（4）Solubilizer, emulsifying agent, bleeding agent, antioxidant are added in the plant extraction liquid while stirring successively, mixed
Afterwards, plants essential oil and propylene Ethyl formate, mixing are eventually adding.
10. the application of a kind of fruit tree efficient pesticides according to described in any one of claim 1-8, it is characterised in that normal
Added water under temperature stirring in the insecticide, it is diluted to after stoste accounts for 10-30wt% concentration and be spray applied.
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| CN107926995A (en) * | 2017-12-06 | 2018-04-20 | 昭平县科学技术实验场 | Plant insecticide containing camptothecine and its preparation method and application |
| CN108041101A (en) * | 2017-11-29 | 2018-05-18 | 兰溪市沉默生物科技有限公司 | Mango sapling method for producing insecticide |
| CN109303079A (en) * | 2018-07-23 | 2019-02-05 | 雷霆 | A kind of agricultural composite insecticide composition |
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