CN106983685A - A kind of suntan lotion and preparation method thereof - Google Patents
A kind of suntan lotion and preparation method thereof Download PDFInfo
- Publication number
- CN106983685A CN106983685A CN201710248447.4A CN201710248447A CN106983685A CN 106983685 A CN106983685 A CN 106983685A CN 201710248447 A CN201710248447 A CN 201710248447A CN 106983685 A CN106983685 A CN 106983685A
- Authority
- CN
- China
- Prior art keywords
- grams
- suntan lotion
- acid
- sunscreen composition
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4966—Triazines or their condensed derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Molecular Biology (AREA)
- Biophysics (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of suntan lotion and preparation method thereof, the suntan lotion includes following component：First sunscreen composition, the second sunscreen composition, isotriacontane, glycerine, isopropyl myristate, ethanol, essence, methyl p-hydroxybenzoate, propylparaben and water；The sun-prevention component in suntan lotion is effectively isolated with the external world using capsule of nano technology in its preparation method.Compared with prior art, suntan lotion of the present invention, its preparation technology is simple, obtained suntan lotion has persistently effective sun-proof ability, chemical sunscreen ingredients after being handled with microencapsulation only stay in the surface of skin, it is small to skin irritatin, safely and effectively, solve the problem of easily being come off after suntan lotion is smeared by the dissolving such as sweat, rainwater, seawater.
Description
Technical field
The present invention relates to sun-proof technical field, and in particular to a kind of suntan lotion and preparation method thereof.
Background technology
Injury of the sunshine to human body skin mostlys come from ultraviolet light,long wave (i.e. UVA) and UV-B (i.e. UVB).UVA makees
For deep skin, effect is slow, but can cause disposable melanism, and UVB acts on skin surface, excites skin keratinocytes,
Make vasodilation, increase CBF, rubefaction can be made until becoming brown.UVA and UVB can make skin produce sunburn, decortication,
It is tanned to wait phenomenon after solarization, and then make skin aging in advance, some irremediable injuries are caused to skin, if long-term by UVA
With UVB influence, it is also possible to cause cutaneum carcinoma.
Supporting anti-ultraviolet sun-proof measure at present mainly includes physical sunscreen and chemical sunscreen, and physical sunscreen refers to anti-with energy
Material (the TiO of shining sun light2, ZnO) skin surface formation layer protecting film, ultraviolet reflection is gone out, so as to reach sun-proof
Effect, and chemical sunscreen refers to that the chemical substance such as phthalate in sunscreen productses absorbs the ultraviolet light degradation for injuring skin
Fall.But there is the problem of sun-proof component is easily come off by the dissolving such as sweat, rainwater, seawater in such product, in the market has occurred many
The cosmetics for possessing water-proof function are planted, it realizes that this causes the price of waterproof product generally by corresponding additive is added
Costliness, and also there is certain stimulation to skin in additive.
The content of the invention
It is a primary object of the present invention to overcome defect of the prior art there is provided a kind of suntan lotion and preparation method thereof,
Its preparation technology is simple, and the suntan lotion of preparation has excellent water-proof function, with lasting sun-proof result.
To achieve the above object, the present invention is adopted the following technical scheme that：
In a first aspect, the present invention provides a kind of suntan lotion, it includes following component：It is first sunscreen composition, second sun-proof
Composition, isotriacontane, glycerine, isopropyl myristate, ethanol, essence, methyl p-hydroxybenzoate, para hydroxybenzene first
Propyl propionate and water；
Wherein, first sunscreen composition includes sorbitan monooleate, ethylhexyl salicylate, Hu Moliu
Ester, SPAN-80,18 carbonic acid, palmityl alcohol, polyglycerol distearate, lecithin, stearyl alcohol, butanediol；
Wherein, second sunscreen composition include Phenylbenzimidazolesulfonic acid, Neo Heliopan AP,
Ethylhexyl methoxy cinnamate, p- methoxycinnamates isoamyl valerate, phenyl benzimidazole sulfonic acid, double-ethylhexylphenol first
Aminobenzene piperazine, 4- Methylbenzylidene subunits camphor, PEG-25 p-aminobenzoic acid, the silica of isoamyl alcohol trimethoxy cinnamic acid ester three
Alkane, Uvinul T 150, pentyl diformazan para amidocyanogen benzoic Acid, the own ester of diethylamino hydroxybenzoyl benzoylbenzoic acid, methylene
Base pair-BTA base tetramethyl butyl phenol, forulic acid and Neo Heliopan E1000.
In order to further optimize above-mentioned technical proposal, the technical measures that the present invention is taken also include：
Preferably, plant extracts is also included in the suntan lotion, the plant extracts is selected from Baical Skullcap root P.E, marine alga
At least one of extract, dried tremella extract and ginkgo biloba extract.
Preferably, weight fraction of the plant extracts in suntan lotion total amount is 1%~3%.
Preferably, the component of the suntan lotion has following parts by weight：
Preferably, the parts by weight of each component are as follows in first sunscreen composition：
Preferably, the parts by weight of each component are as follows in second sunscreen composition：
Second aspect, the present invention provides a kind of method for preparing above-mentioned suntan lotion, comprises the following steps：
Step a, 70~80 DEG C are heated water to, the first sunscreen composition is added under agitation, clear solution is obtained；
Step b, the clear solution prepared in step a is heated to 75~85 DEG C, adds the second sunscreen composition, keep permanent
Temperature stirring, and continuously stirred 2 hours under the protection of inert atmosphere, obtain nontransparent solution；
Step c, obtained nontransparent solution in step b carried out it is ultrasonically treated, until solution transparence, by transparence
Solution is prepared into capsule of nano solution, is cooled to room temperature；
Step d, under mild agitation, different 30 carbon is sequentially added in step c in obtained capsule of nano solution
Alkane, glycerine, isopropyl myristate, ethanol, essence, methyl p-hydroxybenzoate and propylparaben, stirring are mixed
It is even, obtain homogeneous suntan lotion.
Preferably, the preparation of the capsule of nano solution is prepared using conventional technical means, and above-mentioned emulsion is stirred
Mix after mixing, carry out emulsifying homogeneous processing；The wall material used in preparation process is maltodextrin, chitosan, polyacrylate, card
At least one of glue is drawn, capsule-core is described the first sunscreen composition and the second sunscreen composition.
Preferably, the inert atmosphere in the step b is argon gas or nitrogen.
Preferably, the ultrasonic time in the step c is 10min~30min.
Compared with prior art, the invention has the advantages that：The present invention mainly will be anti-using micro- assisting of glue technology
The sun-prevention component shone in liquid is effectively isolated with the external world, is easily dissolved so as to solve after suntan lotion is smeared by sweat, rainwater, seawater etc.
Chemical sunscreen ingredients after the problem of coming off, and use microencapsulation processing only stay in the surface of skin, small to skin irritatin,
Safely and effectively；Its preparation technology is simple, and obtained suntan lotion has persistently effective sun-proof ability, and moderate, it is easy to
Promoted in masses, while plant extracts of the addition with sun-proof repair function, it is directly contacted with skin, can be quickly effective
Alleviate the rubescent hot problem that skin occurs after ground shines, farthest realize the nursing and reparation of skin.
Embodiment
With reference to embodiment, the embodiment to the present invention is further described.Following examples are only used for more
Plus technical scheme is clearly demonstrated, and can not be limited the scope of the invention with this.
Embodiment 1
First by water, 16 grams are heated to 75 DEG C, and 1 gram of sorbitan monooleate, salicylic acid second are sequentially added under agitation
1 gram of the own ester of base, 2 grams of Homosalate, 3 grams of SPAN-80,1 gram of 18 carbonic acid, 2 grams of palmityl alcohol, 2 grams of polyglycerol distearate,
1 gram of lecithin, 2 grams of stearyl alcohol, 1 gram of butanediol.Continue to stir to whole dissolvings, obtain clear solution.Temperature is increased to 80 DEG C,
Then following composition is sequentially added：1 gram of Phenylbenzimidazolesulfonic acid, 2 grams of Neo Heliopan AP, methoxyl group
1 gram of 2-Ethylhexyl cinnamate, 2 grams of p- methoxycinnamates isoamyl valerate, 1 gram of phenyl benzimidazole sulfonic acid, double-ethylhexylphenol
1.5 grams of methylamino benzene piperazine, 1 gram of 4- Methylbenzylidene subunits camphor, 2 grams of PEG-25 p-aminobenzoic acid, isoamyl alcohol trimethoxy meat
1 gram of cinnamic acid ester trisiloxanes, 2 grams of Uvinul T 150,1 gram of pentyl diformazan para amidocyanogen benzoic Acid, diethylamino hydroxybenzoyl
2 grams of the own ester of benzoylbenzoic acid, 2 grams of MBBT, 2 grams of forulic acid and to methoxyl group
1 gram of isoamyl cinnamate.Constant temperature stirring is kept, is continuously stirred under nitrogen protection 2 hours.Then with ultrasonically treated 15min, treat
Gradually transparence, room temperature is cooled to after being completely converted into capsule of nano solution using conventional technical means.
9 grams of isotriacontane, 7 grams of glycerine, 10 grams of isopropyl myristate, ethanol 16 are sequentially added under mild agitation
Gram, 0.5 gram of essence, 1 gram of methyl p-hydroxybenzoate and 1 gram of propylparaben.
Whole mixings are treated, obtains and stops stirring after uniform solution.
Embodiment 2
First by water, 25 grams are heated to 78 DEG C, and 2 grams of sorbitan monooleate, salicylic acid second are sequentially added under agitation
2 grams of the own ester of base, 5 grams of Homosalate, 4 grams of SPAN-80,3 grams of 18 carbonic acid, 7 grams of palmityl alcohol, 4 grams of polyglycerol distearate,
5 grams of lecithin, 7 grams of stearyl alcohol, 5 grams of butanediol.Continue to stir to whole dissolvings, obtain clear solution.Temperature is increased to 83 DEG C,
Then following composition is sequentially added：4 grams of Phenylbenzimidazolesulfonic acid, 5 grams of Neo Heliopan AP, methoxyl group
4 grams of 2-Ethylhexyl cinnamate, 3.5 grams of p- methoxycinnamates isoamyl valerate, 2.5 grams of phenyl benzimidazole sulfonic acid, double-ethylhexyl
2.5 grams of phenol methylamino benzene piperazine, 2 grams of 4- Methylbenzylidene subunits camphor, 5 grams of PEG-25 p-aminobenzoic acid, isoamyl alcohol trimethoxy
2 grams of base cinnamate trisiloxanes, 4 grams of Uvinul T 150,3 grams of pentyl diformazan para amidocyanogen benzoic Acid, diethylamino
3 grams of (2-hydroxybenzoyl) hexyl-benzoate, 2 grams of MBBT, 5 grams of forulic acid and to first
1 gram of epoxide isoamyl cinnamate.Constant temperature stirring is kept, is continuously stirred under nitrogen protection 2 hours.Then with ultrasonically treated
20min, treats gradually transparence, and room temperature is cooled to after being completely converted into capsule of nano solution using conventional technical means.
18 grams of isotriacontane, 14 grams of glycerine, 12 grams of isopropyl myristate, ethanol are sequentially added under mild agitation
1.2 grams of 22 grams, 1 gram of essence, 1.2 grams of methyl p-hydroxybenzoate and propylparaben；Then Baical Skullcap root P.E is added
1g, marine algae extract 1.5g, dried tremella extract 1.5g and ginkgo biloba extract 1.5g.
Whole mixings are treated, obtains and stops stirring after uniform solution.
Embodiment 3
First by water, 10 grams are heated to 70 DEG C, and 1 gram of sorbitan monooleate, salicylic acid second are sequentially added under agitation
1 gram of the own ester of base, 1 gram of Homosalate, 1 gram of SPAN-80,1 gram of 18 carbonic acid, 2 grams of palmityl alcohol, 1 gram of polyglycerol distearate,
1 gram of lecithin, 2 grams of stearyl alcohol, 1 gram of butanediol.Continue to stir to whole dissolvings, obtain clear solution.Temperature is increased to 75 DEG C,
Then following composition is sequentially added：1 gram of Phenylbenzimidazolesulfonic acid, 1 gram of Neo Heliopan AP, methoxyl group
1 gram of 2-Ethylhexyl cinnamate, 1 gram of p- methoxycinnamates isoamyl valerate, 1 gram of phenyl benzimidazole sulfonic acid, double-ethylhexylphenol
1 gram of methylamino benzene piperazine, 1 gram of 4- Methylbenzylidene subunits camphor, 1 gram of PEG-25 p-aminobenzoic acid, isoamyl alcohol trimethoxy Chinese cassia tree
1 gram of acid esters trisiloxanes, 1 gram of Uvinul T 150,1 gram of pentyl diformazan para amidocyanogen benzoic Acid, diethylamino hydroxybenzoyl benzene
1 gram of the own ester of carbamoyl benzoate, 1 gram of MBBT, 1 gram of forulic acid and to methoxyl group meat
1 gram of cinnamate.Constant temperature stirring is kept, is continuously stirred 2 hours under argon gas protection.Then with ultrasonically treated 10min, treat by
Gradually transparence, room temperature is cooled to after being completely converted into capsule of nano solution using conventional technical means.
8 grams of isotriacontane, 2 grams of glycerine, 6 grams of isopropyl myristate, ethanol 10 are sequentially added under mild agitation
Gram, 0.1 gram of essence, 0.5 gram of methyl p-hydroxybenzoate and 0.5 gram of propylparaben；Then Baical Skullcap root P.E is added
0.6g, ginkgo biloba extract 0.5g, marine algae extract 1g.
Whole mixings are treated, obtains and stops stirring after uniform solution.
Embodiment 4
First by water, 30 grams are heated to 80 DEG C, and 5 grams of sorbitan monooleate, salicylic acid second are sequentially added under agitation
5 grams of the own ester of base, 10 grams of Homosalate, 8 grams of SPAN-80,7 grams of 18 carbonic acid, 12 grams of palmityl alcohol, polyglycerol distearate 8
Gram, 10 grams of lecithin, 12 grams of stearyl alcohol, 10 grams of butanediol.Continue to stir to whole dissolvings, obtain clear solution.Temperature is raised
To 85 DEG C, following composition is then sequentially added：8 grams of Phenylbenzimidazolesulfonic acid, Neo Heliopan AP 10
Gram, 8 grams of ethylhexyl methoxy cinnamate, 7 grams of p- methoxycinnamates isoamyl valerate, 5 grams of phenyl benzimidazole sulfonic acid, double-second
5 grams of base hexylphenol methylamino benzene piperazine, 5 grams of 4- Methylbenzylidene subunits camphor, 10 grams of PEG-25 p-aminobenzoic acid, isoamyl alcohol three
5 grams of Methoxycinnamate trisiloxanes, 8 grams of Uvinul T 150,6 grams of pentyl diformazan para amidocyanogen benzoic Acid, diethyl
6 grams of the own ester of hydroxy amino benzoylbenzoic acid, 3 grams of MBBT, 10 grams of forulic acid and
8 grams of Neo Heliopan E1000.Constant temperature stirring is kept, is continuously stirred under nitrogen protection 2 hours.Then with ultrasonically treated
30mim, treats gradually transparence, and room temperature is cooled to after being completely converted into capsule of nano solution using conventional technical means.
35 grams of isotriacontane, 20 grams of glycerine, 15 grams of isopropyl myristate, ethanol are sequentially added under mild agitation
1.5 grams of 30 grams, 2 grams of essence, 1.5 grams of methyl p-hydroxybenzoate and propylparaben；Then in above-mentioned solution, plus
Enter Baical Skullcap root P.E 1.2g, ginkgo biloba extract 2g.
Whole mixings are treated, obtains and stops stirring after uniform solution.
The embedding rate of the capsule of nano of 1~embodiment of embodiment 4 is detected, embodiment 1~implementation is as a result shown
The microcapsule embedded rate of example 4 is more than 95%, with good embedding effect.
Embodiment 5
Performance to the suntan lotion prepared by embodiment 1~2 carries out entry evaluation.
This embodiment uses following 3 kinds of suntan lotions as a comparison case：
Comparative example 1：In preparation process, sun-proof component is handled without capsule of nanoization, also without plant extract
Thing, other components and other preparation processes are same as Example 2.
Comparative example 2：In preparation process, sun-proof component is handled without capsule of nanoization, plant extracts is added,
Its component and other preparation processes are same as Example 2.
Comparative example 3：In preparation process, capsule of nano processing is carried out to sun-proof component, but without plant extract
Thing, remaining component and other preparation processes are same as Example 2.
Smearing comfort level, SPF and water resistance are carried out to suntan lotion prepared by embodiment 1~2 and comparative example 1~3
Detection.
Smear comfort level detection：The people of personnel 100 of selection 20~40 years old, is divided into 5 groups, and everyone takes 0.2 gram of product painting
Smear the description that direct feel is carried out in the back of the hand.
SPF is detected：Detected using SPF measuring instruments.
Water resistance is detected：The people of personnel 100 of selection 20~40 years old, is divided into 5 groups, everyone takes appropriate product to be applied to
On the back of the hand, clear water then is sprayed in hand, is gently dried with cotton pads, observation hand scribble effect and cotton pads dizzy dye situation,
Tester is given a mark according to result, is finally averaged.
Comparative example 1, comparative example 2, smearing comfort level, SPF and the water resistance of comparative example 3 and embodiment 1~2
It is as shown in the table：
As seen from the above table, the suntan lotion after being handled in 1~embodiment of the embodiment of the present invention 2 using microencapsulation, it is smeared
Uniformly, preferably, water resistance is preferable, and SPF is higher, and performance is more excellent for comfort level.
Embodiment 6
Performance and prior art to the suntan lotion prepared by embodiment 1~2 are contrasted.
In the prior art, Chinese patent CN104000740A disclose it is a kind of coat sun-screening agent the sun-proof grain of solid lipid and
Its preparation method, regard the embodiment 1 in Chinese patent CN104000740A as control group of the invention.
Experiment one：The ultraviolet absorption ability of embodiment 1~2 and control group is characterized, using ultraviolet-visible light
Spectrometer carries out detection product and passes through ability to 280-400nm ultraviolet.
Testing result is as follows：The ultraviolet radiation absorption light transmittance of the embodiment of the present invention 1~2 be 6~8%, control group it is ultraviolet
Line absorption light transmittance is 8~14%, it can thus be appreciated that the ultraviolet absorption ability of suntan lotion of the present invention is better than control group.
Experiment two：The water resistance of embodiment 1~2 and control group is detected using artificial skin, 0.2 gram of production is taken
Product are applied on artificial skin, are immersed in the water 20min, are then detected using ultraviolet-visible spectrometer.
Testing result is as follows：The ultraviolet radiation absorption light transmittance of the embodiment of the present invention 1~2 is 10~15%, the purple of control group
Outer line absorption light transmittance is 25~40%, and contrast can be obtained, the UV absorption printing opacity of the suntan lotion described in the embodiment of the present invention 1~2
Rate only rises 4~7%, and the ultraviolet radiation absorption light transmittance of control group rises 17~26%, from the foregoing, it will be observed that of the present invention
Suntan lotion water resistance be better than control group.
The present invention is got up sun-prevention component embedding by microcapsules technology, is solved well after suntan lotion is smeared easily by sweat
The problem of dissolving such as water, rainwater, seawater comes off, and add with sun-proof and after-sun function plant extracts, make to be made
Suntan lotion can play sun-proof and after-sun double effects simultaneously in use, just can be right in the short time after solarization
Skin after solarization is repaired.
The specific embodiment of the present invention is described in detail above, but it is only used as example, and the present invention is not intended to limit
In particular embodiments described above.To those skilled in the art, it is any to the practicality carry out equivalent modifications and replace
In generation, is also all among scope of the invention.Therefore, the equalization made without departing from the spirit and scope of the invention is converted and repaiied
Change, all should be contained within the scope of the invention.
Claims (7)
1. a kind of suntan lotion, it is characterised in that including following component：First sunscreen composition, the second sunscreen composition, different 30
Carbon alkane, glycerine, isopropyl myristate, ethanol, essence, methyl p-hydroxybenzoate, propylparaben and water；
Wherein, first sunscreen composition include sorbitan monooleate, ethylhexyl salicylate, Homosalate,
SPAN-80,18 carbonic acid, palmityl alcohol, polyglycerol distearate, lecithin, stearyl alcohol, butanediol；
Wherein, second sunscreen composition includes Phenylbenzimidazolesulfonic acid, Neo Heliopan AP, methoxy
Base 2-Ethylhexyl cinnamate, p- methoxycinnamates isoamyl valerate, phenyl benzimidazole sulfonic acid, double-ethylhexylphenol methylamino
Benzene piperazine, 4- Methylbenzylidene subunits camphor, PEG-25 p-aminobenzoic acid, isoamyl alcohol trimethoxy cinnamic acid ester trisiloxanes, second
Base hexyl triazinone, pentyl diformazan para amidocyanogen benzoic Acid, the own ester of diethylamino hydroxybenzoyl benzoylbenzoic acid, di-2-ethylhexylphosphine oxide-
BTA base tetramethyl butyl phenol, forulic acid and Neo Heliopan E1000.
2. a kind of suntan lotion according to claim 1, it is characterised in that the component has following parts by weight：
3. a kind of suntan lotion according to claim 2, it is characterised in that the weight of each component in first sunscreen composition
Measure number as follows：
4. a kind of suntan lotion according to claim 2, it is characterised in that the weight of each component in second sunscreen composition
Measure number as follows：
5. a kind of method for preparing suntan lotion as claimed in claim 1, it is characterised in that comprise the following steps：
Step a, 70~80 DEG C are heated water to, the first sunscreen composition is added under agitation, clear solution is obtained；
Step b, the clear solution prepared in step a is heated to 75~85 DEG C, adds the second sunscreen composition, keep constant temperature to stir
Mix, and continuously stirred 2 hours under the protection of inert atmosphere, obtain nontransparent solution；
Step c, obtained nontransparent solution in step b carried out it is ultrasonically treated, until solution transparence, by the solution of transparence
Capsule of nano solution is prepared into, room temperature is cooled to；
Step d, under mild agitation, isotriacontane, third are sequentially added in step c in obtained capsule of nano solution
Triol, isopropyl myristate, ethanol, essence, methyl p-hydroxybenzoate and propylparaben, are stirred and evenly mixed, and are obtained
Obtain homogeneous suntan lotion.
6. method according to claim 5, it is characterised in that the inert atmosphere in the step b is argon gas or nitrogen.
7. method according to claim 5, it is characterised in that the ultrasonic time in the step c is 10min~30min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710248447.4A CN106983685A (en) | 2017-04-17 | 2017-04-17 | A kind of suntan lotion and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710248447.4A CN106983685A (en) | 2017-04-17 | 2017-04-17 | A kind of suntan lotion and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106983685A true CN106983685A (en) | 2017-07-28 |
Family
ID=59416239
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710248447.4A Pending CN106983685A (en) | 2017-04-17 | 2017-04-17 | A kind of suntan lotion and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106983685A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107519025A (en) * | 2017-08-23 | 2017-12-29 | 中山大学惠州研究院 | A kind of hydrophobic sun-proof microcapsules and preparation method thereof |
| CN110314127A (en) * | 2019-08-23 | 2019-10-11 | 杭州千岛湖蓝色天使实业有限公司 | One kind is dispelled striae of pregnancy essence cream and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103083203A (en) * | 2013-01-30 | 2013-05-08 | 曼秀雷敦(中国)药业有限公司 | Sunscreen composition and preparation method thereof |
| CN103816056A (en) * | 2014-03-14 | 2014-05-28 | 天津孚信科技有限公司 | Human body surface coating object containing photochromic sunblock particles |
| CN103932908A (en) * | 2014-04-25 | 2014-07-23 | 北京博辉瑞进生物科技有限公司 | Composition for face whitening and preparation method thereof |
| CN105163706A (en) * | 2013-02-28 | 2015-12-16 | 塔格拉生物技术有限公司 | Microcapsules comprising sunscreen agents |
| CN105434327A (en) * | 2016-01-22 | 2016-03-30 | 蔡婷婷 | Total-effect type skin-moistening sun cream |
| CN105534737A (en) * | 2015-12-31 | 2016-05-04 | 广州市科能化妆品科研有限公司 | Fresh and cool sun-resistant composition with grease controlling function |
| CN106176259A (en) * | 2016-08-31 | 2016-12-07 | 天津达仁堂京万红药业有限公司 | A kind of sunscreen cream with dual resisteance and after-sun effect |
-
2017
- 2017-04-17 CN CN201710248447.4A patent/CN106983685A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103083203A (en) * | 2013-01-30 | 2013-05-08 | 曼秀雷敦(中国)药业有限公司 | Sunscreen composition and preparation method thereof |
| CN105163706A (en) * | 2013-02-28 | 2015-12-16 | 塔格拉生物技术有限公司 | Microcapsules comprising sunscreen agents |
| CN103816056A (en) * | 2014-03-14 | 2014-05-28 | 天津孚信科技有限公司 | Human body surface coating object containing photochromic sunblock particles |
| CN103932908A (en) * | 2014-04-25 | 2014-07-23 | 北京博辉瑞进生物科技有限公司 | Composition for face whitening and preparation method thereof |
| CN105534737A (en) * | 2015-12-31 | 2016-05-04 | 广州市科能化妆品科研有限公司 | Fresh and cool sun-resistant composition with grease controlling function |
| CN105434327A (en) * | 2016-01-22 | 2016-03-30 | 蔡婷婷 | Total-effect type skin-moistening sun cream |
| CN106176259A (en) * | 2016-08-31 | 2016-12-07 | 天津达仁堂京万红药业有限公司 | A kind of sunscreen cream with dual resisteance and after-sun effect |
Non-Patent Citations (1)
| Title |
|---|
| 徐阳等: "《化妆品质量检验》", 30 June 2016, 中国质检出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107519025A (en) * | 2017-08-23 | 2017-12-29 | 中山大学惠州研究院 | A kind of hydrophobic sun-proof microcapsules and preparation method thereof |
| CN110314127A (en) * | 2019-08-23 | 2019-10-11 | 杭州千岛湖蓝色天使实业有限公司 | One kind is dispelled striae of pregnancy essence cream and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110075007B (en) | Oil-in-water sunscreen product with waterproof and skin elasticity improving functions and preparation method thereof | |
| CN102973471B (en) | Antiaging sunscreen cream containing natural plant active ingredients and preparation method thereof | |
| CN105434188A (en) | Sunscreen cream and preparation method thereof | |
| CN102327196A (en) | Sun-proof BB (Blemish Balm) cream and preparation method thereof | |
| CN106619227B (en) | Compound grease, using suncream of the compound grease and preparation method thereof | |
| CN101336874A (en) | Water-solubility active extract in fruit skin, preparation method and use thereof | |
| CN106309147A (en) | Sunscreen cosmetic composition with high safeness and preparation method thereof | |
| CN109199878A (en) | A kind of whitening sun protection W/O/W multiple emulsion and preparation method thereof | |
| CN109077974B (en) | Waterproof and sweat-resistant all-band sunscreen skin care product | |
| CN107296775A (en) | Skin matrix, preparation method and applications and cosmetics and preparation method thereof | |
| CN106983685A (en) | A kind of suntan lotion and preparation method thereof | |
| CN106511151B (en) | A kind of chlorophyll is sun-proof and after-sun skin care item | |
| CN107929124A (en) | One kind isolation sunscreen composition | |
| CN1356100A (en) | Composition containing at least one altraviolet shielding agent and the third position unsabstituted for colouring skin and its usage | |
| KR101128591B1 (en) | Marine red algae extract mixture and cosmetic composition comprising the same | |
| CN107982096A (en) | A kind of suncream | |
| CN108309819A (en) | A kind of oil-in-water type suncream of high spf value and preparation method thereof | |
| CN104586706B (en) | A kind of Phellinus suncream and preparation method thereof | |
| CN111150673B (en) | Ultraviolet-resistant and blue-light-resistant composition and application thereof | |
| CN111150670B (en) | Anti-ultraviolet and anti-blue-light liquid crystal nano-lipid liquid and preparation method thereof | |
| CN109316395A (en) | A kind of fullerene suncream | |
| CN102813710A (en) | Chinese herbal compound composition for preventing sunlight skin injury and application of chinese herbal compound composition | |
| CN107049883A (en) | A kind of preparation method of sunflower seed extract and its application in cosmetics | |
| CN106344431A (en) | Sunscreen | |
| KR20160092910A (en) | Cosmetics of water insoluble sponge containing cosmetic compositions of sunscreen function |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170728 |
|
| RJ01 | Rejection of invention patent application after publication |