CN109316395A - A kind of fullerene suncream - Google Patents
A kind of fullerene suncream Download PDFInfo
- Publication number
- CN109316395A CN109316395A CN201811179230.3A CN201811179230A CN109316395A CN 109316395 A CN109316395 A CN 109316395A CN 201811179230 A CN201811179230 A CN 201811179230A CN 109316395 A CN109316395 A CN 109316395A
- Authority
- CN
- China
- Prior art keywords
- parts
- fullerene
- suncream
- inonotus obliquus
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of fullerene suncreams, include the following raw material: water phase: deionized water, inonotus obliquus extract, titanium dioxide, 1,3-BDO, glycine betaine；Oily phase: fullerene, hydroxyl benzothiazole, ethoxy urea, oxybenzone, OctMet, vaseline, stearyl alcohol, glyceryl monostearate, polyethyl acrylate, fenxizisu, preservative.Fullerene suncream of the present invention, pass through the complex role of oil phase and water phase that different component content forms, the suncream produced has excellent sun-proof result and water resistant effect, stability is good, effectively stop irradiation of the ultraviolet light to skin, the fullerene and inonotus obliquus extract added in raw material plays synergistic function to the effect of suncream.In addition, in use to the non-stimulated fanout free region of skin, safety in utilization is good.
Description
Technical field
The present invention relates to cosmetic technical fields more particularly to a kind of fullerene suncream and preparation method thereof.
Background technique
With the development of society, the raising of quality of life, damage of the ultraviolet light to human skin oneself more and more by people
Recognized, sunscreen product number of species are also growing in the market, have suncream, sunscreen, sunscreen spray etc., simultaneously
The product of high, medium and low times of SPF is complete, and all sunscreen products are all based on antiultraviolet.
Ultraviolet light has very big injury to skin, B16 cell can be made to increase.Lead to pigmentation, such as blackspot occur,
Freckle, the various color spots such as chloasma increase, and increase, deepen；Keratinocyte hyperplasia, dermal collagen fiber and elastomer
It destroys, can lead to pachyderma, relaxation, coarse and formation wrinkle；Telangiectasis can produce erythema；Skin immune function controlling
Decline, can form cutaneum carcinoma or precancerous lesion, such as light keratosis, squamous cell carcinoma, melanoma etc..
Ultraviolet light is four wave bands: UVA wave band, UVB wave band, UVC wave band and UVD wave band according to wavelength division.UVA is also known as
Wave-length coverage for long wave blackspot effect ultraviolet light, wave band is 320~400nm, it has very strong penetration power, can be penetrated big
Partially transparent glass and plastics, 98% long wave ultraviolet is had more than in daylight can penetrate ozone layer and cloud layer reaches the earth
Surface, UVA can go directly the skin corium of skin, elastomer and collagen fabric be destroyed, by our skin tanning；UVB wave
Section, is also known as medium wave erythemal effect ultraviolet wavelength, and wavelength band is 275~320nm, has medium penetration power, its wavelength
Shorter part can be absorbed by transparent glass, and most of ultraviolet B radiation is absorbed by ozone layer, only can reach in ground less than 2%
Ball surface, UVB ultraviolet light have erythema effect to human body, can promote the formation of internal mineral metabolism and vitamin D, but long-term
Or excessive exposure can enable skin tanning, and cause red and swollen decortication.The ultraviolet wavelength of UVC wave band and UVD wave band is shorter, penetrates energy
Power is too weak, can not penetrate most transparent glass and plastics, reaches earth label in daylight and is almost fully absorbed by ozone layer, prevents
(long wave blackspot effect is ultraviolet for the wave band and UVA that the protective range for shining frost is mainly protection UVB (medium wave blackspot effect ultraviolet light)
Line) wave band.
Sun-screening agent is divided into physical sunscreen agent and chemical sun.Most typical physical sunscreen agent is titanium dioxide and oxidation
Zinc, physical sunscreen agent are the modes covered using physics using light-reflecting particles, stop, reflect or scatter ultraviolet light, make to reach
The amount of ultraviolet of skin is reduced sun-proof to achieve the purpose that, physical sunscreen agent generally stays in skin surface, does not change
Reaction is learned, so milder to skin.As sun-screening agent, the screening ability to UVA and UVB is that have difference for titanium dioxide and zinc oxide
Different, titanium dioxide is 250-340nm to the guard band of ultraviolet light, and zinc oxide is 290-380nm to the guard band of ultraviolet light.
General chemical sun is easier to be absorbed by the skin, and the sunscreen products of high spf value easily cause skin allergy.But chemical sun
The shortcomings that be: some only resists UVA, and some only resists UVB, not wide enough to the wave-length coverage of ultraviolet radiation absorption.
Nowadays, people especially women is increasingly particular about oneself skin, especially in terms of whitening.And sun-screening agent
Water repelling property is also increasingly taken seriously.Because sweat, seawater, swimming-pool water etc. are all that we want problems faced, for room
For outer movement, travel enthusiasts, the water repelling property of sun-screening agent is extremely important.Suncream currently on the market is usually chance water can
Molten type, people swimming when be not available, field swim when can also encounter exposure the case where, this, which has brought, asks
Topic.Especially there are sunscreen cosmetic the cosmetics of high sun-proof efficiency usually to use in summer outdoor sports, season and use
The characteristics of environment require sunscreen product have a water resisting property can, i.e., be still able to maintain under the embathing of sweat or when swimming certain
Sun-proof result.The development of sunscreen cosmetic waterproof performance just becomes the fresh target that cosmetic industry is constantly pursued as a result,.
The present invention provides a kind of fullerene suncream, has excellent sun-proof result and water resistant effect, stability is good, effectively
Ground stops irradiation of the ultraviolet light to skin, while certain sun-proof effect can be still kept under the embathing of sweat or when swimming
Fruit, and to the non-stimulated fanout free region of skin.
Summary of the invention
Technical problem to be solved by the present invention lies in, provide it is a kind of with excellent sun-proof result and water resistant effect,
Stability is good and the luxurious suncream of fullerene to the non-stimulated fanout free region of skin.
Present invention fullerene suncream to be provided, is achieved by following technical solution:
A kind of fullerene suncream, includes water phase and oil-phase component.
As a preferred embodiment, the water phase is prepared by the raw material comprising following parts by weight: deionized water 60
~75 parts, 6~12 parts of inonotus obliquus extract, 3~8 parts of titanium dioxide, 0.5~2 part of 1,3-BDO, 1.5~3 parts of glycine betaine.
As a preferred embodiment, the water phase is prepared by the raw material comprising following parts by weight: deionized water 65
~70 parts, 8~10 parts of inonotus obliquus extract, 5~6 parts of titanium dioxide, 1~1.5 part of 1,3-BDO, 2~2.5 parts of glycine betaine.
As a kind of optimal case, the water phase is prepared by the raw material comprising following parts by weight: deionized water 68
Part, 9 parts of inonotus obliquus extract, 5.5 parts of titanium dioxide, 1.3 parts of 1,3- butanediol, 2.2 parts of glycine betaine.
As a preferred embodiment, the preparation method of the inonotus obliquus extract, comprises the following steps:
(1) inonotus obliquus powder is taken, soak is added；The soak is prepared by solvent of distilled water, containing mass concentration 6~
9% dimethyl sulfoxide and 8~11% sodium hydroxides, the dosage of soak are 5.5~6.5 times of inonotus obliquus powder weight, make to soak
Bubble liquid is completely soaked powder, and mixture stands 2~3h under room temperature, obtains mixture 1；
(2) mixture 1 is filtered, and obtains filter residue；
(3) distilled water is added in filter residue, the additional amount of distilled water presses liquid-solid ratio distilled water: filter residue=6~8ml:1g is added,
75~85 DEG C are heated to, 2~4h is kept the temperature, obtains filtrate after filtering；
(4) drying obtains inonotus obliquus extract after mixing filtrate.
As a preferred embodiment, the oily phase, is prepared by the raw material comprising following parts by weight: fullerene 8~
14 parts, 0.5~2.5 part of hydroxyl benzothiazole, 1~3 part of ethoxy urea, 2~5 parts of oxybenzone, OctMet 2~
7 parts, 4~7 parts of vaseline, 2.5~6 parts of stearyl alcohol, 2.5~5 parts of glyceryl monostearate, polyethyl acrylate 0.8~1.5
Part, 0.2~0.9 part of fenxizisu, 0.1~0.3 part of preservative.
As a preferred embodiment, the oily phase, is prepared by the raw material comprising following parts by weight: fullerene 10~
12 parts, 1~2 part of hydroxyl benzothiazole, 1.5~2.5 parts of ethoxy urea, 3~4 parts of oxybenzone, OctMet 4~
5 parts, 5~6 parts of vaseline, 3.5~5 parts of stearyl alcohol, 3~4.5 parts of glyceryl monostearate, 1~1.2 part of polyethyl acrylate,
0.4~0.7 part of fenxizisu, 0.15~0.25 part of preservative.
As a kind of optimal case, the oily phase is prepared: fullerene 11 by the raw material comprising following parts by weight
Part, 1.5 parts of hydroxyl benzothiazole, 2 parts of ethoxy urea, 3.5 parts of oxybenzone, 4.5 parts of OctMet, vaseline
5.5 parts, 4 parts of stearyl alcohol, 4 parts of glyceryl monostearate, 1.1 parts of polyethyl acrylate, 0.5 part of fenxizisu, preservative 0.2
Part.
As a preferred embodiment, the preservative in the oily phase is iodopropynyl butyl formate.
As a preferred embodiment, the fullerene suncream, is prepared by comprising the following steps:
S1. respectively by oily phase and heated aqueous to 60~80 DEG C of dissolutions；
S2. after the titanium dioxide of aqueous portion fully disperse, during the oil phase is added to the aqueous phase, 2000~3000r/
Min stirs 15~20min, obtains fullerene suncream after cooling.
The utility model has the advantages that fullerene suncream of the present invention, the oil phase being made up of different component content and water phase
Complex role, the suncream produced have excellent sun-proof result and water resistant effect, and stability is good, effectively stops ultraviolet light
Irradiation to skin, the fullerene and inonotus obliquus extract added in raw material play synergistic function to the effect of suncream.
In addition, in use to the non-stimulated fanout free region of skin, safety in utilization is good.
Specific embodiment
It is explained further the present invention with reference to embodiments, but embodiment do not do any form to the present invention and limit.
A kind of fullerene suncream of embodiment 1
Composition of raw materials:
Water phase: 68 parts of deionized water, 9 parts of inonotus obliquus extract, 5.5 parts of titanium dioxide, 1.3 parts of 1,3-BDO, beet
2.2 parts of alkali；
Oily phase: 11 parts of fullerene, 1.5 parts of hydroxyl benzothiazole, 2 parts of ethoxy urea, 3.5 parts of oxybenzone, to methoxyl group meat
4.5 parts of cinnamate, 5.5 parts of vaseline, 4 parts of stearyl alcohol, 4 parts of glyceryl monostearate, 1.1 parts of polyethyl acrylate, wind
Sub- 0.5 part, 0.2 part of iodopropynyl butyl formate of element.
The inonotus obliquus extract the preparation method comprises the following steps:
(1) inonotus obliquus powder is taken, soak is added, which prepares by solvent of distilled water, contains mass concentration 8%
Dimethyl sulfoxide and 9% sodium hydroxide, the dosage of soak are 6 times of inonotus obliquus powder weight, and soak is made to be completely soaked powder
End, mixture stand 2.5h under room temperature, obtain mixture 1；
(2) mixture 1 is filtered, and obtains filter residue；
(3) distilled water is added in filter residue, the additional amount of distilled water presses liquid-solid ratio distilled water: filter residue=7ml:1g is added, and adds
Heat keeps the temperature 3h, obtains filtrate after filtering to 80 DEG C；
(4) drying obtains inonotus obliquus extract after mixing filtrate.
The preparation method of the suncream:
S1. respectively by oily phase and heated aqueous to 70 DEG C of dissolutions；
S2. after the titanium dioxide of aqueous portion fully disperse, during the oil phase is added to the aqueous phase, 2500r/min is stirred
20min is mixed, obtains fullerene suncream after cooling.
A kind of fullerene suncream of embodiment 2
Composition of raw materials:
Water phase: 60 parts of deionized water, 6 parts of inonotus obliquus extract, 3 parts of titanium dioxide, 0.5 part of 1,3-BDO, glycine betaine
1.5 part；
Oily phase: 8 parts of fullerene, 0.5 part of hydroxyl benzothiazole, 1 part of ethoxy urea, 2 parts of oxybenzone, p-methoxycinnamic acid
2 parts of monooctyl ester, 4 parts of vaseline, 2.5 parts of stearyl alcohol, 2.5 parts of glyceryl monostearate, 0.8 part of polyethyl acrylate, fenxizisu
0.2 part, 0.1 part of iodopropynyl butyl formate.
The preparation method of the inonotus obliquus extract of embodiment 2 is same as Example 1.
The preparation method of embodiment 2 is same as Example 1.
A kind of fullerene suncream of embodiment 3
Composition of raw materials:
Water phase: 75 parts of deionized water, 12 parts of inonotus obliquus extract, 8 parts of titanium dioxide, 2 parts of 1,3-BDO, glycine betaine 3
Part；
Oily phase: 14 parts of fullerene, 2.5 parts of hydroxyl benzothiazole, 3 parts of ethoxy urea, 5 parts of oxybenzone, to methoxycinnamate
7 parts of misery ester, 7 parts of vaseline, 6 parts of stearyl alcohol, 5 parts of glyceryl monostearate, 1.5 parts of polyethyl acrylate, fenxizisu 0.9
Part, 0.3 part of iodopropynyl butyl formate.
The preparation method of the inonotus obliquus extract of embodiment 3 is same as Example 1
The preparation method of embodiment 3 is same as Example 1.
A kind of fullerene suncream of embodiment 4
The composition of raw materials of embodiment 4 is same as Example 1.
The preparation method of the inonotus obliquus extract of embodiment 4 is same as Example 1
The suncream the preparation method comprises the following steps:
S1. respectively by oily phase and heated aqueous to 60 DEG C of dissolutions；
S2. after the titanium dioxide of aqueous portion fully disperse, oil phase part point is added in water phase, 2000r/
Min stirs 15min, obtains fullerene suncream after cooling.
A kind of fullerene suncream of embodiment 5
The composition of raw materials of embodiment 5 is same as Example 1.
The preparation method of the inonotus obliquus extract of embodiment 4 is same as Example 1.
The suncream the preparation method comprises the following steps:
S1. oil phase part point and aqueous portion are dissolved by heating at 80 DEG C respectively；
S2. the titanium dioxide of aqueous portion is carried out after fully dispersing, oil phase part point is added in water phase, 3000r/
Min stirs 20min, obtains fullerene suncream after cooling.
Comparative example 1
Comparative example 1 is difference from example 1 is that the oil of composition of raw materials is mutually added to 11 parts by weight fowlers less
Alkene, in water phase to be added to 11 parts by weight inonotus obliquus extracts, remaining component, the preparation method of inonotus obliquus extract and sun-proof more
The preparation method of frost is same as Example 1.
Comparative example 2
Comparative example 2 is difference from example 1 is that the water phase of composition of raw materials is added to 9 parts by weight inonotus obliquus less
Extract, in oily phase to be added to 9 parts by weight fullerenes, the preparation method of remaining component and suncream is same as Example 1 more.
Comparative example 3
Comparative example 3 is difference from example 1 is that the water phase of composition of raw materials is added to 9 parts by weight inonotus obliquus less
Extract is added to 11 parts by weight fullerenes in oily phase less, remaining component and preparation method are same as Example 1.
Comparative example 4
The suncream containing fullerene of certain commercially available brand.
Comparative example 5
Composition of raw materials:
Water phase: 68 parts of deionized water, 9 parts of inonotus obliquus extract (being purchased from Xi'an legendary god of farming Biotechnology Co., Ltd), dioxy
Change 5.5 parts of titanium, 1.3 parts of 1,3-BDO, 2.2 parts of glycine betaine；
Oily phase: 11 parts of fullerene, 1.5 parts of hydroxyl benzothiazole, 2 parts of ethoxy urea, 3.5 parts of oxybenzone, to methoxyl group meat
4.5 parts of cinnamate, 5.5 parts of vaseline, 4 parts of stearyl alcohol, 4 parts of glyceryl monostearate, 1.1 parts of polyethyl acrylate, wind
Sub- 0.5 part, 0.2 part of iodopropynyl butyl formate of element.
The composition of raw materials of comparative example 5 the difference from embodiment 1 is that, replaced in water phase with general commercially available inonotus obliquus extract
For inonotus obliquus extract of the present invention, remaining component and content are identical；The preparation method and implementation of the suncream of comparative example 5
Example 1 is identical.
Effect test:
The two indices of suncream, one is SPF (Sun Protection Factor), SPF；One is water resistant
Performance.The sun-proof result of fullerene suncream of the invention will be evaluated by measurement These parameters below.
Test case 1
External SPF (Sun Protection Factor) index test method:
SPF is the height for the sun-proof efficiency that sun protection factor characterization sun-proof articles can play.SPF sun protection factor is suitable for
Everyone, it is determined according to the minimum Erythema Dose of skin.Skin is rubescent after solarization, medically known as " erythema
Disease ", this is the most slight reaction that skin makes solarization.Minimum Erythema Dose, when being that skin the most short solarization of erythema occurs
Between.After sun-proof articles, the minimum Erythema Dose of skin can increase.Calculation method are as follows: assuming that the intensity of ultraviolet light will not be because
Time changes, if a people without any sun-proof measure skin after 20min in the sun can redden, when he uses
When SPF15 sunscreen products, indicate that 15 times of time can be extended, that is, skin just can be by sunburn after 300min.Calculation formula is such as
Under:
The minimum Erythema Dose of SPF=(after sun-proof articles)/minimum Erythema Dose (with before sun-proof articles)
And PA value standard uses Japanese cosmetic Industry Association with PA (Protection grade ofUVA, PA) expression
The degree of protection of UVA.PA is classified according to UVA protecting factor (Protection factor of UVA, PFA), wherein
PFA=smears the MPPD value of sunscreen products skin/do not smear the MPPD value of sunscreen products skin, and MPPD has guided visible melanism or color
Ultraviolet light lowest dose level (J/m2) or most short irradiation time needed for plain calm amount.The representation method of protection UVA gradation of effects is:
2≤PFA < 4 is PA+；4≤PFA is PA++ less than 8；8≤PFA≤16 are PA+++；PFA > 16 is PA++++.
Test method: background curve is tested using blank quartz plate before test, then precise 0.2mg/cm2 sample is in 3M
On adhesive tape face, then with the finger rapid application homogeneous sample for taking latex finger cot.Certainly with shady place by the sample panel after smearing
So dry 30min, is then measured using ultraviolet ray transmissivity analyzer, the sun-proof value of UVA and UVB can be measured, respectively with PA
Value is indicated with spf value.Test result is as shown in table 1.
Test case 2
The measuring method of the water repelling property: " makeup that test method is promulgated for 2007 referring to Ministry of Health of the People's Republic of China
Product hygienic practice " in about sunscreen cosmetic waterproof performance measuring method.
20-40 years old subject is selected, men and women is fifty-fifty, health, rule of life, and no skin disease is randomly divided into 10 groups,
Every group of 10 people, every group of suncream for using Examples 1 to 5 and comparative example 1~5 respectively are 25 DEG C in water temperature, the fresh room of water quality
The water-resistance test that 120 min are carried out in interior pond smears suncream at tested skin position, waits 20min, then allow tested
Person move freely 30min in water, is then discharged rest 10min, forbids wiping experiment position, repeats to wait after water is discharged 4 times
Skin natural air drying.It is constant that water temperature, room temperature and relative humidity are controlled in test process.Finally carried out using SPF measuring method
Ultraviolet light irradiation and measurement.Test result is as shown in table 1.
Sun-proof, the water resistant effect assessment of 1 suncream of table
It can be seen that by 1 data of table, in the embodiment of the present invention 1~5, embodiment 1 is preferred plan, sun-proof, water resistant effect effect
Fruit is best；Embodiment 1 is compared with embodiment 4~5, it is seen that if operating parameter is different from embodiment 1, what is be prepared is sun-proof
Sun-proof, the water resistant effect of frost can be declined；Embodiment 1 is compared with comparative example 1, it is seen that is added to the anti-of the suncream of fullerene
Solarization, water resistant obvious effect are good very much；Embodiment 1 is compared with comparative example 2, it is seen that adding inonotus obliquus extract less will cause suncream
The decline of sun-proof, water resistant effect；Embodiment 1 is compared with comparative example 3, it is seen that adds inonotus obliquus extract less and fullerene causes
The sun-proof of suncream, water resistant effect decline most serious；Embodiment 1 compared with comparative example 4, suncream of the present invention than it is commercially available certain
Brand suncream has in terms of sun-proof, water resistant effect to be obviously improved；Embodiment 1 is compared with comparative example 5, if with general city
It sells inonotus obliquus extract substitution and obtains inonotus obliquus extract by preparation method of the present invention, suncream is in sun-proof, water resistant effect
Also it will substantially reduce.In conclusion the sun-proof water repelling property of fullerene suncream of the present invention is excellent, the richness added in raw material
It strangles alkene and inonotus obliquus extract plays synergistic function to the effect of suncream.In addition, stingless to skin in use
Swash fanout free region, safety in utilization is good.
Claims (9)
1. a kind of fullerene suncream, which is characterized in that the fullerene suncream is by water phase and oily phase composition.
2. fullerene suncream according to claim 1, which is characterized in that the water phase, by including following parts by weight
Raw material be prepared: 60 ~ 75 parts of deionized water, 6 ~ 12 parts of inonotus obliquus extract, 3 ~ 8 parts of titanium dioxide, 1,3-BDO 0.5
~ 2 parts, 1.5 ~ 3 parts of glycine betaine.
3. fullerene suncream according to claim 1, which is characterized in that the water phase, by including following parts by weight
Raw material be prepared: 65 ~ 70 parts of deionized water, 8 ~ 10 parts of inonotus obliquus extract, 5 ~ 6 parts of titanium dioxide, 1,3-BDO 1 ~
1.5 parts, 2 ~ 2.5 parts of glycine betaine.
4. fullerene suncream according to claim 1, which is characterized in that the water phase, by including following parts by weight
Raw material be prepared: 68 parts of deionized water, 9 parts of inonotus obliquus extract, 5.5 parts of titanium dioxide, 1.3 parts of 1,3-BDO, sweet tea
2.2 parts of dish alkali.
5. fullerene suncream according to claim 1, which is characterized in that the preparation side of the inonotus obliquus extract
Method comprises the following steps:
(1) inonotus obliquus powder is taken, soak is added, which prepares by solvent of distilled water, contains mass concentration 6 ~ 9% 2
Methyl sulfoxide and 8 ~ 11% sodium hydroxides, the dosage of soak are 5.5 ~ 6.5 times of inonotus obliquus powder weight, keep soak complete
Powder is impregnated, mixture stands 2 ~ 3h under room temperature, obtains mixture 1；
(2) mixture 1 is filtered, and obtains filter residue；
(3) distilled water is added in filter residue, the additional amount of distilled water presses liquid-solid ratio distilled water: filter residue=6 ~ 8ml:1g is added, and is heated to
75 ~ 85 DEG C, 2 ~ 4h is kept the temperature, obtains filtrate after filtering；
(4) drying obtains inonotus obliquus extract after mixing filtrate.
6. fullerene suncream according to claim 1, which is characterized in that the oily phase, by including following parts by weight
Raw material be prepared: 8 ~ 14 parts of fullerene, 0.5 ~ 2.5 part of hydroxyl benzothiazole, 1 ~ 3 part of ethoxy urea, 2 ~ 5 parts of oxybenzone,
2 ~ 7 parts of OctMet, 2.5 ~ 6 parts of stearyl alcohol, 2.5 ~ 5 parts of glyceryl monostearate, gathers 4 ~ 7 parts of vaseline
0.8 ~ 1.5 part of ethyl acrylate, 0.2 ~ 0.9 part of fenxizisu, 0.1 ~ 0.3 part of preservative.
7. fullerene suncream according to claim 1, which is characterized in that the oily phase, by including following parts by weight
Raw material be prepared: 10 ~ 12 parts of fullerene, 1 ~ 2 part of hydroxyl benzothiazole, 1.5 ~ 2.5 parts of ethoxy urea, oxybenzone 3 ~ 4
Part, 4 ~ 5 parts of OctMet, 5 ~ 6 parts of vaseline, 3.5 ~ 5 parts of stearyl alcohol, 3 ~ 4.5 parts of glyceryl monostearate,
1 ~ 1.2 part of polyethyl acrylate, 0.4 ~ 0.7 part of fenxizisu, 0.15 ~ 0.25 part of preservative.
8. fullerene suncream according to claim 1, which is characterized in that the oily phase, by including following parts by weight
Raw material be prepared: 11 parts of fullerene, 1.5 parts of hydroxyl benzothiazole, 2 parts of ethoxy urea, 3.5 parts of oxybenzone, to methoxyl group
4.5 parts of cinnamic acid monooctyl ester, 5.5 parts of vaseline, 4 parts of stearyl alcohol, 4 parts of glyceryl monostearate, 1.1 parts of polyethyl acrylate, wind
0.5 part, 0.2 part of preservative of element of letter.
9. fullerene suncream according to claim 1, which is characterized in that the preservative in the oil phase is iodopropynyl
Aminocarbamic acid butyl ester.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811179230.3A CN109316395A (en) | 2018-10-10 | 2018-10-10 | A kind of fullerene suncream |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811179230.3A CN109316395A (en) | 2018-10-10 | 2018-10-10 | A kind of fullerene suncream |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109316395A true CN109316395A (en) | 2019-02-12 |
Family
ID=65261178
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811179230.3A Withdrawn CN109316395A (en) | 2018-10-10 | 2018-10-10 | A kind of fullerene suncream |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109316395A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110613630A (en) * | 2019-09-30 | 2019-12-27 | 汕头大学 | Sunscreen cream containing benzophenone derivative nanocrystals and preparation method thereof |
| CN115120531A (en) * | 2022-08-01 | 2022-09-30 | 深圳先进高分子材料研究院 | High-efficiency sunscreen composition and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7195754B1 (en) * | 2002-02-26 | 2007-03-27 | Eikos, Inc. | Nanotube based sunscreen |
| CN104042481A (en) * | 2014-05-31 | 2014-09-17 | 青岛博泓海洋生物技术有限公司 | Moisturizing sunscreen cream |
| CN104840372A (en) * | 2015-02-01 | 2015-08-19 | 中国人民解放军第四军医大学 | Plateau sunscreen cream containing natural product echinacoside |
| CN106309510A (en) * | 2016-08-19 | 2017-01-11 | 广州滋得洛夫生物科技有限责任公司 | Inonotus obliquus complex and preparation method thereof |
| CN108524382A (en) * | 2018-07-25 | 2018-09-14 | 周恒� | A kind of sunscreen spray and preparation method thereof |
-
2018
- 2018-10-10 CN CN201811179230.3A patent/CN109316395A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7195754B1 (en) * | 2002-02-26 | 2007-03-27 | Eikos, Inc. | Nanotube based sunscreen |
| CN104042481A (en) * | 2014-05-31 | 2014-09-17 | 青岛博泓海洋生物技术有限公司 | Moisturizing sunscreen cream |
| CN104840372A (en) * | 2015-02-01 | 2015-08-19 | 中国人民解放军第四军医大学 | Plateau sunscreen cream containing natural product echinacoside |
| CN106309510A (en) * | 2016-08-19 | 2017-01-11 | 广州滋得洛夫生物科技有限责任公司 | Inonotus obliquus complex and preparation method thereof |
| CN108524382A (en) * | 2018-07-25 | 2018-09-14 | 周恒� | A kind of sunscreen spray and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 佚名: "《http://www.cosdna.com/chs/cosmetic_1c755679.html》", 19 March 2008, COSDNA * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110613630A (en) * | 2019-09-30 | 2019-12-27 | 汕头大学 | Sunscreen cream containing benzophenone derivative nanocrystals and preparation method thereof |
| CN110613630B (en) * | 2019-09-30 | 2022-08-30 | 汕头大学 | Sunscreen cream containing benzophenone derivative nanocrystals and preparation method thereof |
| CN115120531A (en) * | 2022-08-01 | 2022-09-30 | 深圳先进高分子材料研究院 | High-efficiency sunscreen composition and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106420471B (en) | It is a kind of to have sun-proof and after-sun function skin care item and preparation method thereof concurrently | |
| CN102327196A (en) | Sun-proof BB (Blemish Balm) cream and preparation method thereof | |
| CN102302417B (en) | Comprehensive-effect sunscreen lotion containing oceanic biological active substances | |
| CN108030718A (en) | A kind of sun-proof whitening and skin-protecting composition and preparation method thereof | |
| CN110559197B (en) | Sunscreen lotion and preparation method thereof | |
| CN102973471B (en) | Antiaging sunscreen cream containing natural plant active ingredients and preparation method thereof | |
| CN105381007B (en) | External medicine composition, preparation with white-skinned face function and its preparation method and application | |
| CN110151650A (en) | A kind of Red blood streak dispelling lotion and preparation method thereof of the ingredient of composite reactive containing horse chestnut | |
| CN107847418A (en) | Humectant composition and its method based on silk | |
| CN105434327A (en) | Total-effect type skin-moistening sun cream | |
| CN103340798A (en) | Natural plant sun cream and preparation process thereof | |
| CN109316395A (en) | A kind of fullerene suncream | |
| CN108014060B (en) | Sunscreen synergistic composition and application thereof | |
| CN110292543A (en) | It is a kind of substitute ultraviolet absorbing agent biological composition and its application | |
| CN114404330A (en) | Sunscreen composition and preparation method thereof | |
| CN104586706B (en) | A kind of Phellinus suncream and preparation method thereof | |
| CN108420779A (en) | A kind of sunscreen and preparation method thereof | |
| CN107982096A (en) | A kind of suncream | |
| CN106691977A (en) | Preparation method for natural compound plant extract sunscreen cream | |
| CN106074226A (en) | A kind of sunscreen composition and prepared cosmetics thereof | |
| CN107669514A (en) | A kind of skin care compositions and preparation method thereof and pigment frost and preparation method thereof | |
| CN106983685A (en) | A kind of suntan lotion and preparation method thereof | |
| CN106491477A (en) | A kind of skin care item and preparation method thereof | |
| CN108567727A (en) | A kind of sun-proof mud and preparation method thereof | |
| CN110279647A (en) | A kind of nti-freckle, cosmetic composition and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190212 |
|
| WW01 | Invention patent application withdrawn after publication |