CN106967986B - 一种具有分级结构的氢氧化镍/镍/石墨烯复合析氢电极的制备方法 - Google Patents
一种具有分级结构的氢氧化镍/镍/石墨烯复合析氢电极的制备方法 Download PDFInfo
- Publication number
- CN106967986B CN106967986B CN201710229319.5A CN201710229319A CN106967986B CN 106967986 B CN106967986 B CN 106967986B CN 201710229319 A CN201710229319 A CN 201710229319A CN 106967986 B CN106967986 B CN 106967986B
- Authority
- CN
- China
- Prior art keywords
- rgo
- electrode
- electro
- deposition
- combination electrode
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F17/00—Multi-step processes for surface treatment of metallic material involving at least one process provided for in class C23 and at least one process covered by subclass C21D or C22F or class C25
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1229—Composition of the substrate
- C23C18/1241—Metallic substrates
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/125—Process of deposition of the inorganic material
- C23C18/1283—Control of temperature, e.g. gradual temperature increase, modulation of temperature
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/02—Hydrogen or oxygen
- C25B1/04—Hydrogen or oxygen by electrolysis of water
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/02—Electrodes; Manufacture thereof not otherwise provided for characterised by shape or form
- C25B11/03—Electrodes; Manufacture thereof not otherwise provided for characterised by shape or form perforated or foraminous
- C25B11/031—Porous electrodes
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
- C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
- C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
- C25B11/073—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material
- C25B11/091—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of at least one catalytic element and at least one catalytic compound; consisting of two or more catalytic elements or catalytic compounds
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D15/00—Electrolytic or electrophoretic production of coatings containing embedded materials, e.g. particles, whiskers, wires
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Mechanical Engineering (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Electrodes For Compound Or Non-Metal Manufacture (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
Description
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710229319.5A CN106967986B (zh) | 2017-04-10 | 2017-04-10 | 一种具有分级结构的氢氧化镍/镍/石墨烯复合析氢电极的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710229319.5A CN106967986B (zh) | 2017-04-10 | 2017-04-10 | 一种具有分级结构的氢氧化镍/镍/石墨烯复合析氢电极的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106967986A CN106967986A (zh) | 2017-07-21 |
CN106967986B true CN106967986B (zh) | 2019-01-04 |
Family
ID=59336390
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710229319.5A Active CN106967986B (zh) | 2017-04-10 | 2017-04-10 | 一种具有分级结构的氢氧化镍/镍/石墨烯复合析氢电极的制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106967986B (zh) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107694584B (zh) * | 2017-10-15 | 2021-06-22 | 华东师范大学 | 一种自支撑磷化镍催化剂及其制备方法和应用 |
CN107761128B (zh) * | 2017-11-10 | 2019-12-03 | 上海应用技术大学 | 一种FeNiNC电极材料、制备方法及其应用 |
CN108144620B (zh) * | 2017-12-05 | 2020-11-06 | 西北工业大学 | 泡沫镍负载复合纳米金属氧化物电极材料制备方法 |
CN110885100B (zh) * | 2018-09-07 | 2023-04-14 | 湖北大学 | 一种分等级结构镍锰酸锂正极材料的制备方法 |
CN110129825B (zh) * | 2019-05-23 | 2022-02-01 | 天津市大陆制氢设备有限公司 | 一种高效Ni/Ni(OH)2析氢电极及其制备方法 |
CN111822000B (zh) * | 2020-06-11 | 2023-04-07 | 安徽师范大学 | 一种Pt纳米颗粒负载二氧化钼/氢氧化镍纳米片阵列结构材料及其制备方法和应用 |
CN112080760B (zh) * | 2020-09-15 | 2021-08-10 | 中南大学 | 一种氧化石墨烯掺杂氧化镍层/镍基复合材料及其制备方法与析氢电极的应用 |
CN112626554B (zh) * | 2020-12-15 | 2023-08-29 | 永州市产商品质量监督检验所 | 一种三维电解复合析氢材料的制备方法 |
CN112647092B (zh) * | 2020-12-18 | 2022-02-15 | 江苏大学 | 一种负载型镍基复合物析氢催化剂及其制备方法和应用 |
CN114618539B (zh) * | 2022-02-23 | 2023-04-07 | 燕山大学 | 一种分级结构硼氢化钠产氢催化剂及其制备方法和应用 |
CN115259139B (zh) * | 2022-06-14 | 2024-02-02 | 江西理工大学 | 一种碲化铋纳米化及其与碳纳米管薄膜复合的方法 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20120120995A (ko) * | 2011-04-25 | 2012-11-05 | 한국과학기술원 | 전이금속 산화물 또는 전이금속 수산화물 입자를 포함하는 그래핀 복합체 제조방법, 이에 의하여 제조된 그래핀 복합체 및 이를 포함하는 전하저장소자 |
KR102051871B1 (ko) * | 2012-09-19 | 2019-12-05 | 에스케이이노베이션 주식회사 | 그래핀 산화물 복합체, 이의 제조방법 및 이를 함유하는 전기화학적 에너지 저장장치 |
KR101641145B1 (ko) * | 2014-12-24 | 2016-07-20 | 인천대학교 산학협력단 | 폴리도파민을 이용한 촉매 합성법, 이에 의해 제조된 촉매, 및 이를 이용한 연료전지 |
US9601763B2 (en) * | 2015-03-27 | 2017-03-21 | Nanotek Instruments, Inc. | Process for mass-producing silicon nanowires and silicon nanowire-graphene hybrid particulates |
CN105070515A (zh) * | 2015-08-19 | 2015-11-18 | 华东理工大学 | 一种制备泡沫镍复合材料的方法和由此获得的泡沫镍复合材料及其应用 |
CN106087002B (zh) * | 2016-06-08 | 2018-07-03 | 燕山大学 | 一种3D结构Ni/rGO复合析氢电极的制备方法 |
CN106098414B (zh) * | 2016-07-27 | 2018-06-01 | 河南师范大学 | 一步水热法合成石墨烯-氢氧化镍复合物超级电容器电极的方法 |
-
2017
- 2017-04-10 CN CN201710229319.5A patent/CN106967986B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN106967986A (zh) | 2017-07-21 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN106967986B (zh) | 一种具有分级结构的氢氧化镍/镍/石墨烯复合析氢电极的制备方法 | |
Laszczyńska et al. | Electrocatalytic activity for the hydrogen evolution of the electrodeposited Co–Ni–Mo, Co–Ni and Co–Mo alloy coatings | |
CN106087002B (zh) | 一种3D结构Ni/rGO复合析氢电极的制备方法 | |
CN109234755A (zh) | 一种层状双金属氢氧化物复合结构电催化剂及制备方法 | |
Ding et al. | Rose-like Cu-doped Ni3S2 nanoflowers decorated with thin NiFe LDH nanosheets for high-efficiency overall water and urea electrolysis | |
CN107988617A (zh) | 水电解高效、双功能催化电极及其制备方法 | |
CN107326395B (zh) | 一种镍/氮掺杂的碳微球复合析氢电极的制备方法 | |
CN106191916A (zh) | 一种高效的多孔Ni‑Mo析氢电极及其制备方法 | |
Zhang et al. | Two-step preparation of porous nickel-sulfur electrode for hydrogen evolution in alkaline water electrolysis | |
CN110129825B (zh) | 一种高效Ni/Ni(OH)2析氢电极及其制备方法 | |
Niu et al. | Ultrarapid synthesis Ni-Cu bifunctional electrocatalyst by self-etching electrodeposition for high-performance water splitting reaction | |
CN110280249A (zh) | 一种非贵金属NiCoFe/NF电催化剂的制备方法及其氧气析出应用 | |
WO2020252820A1 (zh) | 镍铁催化材料、其制备方法及在电解水制氢气、制备液态太阳燃料中的应用 | |
CN108671944A (zh) | 一种镍钼氧化物@镍钼硫化物@泡沫镍复合纳米材料及其制备方法与应用 | |
CN113026045A (zh) | 一种泡沫镍负载Ni(OH)2/FeOOH纳米花材料制备方法 | |
Ji et al. | Full water splitting by a nanoporous CeO 2 nanowire array under alkaline conditions | |
Yan et al. | Cd doped Ni3S2 nanosheet arrays grown on nickel foam as highly efficient and robust bifunctional electrocatalysts for alkaline overall water splitting | |
Sh et al. | Electrocatalysts for water electrolysis | |
Chen et al. | Facile fabrication of flower-like CuS/MnCO3 microspheres clusters on nickel foam as an efficient bifunctional catalyst for overall water splitting | |
Zhang et al. | Nickel hydroxide array coated with NiFe alloy nanosheets for overall mixed water splitting | |
CN106319558B (zh) | 一种高效多孔的MoS2-Zn析氢电极及其制备方法 | |
Gao et al. | High current water electrolysis catalyst based on Fe/Ni (Ni/Fe) hierarchically structured electrode | |
Esmailzadeh et al. | Optimization of nickel selenide for hydrogen and oxygen evolution reactions by response surface methodology | |
Jia et al. | FeNi-LDH@ Ni film modified stainless-steel as self-supported electrodes for efficient and stable overall water splitting in alkaline environments | |
Wang et al. | Ni2P (O)–Fe2P (O)/CeOx as high effective bifunctional catalyst for overall water splitting |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20211110 Address after: 257000 room b420, No. 59, Fuqian street, Dongying District, Dongying City, Shandong Province Patentee after: Dongying Guangli Lingang Industrial Park Co.,Ltd. Address before: 066004 No. 438, west section of Hebei Street, Haigang District, Qinhuangdao City, Hebei Province Patentee before: Yanshan University |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20221222 Address after: 257000 room b420, No. 59, Fuqian street, Dongying District, Dongying City, Shandong Province Patentee after: Dongying Guangli Lingang Industrial Park Co.,Ltd. Patentee after: Dongying Guangli Port Park Operation Co.,Ltd. Address before: 257000 room b420, No. 59, Fuqian street, Dongying District, Dongying City, Shandong Province Patentee before: Dongying Guangli Lingang Industrial Park Co.,Ltd. |