CN106965283B - 一种提高柳条上色稳定性的染色方法 - Google Patents

一种提高柳条上色稳定性的染色方法 Download PDF

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CN106965283B
CN106965283B CN201710227888.6A CN201710227888A CN106965283B CN 106965283 B CN106965283 B CN 106965283B CN 201710227888 A CN201710227888 A CN 201710227888A CN 106965283 B CN106965283 B CN 106965283B
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徐学进
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Abstract

本发明属于柳条加工技术领域,尤其是一种提高柳条上色稳定性的染色方法,具体方法如下:(1)柳条清洗及变温处理;(2)浸泡液浸泡及干燥处理;(3)染色处理;本发明对柳条进行处理后,不但染色纯正均匀、有光泽,具有淡淡花香味、无异味,无任何有毒物质残留,防霉防蛀效果显著,而且有效提高柳条的柔韧性,有效提升其柳编品质,有效避免其在后续的编制过程中断裂现象的发生,且编制更加省力,有效提高工作效率;经染色处理后的柳条不但耐磨性能好,用手或用布进行擦拭均不会会出现掉色现象,而且染色不只是对柳条的外面结构进行染色,颜色能有效进入到柳条的内部,有效提高柳条的编制品质。

Description

一种提高柳条上色稳定性的染色方法
技术领域
本发明属于柳条加工技术领域,尤其是一种提高柳条上色稳定性的染色方法。
背景技术
柳条是一种重要的柳编原材料,柳条具有优良的柔韧性和拉伸强度,十分适合进行柳编,但是柳条不易进行染色,染色后容易褪色,造成制品的颜色单一,或者染色后柳条颜色不均匀,影响柳条编制品的品质,而且极易发霉虫蛀,使得柳条编制品使用寿命大大缩短;因此,发明一种能有效解决以上问题的柳条的染色方法是目前亟待解决的问题。
发明内容
针对上述问题,本发明旨在提供一种提高柳条上色稳定性的染色方法。
本发明通过以下技术方案实现:
一种提高柳条上色稳定性的染色方法,具体方法如下:
(1)柳条清洗及变温处理
选取粗细均匀、表面光洁的柳条,用温度为43~45℃的温水清洗干净,置入温度为-13~-11℃的冷冻箱内冷冻53~55min,取出,置入温度为51~53℃的烘烤箱内烘烤8~9min,取出,室温自然冷却,得一次柳条;
(2)浸泡液浸泡及干燥处理
将一次柳条浸没于浸泡液中浸泡36~38min,取出,用功率为320~330W的微波处理13~14min,在温度为43~45℃、相对湿度为17%~19%的条件下风干至水分含量为9%~10%,得二次柳条;
所述的浸泡液,由以下重量份的原料制成:酒石酸钾18~19份、尼可刹米3.4~3.6份、水杨酸镁7.7~7.9份、冰醋酸15~16份、硼酸钠12.5~13份、水130~140份;
(3)染色处理
将二次柳条浸没于肉桂提取液中浸泡17~18min,取出,用光照强度为970~980Lx的红色光照射24~26min,在温度为43~45℃、相对湿度为17%~19%的条件下风干至水分含量为9%~10%,浸没于染色剂中浸泡15~16h,取出,用光照强度为1100~1200Lx的黄色光照射93~95min,置入温度为47~49℃的烘烤箱内烘烤13~14min,取出,在温度为28~30℃、相对湿度为17%~19%的条件下自然风干;
所述的染色剂,由以下重量份的原料制成:马齿苋13~14份、薄荷叶8~9份、扫帚菜22~23份、桑叶15~16份、桃叶6.5~7份、桂花7.5~8份、月季花5.4~5.8份。
作为发明进一步的方案:步骤(2)所述的浸泡液的温度为53~55℃。
作为发明进一步的方案:步骤(3)所述的肉桂提取液,按以下步骤进行制备:将肉桂粉碎至150~160目,投入到其重量4.5~4.7倍量的水中大火煮沸,文火熬煮76~78min并不断搅拌,过210~220目滤布,取滤液,室温自然冷却,得肉桂提取液。
作为发明进一步的方案:步骤(3)所述的染色剂的制备方法,具体包括以下步骤:
A.将马齿苋、薄荷叶、扫帚菜、桑叶和桃叶投入转速为860~880r/min的粉碎机中粉碎12~13min,取出,投入到马齿苋重量18~19倍量、温度为65~67℃的水中恒温浸泡54~56min,文火熬煮95~100min,过220~230目滤布,取滤液,得染色液一;
B.将桂花和月季花投入转速为860~880r/min的粉碎机中粉碎12~13min,取出,投入到温度为78~80℃的烘烤箱恒温烘烤13~14min,取出,投入到桂花重量4.2~4.4倍量的水中大火煮沸,文火熬煮45~47min,过220~230目滤布,取滤液,得染色液二;
C.将染色液一和染色液二合并,在压力为31~32MPa的条件下均质22~24min,文火熬煮15~16min,在压力为15~16MPa的条件下均质34~36min,得染色剂。
本发明的有益效果:本发明提供的一种提高柳条上色稳定性的染色方法,对柳条进行处理后,不但染色纯正均匀、有光泽,具有淡淡花香味、无异味,无任何有毒物质残留,防霉防蛀效果显著,在正常环境下28个月内不会出现任何程度的发霉虫蛀现象,而且能够有效提高柳条的柔韧性,有效提升其柳编品质,有效避免其在后续的编制过程中断裂现象的发生,且编制更加省力,有效提高工作效率;经染色处理后的柳条不但耐磨性能好,用手或用布进行擦拭均不会会出现掉色现象,而且染色不只是对柳条的外面结构进行染色,颜色能有效进入到柳条的内部,有效提高柳条的编制品质。
具体实施方式
下面用具体实施例说明本发明,但并不是对本发明的限制。
实施例1
本发明实施例中,一种提高柳条上色稳定性的染色方法,具体方法如下:
(1)柳条清洗及变温处理
选取粗细均匀、表面光洁的柳条,用温度为43℃的温水清洗干净,置入温度为-13℃的冷冻箱内冷冻53min,取出,置入温度为51℃的烘烤箱内烘烤8min,取出,室温自然冷却,得一次柳条;
(2)浸泡液浸泡及干燥处理
将一次柳条浸没于浸泡液中浸泡36min,取出,用功率为320W的微波处理13min,在温度为43℃、相对湿度为17%的条件下风干至水分含量为9%,得二次柳条;
所述的浸泡液,由以下重量份的原料制成:酒石酸钾18份、尼可刹米3.4份、水杨酸镁7.7份、冰醋酸15份、硼酸钠12.5份、水130份;
(3)染色处理
将二次柳条浸没于肉桂提取液中浸泡17min,取出,用光照强度为970Lx的红色光照射24min,在温度为43℃、相对湿度为17%的条件下风干至水分含量为9%,浸没于染色剂中浸泡15h,取出,用光照强度为1100Lx的黄色光照射93~95min,置入温度为47℃的烘烤箱内烘烤13min,取出,在温度为28℃、相对湿度为17%的条件下自然风干;
所述的染色剂,由以下重量份的原料制成:马齿苋13份、薄荷叶8份、扫帚菜22份、桑叶15份、桃叶6.5份、桂花7.5份、月季花5.4份。
作为发明进一步的方案:步骤(2)所述的浸泡液的温度为53℃。
作为发明进一步的方案:步骤(3)所述的肉桂提取液,按以下步骤进行制备:将肉桂粉碎至150目,投入到其重量4.5倍量的水中大火煮沸,文火熬煮76min并不断搅拌,过210目滤布,取滤液,室温自然冷却,得肉桂提取液。
作为发明进一步的方案:步骤(3)所述的染色剂的制备方法,具体包括以下步骤:
A.将马齿苋、薄荷叶、扫帚菜、桑叶和桃叶投入转速为860r/min的粉碎机中粉碎12min,取出,投入到马齿苋重量18倍量、温度为65℃的水中恒温浸泡54min,文火熬煮95min,过220目滤布,取滤液,得染色液一;
B.将桂花和月季花投入转速为860r/min的粉碎机中粉碎12min,取出,投入到温度为78℃的烘烤箱恒温烘烤13min,取出,投入到桂花重量4.2倍量的水中大火煮沸,文火熬煮45min,过220目滤布,取滤液,得染色液二;
C.将染色液一和染色液二合并,在压力为31MPa的条件下均质22min,文火熬煮15min,在压力为15MPa的条件下均质34min,得染色剂。
染色后使用温度为60℃、质量分数为4.2%的食盐水浸泡100h,未出现褪色情况。
实施例2
本发明实施例中,一种提高柳条上色稳定性的染色方法,具体方法如下:
(1)柳条清洗及变温处理
选取粗细均匀、表面光洁的柳条,用温度为44℃的温水清洗干净,置入温度为-12℃的冷冻箱内冷冻54min,取出,置入温度为52℃的烘烤箱内烘烤8.5min,取出,室温自然冷却,得一次柳条;
(2)浸泡液浸泡及干燥处理
将一次柳条浸没于浸泡液中浸泡37min,取出,用功率为325W的微波处理13.5min,在温度为44℃、相对湿度为18%的条件下风干至水分含量为9.5%,得二次柳条;
所述的浸泡液,由以下重量份的原料制成:酒石酸钾18.5份、尼可刹米3.5份、水杨酸镁7.8份、冰醋酸15.5份、硼酸钠12.8份、水135份;
(3)染色处理
将二次柳条浸没于肉桂提取液中浸泡17.5min,取出,用光照强度为975Lx的红色光照射25min,在温度为44℃、相对湿度为18%的条件下风干至水分含量为9.5%,浸没于染色剂中浸泡15.5h,取出,用光照强度为1150Lx的黄色光照射94min,置入温度为48℃的烘烤箱内烘烤13.5min,取出,在温度为29℃、相对湿度为18%的条件下自然风干;
所述的染色剂,由以下重量份的原料制成:马齿苋13.5份、薄荷叶8.5份、扫帚菜22.5份、桑叶15.5份、桃叶6.8份、桂花7.8份、月季花5.6份。
作为发明进一步的方案:步骤(2)所述的浸泡液的温度为54℃。
作为发明进一步的方案:步骤(3)所述的肉桂提取液,按以下步骤进行制备:将肉桂粉碎至155目,投入到其重量4.6倍量的水中大火煮沸,文火熬煮77min并不断搅拌,过215目滤布,取滤液,室温自然冷却,得肉桂提取液。
作为发明进一步的方案:步骤(3)所述的染色剂的制备方法与实施例1相同。
染色后使用温度为60℃、质量分数为4.2%的食盐水浸泡100h,未出现褪色情况。
实施例3
本发明实施例中,一种提高柳条上色稳定性的染色方法,具体方法如下:
(1)柳条清洗及变温处理
选取粗细均匀、表面光洁的柳条,用温度为45℃的温水清洗干净,置入温度为-11℃的冷冻箱内冷冻55min,取出,置入温度为53℃的烘烤箱内烘烤9min,取出,室温自然冷却,得一次柳条;
(2)浸泡液浸泡及干燥处理
将一次柳条浸没于浸泡液中浸泡38min,取出,用功率为330W的微波处理14min,在温度为45℃、相对湿度为19%的条件下风干至水分含量为10%,得二次柳条;
所述的浸泡液,由以下重量份的原料制成:酒石酸钾19份、尼可刹米3.6份、水杨酸镁7.9份、冰醋酸16份、硼酸钠13份、水140份;
(3)染色处理
将二次柳条浸没于肉桂提取液中浸泡18min,取出,用光照强度为980Lx的红色光照射26min,在温度为45℃、相对湿度为19%的条件下风干至水分含量为10%,浸没于染色剂中浸泡16h,取出,用光照强度为1200Lx的黄色光照射95min,置入温度为49℃的烘烤箱内烘烤14min,取出,在温度为30℃、相对湿度为19%的条件下自然风干;
所述的染色剂,由以下重量份的原料制成:马齿苋14份、薄荷叶9份、扫帚菜23份、桑叶16份、桃叶7份、桂花8份、月季花5.8份。
作为发明进一步的方案:步骤(2)所述的浸泡液的温度为55℃。
作为发明进一步的方案:步骤(3)所述的肉桂提取液,按以下步骤进行制备:将肉桂粉碎至160目,投入到其重量4.7倍量的水中大火煮沸,文火熬煮78min并不断搅拌,过220目滤布,取滤液,室温自然冷却,得肉桂提取液。
作为发明进一步的方案:步骤(3)所述的染色剂的制备方法与实施例1相同。
染色后使用温度为60℃、质量分数为4.2%的食盐水浸泡100h,未出现褪色情况。
对比例
现有技术的柳条的普通染色方法
染色后使用温度为60℃、质量分数为1.6%的食盐水浸泡24h,出现严重的褪色情况。
分别用实施例和对比例的染色方法对性状相同的柳条进行染色处理,染色处理前所有柳条没有进行任何处理,处理完毕后进行检测,置于温度为40℃,湿度为90%的环境中进行防霉防蛀的效果检测,实施例和对比例的实验对比结果见表1:
表1 实施例和对比例的实验对比结果
色泽 气味 毒性 出现发霉虫蛀时间(天)
实施例1 纯正均匀、有光泽 淡淡花香味、无异味 53~54
实施例2 纯正均匀、有光泽 淡淡花香味、无异味 53~54
实施例3 纯正均匀、有光泽 淡淡花香味、无异味 54~55
对比例 不纯正不均匀、无光泽 刺鼻、有异味 2~3
从表1可知,使用实施例的染色方法对柳条进行染色处理,不但染色纯正均匀、有光泽,具有淡淡花香味、无异味,而且无任何有毒物质残留,防霉防蛀效果显著。

Claims (2)

1.一种提高柳条上色稳定性的染色方法,其特征在于,具体方法如下:
(1)柳条清洗及变温处理
选取粗细均匀、表面光洁的柳条,用温度为43~45℃的温水清洗干净,置入温度为-13~-11℃的冷冻箱内冷冻53~55min,取出,置入温度为51~53℃的烘烤箱内烘烤8~9min,取出,室温自然冷却,得一次柳条;
(2)浸泡液浸泡及干燥处理
将一次柳条浸没于浸泡液中浸泡36~38min,取出,用功率为320~330W的微波处理13~14min,在温度为43~45℃、相对湿度为17%~19%的条件下风干至水分含量为9%~10%,得二次柳条;
所述的浸泡液,由以下重量份的原料制成:酒石酸钾18~19份、尼可刹米3.4~3.6份、水杨酸镁7.7~7.9份、冰醋酸15~16份、硼酸钠12.5~13份、水130~140份;
所述的浸泡液的温度为53~55℃;
(3)染色处理
将二次柳条浸没于肉桂提取液中浸泡17~18min,取出,用光照强度为970~980Lx的红色光照射24~26min,在温度为43~45℃、相对湿度为17%~19%的条件下风干至水分含量为9%~10%,浸没于染色剂中浸泡15~16h,取出,用光照强度为1100~1200Lx的黄色光照射93~95min,置入温度为47~49℃的烘烤箱内烘烤13~14min,取出,在温度为28~30℃、相对湿度为17%~19%的条件下自然风干;
所述的染色剂,由以下重量份的原料制成:马齿苋13~14份、薄荷叶8~9份、扫帚菜22~23份、桑叶15~16份、桃叶6.5~7份、桂花7.5~8份、月季花5.4~5.8份;
所述的肉桂提取液,按以下步骤进行制备:将肉桂粉碎至150~160目,投入到其重量4.5~4.7倍量的水中大火煮沸,文火熬煮76~78min并不断搅拌,过210~220目滤布,取滤液,室温自然冷却,得肉桂提取液。
2.根据权利要求1所述的提高柳条上色稳定性的染色方法,其特征在于,步骤(3)所述的染色剂的制备方法,具体包括以下步骤:
A.将马齿苋、薄荷叶、扫帚菜、桑叶和桃叶投入转速为860~880r/min的粉碎机中粉碎12~13min,取出,投入到马齿苋重量18~19倍量、温度为65~67℃的水中恒温浸泡54~56min,文火熬煮95~100min,过220~230目滤布,取滤液,得染色液一;
B.将桂花和月季花投入转速为860~880r/min的粉碎机中粉碎12~13min,取出,投入到温度为78~80℃的烘烤箱恒温烘烤13~14min,取出,投入到桂花重量4.2~4.4倍量的水中大火煮沸,文火熬煮45~47min,过220~230目滤布,取滤液,得染色液二;
C.将染色液一和染色液二合并,在压力为31~32MPa的条件下均质22~24min,文火熬煮15~16min,在压力为15~16MPa的条件下均质34~36min,得染。
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