CN106947900B - 一种提纯的镁 - Google Patents
一种提纯的镁 Download PDFInfo
- Publication number
- CN106947900B CN106947900B CN201610809414.8A CN201610809414A CN106947900B CN 106947900 B CN106947900 B CN 106947900B CN 201610809414 A CN201610809414 A CN 201610809414A CN 106947900 B CN106947900 B CN 106947900B
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- China
- Prior art keywords
- magnesium
- zirconium
- purified
- impurities
- molten
- Prior art date
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- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 title claims abstract description 293
- 239000011777 magnesium Substances 0.000 title claims abstract description 286
- 229910052749 magnesium Inorganic materials 0.000 title claims abstract description 285
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims abstract description 219
- 229910052726 zirconium Inorganic materials 0.000 claims abstract description 166
- 239000012535 impurity Substances 0.000 claims abstract description 128
- 229910052735 hafnium Inorganic materials 0.000 claims abstract description 28
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 claims abstract description 28
- 238000000034 method Methods 0.000 claims description 111
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 62
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 61
- 239000000463 material Substances 0.000 claims description 53
- 229910052782 aluminium Inorganic materials 0.000 claims description 49
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 49
- 239000000203 mixture Substances 0.000 claims description 35
- 230000008569 process Effects 0.000 claims description 34
- 229910052757 nitrogen Inorganic materials 0.000 claims description 31
- 229910052742 iron Inorganic materials 0.000 claims description 30
- 229910000765 intermetallic Inorganic materials 0.000 claims description 21
- 239000010936 titanium Substances 0.000 claims description 21
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 20
- 229910052719 titanium Inorganic materials 0.000 claims description 19
- 239000011572 manganese Substances 0.000 claims description 16
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 15
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 15
- 229910052748 manganese Inorganic materials 0.000 claims description 15
- 239000011574 phosphorus Substances 0.000 claims description 15
- 229910052698 phosphorus Inorganic materials 0.000 claims description 15
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 14
- 229910052796 boron Inorganic materials 0.000 claims description 14
- 229910052793 cadmium Inorganic materials 0.000 claims description 14
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 claims description 14
- 230000002829 reductive effect Effects 0.000 claims description 9
- 230000001965 increasing effect Effects 0.000 claims description 8
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 7
- 239000011734 sodium Substances 0.000 claims description 6
- 239000010949 copper Substances 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 239000011575 calcium Substances 0.000 claims description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 60
- 230000000670 limiting effect Effects 0.000 description 43
- 239000003638 chemical reducing agent Substances 0.000 description 33
- 239000000047 product Substances 0.000 description 25
- 238000004519 manufacturing process Methods 0.000 description 20
- 150000001875 compounds Chemical class 0.000 description 17
- 229910052751 metal Inorganic materials 0.000 description 16
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 15
- 238000006243 chemical reaction Methods 0.000 description 15
- 239000002184 metal Substances 0.000 description 13
- 238000002844 melting Methods 0.000 description 12
- 230000008018 melting Effects 0.000 description 12
- 239000007787 solid Substances 0.000 description 12
- 238000000746 purification Methods 0.000 description 11
- 239000007795 chemical reaction product Substances 0.000 description 10
- 238000001556 precipitation Methods 0.000 description 9
- 150000003755 zirconium compounds Chemical class 0.000 description 9
- 230000004907 flux Effects 0.000 description 8
- 238000007670 refining Methods 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 7
- 239000001301 oxygen Substances 0.000 description 7
- 229910052760 oxygen Inorganic materials 0.000 description 7
- OMQSJNWFFJOIMO-UHFFFAOYSA-J zirconium tetrafluoride Chemical compound F[Zr](F)(F)F OMQSJNWFFJOIMO-UHFFFAOYSA-J 0.000 description 7
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 6
- 238000005266 casting Methods 0.000 description 6
- 238000012546 transfer Methods 0.000 description 6
- ZVWKZXLXHLZXLS-UHFFFAOYSA-N zirconium nitride Chemical group [Zr]#N ZVWKZXLXHLZXLS-UHFFFAOYSA-N 0.000 description 6
- 229910001629 magnesium chloride Inorganic materials 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 5
- 229910000861 Mg alloy Inorganic materials 0.000 description 4
- 229910045601 alloy Inorganic materials 0.000 description 4
- 239000000956 alloy Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- ORUIBWPALBXDOA-UHFFFAOYSA-L magnesium fluoride Chemical compound [F-].[F-].[Mg+2] ORUIBWPALBXDOA-UHFFFAOYSA-L 0.000 description 4
- 229910001635 magnesium fluoride Inorganic materials 0.000 description 4
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 4
- 230000009467 reduction Effects 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- -1 zirconium metals Chemical class 0.000 description 4
- 229910001928 zirconium oxide Inorganic materials 0.000 description 4
- ZXAUZSQITFJWPS-UHFFFAOYSA-J zirconium(4+);disulfate Chemical compound [Zr+4].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O ZXAUZSQITFJWPS-UHFFFAOYSA-J 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 238000005275 alloying Methods 0.000 description 3
- 229910052786 argon Inorganic materials 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 2
- 229910001209 Low-carbon steel Inorganic materials 0.000 description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 229910003074 TiCl4 Inorganic materials 0.000 description 2
- 229910052770 Uranium Inorganic materials 0.000 description 2
- 229910007873 ZrAl3 Inorganic materials 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 239000012080 ambient air Substances 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- 239000010941 cobalt Substances 0.000 description 2
- 229910017052 cobalt Inorganic materials 0.000 description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 239000002019 doping agent Substances 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 239000002529 flux (metallurgy) Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000001036 glow-discharge mass spectrometry Methods 0.000 description 2
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 description 2
- 238000001095 inductively coupled plasma mass spectrometry Methods 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 239000011733 molybdenum Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000011946 reduction process Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 2
- 229910052721 tungsten Inorganic materials 0.000 description 2
- 239000010937 tungsten Substances 0.000 description 2
- DNYWZCXLKNTFFI-UHFFFAOYSA-N uranium Chemical compound [U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U][U] DNYWZCXLKNTFFI-UHFFFAOYSA-N 0.000 description 2
- 238000005292 vacuum distillation Methods 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 238000004566 IR spectroscopy Methods 0.000 description 1
- 238000007696 Kjeldahl method Methods 0.000 description 1
- 240000007643 Phytolacca americana Species 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- LCKIEQZJEYYRIY-UHFFFAOYSA-N Titanium ion Chemical compound [Ti+4] LCKIEQZJEYYRIY-UHFFFAOYSA-N 0.000 description 1
- 229910008061 ZrFe2 Inorganic materials 0.000 description 1
- 229910008357 ZrMn2 Inorganic materials 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 description 1
- 229910001634 calcium fluoride Inorganic materials 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 230000003009 desulfurizing effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 238000000921 elemental analysis Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000009969 flowable effect Effects 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000007726 management method Methods 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000010309 melting process Methods 0.000 description 1
- 239000012768 molten material Substances 0.000 description 1
- 150000004767 nitrides Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 239000011236 particulate material Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000012254 powdered material Substances 0.000 description 1
- 239000012629 purifying agent Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 229910052845 zircon Inorganic materials 0.000 description 1
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C23/00—Alloys based on magnesium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/10—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals with refining or fluxing agents; Use of materials therefor, e.g. slagging or scorifying agents
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
- C22B26/20—Obtaining alkaline earth metals or magnesium
- C22B26/22—Obtaining magnesium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/14—Obtaining zirconium or hafnium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B5/00—General methods of reducing to metals
- C22B5/02—Dry methods smelting of sulfides or formation of mattes
- C22B5/04—Dry methods smelting of sulfides or formation of mattes by aluminium, other metals or silicon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C23/00—Alloys based on magnesium
- C22C23/02—Alloys based on magnesium with aluminium as the next major constituent
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/585,094 | 2012-08-14 | ||
| US13/585,094 US9090953B2 (en) | 2012-08-14 | 2012-08-14 | Methods for reducing impurities in magnesium, purified magnesium, and zirconium metal production |
| CN201380043674.3A CN104583425B (zh) | 2012-08-14 | 2013-07-18 | 用于减少镁中杂质的方法、提纯的镁和锆金属生产 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201380043674.3A Division CN104583425B (zh) | 2012-08-14 | 2013-07-18 | 用于减少镁中杂质的方法、提纯的镁和锆金属生产 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106947900A CN106947900A (zh) | 2017-07-14 |
| CN106947900B true CN106947900B (zh) | 2020-07-10 |
Family
ID=48917691
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610809414.8A Active CN106947900B (zh) | 2012-08-14 | 2013-07-18 | 一种提纯的镁 |
| CN201380043674.3A Active CN104583425B (zh) | 2012-08-14 | 2013-07-18 | 用于减少镁中杂质的方法、提纯的镁和锆金属生产 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201380043674.3A Active CN104583425B (zh) | 2012-08-14 | 2013-07-18 | 用于减少镁中杂质的方法、提纯的镁和锆金属生产 |
Country Status (7)
| Country | Link |
|---|---|
| US (4) | US9090953B2 (https=) |
| EP (2) | EP3438296B1 (https=) |
| CN (2) | CN106947900B (https=) |
| IN (1) | IN2015DN01192A (https=) |
| RU (1) | RU2641201C2 (https=) |
| TR (1) | TR201820496T4 (https=) |
| WO (1) | WO2014028161A1 (https=) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9090953B2 (en) | 2012-08-14 | 2015-07-28 | Ati Properties, Inc. | Methods for reducing impurities in magnesium, purified magnesium, and zirconium metal production |
| CN104313360A (zh) * | 2014-11-14 | 2015-01-28 | 重庆大学 | 一种加锆纯化镁熔体的方法 |
| JP2017009795A (ja) * | 2015-06-22 | 2017-01-12 | 日東電工株式会社 | 偏光板及び偏光板の製造方法 |
| KR102659032B1 (ko) | 2016-02-23 | 2024-04-22 | 루미리즈 홀딩 비.브이. | 발광 디바이스용 파장 변환 재료 |
| CN107083492B (zh) * | 2017-05-27 | 2018-11-23 | 郑州大学 | 具有分段结晶和余热高效利用的镁还原反应器 |
| RU2669671C1 (ru) * | 2017-09-12 | 2018-10-12 | Публичное Акционерное Общество "Корпорация Всмпо-Ависма" | Способ очистки магния от примесей |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB591225A (en) | 1944-08-08 | 1947-08-12 | Magnesium Elektron Ltd | Improvements in or relating to the production of magnesium base alloys |
| GB730008A (en) | 1951-12-10 | 1955-05-18 | Magnesium Elektron Ltd | Improvements in or relating to etching plates |
| US2779672A (en) | 1953-10-30 | 1957-01-29 | Dow Chemical Co | Method of treating molten magnesium |
| SU390175A1 (ru) | 1972-01-31 | 1973-07-11 | Т. Е. Худайбергенов , А. М. Кунаев Институт металлургии , обогащени Казахской ССР | Способ рафинирования магния |
| US4511399A (en) | 1983-10-04 | 1985-04-16 | Westinghouse Electric Corp. | Control method for large scale batch reduction of zirconium tetrachloride |
| US4668287A (en) | 1985-09-26 | 1987-05-26 | Westinghouse Electric Corp. | Process for producing high purity zirconium and hafnium |
| JPH0247237A (ja) | 1988-08-09 | 1990-02-16 | Furukawa Alum Co Ltd | Ｍｇ合金制振材とその製造方法 |
| US4891065A (en) | 1988-08-29 | 1990-01-02 | The Dow Chemical Company | Process for producing high purity magnesium |
| CN1020199C (zh) * | 1990-03-20 | 1993-03-31 | 武汉冶金研究所 | 作发热剂用的镁铝合金 |
| US5147450A (en) * | 1991-07-26 | 1992-09-15 | The Dow Chemical Company | Process for purifying magnesium |
| US5804138A (en) | 1997-06-30 | 1998-09-08 | The Dow Chmical Company | Flux for fire prevention in magnesium |
| UA46122C2 (uk) * | 1999-03-23 | 2002-05-15 | Державний Науково-Дослідний Та Проектний Інститут Титану | Спосіб безперервного рафінування магнію |
| CN1405346A (zh) * | 2001-08-10 | 2003-03-26 | 郑景纯 | 高纯耐蚀镁基合金生产方法 |
| CN1114708C (zh) * | 2001-12-04 | 2003-07-16 | 上海交通大学 | 低热裂倾向性高强度压铸镁合金 |
| CN101403046A (zh) * | 2008-11-12 | 2009-04-08 | 朝阳百盛锆钛股份有限公司 | 双罐镁法还原生产海绵锆的方法 |
| CN101560610B (zh) * | 2009-05-21 | 2010-08-11 | 太原理工大学 | 一种高纯度镁的精炼方法 |
| US9090953B2 (en) | 2012-08-14 | 2015-07-28 | Ati Properties, Inc. | Methods for reducing impurities in magnesium, purified magnesium, and zirconium metal production |
-
2012
- 2012-08-14 US US13/585,094 patent/US9090953B2/en active Active
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2013
- 2013-07-18 CN CN201610809414.8A patent/CN106947900B/zh active Active
- 2013-07-18 EP EP18193065.2A patent/EP3438296B1/en active Active
- 2013-07-18 WO PCT/US2013/050974 patent/WO2014028161A1/en not_active Ceased
- 2013-07-18 CN CN201380043674.3A patent/CN104583425B/zh active Active
- 2013-07-18 RU RU2015108968A patent/RU2641201C2/ru active
- 2013-07-18 EP EP13745501.0A patent/EP2885435B1/en active Active
- 2013-07-18 TR TR2018/20496T patent/TR201820496T4/tr unknown
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2015
- 2015-02-13 IN IN1192DEN2015 patent/IN2015DN01192A/en unknown
- 2015-06-04 US US14/730,311 patent/US20150329943A1/en not_active Abandoned
- 2015-06-04 US US14/730,306 patent/US20150329939A1/en not_active Abandoned
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2018
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Also Published As
| Publication number | Publication date |
|---|---|
| CN104583425B (zh) | 2016-09-21 |
| IN2015DN01192A (https=) | 2015-06-26 |
| EP2885435B1 (en) | 2018-10-24 |
| US20180327885A1 (en) | 2018-11-15 |
| EP2885435A1 (en) | 2015-06-24 |
| US20140050608A1 (en) | 2014-02-20 |
| US20150329943A1 (en) | 2015-11-19 |
| WO2014028161A1 (en) | 2014-02-20 |
| EP3438296B1 (en) | 2020-12-16 |
| TR201820496T4 (tr) | 2019-02-21 |
| US10422017B2 (en) | 2019-09-24 |
| US20150329939A1 (en) | 2015-11-19 |
| CN106947900A (zh) | 2017-07-14 |
| CN104583425A (zh) | 2015-04-29 |
| EP3438296A1 (en) | 2019-02-06 |
| RU2015108968A (ru) | 2016-10-10 |
| US9090953B2 (en) | 2015-07-28 |
| RU2641201C2 (ru) | 2018-01-16 |
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