CN106905709A - Batik resist printing wax suitable for felt and preparation method thereof - Google Patents
Batik resist printing wax suitable for felt and preparation method thereof Download PDFInfo
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- CN106905709A CN106905709A CN201710240351.3A CN201710240351A CN106905709A CN 106905709 A CN106905709 A CN 106905709A CN 201710240351 A CN201710240351 A CN 201710240351A CN 106905709 A CN106905709 A CN 106905709A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
- C08L91/06—Waxes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/12—Reserving parts of the material before dyeing or printing ; Locally decreasing dye affinity by chemical means
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
A kind of batik resist printing wax suitable for felt and preparation method thereof, belongs to wax-dyeing process field.Resist printing wax includes paraffin, beeswax, palm wax, gum dammar, glycerine, sheep oil and polyoxyethylene amine.During preparation, weigh 30 40 weight portion paraffin and 10 20 weight portion beeswaxs are heated to 70 80 DEG C and melt and be incubated 0.5 1h obtaining the first mixture；5 10 weight portion palm waxs, 24 weight portion gum dammars and 58 parts by weight of glycerin, 1 1.5 weight portion sheep oils and 0.5 1 parts by weight of polyoxyethylene amine are weighed to be heated to 140 150 DEG C and melt and be incubated 0.5 1h obtaining the second mixture；The first mixture is added into the second mixture at a temperature of 120 130 DEG C, 20 30mi n, cooling are stirred with 400 600r/mi n rotating speeds.Preparation method is simple, and osmotic effect of the obtained resist printing wax on felt is good, adhesive capacity strong, waxing is uniform.
Description
Technical field
It is the present invention relates to wax-dyeing process field and more particularly to a kind of suitable for the batik resist printing wax of felt and its preparation side
Method.
Background technology
Batik, is the ancient ethnic group's folk tradition textile printing and dyeing handicraft of China, Gu claim wax, with twist figured silk fabrics (tie dyeing),
Folder figured silk fabrics (hollow out stamp) and the referred to as big stamp skill of Ancient Times in China three.Batik is good at by the nationalitys such as Guizhou, Yunnan Miao ethnic group, the Bouyei.
Batik is to be dipped in after Hua Yubu is painted in dewaxing to be contaminated with indigo with wax spatula, both contaminates wax, and cloth cover takes on blue bottom and spends in vain or white background indigo plant
Colored multiple patterns, meanwhile, in dip-dye, as the wax exposure cracking of resist agent, make cloth cover that special " ice line ", outstanding tool is presented
Glamour.Because batik pattern is abundant, tone is plain, unique style, for making dress and personal adornment and various life utilities, it appears
It is simple generous, pure and fresh pleasing, it is rich in national characters, the market demand increases year by year.
But, the wax material in existing wax printing technology in wax operation is drawn, generally using single paraffin or single
Beeswax heat carries out picture wax operation after melting.The hardness is bigger of paraffin, it is used for the picture wax easy exposure cracking of operation in dyeing course
Pigment figure is produced, but its adhesiveness is relatively low, and easily being come off in dyeing course causes to produce stain.The adhesiveness of beeswax is difficult well
Come off, but its hardness is relatively low, exposure cracking is difficult in dyeing course and produces pigment figure, while it also has relatively costly asking
Topic.For above-mentioned problem, prior art is simply mixed by by paraffin and beeswax, while enabling its adhesiveness preferable
Enough exposure crackings, but it is still present the problems such as permeability is poor, waxing is uneven.And due to the superficiality of different clothes
Different can be surface-treated, it is necessary to be directed to different clothes.
The content of the invention
It is an object of the invention to provide a kind of batik resist printing wax suitable for felt, in picture wax operation is carried out, its
Osmotic effect on felt is good, adhesive capacity is strong, waxing is uniform.
It is obtained anti-another object of the present invention is to provide a kind of preparation method of the batik resist printing wax suitable for felt
Osmotic effect of the dye wax on felt is good, adhesive capacity is strong, waxing is uniform.
The present invention is solved its technical problem and is realized using following technical scheme.
The present invention proposes a kind of batik resist printing wax suitable for felt, includes by weight：Paraffin 30-40 parts, beeswax
10-20 parts, palm wax 5-10 parts, gum dammar 2-4 parts, glycerine 5-8 parts, sheep oil 1-1.5 parts and polyoxyethylene amine 0.5-1
Part.
The present invention also proposes a kind of preparation method of the batik resist printing wax suitable for felt, weighs the stone of 30-40 weight portions
The beeswax of wax and 10-20 weight portions is heated to 70-80 DEG C and melts and be incubated 0.5-1h obtaining the first mixture；Weigh 5-10 weight portions
Palm wax, the glycerine of the gum dammar of 2-4 weight portions and 5-8 weight portions, the sheep oil of 1-1.5 weight portions and 0.5-1 weight
Part polyoxyethylene amine be heated to 140-150 DEG C and melt and be incubated 0.5-1h obtaining the second mixture；Will at a temperature of 120-130 DEG C
First mixture adds the second mixture, and 20-30min, cooling are stirred with 400-600r/min rotating speeds.
The beneficial effect of the embodiment of the present invention is：
The batik resist printing wax suitable for felt that the present invention is provided, paraffin hardness is bigger, easy exposure cracking is in dyeing
Form pigment figure；Beeswax hardness is smaller, and adhesiveness is strong, can strengthen adhesion stability of the resist printing wax on cloth.With paraffin and honeybee
Wax is wax-matrix, and the adhesion of resist printing wax is stable, easily form pigment figure.Palm wax has good Oil keeping, and its proterties is thin and viscid
Degree is small, and its resin content is low, good flowing properties, it is possible to increase the osmosis of resist printing wax is so as to improve resist printing effect.Da Ma trees
Fat is widely used in ink used for plastic, compound oil ink, the adhesive force of table printing ink, the mobility such as enhancing PP and PE, and it can enter one
The osmosis and adhesion property of step enhancing resist printing wax.The surface of felt have it is tiny similar to villous fibre structure,
Cause the surface roughness of felt higher, cause the effect of waxing uneven.The fibre structure on felt surface can influence wax oil
Osmotic effect, while the operation of waxing can cause to damage to the fibre structure on felt surface.The cooperation of glycerine and sheep oil can be comforted
Along the fibre structure on felt surface, make waxing uniform；Glycerine has stronger osmotic effect, and wax oil can be promoted to ooze felt
Thoroughly.Other polyoxyethylene amine and glycerine, the mixture of sheep oil can form protective layer in the fibre structure to felt surface, reduce
What felt was subject in wax-dyeing process damages.
The present invention provide the batik resist printing wax for being used in felt preparation method, due to paraffin and beeswax fusing point compared with
It is low, paraffin and beeswax are first melted at a lower temperature, prevent from causing during high-temperature operation the rotten or oxidation of paraffin and beeswax.
Insulation operation after raw material is melted makes to be sufficiently mixed between raw material, improves the consistency of product, so as to improve resist printing effect
Really.
Specific embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below will be in the embodiment of the present invention
Technical scheme be clearly and completely described.Unreceipted actual conditions person, builds according to normal condition or manufacturer in embodiment
The condition of view is carried out.Agents useful for same or the unreceipted production firm person of instrument, are the conventional product that can be obtained by commercially available purchase
Product.
Batik resist printing wax suitable for felt of the embodiment of the present invention and preparation method thereof is specifically described below.
A kind of batik resist printing wax suitable for felt, includes by weight：Paraffin 30-40 parts, beeswax 10-20 parts, palm fibre
0.5-1 parts of 5-10 parts, gum dammar 2-4 parts, glycerine 5-8 parts, sheep oil 1-1.5 parts of palmitic acid wax and polyoxyethylene amine.
The hardness of paraffin is higher, easy exposure cracking.During batik is dyeed, dyestuff can be by being cracked what is produced
Gap colours on cloth, so as to produce the natural pigment figure of lines.But, because the adhesion property of paraffin is poor, it is used alone
Used as wax-matrix, being come off in dyeing course paraffin can form stain to paraffin on cloth, influence the effect of batik pattern.
The adhesion property of beeswax is preferable, it is not easy to fall off.But because the hardness of beeswax is relatively low, it is not easy to which tortoise occurs
Split generation pigment figure.
Draw during wax, wax oil flows out from wax spatula and permeates and freeze solidly on cloth, reaches the effect of local resist printing.Due to wax
, from sharp temperature drop after wax spatula outflow, the setting rate of wax oil is fast, it is desirable to which wax oil has seepage velocity higher, makes wax oil for oil
Cloth can be impregnated with, so as to ensure the resist printing effect of picture wax.
Palm wax has good Oil keeping, and its proterties is thin and viscosity is small, and its resin content is low, good flowing properties,
The osmosis of batik resist printing wax can be improved, so as to improve resist printing effect.
Gum dammar is widely used in the ink used for plastic such as enhancing PP and PE, compound oil ink, the adhesive force of table printing ink, flowing
Property, its osmosis and adhesion property that can further enhance resist printing wax, resist printing is made good use of, and effectively prevents stain,
Further improve the quality of batikses.
Further, peregal and sapn are added in batik resist printing wax of the invention, it has preferable peptizaiton, energy
Promote peptizaiton of the wax oil in cloth, improve the osmosis of wax oil, so as to further improve the resist printing of batik resist printing wax
Effect.
Wax-dyeing process is especially prevailing in Guizhou province, but different regions like that the cloth for using is not quite similar.The southeast of Guizhou Province
With the south of Guizhou Province one with felt is often used, the west of Guizhou Province, Miao ethnic group of the band of Northwestern Guizhou Province one are then liked with burlap and felt.
The surface of felt has tiny similar to villous fibre structure, causes the surface roughness of felt higher,
Cause the effect of waxing uneven.The fibre structure on felt surface can influence the osmotic effect of wax oil, while the operation meeting of waxing
Fibre structure to felt surface causes to damage.
Studied through inventor and found, glycerine and paraffin and beeswax have stronger penetrating power in being blended in batik operation.Together
When glycerine and sheep oil there is Fushun to act on the surface of felt in batik operation, make the wax layer of waxing more uniform.In the present invention,
The surface treatment of felt is carried out using the mixture of glycerine, sheep oil and polyoxyethylene amine, felt surface fiber structure is carried in Fushun
While resist printing effect high, protective layer is formed on felt surface, reduce the damaging of being subject to during batik of fibre structure of felt
Wound, improves the comfortableness of felt after batik.
This is applied to the preparation method of the batik resist printing wax of felt, including：Weigh the paraffin and 10-20 of 30-40 weight portions
The beeswax of weight portion is heated to 70-80 DEG C and melts and be incubated 0.5-1h obtaining the first mixture；Weigh 5-10 weight portions palm wax,
The polyoxy second of the gum dammar of 2-4 weight portions and the glycerine, the sheep oil of 1-1.5 weight portions and 0.5-1 weight portions of 5-8 weight portions
Enamine is heated to 140-150 DEG C and melts and be incubated 0.5-1h obtaining the second mixture；By the first mixture at a temperature of 120-130 DEG C
The second mixture is added, 20-30min, cooling are stirred with 400-600r/min rotating speeds.
Peregal and sapn are added after first mixture and the mixing of the second mixture, the process with stirring makes the first mixing
Thing and the second mixture are uniformly dispersed, and improve the homogenization of resist printing wax material interior tissue.
Because the fusing point of paraffin and beeswax is relatively low and easy oxidation deterioration, it is melted at low temperature, prevented and it
His raw material melts under the high temperature conditions causes oxidation deterioration etc..Raw material carries out isothermal holding after thawing, can make between raw material
It is sufficiently mixed, disperses, production die is further homogenized, pore size after material condensation can be effectively reduced, improves batik
The consistency of resist printing wax, further improves the resist printing performance of material.
Further, cooling down operation is carried out under the pressure of 0.2-0.3MPa, can promote fine and close combination between raw material, is entered
One step increases the consistency of material, improves the mobility and permeability of wax oil.
Beeswax is a kind of fatty matter being secreted by 4 pairs of wax glands of of the right age worker bee belly in bee colony.In bee colony,
Worker bee builds honeycomb, ovary capping and the capping of feed room using the wax that oneself is secreted.Honeycomb is that honeyflow honeybee hoards food, cultivates
Honeybee and the place for perching conglomeration, beeswax is both the product of bee colony, is again that it is survived and material necessary to breeding, therefore beeswax
In usually contain more insoluble impurities, influence the quality of batik resist printing wax.
Therefore it is further, in the present invention, before paraffin and beeswax heating and melting are mixed, purification behaviour is carried out to beeswax
Make.
Specifically, because the density of beeswax is small compared with water, and insoluble impurities water content and nutrition content in beeswax
Higher, its density is more than water.In purification operations, cooling, beeswax are stood after beeswax and water are mixed and heated into 65-75 DEG C of thawing
In insoluble impurities be sunken to the bottom of water, beeswax floats on the surface of water and gradually condenses, and beeswax is taken out after the completion of condensation and is
Complete purification operations.
In order that insoluble impurities is sufficiently separated with beeswax, preferably the mass ratio of beeswax and water is generally 1:2.Enter one
Step, 2-3 identical purification operations can be repeated, it is easy to be sufficiently separated impurity.
Feature of the invention and performance are described in further detail with reference to embodiments.
Embodiment 1
A kind of preparation method of the batik resist printing wax suitable for felt, including：
The paraffin of 30 weight portions and the beeswax of 10 weight portions are weighed, beeswax and 20g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-1h
Obtain the first mixture；Weigh palm wax, the gum dammar of 2 weight portions, the glycerine of 5 weight portions, the sheep of 1 weight portion of 5 weight portions
The polyoxyethylene amine of oil and 0.5 weight portion is heated to 140-150 DEG C and melts and be incubated 0.5-1h obtaining the second mixture；In 120-
The first mixture is added into the second mixture at a temperature of 130 DEG C, the peregal of 0.5 weight portion and the department of 0.3 weight portion is added
Disk, 20-30min is stirred with 400-600r/min rotating speeds.Cooled down under 0.2-0.3MPa pressure.
Embodiment 2
The paraffin of 33 weight portions and the beeswax of 12 weight portions are weighed, beeswax and 24g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-1h
Obtain the first mixture；Weigh palm wax, the gum dammar of 2.5 weight portions, the glycerine of 6 weight portions, 1.1 weight portions of 7 weight portions
Sheep oil and the polyoxyethylene amine of 0.6 weight portion be heated to 140-150 DEG C and melt and be incubated 0.5-1h obtaining the second mixture；
The first mixture is added into the second mixture at a temperature of 120-130 DEG C, the peregal and 0.35 weight portion of 0.6 weight portion is added
Sapn, with 400-600r/min rotating speeds stir 20-30min.Cooled down under 0.2-0.3MPa pressure.
Embodiment 3
The paraffin of 35 weight portions and the beeswax of 14 weight portions are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-1h
Obtain the first mixture；Weigh palm wax, the gum dammar of 3 weight portions, the glycerine of 6.5 weight portions, 1.2 weight portions of 8 weight portions
Sheep oil and the polyoxyethylene amine of 0.65 weight portion be heated to 140-150 DEG C and melt and be incubated 0.5-1h obtaining the second mixture；
The first mixture is added into the second mixture at a temperature of 120-130 DEG C, the peregal and 0.4 weight of 0.8 weight portion is added
The sapn of part, 20-30min is stirred with 400-600r/min rotating speeds.Cooled down under 0.2-0.3MPa pressure.
Embodiment 4
The paraffin of 37 weight portions and the beeswax of 17 weight portions are weighed, beeswax and 34g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-1h
Obtain the first mixture；Weigh palm wax, the gum dammar of 3.5 weight portions, the glycerine of 7 weight portions, 1.13 weight portions of 9 weight portions
Sheep oil and the polyoxyethylene amine of 0.7 weight portion be heated to 140-150 DEG C and melt and be incubated 0.5-1h obtaining the second mixture；
The first mixture is added into the second mixture at a temperature of 120-130 DEG C, the peregal and 0.5 weight portion of 0.9 weight portion is added
Sapn, with 400-600r/min rotating speeds stir 20-30min.Cooled down under 0.2-0.3MPa pressure.
Embodiment 5
The paraffin of 40 weight portions and the beeswax of 20 weight portions are weighed, beeswax and 40g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-1h
Obtain the first mixture；Weigh the palm wax of 10 weight portions, the gum dammar of 4 weight portions, the glycerine of 8 weight portions, 1.5 weight portions
The polyoxyethylene amine of sheep oil and 1 weight portion is heated to 140-150 DEG C and melts and be incubated 0.5-1h obtaining the second mixture；In 120-
The first mixture is added into the second mixture at a temperature of 130 DEG C, the peregal of 1 weight portion and the sapn of 0.6 weight portion is added,
20-30min is stirred with 400-600r/min rotating speeds.Cooled down under 0.2-0.3MPa pressure.
Embodiment 6
The paraffin of 35 weight portions and the beeswax of 14 weight portions are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-1h
Obtain the first mixture；Weigh palm wax, the gum dammar of 3 weight portions, the glycerine of 6.5 weight portions, 1.2 weight portions of 8 weight portions
Sheep oil and the polyoxyethylene amine of 0.65 weight portion be heated to 140-150 DEG C and melt and be incubated 0.5-1h obtaining the second mixture；
The first mixture is added into the second mixture at a temperature of 120-130 DEG C, 20-30min is stirred with 400-600r/min rotating speeds.
Cooled down under 0.2-0.3MPa pressure.
Comparative example 1
The paraffin of 35 weight portions and the beeswax of 14 weight portions are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-1h
Obtain the first mixture；The gum dammar of the palm wax and 3 weight portions that weigh 8 weight portions is heated to 140-150 DEG C and melts and be incubated
0.5-1h obtains the second mixture；The first mixture is added into the second mixture at a temperature of 120-130 DEG C, 0.8 weight is added
The peregal of part and the sapn of 0.4 weight portion, 20-30min is stirred with 400-600r/min rotating speeds.Under 0.2-0.3MPa pressure
Cooling.
Comparative example 2
The paraffin of 35 weight portions and the beeswax of 14 weight portions are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-1h
Obtain the first mixture；The polyoxyethylene amine for weighing the glycerine, the sheep oil of 1.2 weight portions and 0.65 weight portion of 6.5 weight portions adds
Heat is melted to 140-150 DEG C and is incubated 0.5-1h and obtains the second mixture；The first mixture is added the at a temperature of 120-130 DEG C
Two mixtures, add the peregal of 0.8 weight portion and the sapn of 0.4 weight portion, and 20- is stirred with 400-600r/min rotating speeds
30min.Cooled down under 0.2-0.3MPa pressure.
Comparative example 3
The paraffin of 35 weight portions and the beeswax of 14 weight portions are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-
1h, adds the peregal of 0.8 weight portion and the sapn of 0.4 weight portion, with 400-600r/min rotating speeds at a temperature of 120-130 DEG C
Stirring 20-30min.Cooled down under 0.2-0.3MPa pressure.
Comparative example 4
Weigh the palm wax of the paraffin of 35 weight portions and the weight portion of beeswax 8 of 14 weight portions, the gum dammar of 3 weight portions,
The polyoxyethylene amine of the glycerine of 6.5 weight portions, the sheep oil of 1.2 weight portions and 0.65 weight portion.Beeswax and 28g water are mixed and is added
Heat stands cooling after melting to 65-75 DEG C, takes out the beeswax after purification, and the beeswax after purification and other raw materials are mixed and heated to
140-150 DEG C melts and is incubated 0.5-1h；The peregal and 0.4 weight portion of 0.8 weight portion are added at a temperature of 120-130 DEG C
Sapn, 20-30min is stirred with 400-600r/min rotating speeds.Cooled down under 0.2-0.3MPa pressure.
Comparative example 5
The paraffin of 35 weight portions and the beeswax of 14 weight portions are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts to obtain the first mixing
Thing；Weigh the palm wax of 8 weight portions, the gum dammar of 3 weight portions, the glycerine of 6.5 weight portions, the sheep oil of 1.2 weight portions and
The polyoxyethylene amine of 0.65 weight portion is heated to 140-150 DEG C and melts to obtain the second mixture；By first at a temperature of 120-130 DEG C
Mixture adds the second mixture, the peregal of 0.8 weight portion and the sapn of 0.4 weight portion is added, with 400-600r/min
Rotating speed stirs 20-30min.Cooled down under 0.2-0.3MPa pressure.
Comparative example 6
The paraffin of 35 weight portions and the beeswax of 14 weight portions are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, the beeswax after purification is taken out, and the beeswax after paraffin and purification is heated into 70-80 DEG C melts and be incubated 0.5-1h
Obtain the first mixture；Weigh palm wax, the gum dammar of 3 weight portions, the glycerine of 6.5 weight portions, 1.2 weight portions of 8 weight portions
Sheep oil and the polyoxyethylene amine of 0.65 weight portion be heated to 140-150 DEG C and melt and be incubated 0.5-1h obtaining the second mixture；
The first mixture is added into the second mixture at a temperature of 120-130 DEG C, the peregal and 0.4 weight of 0.8 weight portion is added
The sapn of part, 20-30min is stirred with 400-600r/min rotating speeds.Cooling.
60 specifications are chosen for C 32X32 68X68, size shape identical dimity are divided into 12 groups, every group of 5 hairs
Cloth cloth.Using embodiment 1-6 and batik resist printing wax obtained in comparative example 1-6 is respectively as every group of resist agent of cloth, make
Pattern identical batik works.
The west of Guizhou Province and Northwestern Guizhou Province randomly select respectively 200 people to 60 batik works obtained above successively with regard to comfortableness,
Infiltration resist printing effect and the marking of anti-dewaxing effect, respectively 1,2,3,4,5,6 points of six class, point expression batik effect higher is more
Good, its result average mark is as shown in table 1.
The batik works grade form of table 1.
As shown in Table 1, embodiment 1-6 is obtained is applied to the batik resist printing wax of felt its pigment figure effect, infiltration resist printing effect
Fruit and anti-dewaxing excellent effect.Glycerine etc. is provided without in comparative example 1 and comparative example 3 to be surface-treated felt, wax oil is in hair
The comfortable feel degree of felt is substantially reduced after the osmotic efficiency on cloth surface and batik.Palm fibre is provided without in comparative example 2 and comparative example 3
Palmitic acid wax and gum dammar, the adhesion property reduction of anti-dewaxing, anti-dewaxing effect are substantially reduced, and easily produce stain at resist printing position
Influence batik effect.Raw material is not protected in 140-150 DEG C of high-temperature heating, comparative example 5 to raw material in the lump in comparative example 4
Temperature homogenization, densification operations, without pressurized operation, its batik effect is significantly reduced the cooling procedure in comparative example 6.
In sum, the preparation method of the batik resist printing wax suitable for felt of the embodiment of the present invention is simple to operate, its system
The batik resist printing wax suitable for felt is good to the osmotic effect on felt, adhesive capacity strong, waxing is uniform.
Embodiments described above is a part of embodiment of the invention, rather than whole embodiments.Reality of the invention
The detailed description for applying example is not intended to limit the scope of claimed invention, but is merely representative of selected implementation of the invention
Example.Based on the embodiment in the present invention, what those of ordinary skill in the art were obtained under the premise of creative work is not made
Every other embodiment, belongs to the scope of protection of the invention.
Claims (10)
1. a kind of batik resist printing wax suitable for felt, it is characterised in that by weight, including：Paraffin 30-40 parts, beeswax
10-20 parts, palm wax 5-10 parts, gum dammar 2-4 parts, glycerine 5-8 parts, sheep oil 1-1.5 parts and polyoxyethylene amine 0.5-1
Part.
2. the batik resist printing wax suitable for felt according to claim 1, it is characterised in that by weight, including：Institute
State paraffin 33-37 parts, described beeswax 12-17 parts, described palm wax 7-9 parts, described gum dammar 2.5-3.5 parts, the glycerine
6-7 parts, described sheep oil 1-1.3 parts and 0.5-0.8 parts of the polyoxyethylene amine.
3. the batik resist printing wax suitable for felt according to claim 2, it is characterised in that by weight, including：Institute
State 35 parts of paraffin, 14 parts of the beeswax, 8 parts of the palm wax, 3 parts of the gum dammar, 6.5 parts of the glycerine, the sheep oil
1.2 parts and 0.65 part of the polyoxyethylene amine.
4. the batik resist printing wax suitable for felt according to claim 1, it is characterised in that by weight, also include：
Peregal 0.5-1 parts, sapn 0.3-0.6 parts.
5. the batik resist printing wax suitable for felt according to claim 4, it is characterised in that the peregal and the department
The weight ratio of disk is 2:1.
6. the preparation method of a kind of batik resist printing wax suitable for felt, it is characterised in that including：Weigh 30-40 weight portions
The beeswax of paraffin and 10-20 weight portions is heated to 70-80 DEG C and melts and be incubated 0.5-1h obtaining the first mixture；Weigh 5-10 weight
Part palm wax, the gum dammar of 2-4 weight portions, the glycerine of 5-8 weight portions, the sheep oil of 1-1.5 weight portions and 0.5-1 weight
Part polyoxyethylene amine be heated to 140-150 DEG C and melt and be incubated 0.5-1h obtaining the second mixture；Will at a temperature of 120-130 DEG C
First mixture adds second mixture, and 20-30min, cooling are stirred with 400-600r/min rotating speeds.
7. preparation method according to claim 6, it is characterised in that before by the paraffin and the beeswax heating and melting,
The beeswax is purified.
8. preparation method according to claim 7, it is characterised in that the purification operations of the beeswax are：By the beeswax
Cooling, the precipitation in separation water phase and water phase are stood after being mixed and heated to 65-75 DEG C of thawing with water.
9. preparation method according to claim 6, it is characterised in that first mixture is added into second mixing
After thing, the peregal of 0.5-1 weight portions and the sapn of 0.3-0.6 weight portions are added before stirring.
10. preparation method according to claim 6, it is characterised in that cooled down under 0.2-0.3MPa pressure after stirring.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109266023A (en) * | 2018-11-25 | 2019-01-25 | 福泉市筑梦服装有限公司 | A kind of batik mixing cerate and preparation method thereof |
| CN109370238A (en) * | 2018-11-26 | 2019-02-22 | 福泉市筑梦服装有限公司 | A kind of cerate and preparation method thereof for batik |
| CN109486216A (en) * | 2018-11-26 | 2019-03-19 | 福泉市筑梦服装有限公司 | A kind of batik cerate and preparation method thereof |
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| US5400257A (en) * | 1994-02-22 | 1995-03-21 | Krinsky; Michael C. | Method of producing a batik type image on cloth |
| CN102443992A (en) * | 2010-10-11 | 2012-05-09 | 沈福海 | Wax printing process of fabrics |
| CN104074072A (en) * | 2014-07-06 | 2014-10-01 | 滁州惠智科技服务有限公司 | Batik method of leather |
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| US5400257A (en) * | 1994-02-22 | 1995-03-21 | Krinsky; Michael C. | Method of producing a batik type image on cloth |
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| CN109486216A (en) * | 2018-11-26 | 2019-03-19 | 福泉市筑梦服装有限公司 | A kind of batik cerate and preparation method thereof |
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|---|---|
| CN106905709B (en) | 2019-10-08 |
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