CN106905709B - Batik resist printing wax and preparation method thereof suitable for felt - Google Patents
Batik resist printing wax and preparation method thereof suitable for felt Download PDFInfo
- Publication number
- CN106905709B CN106905709B CN201710240351.3A CN201710240351A CN106905709B CN 106905709 B CN106905709 B CN 106905709B CN 201710240351 A CN201710240351 A CN 201710240351A CN 106905709 B CN106905709 B CN 106905709B
- Authority
- CN
- China
- Prior art keywords
- parts
- weight
- beeswax
- mixture
- wax
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
- C08L91/06—Waxes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/12—Reserving parts of the material before dyeing or printing ; Locally decreasing dye affinity by chemical means
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
A kind of batik resist printing wax and preparation method thereof suitable for felt, belongs to wax-dyeing process field.Resist printing wax includes paraffin, beeswax, palm wax, gum dammar, glycerol, sheep oil and polyoxyethylene amine.When preparation, weighs 30-40 parts by weight paraffin and 10-20 parts by weight beeswax is heated to 70-80 DEG C and melts and keep the temperature 0.5-1h obtaining the first mixture；Weigh 5-10 parts by weight palm wax, 2-4 parts by weight gum dammar and 5-8 parts by weight of glycerin, 1-1.5 parts by weight sheep oil and 0.5-1 parts by weight of polyoxyethylene amine are heated to 140-150 DEG C and melt and keep the temperature 0.5-1h obtaining the second mixture；The second mixture is added in the first mixture at a temperature of 120-130 DEG C, 20-30mi n is stirred with 400-600r/mi n revolving speed, it is cooling.Preparation method is simple, and osmotic effect of the resist printing wax obtained on felt is good, adhesive capacity is strong, waxing is uniform.
Description
Technical field
The present invention relates to wax-dyeing process fields, and in particular to a kind of suitable for the batik resist printing wax of felt and its preparation side
Method.
Background technique
Batik is the ancient ethnic group's folk tradition textile printing and dyeing handicraft in China, Gu claim wax, with twist figured silk fabrics (tie dyeing),
Press from both sides figured silk fabrics (hollow out stamp) and the referred to as big stamp skill of Ancient Times in China three.Batik is good at by the nationalitys such as Guizhou, Yunnan Miao ethnic group, the Bouyei.
Batik is to be dipped in dewaxing with wax spatula and drawn to disseminate with indigo after Hua Yubu, both contaminates wax, cloth cover takes on blue bottom white flower or white background is blue
Colored multiple patterns, meanwhile, in dip dyeing, as the wax exposure cracking of resist agent, make cloth cover that special " ice line " be presented, it is outstanding to have
Glamour.Since batik pattern is abundant, tone is plain, unique style, for making dress and personal adornment and various life utilities, it appears
Simple generous, pure and fresh pleasing, rich in national characters, the market demand increases year by year.
But the wax material in wax operation is being drawn in existing wax printing technology, generally use single paraffin or single
Beeswax heat carries out picture wax operation after melting.The hardness of paraffin is larger, is used for picture wax and operates easy exposure cracking in dyeing course
Pigment figure is generated, but its adhesiveness is lower, being easy to fall off in dyeing course causes to generate stain.The adhesiveness of beeswax is not easy well
It falls off, but its hardness is lower, and exposure cracking is difficult in dyeing course and generates pigment figure, while its asking there is also higher cost
Topic.For above-mentioned problem, the prior art is by the way that paraffin and beeswax to be simply mixed, while keeping its adhesiveness preferable
Enough exposure crackings, but it still has the problems such as permeability is poor, waxing is uneven.And due to the superficiality of different clothes
Can be different, it needs to be surface-treated for different clothes.
Summary of the invention
The purpose of the present invention is to provide a kind of batik resist printing waxes suitable for felt, in carrying out picture wax operation,
Osmotic effect on felt is good, adhesive capacity is strong, waxing is uniform.
It is obtained anti-another object of the present invention is to provide a kind of preparation method of batik resist printing wax suitable for felt
Osmotic effect of the dye wax on felt is good, adhesive capacity is strong, waxing is uniform.
The present invention solves its technical problem and adopts the following technical solutions to realize.
The present invention proposes a kind of batik resist printing wax suitable for felt, by weight includes: 30-40 parts of paraffin, beeswax
10-20 parts, 5-10 parts of palm wax, 2-4 parts of gum dammar, 5-8 parts of glycerol, 1-1.5 parts of sheep oil and polyoxyethylene amine 0.5-1
Part.
The present invention also proposes a kind of preparation method of batik resist printing wax suitable for felt, weighs the stone of 30-40 parts by weight
Wax and the beeswax of 10-20 parts by weight are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h obtaining the first mixture；Weigh 5-10 parts by weight
Palm wax, the gum dammar of 2-4 parts by weight and the sheep oil and 0.5-1 weight of the glycerol of 5-8 parts by weight, 1-1.5 parts by weight
Part polyoxyethylene amine be heated to 140-150 DEG C and melt and keep the temperature 0.5-1h obtaining the second mixture；It will at a temperature of 120-130 DEG C
The second mixture is added in first mixture, stirs 20-30min with 400-600r/min revolving speed, cooling.
The beneficial effect of the embodiment of the present invention is:
Batik resist printing wax provided by the invention suitable for felt, paraffin hardness is larger, is easy exposure cracking in dyeing
Form pigment figure；Beeswax hardness is smaller, and adhesiveness is strong, can enhance adhesion stability of the resist printing wax on cloth.With paraffin and bee
Wax is wax-matrix, and the adherency of resist printing wax stablizes, easily forms pigment figure.Palm wax has good Oil keeping, and character is thin and viscid
Spend small, resin content is low, good flowing properties, can be improved the osmosis of resist printing wax to improve resist printing effect.Da Ma tree
Rouge is widely used in enhancing ink used for plastic, compound oil ink, the adhesive force of table printing ink, mobility such as PP and PE, can be into one
The osmosis and adhesion property of step enhancing resist printing wax.The surface of felt is similar to villous fibre structure with tiny,
Cause the surface roughness of felt higher, causes the effect of waxing uneven.The fibre structure on felt surface will affect wax oil
Osmotic effect, while the operation waxed can cause to damage to the fibre structure on felt surface.The cooperation of glycerol and sheep oil can comfort
Along the fibre structure on felt surface, keep waxing uniform；Glycerol has stronger osmotic effect, and wax oil can be promoted to the infiltration of felt
Thoroughly.In addition the mixture of polyoxyethylene amine and glycerol, sheep oil can form protective layer in the fibre structure to felt surface, reduce
The damage that felt is subject in wax-dyeing process.
The preparation method of the batik resist printing wax provided by the invention for being used in felt, due to the fusing point of paraffin and beeswax compared with
It is low, paraffin and beeswax are first melted at a lower temperature, prevent the rotten or oxidation for causing paraffin and beeswax when high-temperature operation.
Heat preservation operation after raw material is melted makes to be sufficiently mixed between raw material, improves the consistency of product, to improve resist printing effect
Fruit.
Specific embodiment
It in order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below will be in the embodiment of the present invention
Technical solution be clearly and completely described.The person that is not specified actual conditions in embodiment, according to normal conditions or manufacturer builds
The condition of view carries out.Reagents or instruments used without specified manufacturer is the conventional production that can be obtained by commercially available purchase
Product.
The batik resist printing wax and preparation method thereof suitable for felt of the embodiment of the present invention is specifically described below.
A kind of batik resist printing wax suitable for felt includes: 30-40 parts of paraffin, 10-20 parts of beeswax, palm fibre by weight
5-10 parts of palmitic acid wax, 2-4 parts of gum dammar, 5-8 parts of glycerol, 1-1.5 parts of sheep oil and 0.5-1 parts of polyoxyethylene amine.
The hardness of paraffin is higher, is easy exposure cracking.During batik dyeing, what dyestuff can be generated by cracking
Gap colours on cloth, to generate the natural pigment figure of lines.But since the adhesion property of paraffin is poor, it is used alone
For paraffin as wax-matrix, stain can be formed on cloth by falling off in dyeing course paraffin, influence the effect of batik pattern.
The adhesion property of beeswax is preferable, it is not easy to fall off.But since the hardness of beeswax is lower, it is not easy to tortoise occur
Split generation pigment figure.
During drawing wax, wax oil is flowed out from wax spatula to permeate and freezes solidly on cloth, has the function that local resist printing.Due to wax
Oil is fast from sharp temperature drop, the setting rate of wax oil after wax spatula outflow, it is desirable that wax oil seepage velocity with higher makes wax oil
It can be impregnated with cloth, to guarantee the resist printing effect of picture wax.
Palm wax has good Oil keeping, and character is thin and viscosity is small, and resin content is low, good flowing properties,
It can be improved the osmosis of batik resist printing wax, to improve resist printing effect.
Gum dammar is widely used in enhancing the ink used for plastic such as PP and PE, compound oil ink, the adhesive force of table printing ink, flowing
Property, the osmosis and adhesion property of resist printing wax can be further enhanced, resist printing is made good use of, and effectively prevent generating stain,
Further increase the quality of batiks.
Further, peregal and sapn are added in batik resist printing wax of the invention, with preferable peptizaiton, energy
Promote peptizaiton of the wax oil in cloth, the osmosis of wax oil is improved, to further increase the resist printing of batik resist printing wax
Effect.
Wax-dyeing process is especially prevailing in Guizhou province, but different regions like using cloth be not quite similar.The southeast of Guizhou Province
Be often used felt with one band of the south of Guizhou Province, the west of Guizhou Province, one band of Northwestern Guizhou Province Miao ethnic group then like with burlap and felt.
The surface of felt is similar to villous fibre structure with tiny, causes the surface roughness of felt higher,
Cause the effect of waxing uneven.The fibre structure on felt surface will affect the osmotic effect of wax oil, while the operation meeting waxed
The fibre structure on felt surface is caused to damage.
Through inventor the study found that glycerol and paraffin and beeswax, which are blended in batik operation, stronger penetrating power.Together
When glycerol and sheep oil batik operation in have Fushun effect to the surface of felt, make waxing wax layer it is more uniform.In the present invention,
The surface treatment of felt is carried out using the mixture of glycerol, sheep oil and polyoxyethylene amine, felt surface fiber structure mentions in Fushun
While high resist printing effect, protective layer is formed on felt surface, reduces the damage that the fibre structure of felt is subject to during batik
Wound improves the comfort of felt after batik.
This is suitable for the preparation method of the batik resist printing wax of felt, comprising: weighs the paraffin and 10-20 of 30-40 parts by weight
The beeswax of parts by weight is heated to 70-80 DEG C and melts and keep the temperature 0.5-1h obtaining the first mixture；Weigh 5-10 parts by weight palm wax,
The gum dammar of 2-4 parts by weight and glycerol, the sheep oil of 1-1.5 parts by weight and the polyoxy second of 0.5-1 parts by weight of 5-8 parts by weight
Enamine is heated to 140-150 DEG C and melts and keep the temperature 0.5-1h obtaining the second mixture；By the first mixture at a temperature of 120-130 DEG C
The second mixture is added, 20-30min is stirred with 400-600r/min revolving speed, it is cooling.
Peregal and sapn is added after first mixture and the mixing of the second mixture, the process with stirring makes the first mixing
Object and the second mixture are uniformly dispersed, and improve the homogenization of resist printing wax material interior tissue.
Since the fusing point of paraffin and beeswax is lower and easy to oxidize rotten, it is melted at low temperature, prevent and its
His raw material melts under the high temperature conditions leads to oxidation deterioration etc..Raw material carries out isothermal holding after thawing, can make between raw material
It is sufficiently mixed, disperses, homogenize production die further, pore size after material condensation can be effectively reduced, improve batik
The consistency of resist printing wax further increases the resist printing performance of material.
Further, cooling down operation carries out under the pressure of 0.2-0.3MPa, can promote fine and close combination between raw material, into
One step increases the consistency of material, improves the mobility and permeability of wax oil.
Beeswax is a kind of fatty matter being secreted by 4 pairs of wax glands of worker bee abdomen of the right age in bee colony.In bee colony,
Worker bee builds honeycomb, ovary capping and the capping of feed room using the wax that oneself is secreted.Honeycomb is to hoard food, cultivate for honeybee
Bee and the place for inhabiting conglomeration, beeswax is both the product of bee colony and it is survived and the necessary material of breeding, therefore beeswax
In usually contain more insoluble impurities, influence the quality of batik resist printing wax.
Therefore it is further, in the present invention, before paraffin and beeswax heating and melting are mixed, purification behaviour is carried out to beeswax
Make.
Specifically, since the density of beeswax is small compared with water, and insoluble impurities water content and nutrition content in beeswax
Higher, density is greater than water.In purification operations, cooling, beeswax are stood after beeswax and water are mixed and heated to 65-75 DEG C of thawing
In insoluble impurities be sunken to the bottom of water, beeswax floats on the surface of water and gradually condenses, and beeswax is taken out after the completion of condensation and is
Complete purification operations.
In order to be sufficiently separated insoluble impurities with beeswax, the mass ratio of preferable beeswax and water is generally 1:2.Into one
Step, 2-3 identical purification operations can be repeated, convenient for impurity to be sufficiently separated.
Feature and performance of the invention are described in further detail with reference to embodiments.
Embodiment 1
A kind of preparation method of the batik resist printing wax suitable for felt, comprising:
The paraffin of 30 parts by weight and the beeswax of 10 parts by weight are weighed, beeswax and 20g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h
Obtain the first mixture；Weigh the palm wax of 5 parts by weight, the gum dammar of 2 parts by weight, the glycerol of 5 parts by weight, 1 parts by weight sheep
Oil and the polyoxyethylene amine of 0.5 parts by weight are heated to 140-150 DEG C and melt and keep the temperature 0.5-1h obtaining the second mixture；In 120-
The second mixture is added in the first mixture at a temperature of 130 DEG C, adds the peregal of 0.5 parts by weight and the department of 0.3 parts by weight
Disk stirs 20-30min with 400-600r/min revolving speed.It is cooling under 0.2-0.3MPa pressure.
Embodiment 2
The paraffin of 33 parts by weight and the beeswax of 12 parts by weight are weighed, beeswax and 24g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h
Obtain the first mixture；Weigh the palm wax of 7 parts by weight, the gum dammar of 2.5 parts by weight, the glycerol of 6 parts by weight, 1.1 parts by weight
Sheep oil and the polyoxyethylene amine of 0.6 parts by weight be heated to 140-150 DEG C and melt and keep the temperature 0.5-1h obtaining the second mixture；?
The second mixture is added in the first mixture at a temperature of 120-130 DEG C, adds the peregal and 0.35 parts by weight of 0.6 parts by weight
Sapn, with 400-600r/min revolving speed stir 20-30min.It is cooling under 0.2-0.3MPa pressure.
Embodiment 3
The paraffin of 35 parts by weight and the beeswax of 14 parts by weight are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h
Obtain the first mixture；Weigh the palm wax of 8 parts by weight, the gum dammar of 3 parts by weight, the glycerol of 6.5 parts by weight, 1.2 parts by weight
Sheep oil and the polyoxyethylene amine of 0.65 parts by weight be heated to 140-150 DEG C and melt and keep the temperature 0.5-1h obtaining the second mixture；
The second mixture is added in the first mixture at a temperature of 120-130 DEG C, adds the peregal and 0.4 weight of 0.8 parts by weight
The sapn of part stirs 20-30min with 400-600r/min revolving speed.It is cooling under 0.2-0.3MPa pressure.
Embodiment 4
The paraffin of 37 parts by weight and the beeswax of 17 parts by weight are weighed, beeswax and 34g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h
Obtain the first mixture；Weigh the palm wax of 9 parts by weight, the gum dammar of 3.5 parts by weight, the glycerol of 7 parts by weight, 1.13 parts by weight
Sheep oil and the polyoxyethylene amine of 0.7 parts by weight be heated to 140-150 DEG C and melt and keep the temperature 0.5-1h obtaining the second mixture；?
The second mixture is added in the first mixture at a temperature of 120-130 DEG C, adds the peregal and 0.5 parts by weight of 0.9 parts by weight
Sapn, with 400-600r/min revolving speed stir 20-30min.It is cooling under 0.2-0.3MPa pressure.
Embodiment 5
The paraffin of 40 parts by weight and the beeswax of 20 parts by weight are weighed, beeswax and 40g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h
Obtain the first mixture；Weigh the palm wax of 10 parts by weight, the gum dammar of 4 parts by weight, the glycerol of 8 parts by weight, 1.5 parts by weight
The polyoxyethylene amine of sheep oil and 1 parts by weight is heated to 140-150 DEG C and melts and keep the temperature 0.5-1h obtaining the second mixture；In 120-
The second mixture is added in the first mixture at a temperature of 130 DEG C, adds the peregal of 1 parts by weight and the sapn of 0.6 parts by weight,
20-30min is stirred with 400-600r/min revolving speed.It is cooling under 0.2-0.3MPa pressure.
Embodiment 6
The paraffin of 35 parts by weight and the beeswax of 14 parts by weight are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h
Obtain the first mixture；Weigh the palm wax of 8 parts by weight, the gum dammar of 3 parts by weight, the glycerol of 6.5 parts by weight, 1.2 parts by weight
Sheep oil and the polyoxyethylene amine of 0.65 parts by weight be heated to 140-150 DEG C and melt and keep the temperature 0.5-1h obtaining the second mixture；
The second mixture is added in the first mixture at a temperature of 120-130 DEG C, 20-30min is stirred with 400-600r/min revolving speed.?
It is cooling under 0.2-0.3MPa pressure.
Comparative example 1
The paraffin of 35 parts by weight and the beeswax of 14 parts by weight are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h
Obtain the first mixture；The gum dammar of the palm wax and 3 parts by weight that weigh 8 parts by weight is heated to 140-150 DEG C and melts and keep the temperature
0.5-1h obtains the second mixture；The second mixture is added in the first mixture at a temperature of 120-130 DEG C, adds 0.8 weight
The peregal of part and the sapn of 0.4 parts by weight stir 20-30min with 400-600r/min revolving speed.Under 0.2-0.3MPa pressure
It is cooling.
Comparative example 2
The paraffin of 35 parts by weight and the beeswax of 14 parts by weight are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h
Obtain the first mixture；The polyoxyethylene amine for weighing the glycerol of 6.5 parts by weight, the sheep oil of 1.2 parts by weight and 0.65 parts by weight adds
Heat is melted and is kept the temperature 0.5-1h to 140-150 DEG C and obtains the second mixture；The first mixture is added the at a temperature of 120-130 DEG C
Two mixtures add the peregal of 0.8 parts by weight and the sapn of 0.4 parts by weight, stir 20- with 400-600r/min revolving speed
30min.It is cooling under 0.2-0.3MPa pressure.
Comparative example 3
The paraffin of 35 parts by weight and the beeswax of 14 parts by weight are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-
The peregal of 0.8 parts by weight and the sapn of 0.4 parts by weight is added, at a temperature of 120-130 DEG C with 400-600r/min revolving speed in 1h
Stir 20-30min.It is cooling under 0.2-0.3MPa pressure.
Comparative example 4
Weigh the palm wax of the paraffin of 35 parts by weight and 8 parts by weight of beeswax of 14 parts by weight, the gum dammar of 3 parts by weight,
The polyoxyethylene amine of the glycerol of 6.5 parts by weight, the sheep oil of 1.2 parts by weight and 0.65 parts by weight.Beeswax and 28g water are mixed and added
Cooling is stood after heat to 65-75 DEG C of thawing, the beeswax after purification is mixed and heated to by the beeswax after taking out purification with other raw materials
140-150 DEG C melts and keeps the temperature 0.5-1h；The peregal and 0.4 parts by weight of 0.8 parts by weight are added at a temperature of 120-130 DEG C
Sapn stirs 20-30min with 400-600r/min revolving speed.It is cooling under 0.2-0.3MPa pressure.
Comparative example 5
The paraffin of 35 parts by weight and the beeswax of 14 parts by weight are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Cooling is stood afterwards, and the beeswax after paraffin and purification is heated to 70-80 DEG C and melts to obtain the first mixing by the beeswax after taking out purification
Object；Weigh the palm wax of 8 parts by weight, the gum dammar of 3 parts by weight, the glycerol of 6.5 parts by weight, 1.2 parts by weight sheep oil and
The polyoxyethylene amine of 0.65 parts by weight is heated to 140-150 DEG C and melts to obtain the second mixture；By first at a temperature of 120-130 DEG C
The second mixture is added in mixture, the peregal of 0.8 parts by weight and the sapn of 0.4 parts by weight is added, with 400-600r/min
Revolving speed stirs 20-30min.It is cooling under 0.2-0.3MPa pressure.
Comparative example 6
The paraffin of 35 parts by weight and the beeswax of 14 parts by weight are weighed, beeswax and 28g water are mixed and heated to 65-75 DEG C of thawing
Standing cooling afterwards, the beeswax after taking out purification, the beeswax by paraffin and after purifying are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h
Obtain the first mixture；Weigh the palm wax of 8 parts by weight, the gum dammar of 3 parts by weight, the glycerol of 6.5 parts by weight, 1.2 parts by weight
Sheep oil and the polyoxyethylene amine of 0.65 parts by weight be heated to 140-150 DEG C and melt and keep the temperature 0.5-1h obtaining the second mixture；
The second mixture is added in the first mixture at a temperature of 120-130 DEG C, adds the peregal and 0.4 weight of 0.8 parts by weight
The sapn of part stirs 20-30min with 400-600r/min revolving speed.It is cooling.
It chooses 60 specifications and is divided into 12 groups for C 32X32 68X68, the identical dimity of size shape, every group 5 is opened the hair
Cloth cloth.Using batik resist printing wax made from embodiment 1-6 and comparative example 1-6 respectively as the resist agent of every group of cloth, production
The identical batik works of pattern.
The west of Guizhou Province and Northwestern Guizhou Province randomly select respectively 200 people to 60 batik works obtained above successively with regard to comfort,
Resist printing effect and the marking of anti-dewaxing effect are permeated, respectively 1,2,3,4,5,6 point of six class, point higher expression batik effect is more
Good, result average mark is as shown in table 1.
1. batik works grade form of table
As shown in Table 1, embodiment 1-6 is obtained is suitable for its pigment figure effect of the batik resist printing wax of felt, infiltration resist printing effect
Fruit and anti-dewaxing excellent effect.Felt is not surface-treated using glycerol etc. in comparative example 1 and comparative example 3, wax oil is in hair
The comfortable feel degree of felt is substantially reduced after the osmotic efficiency on cloth surface and batik.Not using palm fibre in comparative example 2 and comparative example 3
The adhesion property of palmitic acid wax and gum dammar, anti-dewaxing reduces, and anti-dewaxing effect is substantially reduced, and is easy to generate stain at resist printing position
Influence batik effect.Raw material does not together protect raw material in 140-150 DEG C of high-temperature heating, comparative example 5 in comparative example 4
Temperature homogenization, densification operations, the cooling procedure in comparative example 6 operate without pressurization, and batik effect is significantly reduced.
In conclusion the preparation method of the batik resist printing wax suitable for felt of the embodiment of the present invention is easy to operate, system
The batik resist printing wax suitable for felt obtained is good to the osmotic effect on felt, adhesive capacity is strong, waxing is uniform.
Embodiments described above is a part of the embodiment of the present invention, instead of all the embodiments.Reality of the invention
The detailed description for applying example is not intended to limit the range of claimed invention, but is merely representative of selected implementation of the invention
Example.Based on the embodiments of the present invention, obtained by those of ordinary skill in the art without making creative efforts
Every other embodiment, shall fall within the protection scope of the present invention.
Claims (9)
1. a kind of batik resist printing wax suitable for felt, which is characterized in that by weight, comprising: 30-40 parts of paraffin, beeswax
10-20 parts, 5-10 parts of palm wax, 2-4 parts of gum dammar, 5-8 parts of glycerol, 1-1.5 parts of sheep oil and polyoxyethylene amine 0.5-1
Part；
The batik resist printing wax suitable for felt obtains by the following method: the paraffin and the beeswax are heated to 70-
80 DEG C melt and keep the temperature 0.5-1h and obtain the first mixture, by the palm wax, the gum dammar, the glycerol, the sheep oil
And the polyoxyethylene amine is heated to 140-150 DEG C and melts and keep the temperature 0.5-1h obtaining the second mixture, in 120-130 DEG C of temperature
It is lower that second mixture is added in first mixture, 20-30min is stirred with 400-600r/min revolving speed, in 0.2-
It is cooling under 0.3MPa pressure.
2. the batik resist printing wax according to claim 1 suitable for felt, which is characterized in that by weight, comprising: institute
State 33-37 parts of paraffin, beeswax 12-17 parts described, palm wax 7-9 parts described, the gum dammar 2.5-3.5 parts described, glycerol
6-7 parts, sheep oil 1-1.3 parts and 0.5-0.8 parts of the polyoxyethylene amine.
3. the batik resist printing wax according to claim 2 suitable for felt, which is characterized in that by weight, comprising: institute
State 35 parts of paraffin, 14 parts of the beeswax, 8 parts of the palm wax, 3 parts of the gum dammar, 6.5 parts of the glycerol, the sheep oil
1.2 parts and 0.65 part of the polyoxyethylene amine.
4. the batik resist printing wax according to claim 1 suitable for felt, which is characterized in that by weight, further includes:
0.5-1 parts of peregal, 0.3-0.6 parts of sapn；
The peregal and the sapn are added after second mixture is added in first mixture and before stirring.
5. the batik resist printing wax according to claim 4 suitable for felt, which is characterized in that the peregal and the department
The weight ratio of disk is 2:1.
6. a kind of preparation method of the batik resist printing wax suitable for felt characterized by comprising weigh 30-40 parts by weight
Paraffin and the beeswax of 10-20 parts by weight are heated to 70-80 DEG C and melt and keep the temperature 0.5-1h obtaining the first mixture；Weigh 5-10 weight
Part palm wax, the gum dammar of 2-4 parts by weight, the glycerol of 5-8 parts by weight, 1-1.5 parts by weight sheep oil and 0.5-1 weight
Part polyoxyethylene amine be heated to 140-150 DEG C and melt and keep the temperature 0.5-1h obtaining the second mixture；It will at a temperature of 120-130 DEG C
Second mixture is added in first mixture, 20-30min is stirred with 400-600r/min revolving speed, in 0.2-0.3MPa
It is cooling under pressure.
7. preparation method according to claim 6, which is characterized in that before the paraffin and the beeswax heating and melting,
The beeswax is purified.
8. preparation method according to claim 7, which is characterized in that the purification operations of the beeswax are as follows: by the beeswax
Cooling is stood after being mixed and heated to 65-75 DEG C of thawing with water, separates the precipitating in water phase and water phase.
9. preparation method according to claim 6, which is characterized in that second mixing is added in first mixture
After object, the peregal of 0.5-1 parts by weight and the sapn of 0.3-0.6 parts by weight is added before stirring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710240351.3A CN106905709B (en) | 2017-04-13 | 2017-04-13 | Batik resist printing wax and preparation method thereof suitable for felt |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710240351.3A CN106905709B (en) | 2017-04-13 | 2017-04-13 | Batik resist printing wax and preparation method thereof suitable for felt |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106905709A CN106905709A (en) | 2017-06-30 |
| CN106905709B true CN106905709B (en) | 2019-10-08 |
Family
ID=59209557
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710240351.3A Active CN106905709B (en) | 2017-04-13 | 2017-04-13 | Batik resist printing wax and preparation method thereof suitable for felt |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106905709B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109266023A (en) * | 2018-11-25 | 2019-01-25 | 福泉市筑梦服装有限公司 | A kind of batik mixing cerate and preparation method thereof |
| CN109370238A (en) * | 2018-11-26 | 2019-02-22 | 福泉市筑梦服装有限公司 | A kind of cerate and preparation method thereof for batik |
| CN109486216A (en) * | 2018-11-26 | 2019-03-19 | 福泉市筑梦服装有限公司 | A kind of batik cerate and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051949A (en) * | 1990-06-20 | 1991-06-05 | 惠彬 | Wax painting method of leather |
| CN102443992A (en) * | 2010-10-11 | 2012-05-09 | 沈福海 | Wax printing process of fabrics |
| CN104074072A (en) * | 2014-07-06 | 2014-10-01 | 滁州惠智科技服务有限公司 | Batik method of leather |
| CN104074073A (en) * | 2014-07-06 | 2014-10-01 | 滁州惠智科技服务有限公司 | Production method of cracking imitation leather |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5400257A (en) * | 1994-02-22 | 1995-03-21 | Krinsky; Michael C. | Method of producing a batik type image on cloth |
-
2017
- 2017-04-13 CN CN201710240351.3A patent/CN106905709B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1051949A (en) * | 1990-06-20 | 1991-06-05 | 惠彬 | Wax painting method of leather |
| CN102443992A (en) * | 2010-10-11 | 2012-05-09 | 沈福海 | Wax printing process of fabrics |
| CN104074072A (en) * | 2014-07-06 | 2014-10-01 | 滁州惠智科技服务有限公司 | Batik method of leather |
| CN104074073A (en) * | 2014-07-06 | 2014-10-01 | 滁州惠智科技服务有限公司 | Production method of cracking imitation leather |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106905709A (en) | 2017-06-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106957532B (en) | Batik resist printing wax and preparation method thereof suitable for burlap | |
| CN106894251B (en) | Batik resist printing wax and preparation method thereof suitable for cotton | |
| CN106905709B (en) | Batik resist printing wax and preparation method thereof suitable for felt | |
| CN102613801B (en) | Dry nail polish applique and manufacture method thereof | |
| CN101899786A (en) | Textile inkjet printing acid dye ink and production method thereof | |
| CN107160511B (en) | A kind of the batik method and batik woodwork of woodwork | |
| CN108327441A (en) | A kind of preparation method of stereoscopic crystal glue flower picture | |
| CN109518490A (en) | A kind of nationality's batik cerate and preparation method thereof | |
| CN106366262A (en) | Mixed pulp and method for preparing paper plate buttons | |
| CN107379164B (en) | A kind of peeling method of wicker plaiting article braided material | |
| CN105155308B (en) | The production method of cracking sense leather | |
| CN105220527A (en) | A kind of batik method of sieve | |
| CN104651101A (en) | Preparation method of handmade soap | |
| CN103046261A (en) | Embroidery process for double-layer three-side embroidery | |
| CN110080020A (en) | Batik dyestuff, vegetable leather batik and waxprinting article and vegetable leather batik method | |
| CN107049873A (en) | A kind of method being had hair dyed with extra large Na powder | |
| CN106274244A (en) | A kind of draw craft of tempera painting | |
| CN112442909B (en) | Wax printing drawing process | |
| CN109627852A (en) | A kind of oil immersion colored pencil lead and preparation method thereof | |
| CN104354489A (en) | Digital ink-jet printing heat transfer printing membrane and preparing method thereof | |
| KR101756436B1 (en) | Composition for mask pack sheet fabric, method for transferring mask pack sheet fabric and mask pack sheet fabric manufactured by thereof | |
| CN103992555A (en) | Antifreezing simulated cream adhesive and preparation method thereof | |
| CN110205828A (en) | A kind of plants essential oil microcapsules and preparation method thereof | |
| CN107099203A (en) | A kind of release layer preparation method of heat transfer printing carbon tape | |
| US20220389259A1 (en) | Eco-friendly crayon composition and method for producing eco-friendly crayons |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |