CN106893341A - 分散紫26的工业化生产方法 - Google Patents
分散紫26的工业化生产方法 Download PDFInfo
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- CN106893341A CN106893341A CN201710149565.XA CN201710149565A CN106893341A CN 106893341 A CN106893341 A CN 106893341A CN 201710149565 A CN201710149565 A CN 201710149565A CN 106893341 A CN106893341 A CN 106893341A
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- kettle
- phenol
- water
- disperse violet
- waste water
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- 238000000034 method Methods 0.000 title claims abstract description 27
- GTZCVFVGUGFEME-UHFFFAOYSA-N aconitic acid Chemical compound OC(=O)CC(C(O)=O)=CC(O)=O GTZCVFVGUGFEME-UHFFFAOYSA-N 0.000 title claims abstract description 13
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000002351 wastewater Substances 0.000 claims abstract description 36
- 239000002253 acid Substances 0.000 claims abstract description 23
- 239000002904 solvent Substances 0.000 claims abstract description 20
- 238000000605 extraction Methods 0.000 claims abstract description 14
- 238000009833 condensation Methods 0.000 claims abstract description 10
- 230000005494 condensation Effects 0.000 claims abstract description 10
- 238000001914 filtration Methods 0.000 claims abstract description 9
- 238000004065 wastewater treatment Methods 0.000 claims abstract description 6
- 238000002955 isolation Methods 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 25
- 239000000463 material Substances 0.000 claims description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 239000012452 mother liquor Substances 0.000 claims description 20
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 238000000926 separation method Methods 0.000 claims description 15
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 13
- 238000007792 addition Methods 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 11
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 10
- 239000008234 soft water Substances 0.000 claims description 10
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 9
- 238000004821 distillation Methods 0.000 claims description 8
- NNXSVNHFDAUPRN-UHFFFAOYSA-N 1,4-diamino-2-chloroanthracene-9,10-dione Chemical class O=C1C2=CC=CC=C2C(=O)C2=C1C(N)=C(Cl)C=C2N NNXSVNHFDAUPRN-UHFFFAOYSA-N 0.000 claims description 6
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 6
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 5
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 4
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical class CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 3
- 238000013461 design Methods 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- 239000003350 kerosene Substances 0.000 claims description 3
- 238000006386 neutralization reaction Methods 0.000 claims description 3
- KSSNXJHPEFVKHY-UHFFFAOYSA-N phenol;hydrate Chemical compound O.OC1=CC=CC=C1 KSSNXJHPEFVKHY-UHFFFAOYSA-N 0.000 claims description 3
- 238000004064 recycling Methods 0.000 claims description 3
- 239000003643 water by type Substances 0.000 claims description 3
- LRMDXTVKVHKWEK-UHFFFAOYSA-N 1,2-diaminoanthracene-9,10-dione Chemical class C1=CC=C2C(=O)C3=C(N)C(N)=CC=C3C(=O)C2=C1 LRMDXTVKVHKWEK-UHFFFAOYSA-N 0.000 claims description 2
- 230000033228 biological regulation Effects 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- DKAGJZJALZXOOV-UHFFFAOYSA-N hydrate;hydrochloride Chemical compound O.Cl DKAGJZJALZXOOV-UHFFFAOYSA-N 0.000 claims description 2
- 239000007787 solid Substances 0.000 claims description 2
- 238000013517 stratification Methods 0.000 claims description 2
- 238000010792 warming Methods 0.000 claims description 2
- 239000002994 raw material Substances 0.000 abstract description 3
- 239000012847 fine chemical Substances 0.000 abstract description 2
- 238000012545 processing Methods 0.000 abstract description 2
- 238000001514 detection method Methods 0.000 description 5
- 239000010838 isolation waste Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000007664 blowing Methods 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 206010054949 Metaplasia Diseases 0.000 description 1
- 229920004933 Terylene® Polymers 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000000986 disperse dye Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 230000015689 metaplastic ossification Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- BAPROVDXKNPHAM-UHFFFAOYSA-N n-(2-aminoethyl)-3-(3,5-ditert-butyl-4-hydroxyphenyl)propanamide Chemical compound CC(C)(C)C1=CC(CCC(=O)NCCN)=CC(C(C)(C)C)=C1O BAPROVDXKNPHAM-UHFFFAOYSA-N 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- WYRNWLMLMJGFIR-UHFFFAOYSA-N phenol;dihydrate Chemical compound O.O.OC1=CC=CC=C1 WYRNWLMLMJGFIR-UHFFFAOYSA-N 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000000992 solvent dye Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
- C09B1/50—Amino-hydroxy-anthraquinones; Ethers and esters thereof
- C09B1/54—Amino-hydroxy-anthraquinones; Ethers and esters thereof etherified
- C09B1/547—Anthraquinones with aromatic ether groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
- Physical Water Treatments (AREA)
Abstract
Description
Claims (7)
Priority Applications (1)
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CN201710149565.XA CN106893341B (zh) | 2017-03-14 | 2017-03-14 | 分散紫26的工业化生产方法 |
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CN201710149565.XA CN106893341B (zh) | 2017-03-14 | 2017-03-14 | 分散紫26的工业化生产方法 |
Publications (2)
Publication Number | Publication Date |
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CN106893341A true CN106893341A (zh) | 2017-06-27 |
CN106893341B CN106893341B (zh) | 2019-10-29 |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108659567A (zh) * | 2018-05-25 | 2018-10-16 | 江苏道博化工有限公司 | 溶剂紫59的合成工艺 |
CN111073333A (zh) * | 2019-12-20 | 2020-04-28 | 南京金浩医药科技有限公司 | 一种分散紫26的制备方法 |
CN111675918A (zh) * | 2020-06-08 | 2020-09-18 | 扬州日兴生物科技股份有限公司 | 一种分散红60的制备方法 |
CN114479507A (zh) * | 2022-02-09 | 2022-05-13 | 江苏亚邦染料股份有限公司 | 一种环保型分散紫26的制备方法 |
CN114539802A (zh) * | 2022-02-16 | 2022-05-27 | 安徽清科瑞洁新材料有限公司 | 一种溶剂紫59精制工艺 |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB405632A (en) * | 1932-04-05 | 1934-01-29 | Ig Farbenindustrie Ag | Improvements in the manufacture and production of 1.4-diamino-2-aryloxyanthraquinone-3-sulphonic acids |
GB452203A (en) * | 1934-11-14 | 1936-08-14 | Ici Ltd | New anthraquinone dyestuffs |
JPS55102535A (en) * | 1979-01-30 | 1980-08-05 | Mitsui Toatsu Chem Inc | Separation of 1,5-diphenoxyanthraquinone and 1,8- diphenoxyanthraquinone |
JPS59142253A (ja) * | 1983-02-01 | 1984-08-15 | Sumitomo Chem Co Ltd | 1,4−ジアミノ−2,3−ジフエノキシアントラキノンの製造方法 |
JPS6099168A (ja) * | 1983-11-02 | 1985-06-03 | Sumitomo Chem Co Ltd | 1,4−ジアミノ−2,3−ジフエノキシアントラキノンの製造方法 |
CN101225239A (zh) * | 2007-12-14 | 2008-07-23 | 浙江长征化工有限公司 | 分散红60副产物的回收综合利用方法 |
CN102276438A (zh) * | 2011-07-08 | 2011-12-14 | 江苏吉华化工有限公司 | 一种1,5(1,8)–二苯氧基蒽醌的生产方法 |
CN102618058A (zh) * | 2012-03-16 | 2012-08-01 | 苏州市罗森助剂有限公司 | 一种分散紫26的制备方法 |
CN106349733A (zh) * | 2016-08-29 | 2017-01-25 | 安庆市长虹化工有限公司 | 一种合成分散红fb的工艺及其设备 |
-
2017
- 2017-03-14 CN CN201710149565.XA patent/CN106893341B/zh active Active
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB405632A (en) * | 1932-04-05 | 1934-01-29 | Ig Farbenindustrie Ag | Improvements in the manufacture and production of 1.4-diamino-2-aryloxyanthraquinone-3-sulphonic acids |
GB452203A (en) * | 1934-11-14 | 1936-08-14 | Ici Ltd | New anthraquinone dyestuffs |
JPS55102535A (en) * | 1979-01-30 | 1980-08-05 | Mitsui Toatsu Chem Inc | Separation of 1,5-diphenoxyanthraquinone and 1,8- diphenoxyanthraquinone |
JPS59142253A (ja) * | 1983-02-01 | 1984-08-15 | Sumitomo Chem Co Ltd | 1,4−ジアミノ−2,3−ジフエノキシアントラキノンの製造方法 |
JPS6099168A (ja) * | 1983-11-02 | 1985-06-03 | Sumitomo Chem Co Ltd | 1,4−ジアミノ−2,3−ジフエノキシアントラキノンの製造方法 |
CN101225239A (zh) * | 2007-12-14 | 2008-07-23 | 浙江长征化工有限公司 | 分散红60副产物的回收综合利用方法 |
CN102276438A (zh) * | 2011-07-08 | 2011-12-14 | 江苏吉华化工有限公司 | 一种1,5(1,8)–二苯氧基蒽醌的生产方法 |
CN102618058A (zh) * | 2012-03-16 | 2012-08-01 | 苏州市罗森助剂有限公司 | 一种分散紫26的制备方法 |
CN106349733A (zh) * | 2016-08-29 | 2017-01-25 | 安庆市长虹化工有限公司 | 一种合成分散红fb的工艺及其设备 |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108659567A (zh) * | 2018-05-25 | 2018-10-16 | 江苏道博化工有限公司 | 溶剂紫59的合成工艺 |
CN111073333A (zh) * | 2019-12-20 | 2020-04-28 | 南京金浩医药科技有限公司 | 一种分散紫26的制备方法 |
CN111675918A (zh) * | 2020-06-08 | 2020-09-18 | 扬州日兴生物科技股份有限公司 | 一种分散红60的制备方法 |
CN111675918B (zh) * | 2020-06-08 | 2022-01-21 | 扬州日兴生物科技股份有限公司 | 一种分散红60的制备方法 |
CN114479507A (zh) * | 2022-02-09 | 2022-05-13 | 江苏亚邦染料股份有限公司 | 一种环保型分散紫26的制备方法 |
CN114539802A (zh) * | 2022-02-16 | 2022-05-27 | 安徽清科瑞洁新材料有限公司 | 一种溶剂紫59精制工艺 |
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CN106893341B (zh) | 2019-10-29 |
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Effective date of registration: 20230707 Address after: 222000 duigougang Town, Guannan County, Lianyungang City, Jiangsu Province (Chemical Industrial Park) Patentee after: JIANGSU HUAER CHEMICAL Co.,Ltd. Address before: Jiangsu Yabang Dyestuff Co., Ltd., No. 105, Renmin West Road, Niutang Town, Wujin District, Changzhou City, Jiangsu Province, 213163 Patentee before: Jiangsu Yabang Dye Co.,Ltd. |
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CP03 | Change of name, title or address |
Address after: 222000 duigougang Town, Guannan County, Lianyungang City, Jiangsu Province (Chemical Industrial Park) Patentee after: Jiangsu Yabang Wall Dyestuff Co.,Ltd. Country or region after: China Address before: 222000 duigougang Town, Guannan County, Lianyungang City, Jiangsu Province (Chemical Industrial Park) Patentee before: JIANGSU HUAER CHEMICAL Co.,Ltd. Country or region before: China |