CN106857726A - Pure natural insecticide and preparation method thereof - Google Patents
Pure natural insecticide and preparation method thereof Download PDFInfo
- Publication number
- CN106857726A CN106857726A CN201710048981.0A CN201710048981A CN106857726A CN 106857726 A CN106857726 A CN 106857726A CN 201710048981 A CN201710048981 A CN 201710048981A CN 106857726 A CN106857726 A CN 106857726A
- Authority
- CN
- China
- Prior art keywords
- parts
- pure natural
- insecticide
- natural method
- castor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Pest Control & Pesticides (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention provides a kind of pure natural insecticide, and the insecticide includes following component and its weight portion：42 53 parts of garlic, 20 30 parts of shallot, 40 50 parts of balsam pear, 35 45 parts of ginger, 10 20 parts of castor-oil plant, 5 10 parts of matrine, 48 parts of rotenone, 36 parts of chilli oil, 10 15 parts of chinaberry of print, 0.2 0.6 parts of creeping dichondra herb, 0.4 0.8 parts of keel wind, this pure natural insecticide that the present invention is provided and preparation method thereof, it is convenient to prepare, constituents extraction purity is high during preparation, the effect of creeping dichondra herb and keel wind have desinsection, improve disinsection efficiency, increase EDD, environmental protection, it is degradable, people and animals are safe from harm.
Description
Technical field
The present invention relates to prevention and elimination of disease and pests field, especially a kind of pure natural insecticide and preparation method thereof.
Background technology
With the progress of science, insecticide control pest and disease damage is used in continuing to develop for agricultural, existing 1500 in China
History,《Compendium of Materia Medica》In just have record with herbal medicine desinsection.Study according to investigations, there are 200 various plants to be processed into pure
Natural insecticide, for preventing and treating agricultural fruit trees and vegetables pest and disease damage.How the world today mitigates chemical pesticide pollution, it is ensured that food is pacified
Entirely, production organic food, pollution-free green food, increasingly get more and more people's extensive concerning.It can be said that using the feature of environmental protection
Insecticide, in terms of ecological protection, with special not replaceable advantage.
In the production of insecticide and its technology of preparing, such as a kind of peach natural insecticide and preparation method thereof,
A kind of CN103349009A, peach natural insecticide that the invention is provided, is made up of following component：Balsam pear, reed, Chang Chun
Rattan, clover, the bighead atractylodes rhizome, asarum, Radix Isatidis, Pogostemon cablin, the bark of official magnolia, cubeb litsen tree.The peach is abundant with natural insecticide raw material sources, into
This is cheap, is made of pure natural component, not only Nonpoisonous, non-environmental-pollution, and can effectively prevent and treat the common germ of peach.
This natural insecticide of the invention, extracting concentration is relatively low during preparation causes insecticidal effect not notable, and lasting effect is not
Strong the shortcomings of.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of raising insecticide efficiency, increase EDD, green ring
Protecting degradable and the pure natural insecticide to people and animals' non-hazardous and preparation method thereof.
To solve above-mentioned existing technical problem, the present invention uses following scheme：A kind of pure natural insecticide, the desinsection
Agent includes following component and its weight portion：Garlic 42-53 parts, shallot 20-30 parts, balsam pear 40-50 parts, ginger 35-45 parts, castor-oil plant
10-20 parts, matrine 5-10 parts, rotenone 4-8 parts, chilli oil 3-6 parts, 10-15 part of chinaberry of print, creeping dichondra herb 0.2-0.6 parts, it is imperial
0.4-0.8 parts of bone wind.
A kind of pure natural method for producing insecticide, it is characterised in that：Comprise the following steps：
1）Garlic, shallot, balsam pear, ginger, castor-oil plant, print chinaberry, creeping dichondra herb, keel are weighed by the weight portion in insecticidal formulation
Wind, cleaning, dry, pulverize to 210-240 mesh, obtain mixed-powder；
2）In the ethanol of middle addition 75-86%, stirring, immersion, refluxing extraction 2-3 times merges to obtain leaching liquid；
3）Matrine, rotenone, chilli oil are added in gained leaching liquid, 2-4h is soaked in stirring, and filtering obtains filtrate；
4）Concentration filtrate, storage obtains insecticide.
Preferably, in step 1 drying mode be microwave drying, wherein shallot, balsam pear, castor-oil plant, print chinaberry, creeping dichondra herb,
The frequency of the microwave drying of keel wind is 2000-3000MHz, and drying time is 15-20min, the microwave drying of garlic and ginger
Frequency be 2500-3000MHz, drying time is 18-26min, and different dried process are carried out according to different compositions, is prevented
Effect of composition is damaged when drying, and certain bactericidal action is played when drying.
Preferably, it is 1.7-2.6 times of mixed-powder volume that ethanol volume is added in step 2, powder and ethanol are improved
Contact, improve powder solubility, increase composition extracting concentration, strengthen insecticide effect.
Preferably, soak time is 18-26h in step 2, the frequency that ultrasonic wave hydrotropy, ultrasonic wave is just used during immersion is
50000-80000Hz, solubility is improved using ultrasonic wave hydrotropy, strengthens effect of insecticide.
Preferably, agitating mode is to be stirred once every 5-7min in step 3,1-2min is stirred every time, improve kuh-seng
The solubility of alkali, rotenone, chilli oil in leaching liquor, improves insecticidal action, increases EDD.
Preferably, concentrating the 7-13% of filtrate to gained filtrate in step 4.
Preferably, stored manner dries lucifuge to be placed in light tight container in the environment of 15-23 DEG C in step 4,
Prevent insecticide from occurring rotten, influence effect of insecticide, increase use time.
Beneficial effect：This pure natural insecticide that the present invention is provided and preparation method thereof, it is convenient to prepare, composition during preparation
DNA purity is high, the effect of creeping dichondra herb and keel wind have desinsection, improves disinsection efficiency, increases EDD, environmental protection,
It is degradable, people and animals are safe from harm, creeping dichondra herb and keel wind can extend insecticidal properties by castor-oil plant, matrine, never increase
EDD, a kind of pure natural insecticide and preparation method thereof is provided present invention employs above-mentioned technical proposal, be compensate for existing
The deficiency of technology, it is reasonable in design, it is easy to operate.
Specific embodiment
Following examples are described in further detail：
Embodiment 1：
A kind of pure natural insecticide, the insecticide includes following component and its preferred weight part：53 parts of garlic, 30 parts of shallot,
50 parts of balsam pear, 45 parts of ginger, 20 parts of castor-oil plant, 10 parts of matrine, 8 parts of rotenone, 6 parts of chilli oil, 15 parts of chinaberry of print, creeping dichondra herb
0.6 part, 0.8 part of keel wind.
A kind of pure natural method for producing insecticide, it is characterised in that：Comprise the following steps：
1）Garlic, shallot, balsam pear, ginger, castor-oil plant, print chinaberry, creeping dichondra herb, keel are weighed by the weight portion in insecticidal formulation
Wind, cleaning, dry, pulverize to 240 mesh, obtain mixed-powder；
2）In the ethanol of middle addition 82%, stirring, immersion, refluxing extraction 3 times merges to obtain leaching liquid；
3）Matrine, rotenone, chilli oil are added in gained leaching liquid, 4h is soaked in stirring, and filtering obtains filtrate；
4）Concentration filtrate, storage obtains insecticide.
In step 1 drying mode be microwave drying, wherein shallot, balsam pear, castor-oil plant, print chinaberry, creeping dichondra herb, keel wind it is micro-
The dry frequency of ripple is 3000MHz, and drying time is 20min, and the frequency of the microwave drying of garlic and ginger is 2500MHz, is done
The dry time is 26min, and different dried process are carried out according to different compositions, effect of damage composition when preventing from drying, and
Certain bactericidal action is played when drying.
It is 1.7 times of mixed-powder volume that ethanol volume is added in step 2, improves contact of the powder with ethanol, improves powder
The solubility at end, increases the extracting concentration of composition, strengthens effect of insecticide.
Soak time is 24h in step 2, and ultrasonic wave hydrotropy is just used during immersion, and the frequency of ultrasonic wave is 50000-
80000Hz, solubility is improved using ultrasonic wave hydrotropy, strengthens effect of insecticide.
Agitating mode is to be stirred once every 5min in step 3, and 1min is stirred every time, improves matrine, rotenone, capsicum
Solubility of the oil in leaching liquor, improves insecticidal action, increases EDD.
Filtrate to the 11% of gained filtrate is concentrated in step 4.
Stored manner dries lucifuge to be placed in light tight container in the environment of 18 DEG C in step 4, prevents insecticide from sending out
Change matter, influences effect of insecticide, increases use time.
Embodiment 2：
A kind of pure natural insecticide, the weight portion of preferred component：50 parts of garlic, 27 parts of shallot, 45 parts of balsam pear, 40 parts of ginger, castor
15 parts of fiber crops, 10 parts of matrine, 6 parts of rotenone, 4 parts of chilli oil, 13 parts of chinaberry of print, 0.2 part of creeping dichondra herb, 0.7 part of keel wind, according to
Preparation method in embodiment 1 is prepared into pure natural insecticide, and 500 times are diluted respectively, desinsection reality is carried out to peach after 2000 times
Test, after the common insect pests of peach have aphid, red spider, Pseudaulacaspis pentagona, small heart-eating peach worm, oriental fruit months, the above-mentioned insect of selection（Often
Plant insect and choose 100）, it is separately added into the insecticide after dilution, the situation for charging to insect of discontinuity, as a result such as table one and table
Shown in two：
Table one dilutes desinsection result of the insecticide to peach common insect pests after 500 times
| Insect | Before dispenser（Head） | After 3h（Head） | After 12h（Head） | After 24h（Head） | After 48h（Head） | Killing rate（%） |
| Aphid | 100 | 92 | 21 | 4 | 0 | 0 |
| Red spider | 100 | 94 | 30 | 8 | 0 | 0 |
| Pseudaulacaspis pentagona | 100 | 100 | 27 | 7 | 0 | 0 |
| Small heart-eating peach worm | 100 | 93 | 24 | 3 | 0 | 0 |
| Oriental fruit months | 100 | 96 | 20 | 2 | 0 | 0 |
Table two dilutes desinsection result of the insecticide to peach common insect pests after 2000 times
| Insect | Before dispenser（Head） | After 3h（Head） | After 12h（Head） | After 24h（Head） | After 48h（Head） | Killing rate（%） |
| Aphid | 100 | 97 | 53 | 26 | 13 | 87 |
| Red spider | 100 | 94 | 57 | 37 | 16 | 84 |
| Pseudaulacaspis pentagona | 100 | 96 | 63 | 24 | 12 | 88 |
| Small heart-eating peach worm | 100 | 100 | 52 | 31 | 19 | 81 |
| Oriental fruit months | 100 | 98 | 61 | 27 | 10 | 90 |
Obtained by table one and table two, the insect after 500 times of pure natural desinsection dilution agent of the invention to peach has stronger desinsection to imitate
The fruit and duration is more long, the effect of insecticide has a declining tendency after 2000 times of dilution, but still plays certain insecticidal effect,
Thus prove that insecticide of the invention has stronger lethality to insect.
Specific embodiment described herein is only to explanation for example of the invention.The technical field of the invention
Technical staff can be made various modifications or supplement to described specific embodiment or be substituted using similar mode, but
Without departing from of the invention or surmount scope defined in appended claims.
Claims (8)
1. a kind of pure natural insecticide, it is characterised in that the insecticide includes following component and its weight portion：Garlic 42-53
Part, shallot 20-30 parts, balsam pear 40-50 parts, ginger 35-45 parts, castor-oil plant 10-20 parts, matrine 5-10 parts, rotenone 4-8 parts,
Chilli oil 3-6 parts, print 10-15 parts of chinaberry, creeping dichondra herb 0.2-0.6 parts, 0.4-0.8 parts of keel wind.
2. a kind of pure natural method for producing insecticide, it is characterised in that：Comprise the following steps：
1）Garlic, shallot, balsam pear, ginger, castor-oil plant, print chinaberry, creeping dichondra herb, keel are weighed by the weight portion in insecticidal formulation
Wind, cleaning, dry, pulverize to 210-240 mesh, obtain mixed-powder；
2）In the ethanol of middle addition 75-86%, stirring, immersion, refluxing extraction 2-3 times merges to obtain leaching liquid；
3）Matrine, rotenone, chilli oil are added in gained leaching liquid, 2-4h is soaked in stirring, and filtering obtains filtrate；
4）Concentration filtrate, storage obtains insecticide.
3. a kind of pure natural method for producing insecticide according to claim 2, it is characterised in that done in the step 1
Dry mode is microwave drying, and wherein shallot, balsam pear, castor-oil plant, print chinaberry, creeping dichondra herb, the frequency of the microwave drying of keel wind are
2000-3000MHz, drying time is 15-20min, and the frequency of the microwave drying of garlic and ginger is 2500-3000MHz, is dried
Time is 18-26min.
4. a kind of pure natural method for producing insecticide according to claim 2, it is characterised in that in the step 2 plus
It is 1.7-2.6 times of mixed-powder volume to enter ethanol volume.
5. a kind of pure natural method for producing insecticide according to claim 2, it is characterised in that soaked in the step 2
The bubble time is 18-26h, and ultrasonic wave hydrotropy is just used during immersion, and the frequency of ultrasonic wave is 50000-80000Hz.
6. a kind of pure natural method for producing insecticide according to claim 2, it is characterised in that stirred in the step 3
The mode of mixing is to be stirred once every 5-7min, and 1-2min is stirred every time.
7. a kind of pure natural method for producing insecticide according to claim 2, it is characterised in that dense in the step 4
Contracting filtrate to gained filtrate 7-13%.
8. a kind of pure natural method for producing insecticide according to claim 2, it is characterised in that stored up in the step 4
Tibetan mode dries lucifuge to be placed in light tight container in the environment of 15-23 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710048981.0A CN106857726A (en) | 2017-01-23 | 2017-01-23 | Pure natural insecticide and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710048981.0A CN106857726A (en) | 2017-01-23 | 2017-01-23 | Pure natural insecticide and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106857726A true CN106857726A (en) | 2017-06-20 |
Family
ID=59158667
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710048981.0A Pending CN106857726A (en) | 2017-01-23 | 2017-01-23 | Pure natural insecticide and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106857726A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107788044A (en) * | 2017-12-05 | 2018-03-13 | 徐州农丰生物化工有限公司 | A kind of Purely natural plant insecticide and preparation method thereof |
| CN108186746A (en) * | 2018-02-01 | 2018-06-22 | 芜湖市三山区绿色食品产业协会 | Drug for livestock body surface expelling parasite and preparation method thereof |
| CN108392527A (en) * | 2018-02-01 | 2018-08-14 | 芜湖市三山区绿色食品产业协会 | A kind of pest repellant and its production method suitable for livestock body surface |
| CN108402097A (en) * | 2018-02-01 | 2018-08-17 | 芜湖市三山区绿色食品产业协会 | A kind of insect-repelling method of domestic animal body surface |
| CN108403250A (en) * | 2018-02-01 | 2018-08-17 | 芜湖市三山区绿色食品产业协会 | Livestock body surface insect-repelling method |
| CN108684736A (en) * | 2018-04-28 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | Plant pesticide |
| CN108684733A (en) * | 2018-04-28 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of plant pesticide formula |
| CN109392966A (en) * | 2018-11-14 | 2019-03-01 | 合肥华盖生物科技有限公司 | A kind of green and environment-friendly pesticide and preparation method thereof for rice |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101731287A (en) * | 2009-12-09 | 2010-06-16 | 岳朝亮 | Purely natural plant insecticide |
| CN103461403A (en) * | 2013-08-30 | 2013-12-25 | 广东德利生物科技有限公司 | Natural plant pesticide and preparation method thereof |
| CN104644994A (en) * | 2015-03-10 | 2015-05-27 | 张秀春 | Sterilization and disinfection solution for clinical laboratory and preparation method thereof |
| CN105638772A (en) * | 2015-12-29 | 2016-06-08 | 张旭东 | Microorganism-containing green insecticide |
-
2017
- 2017-01-23 CN CN201710048981.0A patent/CN106857726A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101731287A (en) * | 2009-12-09 | 2010-06-16 | 岳朝亮 | Purely natural plant insecticide |
| CN103461403A (en) * | 2013-08-30 | 2013-12-25 | 广东德利生物科技有限公司 | Natural plant pesticide and preparation method thereof |
| CN104644994A (en) * | 2015-03-10 | 2015-05-27 | 张秀春 | Sterilization and disinfection solution for clinical laboratory and preparation method thereof |
| CN105638772A (en) * | 2015-12-29 | 2016-06-08 | 张旭东 | Microorganism-containing green insecticide |
Non-Patent Citations (5)
| Title |
|---|
| 国家食品药品监督管理总局执业药师资格认证中心组织编写: "《中药学专业知识（一）第七版》", 31 January 2016, 中国医药科技出版社 * |
| 江苏省植物研究所 等编: "《新华本草纲要（第三册）》", 31 December 1990, 上海科学技术出版社 * |
| 温辉梁 等编: "《生物化工产品生产技术》", 31 December 2004, 江西科学技术出版社 * |
| 肖永庆 等主编: "《中华医学百科全书-中医药学中药炮制学》", 30 November 2016, 中国协和医科大学出版社 * |
| 赵玉英等: "《天然药物化学》", 31 March 2012, 北京大学医学出版社 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107788044A (en) * | 2017-12-05 | 2018-03-13 | 徐州农丰生物化工有限公司 | A kind of Purely natural plant insecticide and preparation method thereof |
| CN108186746A (en) * | 2018-02-01 | 2018-06-22 | 芜湖市三山区绿色食品产业协会 | Drug for livestock body surface expelling parasite and preparation method thereof |
| CN108392527A (en) * | 2018-02-01 | 2018-08-14 | 芜湖市三山区绿色食品产业协会 | A kind of pest repellant and its production method suitable for livestock body surface |
| CN108402097A (en) * | 2018-02-01 | 2018-08-17 | 芜湖市三山区绿色食品产业协会 | A kind of insect-repelling method of domestic animal body surface |
| CN108403250A (en) * | 2018-02-01 | 2018-08-17 | 芜湖市三山区绿色食品产业协会 | Livestock body surface insect-repelling method |
| CN108684736A (en) * | 2018-04-28 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | Plant pesticide |
| CN108684733A (en) * | 2018-04-28 | 2018-10-23 | 芜湖扬展新材料科技服务有限公司 | A kind of plant pesticide formula |
| CN109392966A (en) * | 2018-11-14 | 2019-03-01 | 合肥华盖生物科技有限公司 | A kind of green and environment-friendly pesticide and preparation method thereof for rice |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106857726A (en) | Pure natural insecticide and preparation method thereof | |
| CN102805115B (en) | Plant-source natural fungicide for preventing and controlling botrytis cinerea and preparation method thereof | |
| CN105594765A (en) | Environment-friendly pesticide | |
| CN102805114A (en) | Botanical natural fungicide for fungus and preparation method thereof | |
| CN107279196A (en) | Plant source environment-friendly pesticide | |
| CN106386886A (en) | Environment-friendly pesticide for vegetables, melons and fruits and preparation method thereof | |
| CN107494713A (en) | A kind of vegetable and fruit antistaling agent and preparation method thereof | |
| CN107006543A (en) | It is a kind of for insect-proof agent of flower planting and preparation method thereof | |
| CN106490055A (en) | A kind of novel watermelon seed dressing | |
| CN107347407A (en) | A kind of cultural method of selenium-enriched high-calcium purple sweetpotato | |
| KR20080009798A (en) | Manufacturing method of oriental red pepper soy | |
| KR101994394B1 (en) | Composition for Malodor Removal of Animal Corpse and Manufacturing Method of thereof | |
| CN101843267A (en) | High-efficiency nontoxic insecticide and preparation method thereof | |
| CN106490056A (en) | A kind of safety and environmental protection wheat seed dressing agent | |
| CN107216218A (en) | A kind of straw mushroom plantation insect pest planting matrix and preparation method thereof | |
| CN103858944A (en) | Pyrethrum mosquito incense repellent and manufacturing method thereof | |
| CN103999883A (en) | Traditional Chinese medicinal preparation having advantages of environmental protection, no residual and long-acting sterilization desinsection, and preparation method thereof | |
| CN1545886A (en) | Chinese herbal medicine plant pesticide and preparation method thereof | |
| CN101755859A (en) | Traditional Chinese medicine composition for preventing parasite in water, preparation method and application thereof | |
| CN109169736A (en) | It is a kind of using peppermint and balsam pear as the pest repellant of substrate and preparation method, application | |
| KR102509566B1 (en) | Manufacturing method of microorganism using medical properties of a plant and obtained by fermentation of sulfur, and manufacturing method of insecticide, germicide and deodorizer using thereof | |
| CN105248481A (en) | Aphid control liquid for facility crops and preparation method thereof | |
| CN106187403A (en) | A kind of fermentation substrate of ornamental trees and shrubs large area field planting and preparation method thereof | |
| CN106008053A (en) | Salix babylonica culture substance improving soil adsorption capacity and preparation method thereof | |
| CN106417412A (en) | Biological bacterial killing agent for control of apple tree growth ring disease and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |