CN106831158A - Extend auxiliary agent of Plant leaf fertilizer lasting period and preparation method thereof - Google Patents
Extend auxiliary agent of Plant leaf fertilizer lasting period and preparation method thereof Download PDFInfo
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- CN106831158A CN106831158A CN201710116143.2A CN201710116143A CN106831158A CN 106831158 A CN106831158 A CN 106831158A CN 201710116143 A CN201710116143 A CN 201710116143A CN 106831158 A CN106831158 A CN 106831158A
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- parts
- auxiliary agent
- plant leaf
- lasting period
- fertilizer
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
Abstract
The present invention provides a kind of auxiliary agent for extending the Plant leaf fertilizer lasting period and preparation method thereof, and chemical fertilizer auxiliary agent is made up of following component and weight portion：24 parts of stalk, 12 parts of flyash, 13 parts of attapulgite, 12 parts of lignin, 5 10 parts of sodium metaphosphate, 13 parts of biochemical fulvic acid potassium, 2 10 parts of sodium pyrophosphate, 5 30 parts of aminopropyl triethoxysilane, 0.6 1 parts of photosynthesis promoter, present invention also offers the preparation method of auxiliary agent, auxiliary agent of the invention can improve adhesive ability of the foliar fertilizer on plant leaf surface, may additionally facilitate the photosynthesis of plant leaf surface and shorten plant growing cycle, reduction is flown away, leaching loss and volatilization loss, so as to reach the extension lasting period, improve plant recovery of nutrient purpose, main raw material(s) natural environmental-protective of the invention, secondary pollution will not be introduced；Fertilising consumption and number of times are reduced simultaneously, labour and cost is saved, and reduce environmental pollution.
Description
Technical field
The invention belongs to chemical fertilizer auxiliary agent technical field, and in particular to a kind of chemical fertilizer auxiliary agent of extension foliar fertilizer lasting period and its
Preparation method.
Background technology
In the last few years, the production and application of foliar fertilizer are taken much count of both at home and abroad.The commercialization of Chinese foliar fertilizer be from
What the 1980s started, by the development of more than 20 years, the production of foliar fertilizer obtained huge development, from single
Composition develops into composite parts, and trace element and beneficial element are developed into from macronutrient, has been developed into from inorganic nutrients
Machine nutrient, addition plant growth regulator is developed into from mineral nutrient, and foliar fertilizer item are various, and species is various, multifarious,
The whole country there are about as many as thousands of kinds.
However, because technique and technology be not still very ripe, foliar fertilizer adhesive ability on plant leaf surface is not enough, sprays
To plant surface nutriment easily wind, drench with rain, fly away in the presence of Exposure to Sunlight, leaching loss and volatilization, cause fertilizer loss
Seriously, the lasting period is short, utilization rate is low, it is necessary to apply repeatedly, has both wasted a large amount of human and material resources and financial resources, causes environment dirty again
Dye.So, one of foliar fertilizer industry development direction be exactly improve blade face adhesive ability and extension the lasting period, but at present on
The technology of this respect is rarely reported.This patent provides a kind of raising foliar fertilizer adhesive ability for the problem, extends the lasting period
Technology.Be fixed on foliar fertilizer nutrient on blade face using the micro-nano structure of natural inorganic nano material mainly by the technology, is subtracted
Volatilization that few its is flown away, woods is become estranged, so as to extend the lasting period, meets industry development direction, with larger market potential.
Prior art such as, Chinese invention granted patent document, the B of Authorization Notice No. CN 103145494, the mesh of the invention
Be to provide a kind of new foliar fertilizer auxiliary agent, by the natural nano-material such as power plant straw ash compound carried out physical modification and
Chemical modification, increases its surface hydroxyl quantity, dispersive property and absorption property, and blade face fertilizer nutrient is preferably adsorbed in auxiliary agent material
In the micro-nano structure of material, and fixed by coarse plant leaf surface, so as to reach the energy of attachment for improving foliar fertilizer on plant leaf surface
Power, reduction is flown away, leaching loss and volatilization loss, so as to reach the extension lasting period, improve plant recovery of nutrient purpose, the invention it is main
Raw material natural environmental-protective, will not introduce secondary pollution；Fertilising consumption and number of times are reduced simultaneously, labour and cost is saved, and reduce ring
Border is polluted, and the technology meets foliar fertilizer developing direction, with larger market potential, but water holding capacity of the auxiliary agent on leaf
Also there is certain room for promotion with the promotion photosynthetic effect in blade face.
The content of the invention
It is an object of the invention to provide a kind of auxiliary agent for extending the Plant leaf fertilizer lasting period and preparation method thereof, auxiliary agent can make
Blade face fertilizer nutrient is preferably adsorbed in promoter material micro-nano structure, and is fixed by coarse plant leaf surface, reaches raising blade face
Adhesive ability of the fertilizer on plant leaf surface, reduces and is lost in, and extends the fertilizer lasting period, and auxiliary agent also has certain promotion plant
The effect of photosynthesis, growth promotion and water conservation.
It is for above-mentioned purpose the technical solution used in the present invention：Extend the chemical fertilizer auxiliary agent of Plant leaf fertilizer lasting period,
Chemical fertilizer auxiliary agent is made up of following component and weight portion：Stalk 2-4 parts, flyash 1-2 parts, attapulgite 1-3 parts, lignin 1-2
Part, sodium metaphosphate 5-10 parts, 1-3 parts of biochemical fulvic acid potassium, sodium pyrophosphate 2-10 parts, aminopropyl triethoxysilane 5-30 parts,
Photosynthesis promoter 0.6-1 parts.
Preferably, photosynthesis promoter is made up of following component and weight portion：5- amino-laevulic acids and its salt
0.5-10 parts, triacontanol 0.05-1 parts, clostridium butyricum 0.5-1 parts, potash fertilizer 70-95 parts, cyclodextrin 1-10 parts, dimethyl-β-
DMPT 0.1-0.5 parts, sodium carboxymethyl starch 0.2-0.4 parts, moistening 0.5-5 parts of spreader-sticker, uv-protection agent 0.1-5
Part, uv-protection agent is one or more in sodium lignin sulfonate, p-aminobenzoic acid, sorbierite, moistens spreader-sticker bag
Include modified three silicon of anhydrous sorbitol APEO fatty acid ester, lauryl sodium sulfate, neopelex, ethyoxyl
One or more in oxygen alkane, add after photosynthesis promoter can make promoter effect plant surface in this auxiliary agent and lift plant
Photosynthetic efficiency, dimethyl-β-DMPT and sodium carboxymethyl starch can also lift the cold-resistant of plant by triacontanol
Performance, may additionally facilitate plant growth and water retention property.
Extend the auxiliary agent preparation method of Plant leaf fertilizer lasting period, comprise the following steps：
1）By weight, take stalk, flyash, attapulgite and lignin it is well mixed after add 5-10 times of volume water and
Lytic agent, stirs 30min, and complex liquid is obtained；
2）Use 5-10 MeV, the high-energy electron beam irradiation complex liquid of 10-50 kGy 5-10 minutes；
3）It is passed through ozone 10-30 minutes to the suspension after irradiation using ozone generator, 10- is utilized while being passed through ozone
The uv light irradiation of 30W；
4）50-60 DEG C of aminopropyl triethoxysilane is added in complex liquid, 20-60min is stood after ultrasonic oscillation treatment,
Centrifuging and taking supernatant and residue, respectively dry supernatant and residue, mix after crushing respectively；
5）The powder of mixing is well mixed with sodium metaphosphate, biochemical fulvic acid potassium, sodium pyrophosphate and photosynthesis promoter, is obtained
Extend the auxiliary agent of Plant leaf fertilizer lasting period.
Preferably, lytic agent is made up of following component and weight portion in step 1：Sodium citrate 3-7 parts, sodium chloride 5-9
Part, magnesium sulfate 8-12 parts, p-aminobenzoic acid 2-4 parts, 4-AA 1-5 parts, disodium hydrogen phosphate 3-7 parts, di(2-ethylhexyl)phosphate
1-5 parts of hydrogen potassium.
Preferably, the lytic agent addition in step 1 is stalk, flyash, attapulgite and lignin gross weight
0.5-3%。
Compared with prior art, useful achievement of the invention is：Main raw material(s) natural environmental-protective, will not introduce secondary dirt
Dye；Effectively enhancing foliar fertilizer in the adhesive ability of plant surface, fly away, leaching loss and volatilization loss, extends the lasting period, improves by reduction
Plant recovery of nutrient；The photosynthesis that plant is lifted after photosynthesis promoter can make promoter effect plant surface is added in auxiliary agent
Efficiency, can also lift the cold tolerance of plant, may additionally facilitate plant growth and water retention property, by stalk, flyash, attapulgite
Fully decomposite to come with the protein in lignin, the nutritional ingredient of raising auxiliary agent, more conducively plant absorption delay fertilizer loss
Speed, improves utilization rate of fertilizer, reduces fertilising consumption and number of times, saves labour and cost, reduces environmental pollution.
Specific embodiment
It is described in further detail with reference to embodiments：
Embodiment 1：
Extend the chemical fertilizer auxiliary agent of Plant leaf fertilizer lasting period, chemical fertilizer auxiliary agent is made up of following component and weight portion：3 parts of stalk, powder
1.5 parts of coal ash, 2 parts of attapulgite, 1.2 parts of lignin, 6 parts of sodium metaphosphate, 2 parts of biochemical fulvic acid potassium, 8 parts of sodium pyrophosphate, ammonia
22 parts of propyl-triethoxysilicane, 0.8 part of photosynthesis promoter.
Photosynthesis promoter is made up of following component and weight portion：5- amino-laevulic acids and its 3 parts of salt, melissane
0.3 part of alcohol, 0.6 part of clostridium butyricum, 82 parts of potash fertilizer, 8 parts of cyclodextrin, 0.4 part of dimethyl-β-DMPT, sodium carboxymethyl starch
0.3 part, moistening 1 part of spreader-sticker, 4 parts of uv-protection agent, uv-protection agent be p-aminobenzoic acid, moistening spreader-sticker for lose
Water sorbitol polyoxyethylene ether fatty acid ester, above experimental data is in non-linear, and its mechanism of action is still to be tested.
Extend the auxiliary agent preparation method of Plant leaf fertilizer lasting period, comprise the following steps：
1）By weight, take stalk, flyash, attapulgite and lignin it is well mixed after add the water of 8 times of volumes and molten
Solution agent, lytic agent addition is the 2% of stalk, flyash, attapulgite and lignin gross weight, stirs 30min, is obtained compound
Liquid；
2）Use 5-10 MeV, the high-energy electron beam irradiation complex liquid of 10-50 kGy 8 minutes；
3）It is passed through ozone 10-30 minutes to the suspension after irradiation using ozone generator, using 20W's while being passed through ozone
Uv light irradiation；
4）55 DEG C of aminopropyl triethoxysilane is added in complex liquid, 35min, centrifuging and taking are stood after ultrasonic oscillation treatment
Supernatant and residue, respectively dry supernatant and residue, mix after crushing respectively；
5）The powder of mixing is well mixed with sodium metaphosphate, biochemical fulvic acid potassium, sodium pyrophosphate and photosynthesis promoter, is obtained
Extend the auxiliary agent of Plant leaf fertilizer lasting period.
Lytic agent is made up of following component and weight portion in step 1：4 parts of sodium citrate, 6 parts of sodium chloride, 11 parts of magnesium sulfate,
3 parts of p-aminobenzoic acid, 3 parts of 4-AA, 4 parts of disodium hydrogen phosphate, 4 parts of potassium dihydrogen phosphate.
Embodiment 2：
Extend the chemical fertilizer auxiliary agent of Plant leaf fertilizer lasting period, chemical fertilizer auxiliary agent is made up of following component and weight portion：3 parts of stalk, powder
1 part of coal ash, 1 part of attapulgite, 2 parts of lignin, 6 parts of sodium metaphosphate, 1 part of biochemical fulvic acid potassium, 7 parts of sodium pyrophosphate, aminopropyl
14 parts of triethoxysilane, 1 part of photosynthesis promoter.
Photosynthesis promoter is made up of following component and weight portion：5- amino-laevulic acids and its 2 parts of salt, melissane
0.3 part of alcohol, 0.7 part of clostridium butyricum, 80 parts of potash fertilizer, 2 parts of cyclodextrin, 0.2 part of dimethyl-β-DMPT, sodium carboxymethyl starch
0.28 part, 1 part of spreader-sticker of moistening, 2 parts of uv-protection agent, uv-protection agent is that p-aminobenzoic acid and sorbierite mix
Thing, moistening spreader-sticker is lauryl sodium sulfate.
Extend the auxiliary agent preparation method of Plant leaf fertilizer lasting period, comprise the following steps：
1）By weight, take stalk, flyash, attapulgite and lignin it is well mixed after add the water of 7 times of volumes and molten
Solution agent, lytic agent addition is the 1% of stalk, flyash, attapulgite and lignin gross weight, stirs 30min, is obtained compound
Liquid；
2）Use 5-10 MeV, the high-energy electron beam irradiation complex liquid of 10-50 kGy 8 minutes；
3）It is passed through ozone 10-30 minutes to the suspension after irradiation using ozone generator, using 25W's while being passed through ozone
Uv light irradiation；
4）50-60 DEG C of aminopropyl triethoxysilane is added in complex liquid, 40min is stood after ultrasonic oscillation treatment, from
The heart takes supernatant and residue, respectively dries supernatant and residue, mixes after crushing respectively；
5）The powder of mixing is well mixed with sodium metaphosphate, biochemical fulvic acid potassium, sodium pyrophosphate and photosynthesis promoter, is obtained
Extend the auxiliary agent of Plant leaf fertilizer lasting period.
Lytic agent is made up of following component and weight portion in step 1：3 parts of sodium citrate, 6 parts of sodium chloride, 9 parts of magnesium sulfate,
2 parts of p-aminobenzoic acid, 2 parts of 4-AA, 3 parts of disodium hydrogen phosphate, 2 parts of potassium dihydrogen phosphate.
In the prior art of the routine techniques dawn known to those skilled in the art in above-described embodiment, for example, high energy electron
The prior arts such as beam irradiation, ultrasonic oscillation treatment, therefore in this not go into detail.
Embodiment of above is merely to illustrate the present invention, and not limitation of the present invention, the ordinary skill people of this area
Member, without departing from the spirit and scope of the present invention, can also make a variety of changes and modification, therefore, it is all equivalent
Technical scheme fall within scope of the invention, scope of patent protection of the invention should be defined by the claims.
Claims (5)
1. the chemical fertilizer auxiliary agent of Plant leaf fertilizer lasting period is extended, it is characterised in that：The chemical fertilizer auxiliary agent is by following component and weight
Part composition：Stalk 2-4 parts, flyash 1-2 parts, attapulgite 1-3 parts, lignin 1-2 parts, sodium metaphosphate 5-10 parts, biochemical Huang
Rotten 1-3 parts, sodium pyrophosphate 2-10 parts, aminopropyl triethoxysilane 5-30 parts, photosynthesis promoter 0.6-1 parts of potassium of acid.
2. it is according to claim 1 extension the Plant leaf fertilizer lasting period chemical fertilizer auxiliary agent, it is characterised in that：The light cooperation
It is made up of following component and weight portion with accelerator：5- amino-laevulic acids and its salt 0.5-10 parts, triacontanol 0.05-1
Part, clostridium butyricum 0.5-1 parts, potash fertilizer 70-95 parts, cyclodextrin 1-10 parts, dimethyl-β-DMPT 0.1-0.5 parts, carboxymethyl
Sodium starch 0.2-0.4 parts, moistening 0.5-5 part of spreader-sticker, 0.1-5 parts of uv-protection agent, the uv-protection agent be it is wooden
One or more in plain sodium sulfonate, p-aminobenzoic acid, sorbierite.
3. the auxiliary agent preparation method of Plant leaf fertilizer lasting period is extended, it is characterised in that：Comprise the following steps：
1）By weight, take stalk, flyash, attapulgite and lignin it is well mixed after add 5-10 times of volume water and
Lytic agent, stirs 30min, and complex liquid is obtained；
2）Use 5-10 MeV, the high-energy electron beam irradiation complex liquid of 10-50 kGy 5-10 minutes；
3）It is passed through ozone 10-30 minutes to the suspension after irradiation using ozone generator, 10- is utilized while being passed through ozone
The uv light irradiation of 30W；
4）50-60 DEG C of aminopropyl triethoxysilane is added in complex liquid, 20-60min is stood after ultrasonic oscillation treatment,
Centrifuging and taking supernatant and residue, respectively dry supernatant and residue, mix after crushing respectively；
5）The powder of mixing is well mixed with sodium metaphosphate, biochemical fulvic acid potassium, sodium pyrophosphate and photosynthesis promoter, is obtained
Extend the auxiliary agent of Plant leaf fertilizer lasting period.
4. it is according to claim 3 extension the Plant leaf fertilizer lasting period auxiliary agent preparation method, it is characterised in that：The step
Lytic agent is made up of following component and weight portion in rapid 1：Sodium citrate 3-7 parts, sodium chloride 5-9 parts, magnesium sulfate 8-12 parts, to ammonia
Yl benzoic acid 2-4 parts, 4-AA 1-5 parts, disodium hydrogen phosphate 3-7 parts, potassium dihydrogen phosphate 1-5 parts.
5. it is according to claim 3 extension the Plant leaf fertilizer lasting period auxiliary agent preparation method, it is characterised in that：The step
Lytic agent addition in rapid 1 is the 0.5-3% of stalk, flyash, attapulgite and lignin gross weight.
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| CN201710116143.2A CN106831158A (en) | 2017-03-01 | 2017-03-01 | Extend auxiliary agent of Plant leaf fertilizer lasting period and preparation method thereof |
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| CN201710116143.2A CN106831158A (en) | 2017-03-01 | 2017-03-01 | Extend auxiliary agent of Plant leaf fertilizer lasting period and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108911897A (en) * | 2018-09-20 | 2018-11-30 | 赵建平 | A kind of nutrient solution for soilless pot culture and preparation method thereof |
| CN111825492A (en) * | 2019-04-15 | 2020-10-27 | 中国科学院微生物研究所 | Water-soluble fertilizer synergistic additive and preparation method thereof |
| CN112142513A (en) * | 2020-09-27 | 2020-12-29 | 陕西科技大学 | Chelated foliar fertilizer for vegetables and preparation method and application thereof |
| CN113773137A (en) * | 2021-09-07 | 2021-12-10 | 山东农大肥业科技有限公司 | Universal low-temperature-resistant liquid fertilizer and preparation method thereof |
| CN114073252A (en) * | 2020-08-12 | 2022-02-22 | 中国热带农业科学院环境与植物保护研究所 | Litchi spreading agent and preparation method thereof |
| WO2023106413A1 (en) * | 2021-12-10 | 2023-06-15 | ネオファーマジャパン株式会社 | Stabilized 5-aminolevulinic acid composition |
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| CN101234918A (en) * | 2008-02-29 | 2008-08-06 | 师进 | High-activity biological moisture-keeping multifunctional foliage fertilizer and preparation method thereof |
| CN101913951A (en) * | 2010-08-26 | 2010-12-15 | 中国科学院遗传与发育生物学研究所 | Plant photosynthesis promoter and preparation method thereof |
| CN102503739A (en) * | 2011-11-04 | 2012-06-20 | 广西田园生化股份有限公司 | Compound fertilizer of toxic fluorine-phosphorus and foliage fertilizer |
| CN103145494A (en) * | 2013-02-27 | 2013-06-12 | 中国科学院合肥物质科学研究院 | Production method of chemical fertilizer accessory ingredient for prolonging leaf fertilizer lasting period |
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2017
- 2017-03-01 CN CN201710116143.2A patent/CN106831158A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101234918A (en) * | 2008-02-29 | 2008-08-06 | 师进 | High-activity biological moisture-keeping multifunctional foliage fertilizer and preparation method thereof |
| CN101913951A (en) * | 2010-08-26 | 2010-12-15 | 中国科学院遗传与发育生物学研究所 | Plant photosynthesis promoter and preparation method thereof |
| CN102503739A (en) * | 2011-11-04 | 2012-06-20 | 广西田园生化股份有限公司 | Compound fertilizer of toxic fluorine-phosphorus and foliage fertilizer |
| CN103145494A (en) * | 2013-02-27 | 2013-06-12 | 中国科学院合肥物质科学研究院 | Production method of chemical fertilizer accessory ingredient for prolonging leaf fertilizer lasting period |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108911897A (en) * | 2018-09-20 | 2018-11-30 | 赵建平 | A kind of nutrient solution for soilless pot culture and preparation method thereof |
| CN111825492A (en) * | 2019-04-15 | 2020-10-27 | 中国科学院微生物研究所 | Water-soluble fertilizer synergistic additive and preparation method thereof |
| CN114073252A (en) * | 2020-08-12 | 2022-02-22 | 中国热带农业科学院环境与植物保护研究所 | Litchi spreading agent and preparation method thereof |
| CN114073252B (en) * | 2020-08-12 | 2022-11-08 | 中国热带农业科学院环境与植物保护研究所 | Litchi spreading agent and preparation method thereof |
| CN112142513A (en) * | 2020-09-27 | 2020-12-29 | 陕西科技大学 | Chelated foliar fertilizer for vegetables and preparation method and application thereof |
| CN113773137A (en) * | 2021-09-07 | 2021-12-10 | 山东农大肥业科技有限公司 | Universal low-temperature-resistant liquid fertilizer and preparation method thereof |
| WO2023106413A1 (en) * | 2021-12-10 | 2023-06-15 | ネオファーマジャパン株式会社 | Stabilized 5-aminolevulinic acid composition |
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