CN106822316A - A kind of invigorate blood circulation smokeless moxibustion bar and preparation method thereof - Google Patents
A kind of invigorate blood circulation smokeless moxibustion bar and preparation method thereof Download PDFInfo
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Abstract
The present invention relates to a kind of invigorate blood circulation smokeless moxibustion bar and preparation method thereof, according to weight ratio, the preparing raw material of described Moxibustion strip is made up of 1,000 1100 portions of folium artemisiae argyis, 40 60 parts of Radix Angelicae Sinensis, 30 50 portions of evodia rutaecarpas and 1 10 parts of Ligusticum wallichiis；Invigorate blood circulation smokeless moxibustion bar of the present invention and preparation method thereof can effectively treat closed dysmenorrhea by adding Radix Angelicae Sinensis, evodia rutaecarpa and Ligusticum wallichii, asthenia cold abdominalgia, arthralgia pain due to rheumatism, moxa-moxibustion is convenient, other drugs need not be aided in can reach the effect of invigorate blood circulation, alleviate the medication pain of patient, it is easy to use, save expense, it is adaptable to the patient of all age group.
Description
Technical field
The invention belongs to Chinese medicine preparation field, specially a kind of invigorate blood circulation smokeless moxibustion bar and preparation method thereof.
Background technology
Moxa-moxibustion originates from ancient Chinese as one of main treatment means of the traditional Chinese medical science, is the moxa-moxibustion material being made of folium artemisiae argyi
The Ai heat of generation stimulates body surface point or specific position, by exciting the vein active physiology to adjust human disorder of ventilation
Biochemical function, play promoting qi circulation and removing obstruction in the collateral, supporting YANG to cure collaps-syndrome as emergency treatment, it is promoting blood circulation and removing blood stasis, draw out pus by applying a plaster to the affected part expel the heat-evil, macrobiosis beauty the effects such as, so as to reach diseases prevention
The purpose cured the disease.
But conventional moxa-moxibustion is in the preparation, is just processed using Chen Aiye more, because containing substantial amounts of folium artemisiae argyi in raw tarragon
Oil, vigor is swift and violent during burning, and heating power is not persistently thorough enough, and it produces substantial amounts of volatile materials and Chinese mugwort tar in burning,
These materials are sucked for a long time and easily suffers from tuberculosis, pollute Curing circumstance, be unfavorable for health, thus it is many using Chen Ai treatment,
Blumea oil in the middle of Chen Ai is effectively volatilized so that the Moxibustion strip made can persistently burn and vigor is gentle, but Chen Ai
Standing time is long, leverages the fabrication cycle of Moxibustion strip, is unfavorable for a large amount of productions of Moxibustion strip.Though folium artemisiae argyi is used now
It is carbonized to prepare smokeless moxibustion bar, but is relied solely on carbonization, the toxicity of folium artemisiae argyi can not be completely eliminated, is worked as during moxa-moxibustion and lean on
The effect of folium artemisiae argyi is treated, and curative effect is general, in addition it is also necessary to which the other medicines of auxiliary could play a role well, increase patient
Pain, increase expense, therefore need badly and a kind of can merge other drugs curative effect and Moxibustion strip with short production cycle.
The content of the invention
In order to solve that the Moxibustion strip production cycle is long, curative effect general, burning when smog weight, pollute environment, therapeutic process is more
Painful and costly etc. the problems such as, the purpose of the present invention is to propose to a kind of invigorate blood circulation Moxibustion strip and preparation method thereof, the work
The blood smokeless moxibustion bar that stimulates the menstrual flow can effectively treat closed dysmenorrhea, and asthenia cold abdominalgia, arthralgia pain due to rheumatism, moxa-moxibustion is convenient, without aiding in it
His medicine is the effect that can reach invigorate blood circulation, alleviates the medication pain of patient, easy to use, saves expense, it is adaptable to
The patient of all age group.
The technical scheme is that：A kind of invigorate blood circulation smokeless moxibustion bar, according to weight ratio, the system of described Moxibustion strip
Standby raw material is made up of 1000-1100 portions of folium artemisiae argyi, 40-60 parts of Radix Angelicae Sinensis, 30-50 portions of evodia rutaecarpa and 1-10 parts of Ligusticum wallichii；
A kind of preparation method of invigorate blood circulation smokeless moxibustion bar, described Moxibustion strip successively through getting the raw materials ready, it is folium artemisiae argyi vinegar carbonization treatment, super
Critical CO2 extractions, extraction process, leaching filter dry and it is compressing can be prepared by, concrete operations are：Aforementioned proportion is first according to claim
Each material is taken, folium artemisiae argyi is carried out into vinegar carbonization treatment, Radix Angelicae Sinensis and Ligusticum wallichii are then carried out into SCF-CO 2, then evodia rutaecarpa is entered
Row extract, afterwards vinegar carbonization folium artemisiae argyi leaching filter in the mixed liquor of extract and extract solution, then after freeze-drying it is compressing i.e.
The invigorate blood circulation smokeless moxibustion bar can be obtained；Described vinegar carbonization treatment refers to immerse folium artemisiae argyi weight after folium artemisiae argyi is cleaned into dries pulverizing
Mixed in the jujube vinegar of 3-4 times of amount and stand 2-3h, dried in pot afterwards, then the uniform jujube vinegar for spraying 1-2 times of folium artemisiae argyi weight
Dried in pot afterwards, being dried in pot after the jujube vinegar of uniform 1-2 times of spray folium artemisiae argyi weight again must contain vinegar folium artemisiae argyi afterwards, then will
Folium artemisiae argyi is positioned in carbonization kettle to be carbonized at 500-600 DEG C and 5-6h and crushes to obtain vinegar carbon Chinese mugwort；
Described jujube vinegar is prepared from by jujube through stoning, dries pulverizing, boiling, fermentation, and concrete operations are：First by jujube
Stoning drying is cleaned, red date powder is then crushed to obtain, the water boiling 1-2h for adding 3-5 times of red date powder weight obtains jujube juice, then
It is cooled to after 35-40 DEG C and adds the yeast of jujube juice weight 1-5% and the distiller's yeast of 5-8% to mix, adjusting the temperature to 17-18 DEG C is carried out
One time fermentation 12-14h, then heat to 28-30 DEG C fermentation 6-8 days after filter can be prepared by jujube vinegar；
Described supercritical CO2Extraction refers to the mixed-powder cleaned Ligusticum wallichii and Radix Angelicae Sinensis dry and be ground into 40-60 mesh first,
Then the ethanol for being added thereto to 3-4 times of mixed-powder carries out supercritical CO as entrainer2Extraction 2-3h obtains extract；It is described
Supercritical CO2The extracting pressure of extraction is 40-45MPa, and extraction temperature is 50-55 DEG C, and parsing pressure is 6-8MPa, parsing temperature
It is 40-45 DEG C to spend, CO2Flow be 20-30L/h；It refers to clean evodia rutaecarpa to dry and be crushed to that described evodia rutaecarpa is extracted
40-60 mesh, be subsequently adding the water of 8-10 times of evodia rutaecarpa weight carry out decoct 1-2h obtain extract solution I and residue I, then to residue I
The water of middle 8-10 times of addition residue I weight carries out decoction 1-2h and obtains extract solution II, merges extract solution I and extract solution II obtains mixed liquor
And be concentrated into the 10% of mixed liquor and obtain extract solution III；
Described leaching drying process of filtering refers to, first by extract and the mixing of extract solution III, vinegar carbon Chinese mugwort to be immersed in into mixed liquor afterwards
Middle 3-5h, carries out freeze-drying afterwards, finally compressing to can be prepared by the invigorate blood circulation smokeless moxibustion bar.
Beneficial effects of the present invention：
1st, invigorate blood circulation smokeless moxibustion bar of the present invention and preparation method thereof, for the closed dysmenorrhea that a variety of causes causes,
Asthenia cold abdominalgia, arthralgia pain due to rheumatism is taken effect rapid, wherein Chinese mugwort vinegar charcoal has eliminating cold to stop pain, clearing and activating the channels and collaterals effect, Radix Angelicae Sinensis has to be mended
Blood, the effect invigorated blood circulation, stimulate the menstrual flow, evodia rutaecarpa have eliminating cold to stop pain, and there is stopping nausea and vomiting by lowering the adverse flow of QI, the effect of supporing yang antidiarrheal, Ligusticum wallichii promoting blood circulation to go
The effect of gas, wind-expelling pain-stopping, moxa-moxibustion two to three days can alleviate asthenia cold abdominalgia, can recover after one week according to state of an illness moxa-moxibustion, consolidate
Gu moxa-moxibustion can fully recover after two weeks, and effect is significant is rapid, it is adaptable to the patient of all age group, easy to use, alleviates disease
The pain of people's medication, while being easy to mass production to promote；
2nd, Moxibustion strip of the present invention carries out vinegar carbonization treatment by folium artemisiae argyi, and folium artemisiae argyi is processed using jujube vinegar,
The technique such as filter, spray and bakee with reference to leaching, the composition in jujube vinegar is fully infiltrated into folium artemisiae argyi, by after carbonization, subtracting significantly
The smoke generation of Moxibustion strip is lacked, the content of Blumea oil greatly reduces, and effectively reduces the toxicity of folium artemisiae argyi, improves treatment ring
Border, and jujube vinegar shares also tonifying Qi and blood with Radix Angelicae Sinensis, Ligusticum wallichii and evodia rutaecarpa, clearing and activating the channels and collaterals effect is increased promoting blood circulation and removing obstruction in channels
Effect；
3rd, the present invention is extracted by by Ligusticum wallichii and Radix Angelicae Sinensis using SCF-CO 2 method, and with ethanol as entrainer,
Extraction effect is good, and leaching is filtered in vinegar charcoal Chinese mugwort after mixing with the extract solution of evodia rutaecarpa, using the method for freeze-drying, reduces medicine
In active ingredient scatter and disappear, this several drugs and moxa are shared, then be aided with appropriate Moxibustion on Acupoints, invigorate blood circulation effect
It is good.
Specific embodiment
With reference to specific examples below, the present invention is described in further detail, and protection scope of the present invention is not limited to
In following examples.Implement process of the invention, condition, reagent, experimental technique etc., in addition to the following special content for referring to,
The universal knowledege and common knowledge of this area are, the present invention is not particularly limited content.
A kind of invigorate blood circulation smokeless moxibustion bar, according to weight ratio, the preparing raw material of described Moxibustion strip is by 1000-1100 parts
Folium artemisiae argyi, 40-60 part Radix Angelicae Sinensis, 30-50 portions of evodia rutaecarpa and 1-10 parts of Ligusticum wallichii composition.
A kind of preparation method of invigorate blood circulation smokeless moxibustion bar, described Moxibustion strip is successively through getting the raw materials ready, at folium artemisiae argyi vinegar carbonization
Reason, SCF-CO 2, extraction process, leaching filter dry and it is compressing can be prepared by, concrete operations are：It is first according to above-mentioned
Ratio weighs each material, and folium artemisiae argyi is carried out into vinegar carbonization treatment, and Radix Angelicae Sinensis and Ligusticum wallichii then carried out into SCF-CO 2, then by Wu
The fruit of medicinal cornel is extracted, and the folium artemisiae argyi leaching of vinegar carbonization afterwards is filtered in the mixed liquor of extract and extract solution, then is suppressed after freeze-drying
Shaping can be prepared by the invigorate blood circulation smokeless moxibustion bar；Described vinegar carbonization treatment refers to be immersed after folium artemisiae argyi is cleaned into dries pulverizing
Mixed in the jujube vinegar of 3-4 times of folium artemisiae argyi weight and stand 2-3h, dried in pot afterwards, then uniform 1-2 times of spray folium artemisiae argyi weight
Dried in pot after jujube vinegar, being dried in pot after the jujube vinegar of uniform 1-2 times of spray folium artemisiae argyi weight again must contain vinegar folium artemisiae argyi afterwards,
Then folium artemisiae argyi is positioned in carbonization kettle and 5-6h is carbonized at 500-600 DEG C and vinegar carbon Chinese mugwort is crushed to obtain.
Described jujube vinegar is prepared from by jujube through stoning, dries pulverizing, boiling, fermentation, and concrete operations are：First will
Jujube cleans stoning drying, then crushes to obtain red date powder, and the water boiling 1-2h for adding 3-5 times of red date powder weight obtains jujube juice,
Then it is cooled to after 35-40 DEG C and adds the yeast of jujube juice weight 1-5% and the distiller's yeast of 5-8% to mix, adjusts the temperature to 17-18 DEG C
Carry out one time fermentation 12-14h, then heat to 28-30 DEG C fermentation 6-8 days after filter can be prepared by jujube vinegar.
Described supercritical CO2Extraction refers to the mixing cleaned Ligusticum wallichii and Radix Angelicae Sinensis dry and be ground into 40-60 mesh first
Powder, the ethanol for being then added thereto to 3-4 times of mixed-powder carries out supercritical CO as entrainer2Extraction 2-3h must be extracted
Liquid；Described supercritical CO2The extracting pressure of extraction is 40-45MPa, and extraction temperature is 50-55 DEG C, and parsing pressure is 6-
8MPa, resolution temperature is 40-45 DEG C, CO2Flow be 20-30L/h；It refers to clean evodia rutaecarpa to dry that described evodia rutaecarpa is extracted
Dry doubling is crushed to 40-60 mesh, be subsequently adding the water of 8-10 times of evodia rutaecarpa weight carry out decoct 1-2h obtain extract solution I and residue I, so
Add the water of 8-10 times of residue I weight to carry out decoction 1-2h in backward residue I and obtain extract solution II, merge extract solution I and extract solution
II mixed liquor and be concentrated into the 10% of mixed liquor and obtain extract solution III.
Described leaching drying process of filtering refers to, first by extract and the mixing of extract solution III, to be afterwards immersed in vinegar carbon Chinese mugwort mixed
3-5h in liquid is closed, freeze-drying is carried out afterwards, it is finally compressing to can be prepared by the invigorate blood circulation smokeless moxibustion bar.
The Chinese mugwort vinegar charcoal formed after described folium artemisiae argyi pretreatment, function with cure mainly qi and blood circulation promotion, by cold-dampness.For wind-cold-dampness arthralgia,
Ji Rou Acid fiber crops, joint limbs pain, coldness and pain in the epigastrium.
Described Radix Angelicae Sinensis, sweet, acrid, warm.Return liver, the heart, the spleen channel.Indication replenishing and activating blood, menstruction regulating and pain relieving relaxes bowel.
For blood deficiency chlorosis, dizziness palpitaition, irregular menstruation, closed dysmenorrhea, asthenia cold abdominalgia, arthralgia pain due to rheumatism, injury from falling down, ulcer sores,
Dry constipation of intestines.Prepared RADIX ANGELICAE SINENSIS with yellow rice wine invigorate blood circulation, for closed dysmenorrhea, arthralgia pain due to rheumatism, injury from falling down.
Described Ligusticum wallichii, pungent, temperature.Return liver, courage, pericardium channel.Indication blood-activating and qi-promoting, wind-expelling pain-stopping.For the obstruction of qi in the chest heart
Bitterly, chest side of body shouting pain, tumbling and swelling, irregular menstruation, closed dysmenorrhea , Disorder lump in the abdomen is suffered from abdominal pain, headache, arthralgia pain due to rheumatism is the good of regulating qi to disperse stagnation
Medicine.
Described evodia rutaecarpa, pungent, hardship, heat；It is slightly poisonous.Return liver, spleen, stomach, kidney channel.Indication eliminating cold to stop pain, drops inverse
Preventing or arresting vomiting, supporing yang antidiarrheal, for jueyin headache, cold hernia stomachache, the disturbance of lower legs due to pathogenic cold and dampness, dysmenorrhea, abdominal distention vomits acid regurgitation, just before dawn
Diarrhea.
Embodiment 1
A kind of invigorate blood circulation smokeless moxibustion bar, according to weight ratio, the preparing raw material of described Moxibustion strip by 1000 portions of folium artemisiae argyis, 40 parts
Radix Angelicae Sinensis, 30 portions of evodia rutaecarpas and 1 part of Ligusticum wallichii composition.
A kind of preparation method of invigorate blood circulation smokeless moxibustion bar, described Moxibustion strip is successively through getting the raw materials ready, at folium artemisiae argyi vinegar carbonization
Reason, SCF-CO 2, extraction process, leaching filter dry and it is compressing can be prepared by, concrete operations are：It is first according to above-mentioned
Ratio weighs each material, and folium artemisiae argyi is carried out into vinegar carbonization treatment, and Radix Angelicae Sinensis and Ligusticum wallichii then carried out into SCF-CO 2, then by Wu
The fruit of medicinal cornel is extracted, and the folium artemisiae argyi leaching of vinegar carbonization afterwards is filtered in the mixed liquor of extract and extract solution, then is suppressed after freeze-drying
Shaping can be prepared by the invigorate blood circulation smokeless moxibustion bar；Described vinegar carbonization treatment refers to be immersed after folium artemisiae argyi is cleaned into dries pulverizing
Mixed in the jujube vinegar of 3-4 times of folium artemisiae argyi weight and stand 2-3h, dried in pot afterwards, then uniform 1-2 times of spray folium artemisiae argyi weight
Dried in pot after jujube vinegar, being dried in pot after the jujube vinegar of uniform 1-2 times of spray folium artemisiae argyi weight again must contain vinegar folium artemisiae argyi afterwards,
Then folium artemisiae argyi is positioned in carbonization kettle and 5-6h is carbonized at 500-600 DEG C and vinegar carbon Chinese mugwort is crushed to obtain.
Described jujube vinegar is prepared from by jujube through stoning, dries pulverizing, boiling, fermentation, and concrete operations are：First will
Jujube cleans stoning drying, then crushes to obtain red date powder, and the water boiling 1-2h for adding 3-5 times of red date powder weight obtains jujube juice,
Then it is cooled to after 35-40 DEG C and adds the yeast of jujube juice weight 1-5% and the distiller's yeast of 5-8% to mix, adjusts the temperature to 17-18 DEG C
Carry out one time fermentation 12-14h, then heat to 28-30 DEG C fermentation 6-8 days after filter can be prepared by jujube vinegar.
Described supercritical CO2Extraction refers to the mixing cleaned Ligusticum wallichii and Radix Angelicae Sinensis dry and be ground into 40-60 mesh first
Powder, the ethanol for being then added thereto to 3-4 times of mixed-powder carries out supercritical CO as entrainer2Extraction 2-3h must be extracted
Liquid；Described supercritical CO2The extracting pressure of extraction is 40-45MPa, and extraction temperature is 50-55 DEG C, and parsing pressure is 6-
8MPa, resolution temperature is 40-45 DEG C, CO2Flow be 20-30L/h；It refers to clean evodia rutaecarpa to dry that described evodia rutaecarpa is extracted
Dry doubling is crushed to 40-60 mesh, be subsequently adding the water of 8-10 times of evodia rutaecarpa weight carry out decoct 1-2h obtain extract solution I and residue I, so
Add the water of 8-10 times of residue I weight to carry out decoction 1-2h in backward residue I and obtain extract solution II, merge extract solution I and extract solution
II mixed liquor and be concentrated into the 10% of mixed liquor and obtain extract solution III.
Described leaching drying process of filtering refers to, first by extract and the mixing of extract solution III, to be afterwards immersed in vinegar carbon Chinese mugwort mixed
3-5h in liquid is closed, freeze-drying is carried out afterwards, it is finally compressing to can be prepared by the invigorate blood circulation smokeless moxibustion bar.
Embodiment 2
A kind of invigorate blood circulation smokeless moxibustion bar, according to weight ratio, the preparing raw material of described Moxibustion strip by 1020 portions of folium artemisiae argyis, 45 parts
Radix Angelicae Sinensis, 40 portions of evodia rutaecarpas and 3 parts of Ligusticum wallichii compositions.
A kind of preparation method of invigorate blood circulation smokeless moxibustion bar, described Moxibustion strip is successively through getting the raw materials ready, at folium artemisiae argyi vinegar carbonization
Reason, SCF-CO 2, extraction process, leaching filter dry and it is compressing can be prepared by, concrete operations are：It is first according to above-mentioned
Ratio weighs each material, and folium artemisiae argyi is carried out into vinegar carbonization treatment, and Radix Angelicae Sinensis and Ligusticum wallichii then carried out into SCF-CO 2, then by Wu
The fruit of medicinal cornel is extracted, and the folium artemisiae argyi leaching of vinegar carbonization afterwards is filtered in the mixed liquor of extract and extract solution, then is suppressed after freeze-drying
Shaping can be prepared by the invigorate blood circulation smokeless moxibustion bar；Described vinegar carbonization treatment refers to be immersed after folium artemisiae argyi is cleaned into dries pulverizing
Mixed in the jujube vinegar of 3-4 times of folium artemisiae argyi weight and stand 2-3h, dried in pot afterwards, then uniform 1-2 times of spray folium artemisiae argyi weight
Dried in pot after jujube vinegar, being dried in pot after the jujube vinegar of uniform 1-2 times of spray folium artemisiae argyi weight again must contain vinegar folium artemisiae argyi afterwards,
Then folium artemisiae argyi is positioned in carbonization kettle and 5-6h is carbonized at 500-600 DEG C and vinegar carbon Chinese mugwort is crushed to obtain.
Described jujube vinegar is prepared from by jujube through stoning, dries pulverizing, boiling, fermentation, and concrete operations are：First will
Jujube cleans stoning drying, then crushes to obtain red date powder, and the water boiling 1-2h for adding 3-5 times of red date powder weight obtains jujube juice,
Then it is cooled to after 35-40 DEG C and adds the yeast of jujube juice weight 1-5% and the distiller's yeast of 5-8% to mix, adjusts the temperature to 17-18 DEG C
Carry out one time fermentation 12-14h, then heat to 28-30 DEG C fermentation 6-8 days after filter can be prepared by jujube vinegar.
Described supercritical CO2Extraction refers to the mixing cleaned Ligusticum wallichii and Radix Angelicae Sinensis dry and be ground into 40-60 mesh first
Powder, the ethanol for being then added thereto to 3-4 times of mixed-powder carries out supercritical CO as entrainer2Extraction 2-3h must be extracted
Liquid；Described supercritical CO2The extracting pressure of extraction is 40-45MPa, and extraction temperature is 50-55 DEG C, and parsing pressure is 6-
8MPa, resolution temperature is 40-45 DEG C, CO2Flow be 20-30L/h；It refers to clean evodia rutaecarpa to dry that described evodia rutaecarpa is extracted
Dry doubling is crushed to 40-60 mesh, be subsequently adding the water of 8-10 times of evodia rutaecarpa weight carry out decoct 1-2h obtain extract solution I and residue I, so
Add the water of 8-10 times of residue I weight to carry out decoction 1-2h in backward residue I and obtain extract solution II, merge extract solution I and extract solution
II mixed liquor and be concentrated into the 10% of mixed liquor and obtain extract solution III.
Described leaching drying process of filtering refers to, first by extract and the mixing of extract solution III, to be afterwards immersed in vinegar carbon Chinese mugwort mixed
3-5h in liquid is closed, freeze-drying is carried out afterwards, it is finally compressing to can be prepared by the invigorate blood circulation smokeless moxibustion bar.
Embodiment 3
A kind of invigorate blood circulation smokeless moxibustion bar, according to weight ratio, the preparing raw material of described Moxibustion strip by 1050 portions of folium artemisiae argyis, 50 parts
Radix Angelicae Sinensis, 35 portions of evodia rutaecarpas and 5 parts of Ligusticum wallichii compositions.
A kind of preparation method of invigorate blood circulation smokeless moxibustion bar, described Moxibustion strip is successively through getting the raw materials ready, at folium artemisiae argyi vinegar carbonization
Reason, SCF-CO 2, extraction process, leaching filter dry and it is compressing can be prepared by, concrete operations are：It is first according to above-mentioned
Ratio weighs each material, and folium artemisiae argyi is carried out into vinegar carbonization treatment, and Radix Angelicae Sinensis and Ligusticum wallichii then carried out into SCF-CO 2, then by Wu
The fruit of medicinal cornel is extracted, and the folium artemisiae argyi leaching of vinegar carbonization afterwards is filtered in the mixed liquor of extract and extract solution, then is suppressed after freeze-drying
Shaping can be prepared by the invigorate blood circulation smokeless moxibustion bar；Described vinegar carbonization treatment refers to be immersed after folium artemisiae argyi is cleaned into dries pulverizing
Mixed in the jujube vinegar of 3-4 times of folium artemisiae argyi weight and stand 2-3h, dried in pot afterwards, then uniform 1-2 times of spray folium artemisiae argyi weight
Dried in pot after jujube vinegar, being dried in pot after the jujube vinegar of uniform 1-2 times of spray folium artemisiae argyi weight again must contain vinegar folium artemisiae argyi afterwards,
Then folium artemisiae argyi is positioned in carbonization kettle and 5-6h is carbonized at 500-600 DEG C and vinegar carbon Chinese mugwort is crushed to obtain.
Described jujube vinegar is prepared from by jujube through stoning, dries pulverizing, boiling, fermentation, and concrete operations are：First will
Jujube cleans stoning drying, then crushes to obtain red date powder, and the water boiling 1-2h for adding 3-5 times of red date powder weight obtains jujube juice,
Then it is cooled to after 35-40 DEG C and adds the yeast of jujube juice weight 1-5% and the distiller's yeast of 5-8% to mix, adjusts the temperature to 17-18 DEG C
Carry out one time fermentation 12-14h, then heat to 28-30 DEG C fermentation 6-8 days after filter can be prepared by jujube vinegar.
Described supercritical CO2Extraction refers to the mixing cleaned Ligusticum wallichii and Radix Angelicae Sinensis dry and be ground into 40-60 mesh first
Powder, the ethanol for being then added thereto to 3-4 times of mixed-powder carries out supercritical CO as entrainer2Extraction 2-3h must be extracted
Liquid；Described supercritical CO2The extracting pressure of extraction is 40-45MPa, and extraction temperature is 50-55 DEG C, and parsing pressure is 6-
8MPa, resolution temperature is 40-45 DEG C, CO2Flow be 20-30L/h；It refers to clean evodia rutaecarpa to dry that described evodia rutaecarpa is extracted
Dry doubling is crushed to 40-60 mesh, be subsequently adding the water of 8-10 times of evodia rutaecarpa weight carry out decoct 1-2h obtain extract solution I and residue I, so
Add the water of 8-10 times of residue I weight to carry out decoction 1-2h in backward residue I and obtain extract solution II, merge extract solution I and extract solution
II mixed liquor and be concentrated into the 10% of mixed liquor and obtain extract solution III.
Described leaching drying process of filtering refers to, first by extract and the mixing of extract solution III, to be afterwards immersed in vinegar carbon Chinese mugwort mixed
3-5h in liquid is closed, freeze-drying is carried out afterwards, it is finally compressing to can be prepared by the invigorate blood circulation smokeless moxibustion bar.
Embodiment 4
A kind of invigorate blood circulation smokeless moxibustion bar, according to weight ratio, the preparing raw material of described Moxibustion strip by 1080 portions of folium artemisiae argyis, 60 parts
Radix Angelicae Sinensis, 30-50 portion of evodia rutaecarpa and 10 parts of Ligusticum wallichii compositions.
A kind of preparation method of invigorate blood circulation smokeless moxibustion bar, described Moxibustion strip is successively through getting the raw materials ready, at folium artemisiae argyi vinegar carbonization
Reason, SCF-CO 2, extraction process, leaching filter dry and it is compressing can be prepared by, concrete operations are：It is first according to above-mentioned
Ratio weighs each material, and folium artemisiae argyi is carried out into vinegar carbonization treatment, and Radix Angelicae Sinensis and Ligusticum wallichii then carried out into SCF-CO 2, then by Wu
The fruit of medicinal cornel is extracted, and the folium artemisiae argyi leaching of vinegar carbonization afterwards is filtered in the mixed liquor of extract and extract solution, then is suppressed after freeze-drying
Shaping can be prepared by the invigorate blood circulation smokeless moxibustion bar；Described vinegar carbonization treatment refers to be immersed after folium artemisiae argyi is cleaned into dries pulverizing
Mixed in the jujube vinegar of 3-4 times of folium artemisiae argyi weight and stand 2-3h, dried in pot afterwards, then uniform 1-2 times of spray folium artemisiae argyi weight
Dried in pot after jujube vinegar, being dried in pot after the jujube vinegar of uniform 1-2 times of spray folium artemisiae argyi weight again must contain vinegar folium artemisiae argyi afterwards,
Then folium artemisiae argyi is positioned in carbonization kettle and 5-6h is carbonized at 500-600 DEG C and vinegar carbon Chinese mugwort is crushed to obtain.
Described jujube vinegar is prepared from by jujube through stoning, dries pulverizing, boiling, fermentation, and concrete operations are：First will
Jujube cleans stoning drying, then crushes to obtain red date powder, and the water boiling 1-2h for adding 3-5 times of red date powder weight obtains jujube juice,
Then it is cooled to after 35-40 DEG C and adds the yeast of jujube juice weight 1-5% and the distiller's yeast of 5-8% to mix, adjusts the temperature to 17-18 DEG C
Carry out one time fermentation 12-14h, then heat to 28-30 DEG C fermentation 6-8 days after filter can be prepared by jujube vinegar.
Described supercritical CO2Extraction refers to the mixing cleaned Ligusticum wallichii and Radix Angelicae Sinensis dry and be ground into 40-60 mesh first
Powder, the ethanol for being then added thereto to 3-4 times of mixed-powder carries out supercritical CO as entrainer2Extraction 2-3h must be extracted
Liquid；Described supercritical CO2The extracting pressure of extraction is 40-45MPa, and extraction temperature is 50-55 DEG C, and parsing pressure is 6-
8MPa, resolution temperature is 40-45 DEG C, CO2Flow be 20-30L/h；It refers to clean evodia rutaecarpa to dry that described evodia rutaecarpa is extracted
Dry doubling is crushed to 40-60 mesh, be subsequently adding the water of 8-10 times of evodia rutaecarpa weight carry out decoct 1-2h obtain extract solution I and residue I, so
Add the water of 8-10 times of residue I weight to carry out decoction 1-2h in backward residue I and obtain extract solution II, merge extract solution I and extract solution
II mixed liquor and be concentrated into the 10% of mixed liquor and obtain extract solution III.
Described leaching drying process of filtering refers to, first by extract and the mixing of extract solution III, to be afterwards immersed in vinegar carbon Chinese mugwort mixed
3-5h in liquid is closed, freeze-drying is carried out afterwards, it is finally compressing to can be prepared by the invigorate blood circulation smokeless moxibustion bar.
Embodiment 5
A kind of invigorate blood circulation smokeless moxibustion bar, according to weight ratio, the preparing raw material of described Moxibustion strip by 1100 portions of folium artemisiae argyis, 55 parts
Radix Angelicae Sinensis, 50 portions of evodia rutaecarpas and 8 parts of Ligusticum wallichii compositions.
A kind of preparation method of invigorate blood circulation smokeless moxibustion bar, described Moxibustion strip is successively through getting the raw materials ready, at folium artemisiae argyi vinegar carbonization
Reason, SCF-CO 2, extraction process, leaching filter dry and it is compressing can be prepared by, concrete operations are：It is first according to above-mentioned
Ratio weighs each material, and folium artemisiae argyi is carried out into vinegar carbonization treatment, and Radix Angelicae Sinensis and Ligusticum wallichii then carried out into SCF-CO 2, then by Wu
The fruit of medicinal cornel is extracted, and the folium artemisiae argyi leaching of vinegar carbonization afterwards is filtered in the mixed liquor of extract and extract solution, then is suppressed after freeze-drying
Shaping can be prepared by the invigorate blood circulation smokeless moxibustion bar；Described vinegar carbonization treatment refers to be immersed after folium artemisiae argyi is cleaned into dries pulverizing
Mixed in the jujube vinegar of 3-4 times of folium artemisiae argyi weight and stand 2-3h, dried in pot afterwards, then uniform 1-2 times of spray folium artemisiae argyi weight
Dried in pot after jujube vinegar, being dried in pot after the jujube vinegar of uniform 1-2 times of spray folium artemisiae argyi weight again must contain vinegar folium artemisiae argyi afterwards,
Then folium artemisiae argyi is positioned in carbonization kettle and 5-6h is carbonized at 500-600 DEG C and vinegar carbon Chinese mugwort is crushed to obtain.
Described jujube vinegar is prepared from by jujube through stoning, dries pulverizing, boiling, fermentation, and concrete operations are：First will
Jujube cleans stoning drying, then crushes to obtain red date powder, and the water boiling 1-2h for adding 3-5 times of red date powder weight obtains jujube juice,
Then it is cooled to after 35-40 DEG C and adds the yeast of jujube juice weight 1-5% and the distiller's yeast of 5-8% to mix, adjusts the temperature to 17-18 DEG C
Carry out one time fermentation 12-14h, then heat to 28-30 DEG C fermentation 6-8 days after filter can be prepared by jujube vinegar.
Described supercritical CO2Extraction refers to the mixing cleaned Ligusticum wallichii and Radix Angelicae Sinensis dry and be ground into 40-60 mesh first
Powder, the ethanol for being then added thereto to 3-4 times of mixed-powder carries out supercritical CO as entrainer2Extraction 2-3h must be extracted
Liquid；Described supercritical CO2The extracting pressure of extraction is 40-45MPa, and extraction temperature is 50-55 DEG C, and parsing pressure is 6-
8MPa, resolution temperature is 40-45 DEG C, CO2Flow be 20-30L/h；It refers to clean evodia rutaecarpa to dry that described evodia rutaecarpa is extracted
Dry doubling is crushed to 40-60 mesh, be subsequently adding the water of 8-10 times of evodia rutaecarpa weight carry out decoct 1-2h obtain extract solution I and residue I, so
Add the water of 8-10 times of residue I weight to carry out decoction 1-2h in backward residue I and obtain extract solution II, merge extract solution I and extract solution
II mixed liquor and be concentrated into the 10% of mixed liquor and obtain extract solution III.
Described leaching drying process of filtering refers to, first by extract and the mixing of extract solution III, to be afterwards immersed in vinegar carbon Chinese mugwort mixed
3-5h in liquid is closed, freeze-drying is carried out afterwards, it is finally compressing to can be prepared by the invigorate blood circulation smokeless moxibustion bar.
Clinical case：
Liu so-and-so, female, 36 years old, irregular menstruation, the time in menstrual period was not fixed, qi-blood deficiency, 2-3 days of the present invention of moxa-moxibustion, once a day,
Each 25-30min, symptom is relieved, and lower abdomen crymodynia mitigates, and is fully recovered the acupuncture January that holds on again after.
King so-and-so, female, 20 years old, dysmenorrhoea, menstruation was not smooth, and trick is ice-cold, qi-blood deficiency, 3-4 days of the present invention of moxa-moxibustion, daily 1
Secondary, each 25-30min, symptom is relieved, and during next menstruation, pain relief is fully recovered after continuing moxa-moxibustion January.
Week so-and-so, female 15 years old, comes half a year at the beginning of menstruation, and menstrual period are extremely disorderly, and qi and blood is not lived, lower abdomen hurt like hell during menstruation,
2-3 days of the present invention of moxa-moxibustion, once a day, each 25-30min, pain is relieved, and is fully recovered after continuing moxa-moxibustion January.
Zhang, female, 40 years old, menstruation disorder of menstrual cycle, Hypomenorrhea, qi-blood deficiency, lower abdomen crymodynia, moxa-moxibustion 1-3 of the present invention
My god, once a day, each 25-30min, symptom is relieved, and is fully recovered after continuing moxa-moxibustion two months.
Gong so-and-so, female, 25 years old, dysmenorrhoea had clot during menstruation, qi and blood is not lived, lower abdomen pendant pain, 3-5 days of the present invention of moxa-moxibustion, often
It 1 time, each 25-30min, symptom is relieved, and is fully recovered after continuing moxa-moxibustion January.
Claims (5)
1. a kind of invigorate blood circulation smokeless moxibustion bar, it is characterised in that：According to weight ratio, the preparing raw material of described Moxibustion strip by
1000-1100 portions of folium artemisiae argyi, 40-60 parts of Radix Angelicae Sinensis, 30-50 portions of evodia rutaecarpa and 1-10 parts of Ligusticum wallichii composition.
2. a kind of preparation method of invigorate blood circulation smokeless moxibustion bar as claimed in claim 1, it is characterised in that：Described moxa-moxibustion
Bar successively through getting the raw materials ready, folium artemisiae argyi vinegar carbonization treatment, supercritical CO2Extraction, extraction process, leaching are filtered by drying and being compressing and are made
, concrete operations are：It is first according to aforementioned proportion and weighs each material, folium artemisiae argyi is carried out into vinegar carbonization treatment, then by Radix Angelicae Sinensis and river
Rhizome of chuanxiong carries out supercritical CO2Extraction, then evodia rutaecarpa is extracted, and the folium artemisiae argyi leaching of vinegar carbonization afterwards is filtered to extract and extract solution
In mixed liquor, then compressing after freeze-drying can be prepared by the invigorate blood circulation smokeless moxibustion bar；Described vinegar carbonization treatment is
Refer to 2-3h in the jujube vinegar that 3-4 times of folium artemisiae argyi weight is immersed after the clean dries pulverizing of folium artemisiae argyi, dry afterwards, then uniform spray folium artemisiae argyi
Dried after the jujube vinegar of 1-2 times of weight, being dried after the jujube vinegar of uniform 1-2 times of spray folium artemisiae argyi weight again must contain vinegar folium artemisiae argyi afterwards,
Then the 5-6h that folium artemisiae argyi is carbonized at 500-600 DEG C obtains vinegar carbon Chinese mugwort.
3. a kind of preparation method of invigorate blood circulation smokeless moxibustion bar as claimed in claim 2, it is characterised in that：Described jujube
Vinegar is prepared from by jujube through stoning, dries pulverizing, boiling, fermentation, and concrete operations are：Jujube is cleaned into stoning drying first,
Then red date powder is crushed to obtain, the water boiling 1-2h for adding 3-5 times of red date powder weight obtains jujube juice, is then cooled to 35-40 DEG C
The yeast of jujube juice weight 1-5% and the distiller's yeast of 5-8% is added to mix afterwards, adjusting the temperature to 17-18 DEG C carries out one time fermentation 12-
14h, then heat to 28-30 DEG C fermentation 6-8 days after filter can be prepared by jujube vinegar.
4. a kind of preparation method of invigorate blood circulation smokeless moxibustion bar as claimed in claim 2, it is characterised in that：It is described super to face
CO2 extractions in boundary refer to the mixed-powder cleaned Ligusticum wallichii and Radix Angelicae Sinensis dry and be ground into 40-60 mesh first, are then added thereto to
The ethanol of 3-4 times of mixed-powder carries out SCF-CO 2 2-3h and obtains extract as entrainer；Described supercritical CO 2 extraction
The extracting pressure for taking is 40-45MPa, and extraction temperature is 50-55 DEG C, and parsing pressure is 6-8MPa, and resolution temperature is 40-45 DEG C,
The flow of CO2 is 20-30L/h；It refers to clean evodia rutaecarpa to dry and be crushed to 40-60 mesh that described evodia rutaecarpa is extracted, then
Add the water of 8-10 times of evodia rutaecarpa weight to carry out decoction 1-2h and obtain extract solution I and residue I, then to addition residue I weights in residue I
The water of 8-10 times of amount carries out decoction 1-2h and obtains extract solution II, merges extract solution I and extract solution II obtains mixed liquor and is concentrated into mixing
The 10% of liquid obtains extract solution III.
5. a kind of preparation method of invigorate blood circulation smokeless moxibustion bar as claimed in claim 4, it is characterised in that：Described leaching is filtered
Drying process refers to, first by extract and the mixing of extract solution III, vinegar carbon Chinese mugwort to be immersed in into 3-5h in mixed liquor afterwards, it is laggard
Row freeze-drying, it is finally compressing to can be prepared by the invigorate blood circulation smokeless moxibustion bar.
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| CN107335046A (en) * | 2017-08-29 | 2017-11-10 | 南京多宝生物科技有限公司 | A kind of medicine moxa roll for treating dysmenorrhoea and preparation method thereof |
| CN109260445A (en) * | 2018-11-27 | 2019-01-25 | 李丹丹 | A kind of draft liquid and preparation method thereof |
| CN111939240A (en) * | 2020-08-10 | 2020-11-17 | 国人健康管理(杭州)有限公司 | Medicinal moxibustion for regulating qi and blood and improving dysmenorrhea and preparation method thereof |
| CN112121080A (en) * | 2020-09-30 | 2020-12-25 | 庞伟 | A Chinese medicinal composition for moxibustion, and its preparation method |
| CN112156001A (en) * | 2020-08-24 | 2021-01-01 | 江苏三才五妍医疗科技发展有限公司 | Preparation method of smokeless moxa cone |
| CN116850255A (en) * | 2023-08-22 | 2023-10-10 | 甘肃中医药大学 | Traditional Chinese medicine foot bath composition for treating dysmenorrhea and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107335046A (en) * | 2017-08-29 | 2017-11-10 | 南京多宝生物科技有限公司 | A kind of medicine moxa roll for treating dysmenorrhoea and preparation method thereof |
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| CN111939240A (en) * | 2020-08-10 | 2020-11-17 | 国人健康管理(杭州)有限公司 | Medicinal moxibustion for regulating qi and blood and improving dysmenorrhea and preparation method thereof |
| CN112156001A (en) * | 2020-08-24 | 2021-01-01 | 江苏三才五妍医疗科技发展有限公司 | Preparation method of smokeless moxa cone |
| CN112121080A (en) * | 2020-09-30 | 2020-12-25 | 庞伟 | A Chinese medicinal composition for moxibustion, and its preparation method |
| CN116850255A (en) * | 2023-08-22 | 2023-10-10 | 甘肃中医药大学 | Traditional Chinese medicine foot bath composition for treating dysmenorrhea and preparation method thereof |
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Application publication date: 20170613 |