CN106726681A - A kind of method that sericin prepares mask sheet - Google Patents
A kind of method that sericin prepares mask sheet Download PDFInfo
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- CN106726681A CN106726681A CN201611159827.2A CN201611159827A CN106726681A CN 106726681 A CN106726681 A CN 106726681A CN 201611159827 A CN201611159827 A CN 201611159827A CN 106726681 A CN106726681 A CN 106726681A
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- Prior art keywords
- sericin
- solution
- mask sheet
- facial mask
- prepares
- Prior art date
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- 108010013296 Sericins Proteins 0.000 title claims abstract description 57
- 238000000034 method Methods 0.000 title claims abstract description 18
- 230000001815 facial effect Effects 0.000 claims abstract description 30
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 10
- 229920001817 Agar Polymers 0.000 claims abstract description 8
- 239000008272 agar Substances 0.000 claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 5
- 150000001875 compounds Chemical class 0.000 claims abstract description 3
- 238000004090 dissolution Methods 0.000 claims abstract description 3
- 238000003756 stirring Methods 0.000 claims abstract description 3
- 239000000243 solution Substances 0.000 claims description 28
- 108010022355 Fibroins Proteins 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 238000004140 cleaning Methods 0.000 claims description 7
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 238000007605 air drying Methods 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 238000000502 dialysis Methods 0.000 claims description 3
- 239000000284 extract Substances 0.000 claims description 3
- 238000005192 partition Methods 0.000 claims description 3
- 238000000746 purification Methods 0.000 claims description 3
- 241000255794 Bombyx mandarina Species 0.000 claims description 2
- 241000255789 Bombyx mori Species 0.000 claims description 2
- 210000001061 forehead Anatomy 0.000 claims description 2
- 238000007654 immersion Methods 0.000 claims description 2
- 239000012460 protein solution Substances 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- 230000008901 benefit Effects 0.000 abstract description 4
- 230000003020 moisturizing effect Effects 0.000 abstract description 4
- 230000002087 whitening effect Effects 0.000 abstract description 4
- 230000003712 anti-aging effect Effects 0.000 abstract description 3
- 230000000704 physical effect Effects 0.000 abstract description 2
- 210000003491 skin Anatomy 0.000 description 12
- 239000000499 gel Substances 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 150000001413 amino acids Chemical class 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- DWNBOPVKNPVNQG-LURJTMIESA-N (2s)-4-hydroxy-2-(propylamino)butanoic acid Chemical compound CCCN[C@H](C(O)=O)CCO DWNBOPVKNPVNQG-LURJTMIESA-N 0.000 description 2
- 206010020649 Hyperkeratosis Diseases 0.000 description 2
- 208000001126 Keratosis Diseases 0.000 description 2
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 description 2
- COLNVLDHVKWLRT-QMMMGPOBSA-N L-phenylalanine Chemical compound OC(=O)[C@@H](N)CC1=CC=CC=C1 COLNVLDHVKWLRT-QMMMGPOBSA-N 0.000 description 2
- OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 description 2
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000002242 deionisation method Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 239000004471 Glycine Substances 0.000 description 1
- 102000003425 Tyrosinase Human genes 0.000 description 1
- 108060008724 Tyrosinase Proteins 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000019522 cellular metabolic process Effects 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 210000001339 epidermal cell Anatomy 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 230000000873 masking effect Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000004745 nonwoven fabric Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 description 1
- 229920001184 polypeptide Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 230000011218 segmentation Effects 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 210000000106 sweat gland Anatomy 0.000 description 1
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
Abstract
The invention discloses a kind of method that mask sheet is prepared with sericin,Including the sericin solution that compound concentration is 2% 5%,0.5% 3% agar powder is added in sericin solution,After heating stirring to uniform dissolution,It is injected into facial mask mould,Drying forms sericin facial mask,The steps such as 10h 15h are soaked in the ethanol solution of 50% 80% concentration,The present invention has power consumption low in whole processing procedure,Biological safety is high,It is cheap,It is simple to operate,The advantage such as environmentally safe,There is whitening by sericin facial mask obtained in the invention,Moisturizing,The biological characteristics of anti-aging and frivolous transparent physical property,By sericin facial mask obtained in the invention,Using upper more flexibility,Can be needed to select the mask sheet of different parts to use according to individual difference.
Description
Technical field
The present invention relates to a kind of method that mask sheet is prepared with sericin, the processing method for belonging to sericin.
Background technology
Silk gum is a kind of globular preteins, and relative molecular mass is 1.4~31.4 ten thousand, is made up of 18 kinds of amino acid, wherein silk
Propylhomoserin (Ser), asparatate (Asp) and glycine (Gly) content are higher, relative mass respectively reaches 33.43%,
16.71% and 13.49%.The secondary structure of silk gum containing part β conceptions, is practically free of α spiral knots with without based on crimpiness
Structure.Silk gum amino acid composition in, polar side chains account for 74.61%, these be located at sericin chain on side chain compared with
Amino acid long and polar hydrophilic group are in polypeptide surface, can make the moisture in structure be delivered to keratoderma and and its
With reference to absorption of the skin to moisture can be promoted.Silk gum soluble in water is placed under field conditions (factors), be can obtain reversible
Sericin gel.Sol is general below 60 DEG C to the temperature of gel conversion, and gel is 50~70 DEG C to the temperature that sol is converted.
During sol is to gel conversion, along with irreversible conversion from part random coil to β conformations.The intensity and gel of gel
Concentration be directly proportional.The silk gum aqueous solution and other materials are mixed and made into hybrid films, the physicochemical property of film can then be improved.
Facial mask is to apply or spread on human skin, through take off after a period of time from, clean or retain, can play concentration shield
The product of reason or cleaning action.The principle of facial mask, exactly using the of short duration time for being covered in face, is temporarily isolating the air in the external world
With pollution, skin temperature is improved, the pore expansion of skin promotes sweat gland secretion and metabolism, the oxygen content of skin is increased,
Skin is conducive to exclude the product of epidermal cell metabolism and the oil substances of accumulation, the moisture in facial mask penetrates into epidermis
Cuticula, skin becomes soft, and light is flexible naturally for skin.According to the material of facial mask, powder mediation facial mask, height can be classified as
The native facial mask in ridge, non-woven fabrics facial mask and silk mask.Due to silk mask using it is rear directly take off from, without cleaning face again,
So, it enjoys the favor of consumers in general.
The facial mask being made of sericin using this method has good hygroscopicity, can function similarly to keratoderma
The effect of middle NMF (Natural moisturizing factor, NMF), prevents skin from wrinkling.And with suppression
The characteristic of tyrosinase activity, can prevent the formation of melanin in skin, skin whitening.And tyrosine (Tyr), color in silk gum
Propylhomoserin (Trp), phenylalanine (Phe) etc. can effectively absorb ultraviolet, effectively injury of the prevention solar ultraviolet to skin, reduce
Color spot occurs.
The content of the invention
The present invention is just being directed to the characteristic of sericin and the vacancy field of existing silk mask, have developed a kind of technique
Simply, method prepared by convenient and with whitening, moisturizing, the effect of anti-aging sericin mask sheet is processed.
To achieve these goals, concrete technical scheme of the invention is as follows：
The invention discloses a kind of method that mask sheet is prepared with sericin, specific preparation process is as follows：
1) compound concentration is the sericin solution of 2%-5%；
2) the agar powder of 0.5%-3% is added in sericin solution, after heating stirring to uniform dissolution, injection
To in facial mask mould；
3) drying forms sericin facial mask, and 10h-15h is soaked in the ethanol solution of 50%-80% concentration；Work as the time
When too short, facial mask does not have completion of cure, can still be dissolved in water；When overlong time, time cost is increased；When concentration is too low
When, product solidification is incomplete, meets the water capacity soluble；When the concentration is too high, the easy dehydration of product cause it is more crisp frangible, under complete performance
Drop, also results in the waste of ethanol, increases cost.
4) after deionized water cleaning, 1h-4h is soaked in the fibroin solutions of 0.5%-3%, you can use.Work as the time
When too short, not enough, performance of keeping humidity declines fibroin content in facial mask；When overlong time, time cost is increased, also easily
Breed bacteria.When fibroin solutions concentration is too low, fibroin content is not high, influences using effect；When fibroin is dense
When spending high, because facial mask adsorbance is limited, service efficiency is reduced, improve cost.
As further improving, sericin solution of the present invention be freshly prepared sericin solution or
Dissolved using sericin powder and prepared, if using freshly prepared sericin solution, preparation method is according to 1:20-1:
40 bath raio extracts sericin solution, carries out dialysis purification；When bath raio is too small, the sericin concentration extracted is too low,
Water, heat and waste of time are caused, economic benefit declines；When bath raio is too high, sericin extracts and not exclusively causes to waste.
Used as further improving, sericin of the present invention is silkworm sericin or wild silkworm sericin.
Used as further improving, facial mask mould of the present invention includes monoblock type facial mask and partition type facial mask, segmentation
Formula mask sheet is forehead patch, and eye sticker, nose patch, face is pasted, any one in lower jaw patch.
Used as further improving, agar concentration of the present invention is 0.5%-3%.When the concentration is too low, product is thick
Spend thin, poor mechanical property；When the concentration is too high, product thickness is blocked up, and permeability declines, and is susceptible to coagulate in injection molding
Glue, is difficult to form complete uniform facial mask.
Used as further improving, immersion fibroin solutions of the present invention are sericin solution or fibroin albumen
Solution.
Used as further improving, drying of the present invention is that natural air drying or machine are dried.
Compared with prior art, the present invention has following prominent characteristics：
(1) present invention is low with power consumption in whole processing procedure, and biological safety is high, cheap, side simple to operate
Just, the advantage such as environmentally safe.
(2) there is whitening, moisturizing, the biological characteristics of anti-aging and frivolous by sericin facial mask obtained in the invention
Transparent physical property.
(3) by sericin facial mask obtained in the invention, exclusive use can just reach target property.
(4) by sericin facial mask obtained in the invention, can be coordinated according to individual different demand has heterogeneity
Fibroin Essence use.
(5) by sericin facial mask obtained in the invention, have in the absorption to nutrient solution and absorption property bigger
Advantage.
(6) whole preparation process is completed in aqueous, and reaction condition is gentle, avoids environment is made using organic solvent
Into pollution, operating procedure is simple.
(7) by sericin facial mask obtained in the invention, flexibility is being had more using upper, can be according to individual difference needs
The mask sheet of different parts is selected to use.
Specific embodiment
Technical scheme is further described below by specific embodiment：
It is of the invention main by following scheme implementation：
Agar is dissolved in a certain amount of sericin solution, finite concentration is made into, heating and being stirred continuously mixes it
Close uniform.Take a certain amount of solution and pour into masking in mask sheet mould.
Technical scheme is described in further detail below by specific embodiment, following examples are right
It is of the invention explanation and the invention is not limited in following examples.
Embodiment 1
Hot 30min, the filtering altogether in 200ml, 300ml, 400ml deionization boiling water by the dry silk cocoons of 10g respectively, takes
150ml adds 3.0g agar powders, and heating for dissolving pours into 10 nose patch moulds while hot.After natural air drying 24h, 50% ethanol postincubation
10h；It is soaked in 0.5% sericin solution after deionized water cleaning, is taken out after 1h.
Embodiment 2
The dry silk cocoons of 10g are total to hot 30min in 300ml deionization boiling water, the solution obtained by 300ml dialysis purifications is taken
6 parts are equally divided into, 0.25g, 0.5g, 0.75g, 1.0g, 1.25g, 1.5g agar powder is separately added into, heating for dissolving pours into 6 while hot
Individual complete type facial mask.After natural air drying 24h, 70% ethanol postincubation 12h；3% sericin is soaked in after deionized water cleaning
In solution, taken out after 2h.
Embodiment 3
1.5g sericin powder is dissolved in 100mL deionized waters, addition 0.5g agar powders, heating for dissolving, while hot
Pour into 5 lower jaw patch moulds.After 6h being dried in baking oven, 75% ethanol postincubation 15h；2% silk is soaked in after deionized water cleaning
In fibroin solution, taken out after 4h.
Finally, in addition it is also necessary to it is noted that listed above is only several specific embodiments of the invention.Obviously, the present invention
Above example is not limited to, there can also be many deformations.One of ordinary skill in the art can be straight from present disclosure
The all deformations derived or associate are connect, protection scope of the present invention is considered as.
Claims (7)
1. a kind of method that sericin prepares mask sheet, it is characterised in that specific preparation process is as follows：
1) compound concentration is the sericin solution of 2%-5%；
2) the agar powder of 0.5%-3% is added in sericin solution, after heating stirring to uniform dissolution, facial mask is injected into
In mould；
3) drying forms sericin facial mask, and 10h-15h is soaked in the ethanol solution of 50%-80% concentration；
4) after deionized water cleaning, 1h-4h is soaked in the fibroin solutions of 0.5%-3%, you can use.
2. the method that sericin according to claim 1 prepares mask sheet, it is characterised in that described sericin
Solution manufacturing method has dissolving sericin powder and fresh extractor sericin solution, the side of fresh extractor sericin solution
Method is according to 1:20-1:40 bath raio extracts sericin solution, carries out dialysis purification.
3. the method that sericin according to claim 1 and 2 prepares mask sheet, it is characterised in that described silk gum
Albumen is silkworm sericin or wild silkworm sericin.
4. the method that sericin according to claim 1 prepares mask sheet, it is characterised in that described facial mask mould
Including complete formula mask sheet and partition type mask sheet.
5. the method that sericin according to claim 4 prepares mask sheet, it is characterised in that described partition type face
Film patch be lower jaw patch, nose patch, eye sticker, forehead paste in any one.
6. the method that sericin according to claim 1 prepares mask sheet, it is characterised in that described drying means
It is that natural air drying and machine are dried.
7. the method that sericin according to claim 1 prepares mask sheet, it is characterised in that described immersion silk
Protein solution is sericin solution or silk fibroin protein solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611159827.2A CN106726681B (en) | 2016-12-15 | 2016-12-15 | A method of mask sheet is prepared with sericin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611159827.2A CN106726681B (en) | 2016-12-15 | 2016-12-15 | A method of mask sheet is prepared with sericin |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106726681A true CN106726681A (en) | 2017-05-31 |
| CN106726681B CN106726681B (en) | 2019-11-12 |
Family
ID=58889167
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611159827.2A Active CN106726681B (en) | 2016-12-15 | 2016-12-15 | A method of mask sheet is prepared with sericin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106726681B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107280996A (en) * | 2017-08-24 | 2017-10-24 | 郭志军 | A kind of face mask of traditional Chinese medicine and preparation method thereof and application method |
| CN108149387A (en) * | 2018-01-17 | 2018-06-12 | 青岛大学 | A kind of hydrogel filament mask substrate |
| CN111437213A (en) * | 2020-04-24 | 2020-07-24 | 中科国思生物科技研究（广州）有限公司 | Cloth-free skin-nourishing facial mask based on active silk micellar protein and preparation method thereof |
| CN113265768A (en) * | 2021-06-10 | 2021-08-17 | 盐城工业职业技术学院 | Method for producing flat silk surface membrane material from whole silk glue silkworm and common castor silkworm |
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| JP2001129371A (en) * | 1999-11-09 | 2001-05-15 | Ube Ind Ltd | Membrane comprising mixture containing sericin, and compound containing agar and/or agarose and its manufacturing method |
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| CN103462867A (en) * | 2013-09-05 | 2013-12-25 | 浙江大学 | Preparation method of silk glue/trehalose skin-care facial mask |
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| JP2001129371A (en) * | 1999-11-09 | 2001-05-15 | Ube Ind Ltd | Membrane comprising mixture containing sericin, and compound containing agar and/or agarose and its manufacturing method |
| WO2008072817A1 (en) * | 2006-12-14 | 2008-06-19 | Fineco Ltd. | Hydrogel mask pack, method of preparing the same, and related composition |
| CN103462867A (en) * | 2013-09-05 | 2013-12-25 | 浙江大学 | Preparation method of silk glue/trehalose skin-care facial mask |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107280996A (en) * | 2017-08-24 | 2017-10-24 | 郭志军 | A kind of face mask of traditional Chinese medicine and preparation method thereof and application method |
| CN108149387A (en) * | 2018-01-17 | 2018-06-12 | 青岛大学 | A kind of hydrogel filament mask substrate |
| CN111437213A (en) * | 2020-04-24 | 2020-07-24 | 中科国思生物科技研究（广州）有限公司 | Cloth-free skin-nourishing facial mask based on active silk micellar protein and preparation method thereof |
| CN111437213B (en) * | 2020-04-24 | 2023-06-02 | 中科国思生物科技研究（广州）有限公司 | Active silk collagen-based non-cloth skin care mask and preparation method thereof |
| CN113265768A (en) * | 2021-06-10 | 2021-08-17 | 盐城工业职业技术学院 | Method for producing flat silk surface membrane material from whole silk glue silkworm and common castor silkworm |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106726681B (en) | 2019-11-12 |
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