CN106699425A - Flower increasing and pod protecting soybean fertilizer - Google Patents
Flower increasing and pod protecting soybean fertilizer Download PDFInfo
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- CN106699425A CN106699425A CN201710128079.XA CN201710128079A CN106699425A CN 106699425 A CN106699425 A CN 106699425A CN 201710128079 A CN201710128079 A CN 201710128079A CN 106699425 A CN106699425 A CN 106699425A
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- soybean
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B3/00—Fertilisers based essentially on di-calcium phosphate
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a flower increasing and pod protecting soybean fertilizer which is prepared from the following raw materials in parts by weight: 14-15 parts of paulownia sawdust, 42-46 parts of cottonseed hull, 8-9 parts of fly ash, 0.6-0.7 part of propylene glycol alginate, 5-7 parts of ammonium sulfate, 2-3 parts of calcium hydrogen phosphate, 0.4-0.5 part of silica fume, 18-20 parts of waste newspaper, 1-2 parts of potassium persulfate, 35-40 parts of yellow mealworm dung, 0.8-0.9 part of ferric chloride hexahydrate, 0.4-0.5 part of ammonium ferrous sulfate hexahydrate and appropriate 25% phosphoric acid solution and water. The fertilizer disclosed by the invention is reasonably proportioned according to the release characteristic of the coating materials such as propylene glycol alginate and the absorption law of soybean nutrients, the nutrients can be accurately released in the early flowering period and pod bearing period of soybean, the accumulation of soybean biomass is promoted, the leaf area index is increased, the nutrition for pod growth is guaranteed, thus the aims of increasing flowers and protecting pods and boosting yield are achieved, and a perfect effect of increasing soybean yield is realized.
Description
Technical field
The present invention relates to technical field of fertilizers, more particularly to a kind of soybean fertilizer for increasing flower guarantor pod.
Background technology
China is large agricultural country, and the usage amount of fertilizer is high, and current fertilizer and its corresponding fertilizer practice so that I
State's utilization rate of fertilizer is chronically at reduced levels, the serious enthusiasm that have impact on peasant planting, and environment is produced serious
Pollution, is unfavorable for the modernization industry technical system of the efficient high yield of structure China sustainable development.Safely based on state food
Ask and high yield target, cause fertilizer application amount to be continuously increased, the fertilising of some peasant's blindnesses causes soil, water quality, crops
Pollution, fertilizer efficiency declines, and food cost increases.Therefore it provides new-type fertilizer, controls farmland nutrient loss, fertilizer profit is improved
With rate, have important practical significance.
Yellow meal worm is a kind of more ripe resource insect of artificial culture technology, and have many decades propagates history artificially,
There is preferable application prospect in industries such as special cultivation, food, cosmetics.But in yellow meal worm breeding process, can produce big
Amount excrement.According to surveying and determination, the frass that adult about produces 3kg is grown into per 1kg larvas.If these frass are dealt with improperly, not only cause
How the wasting of resources, and pollution environment, make good use of frass, has caused the concern of people.At present, by frass as organic
Fertilizer, animal feed and culturing edible fungus etc., but, the simple application of these application only frass, added value is not high.Bloom frass
Particle is uniform, thin such as husky, dry, free from extraneous odour, and these features are not available for other raw materials.If being that raw material passes through deeply with frass
Core crab in the fertilizer of high adsorption is processed into, the value of fertilizer can not only be effectively improved, meanwhile, frass pair can be reduced
The pollution of environment, realizes the recycling of frass.
Cellulose is the most abundant natural polymer of nature content, abundance, cheap, is renewable
With environment-friendly macromolecular material.Because cellulose is fibrous multiple capillary, regularity high molecular polymer, with porous
The characteristic big with specific surface area, while the hydroxyl on its surface easily forms hydrogen bond, it is difficult to be dissolved in water, therefore, by suitably changing
Property be applied to the cladding of fertiliser granulates, can effectively prevent the too fast hydrolysis of fertilizer, improve the duration of fertilizer efficiency.
The present inventor is based on the further investigation to the above material, is arbor in fertilizer by deep processing bloom frass
Frame, and using modified cellulose as covering material, there is provided a kind of new function type fertilizer.
The content of the invention
The object of the invention is exactly to make up the defect of prior art, there is provided a kind of increasing flower protects the soybean fertilizer of pod.
The present invention is achieved by the following technical solutions：
It is a kind of to increase the soybean fertilizer that flower protects pod, it is made from the following raw materials in parts by weight：Paulownia sawdust 14-15, cotton seed hulls 42-
46th, flyash 8-9, propylene glycol alginate 0.6-0.7, ammonium sulfate 5-7, calcium monohydrogen phosphate 2-3, SILICA FUME 0.4-0.5, old newsprint
18-20, potassium peroxydisulfate 1-2, bloom frass 35-40, ferric chloride (FeCl36H2O) 0.8-0.9, six aqueous ferrous sulfate ammonium 0.4-0.5,25%
Appropriate phosphoric acid solution, appropriate amount of water.
Described increasing flower protects comprising the following steps that for the soybean method for preparing fertilizer of pod：
（1）By in old newsprint and paulownia sawdust mixing feeding fermentation tank, add water to material moisture and reach 42-46%, ferment 1-2
Taken out after week, collect filter residue respectively through squeeze and filter and filtrate is standby；
（2）Take bloom frass to be sufficiently mixed with 25% isometric phosphoric acid solution, immersion is filtered after 12-15 minutes, after removal filtrate
By material send into high temperature furnace in, be warming up to 400-450 DEG C and react 50-60 minute, after the completion of taking-up be cooled to room temperature, wash with water
It is standby that net rear dries pulverizing obtains powder；
（3）It is small prior to impregnating 6-7 in water after step 1 gained filter residue, step 2 gained powder and cotton seed hulls, flyash are mixed
When, take out afterwards and put into fermentation vat, to ferment 24-25 days at room temperature, period carried out a turning every 7-8 days, had fermented
It is after that gained fermentation material dries pulverizing is standby；
（4）It is dissolved in 30 times of water of mixture quality after ferric chloride (FeCl36H2O) and six aqueous ferrous sulfate ammoniums are mixed, is heated to
, while adjusting pH value of solution to 9.0-9.5,75-80 DEG C is warming up to afterwards, stirring is collected by filtration precipitation after 2 hours, uses by 40-42 DEG C
Precipitation is washed till neutrality by water, after drying in input step 1 gained filtrate, while again to addition potassium peroxydisulfate, alginic acid third in filtrate
Diol ester, is stirred continuously reaction 10-12 hours after being heated to 45-50 DEG C, room temperature is cooled to afterwards, obtains modified complex liquid standby
With；
（5）After step 3 gained powder is mixed with ammonium sulfate, calcium monohydrogen phosphate, SILICA FUME by conveyer belt send into comminutor in, and
Step 4 gained complex liquid constantly is sprayed until granulating completion to comminutor is atomization in granulation process, and gained particle is chilled
Weighed after drying packaging, obtain final product fertilizer of the present invention.
It is an advantage of the invention that：
The present invention is processed by bloom frass multistep, makes its surface form more uniform a large amount of small spaces, these spaces
Presence, can greatly increase the combination of core raw material in itself and residue, improve fertiliser granulates intensity, and itself is used as natural organic original
Material progressively disintegrating with particle, using the teaching of the invention it is possible to provide considerable nutrient, while being not only increased to cellulose modified using Armco magnetic iron
Hydrolytic stability of the fertilizer in soil, subsidiary magnetic field effect can also activating soil nutrient element, the physiology work of stimulation root system
It is dynamic, improve the use surcharge of fertilizer.
Fertilizer of the present invention is closed according to the release characteristics of the covering materials such as propylene glycol alginate and the absorbing rule of soybean nutrient
Reason proportioning, in soybean early flowering season and the accurate Releasing nutrient of fruiting period energy, promotes the accumulation of soybean biomass, improves leaf area and refers to
Number, the nutrition that order flower pod grows is guaranteed, and the purpose that flower protects pod and increase yield is increased so as to play, and is had to improving soybean yields
Good effect.
Specific embodiment
It is a kind of to increase the soybean fertilizer that flower protects pod, it is made up of the raw material of following weight portion (kg)：Paulownia sawdust 14, cotton seed hulls
42nd, flyash 8, propylene glycol alginate 0.6, ammonium sulfate 5, calcium monohydrogen phosphate 2, SILICA FUME 0.4, old newsprint 18, potassium peroxydisulfate 1, Huang
Mealworm excrement 35, ferric chloride (FeCl36H2O) 0.8, six aqueous ferrous sulfate ammoniums 0.4,25% phosphoric acid solution are appropriate, appropriate amount of water.
Described increasing flower protects comprising the following steps that for the soybean method for preparing fertilizer of pod：
（1）By in old newsprint and paulownia sawdust mixing feeding fermentation tank, add water to material moisture and reach 42%, fermentation takes after 1 week
Go out, collect filter residue respectively through squeeze and filter and filtrate is standby；
（2）Take bloom frass to be sufficiently mixed with 25% isometric phosphoric acid solution, immersion is filtered after 12 minutes, will after removal filtrate
Material feeding high temperature furnace in, be warming up to 400 DEG C and react 50 minutes, after the completion of take out be cooled to room temperature, after washing drying
Crush powder is standby；
（3）Prior to being impregnated 6 hours in water after step 1 gained filter residue, step 2 gained powder and cotton seed hulls, flyash are mixed,
Take out afterwards and put into fermentation vat, ferment 24 days at room temperature, period carried out a turning every 7 days, by institute after the completion of fermentation
Obtain fermentation material dries pulverizing standby；
（4）It is dissolved in 30 times of water of mixture quality after ferric chloride (FeCl36H2O) and six aqueous ferrous sulfate ammoniums are mixed, is heated to
, while adjusting pH value of solution to 9.0,75 DEG C are warming up to afterwards, stirring is collected by filtration precipitation after 2 hours, is washed precipitation with water by 40 DEG C
To neutral, after drying in input step 1 gained filtrate, while being heated to potassium peroxydisulfate, propylene glycol alginate is added in filtrate again
Reaction 10 hours is stirred continuously after to 45 DEG C, room temperature is cooled to afterwards, obtain modified complex liquid standby；
（5）After step 3 gained powder is mixed with ammonium sulfate, calcium monohydrogen phosphate, SILICA FUME by conveyer belt send into comminutor in, and
Step 4 gained complex liquid constantly is sprayed until granulating completion to comminutor is atomization in granulation process, and gained particle is chilled
Weighed after drying packaging, obtain final product fertilizer of the present invention.
In order to further illustrate application value of the invention, inventor uses fertilizer of the present invention and commercially available common fertilizer respectively
Soybean planting experiment is carried out as experimental group and control group, yield and soil physico-chemical property are detected after soybean harvest, it is real
Test a group mu Yield of Soybean and averagely reach 152.6kg, and control group is 143.8kg, while experimental group Soil Nitrogen, phosphorus, potassium effective content
35.7%, 14.2%, 18.6% is improve compared with control group, it is seen that there is fertilizer of the present invention preferably promotion to make to soybean planting respectively
With.
Claims (2)
1. it is a kind of to increase the soybean fertilizer that flower protects pod, it is characterised in that to be made from the following raw materials in parts by weight：Paulownia sawdust 14-
15th, cotton seed hulls 42-46, flyash 8-9, propylene glycol alginate 0.6-0.7, ammonium sulfate 5-7, calcium monohydrogen phosphate 2-3, SILICA FUME 0.4-
0.5th, old newsprint 18-20, potassium peroxydisulfate 1-2, bloom frass 35-40, ferric chloride (FeCl36H2O) 0.8-0.9, six aqueous ferrous sulfate ammoniums
0.4-0.5,25% phosphoric acid solution are appropriate, appropriate amount of water.
2. the increasing flower according to claims 1 protects the soybean fertilizer of pod, it is characterised in that the specific steps of preparation method
It is as follows：
（1）By in old newsprint and paulownia sawdust mixing feeding fermentation tank, add water to material moisture and reach 42-46%, ferment 1-2
Taken out after week, collect filter residue respectively through squeeze and filter and filtrate is standby；
（2）Take bloom frass to be sufficiently mixed with 25% isometric phosphoric acid solution, immersion is filtered after 12-15 minutes, removes filtrate
Afterwards by material send into high temperature furnace in, be warming up to 400-450 DEG C and react 50-60 minute, after the completion of taking-up be cooled to room temperature, use water
It is standby that clean rear dries pulverizing obtains powder；
（3）It is small prior to impregnating 6-7 in water after step 1 gained filter residue, step 2 gained powder and cotton seed hulls, flyash are mixed
When, take out afterwards and put into fermentation vat, to ferment 24-25 days at room temperature, period carried out a turning every 7-8 days, had fermented
It is after that gained fermentation material dries pulverizing is standby；
（4）It is dissolved in 30 times of water of mixture quality after ferric chloride (FeCl36H2O) and six aqueous ferrous sulfate ammoniums are mixed, is heated to
, while adjusting pH value of solution to 9.0-9.5,75-80 DEG C is warming up to afterwards, stirring is collected by filtration precipitation after 2 hours, uses by 40-42 DEG C
Precipitation is washed till neutrality by water, after drying in input step 1 gained filtrate, while again to addition potassium peroxydisulfate, alginic acid third in filtrate
Diol ester, is stirred continuously reaction 10-12 hours after being heated to 45-50 DEG C, room temperature is cooled to afterwards, obtains modified complex liquid standby
With；
（5）After step 3 gained powder is mixed with ammonium sulfate, calcium monohydrogen phosphate, SILICA FUME by conveyer belt send into comminutor in,
And step 4 gained complex liquid constantly is sprayed until granulation completion, gained particle is through cold to comminutor is atomization in granulation process
It is lyophilized it is dry after weigh packaging, obtain final product fertilizer of the present invention.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710128079.XA CN106699425A (en) | 2017-03-06 | 2017-03-06 | Flower increasing and pod protecting soybean fertilizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710128079.XA CN106699425A (en) | 2017-03-06 | 2017-03-06 | Flower increasing and pod protecting soybean fertilizer |
Publications (1)
| Publication Number | Publication Date |
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| CN106699425A true CN106699425A (en) | 2017-05-24 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710128079.XA Pending CN106699425A (en) | 2017-03-06 | 2017-03-06 | Flower increasing and pod protecting soybean fertilizer |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102786362A (en) * | 2012-07-23 | 2012-11-21 | 安徽金农生态农业科技发展有限公司 | Biological pesticidal organic fertilizer |
| CN103724139A (en) * | 2013-12-23 | 2014-04-16 | 青岛友铭辰生物技术有限公司 | Biological pesticidal organic fertilizer and preparation method thereof |
| CN104446928A (en) * | 2014-11-15 | 2015-03-25 | 重庆市大足区炫天养殖有限责任公司 | Bio-fertilizer and preparation method thereof |
-
2017
- 2017-03-06 CN CN201710128079.XA patent/CN106699425A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102786362A (en) * | 2012-07-23 | 2012-11-21 | 安徽金农生态农业科技发展有限公司 | Biological pesticidal organic fertilizer |
| CN103724139A (en) * | 2013-12-23 | 2014-04-16 | 青岛友铭辰生物技术有限公司 | Biological pesticidal organic fertilizer and preparation method thereof |
| CN104446928A (en) * | 2014-11-15 | 2015-03-25 | 重庆市大足区炫天养殖有限责任公司 | Bio-fertilizer and preparation method thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170524 |