CN106638160B - A kind of additive for reducing cigarette bobbin paper xylon gas and its preparation method and application - Google Patents
A kind of additive for reducing cigarette bobbin paper xylon gas and its preparation method and application Download PDFInfo
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- CN106638160B CN106638160B CN201610900959.XA CN201610900959A CN106638160B CN 106638160 B CN106638160 B CN 106638160B CN 201610900959 A CN201610900959 A CN 201610900959A CN 106638160 B CN106638160 B CN 106638160B
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- bobbin paper
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- molecular distillation
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 91
- 239000000654 additive Substances 0.000 title claims abstract description 46
- 230000000996 additive effect Effects 0.000 title claims abstract description 46
- 229940089401 xylon Drugs 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 241000208125 Nicotiana Species 0.000 claims abstract description 52
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 52
- 238000000199 molecular distillation Methods 0.000 claims abstract description 29
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 28
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 229960001867 guaiacol Drugs 0.000 claims abstract description 9
- VMUXSMXIQBNMGZ-UHFFFAOYSA-N 3,4-dihydrocoumarin Chemical compound C1=CC=C2OC(=O)CCC2=C1 VMUXSMXIQBNMGZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- DMSHWWDRAYHEBS-UHFFFAOYSA-N dihydrocoumarin Natural products C1CC(=O)OC2=C1C=C(OC)C(OC)=C2 DMSHWWDRAYHEBS-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000007788 liquid Substances 0.000 claims abstract description 5
- 238000002156 mixing Methods 0.000 claims abstract 2
- 239000000203 mixture Substances 0.000 claims description 19
- 239000001674 (E)-1-(2,6,6-trimethyl-1-cyclohexenyl)but-2-en-1-one Substances 0.000 claims description 8
- BGTBFNDXYDYBEY-UHFFFAOYSA-N 1-(2,6,6-trimethylcyclohexen-1-yl)but-2-en-1-one Chemical compound CC=CC(=O)C1=C(C)CCCC1(C)C BGTBFNDXYDYBEY-UHFFFAOYSA-N 0.000 claims description 8
- POIARNZEYGURDG-UHFFFAOYSA-N beta-damascenone Natural products CC=CC(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-UHFFFAOYSA-N 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 230000008569 process Effects 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000007921 spray Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000010025 steaming Methods 0.000 claims description 4
- 238000005507 spraying Methods 0.000 claims description 3
- 241000218691 Cupressaceae Species 0.000 claims 1
- 238000009826 distribution Methods 0.000 claims 1
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 claims 1
- 239000002023 wood Substances 0.000 claims 1
- 239000003921 oil Substances 0.000 abstract description 25
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 abstract description 16
- 239000010627 cedar oil Substances 0.000 abstract description 8
- 229940073505 ethyl vanillin Drugs 0.000 abstract description 8
- 239000002304 perfume Substances 0.000 abstract description 4
- 239000011248 coating agent Substances 0.000 abstract description 3
- 238000000576 coating method Methods 0.000 abstract description 3
- 230000035943 smell Effects 0.000 abstract description 2
- 235000013599 spices Nutrition 0.000 abstract description 2
- 230000001476 alcoholic effect Effects 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 29
- 230000000391 smoking effect Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- BGTBFNDXYDYBEY-FNORWQNLSA-N 4-(2,6,6-Trimethylcyclohex-1-enyl)but-2-en-4-one Chemical compound C\C=C\C(=O)C1=C(C)CCCC1(C)C BGTBFNDXYDYBEY-FNORWQNLSA-N 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- CNOPDZWOYFOHGN-BQYQJAHWSA-N Beta-Ionol Chemical compound CC(O)\C=C\C1=C(C)CCCC1(C)C CNOPDZWOYFOHGN-BQYQJAHWSA-N 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- CNOPDZWOYFOHGN-UHFFFAOYSA-N beta-ionol Natural products CC(O)C=CC1=C(C)CCCC1(C)C CNOPDZWOYFOHGN-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000000116 mitigating effect Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000001303 quality assessment method Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/18—Paper- or board-based structures for surface covering
- D21H27/22—Structures being applied on the surface by special manufacturing processes, e.g. in presses
- D21H27/26—Structures being applied on the surface by special manufacturing processes, e.g. in presses characterised by the overlay sheet or the top layers of the structures
- D21H27/28—Structures being applied on the surface by special manufacturing processes, e.g. in presses characterised by the overlay sheet or the top layers of the structures treated to obtain specific resistance properties, e.g. against wear or weather
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
Abstract
The present invention provides a kind of additive for reducing cigarette bobbin paper xylon gas and its preparation method and application.The additive is obtained using being stood by pure tobacco oil light component, cedar wood oil, guaiacol, β damascones, dihydrocoumarin, Ethyl vanillin and alcohol as raw material, after mixing.Wherein described pure tobacco oil light component is that tobacco leaf is concentrated to give into tobacco extract after alcoholic extraction, filtered after tobacco extract is mixed with alcohol again, clear liquid is taken to be concentrated to give pure tobacco oil, it is pure tobacco oil light component that pure tobacco oil finally is obtained into 40 60 DEG C of cuts through two-stage molecular distillation.After on heretofore described additive coating to cigarette paper, xylon gas caused by the cigarette bobbin paper burning are significantly less than regular-size cigarette obbbin, and the cigarette that can assign cigarette pleasant smells perfume (or spice).
Description
Technical field
The present invention relates to a kind of additive of cigarette bobbin paper, particularly a kind of additive for reducing cigarette paper xylon gas and its
Using.
Background technology
Cigarette bobbin paper be it is a kind of specialize in, the tissue paper for wrapping up pipe tobacco, as cigarette auxiliary material, in tobacco industry
In occupy more important status.Before 20 years, cigarette bobbin paper only serves a kind of, is exactly the volume in 5000~6000/min of speed
Bag pipe tobacco is rolled up on cigarette machine, makes a kind of solid intact cigarette.Seen as cigarette quality improves constantly, Smoking is harmful to your health
Thought is rooted in the hearts of the people and the appearance of various countries' limitation coke tar in cigarette laws and regulations, people it is also proposed many new want to cigarette bobbin paper
Ask, while such as meeting smoking quality, attractive appearance is provided, it is also necessary to reduce flue gas (master, effluent) harmful components and reduce and fire
Burn igniting property of cigarette etc..Cigarette bobbin paper is quantitatively generally 25~30g/m2, the 5% of cigarette gross mass is accounted for, main component is day
Right fiber.Cigarette bobbin paper directly participates in burning, and flue gas composition is influenceed in combustion huge.Current most of cigarette bobbin papers
Xylon gas can be all produced in burning and enter main flume, so as to reduce the suction quality of cigarette.By improveing cigarette paper, drop
Xylon gas caused by low cigarette bobbin paper burning are a measures for lifting cigarette smoking quality well.
The content of the invention
It is an object of the invention to provide a kind of additive for reducing cigarette bobbin paper xylon gas and its preparation and application, the addition
Agent can improve cigarette bobbin paper performance, reduce xylon gas caused by cigarette bobbin paper burning, lifting cigarette smoking quality.
Technical scheme provided by the invention is：A kind of additive for reducing cigarette bobbin paper xylon gas, is by following heavy
Measure the raw material composition of number：Pure tobacco oil light component 5-15 parts, cedar wood oil 0.05-0.2 parts, guaiacol 0.004-0.01 parts,
β-damascone 0.3-0.7 parts, dihydrocoumarin 1-6 parts, Ethyl vanillin 2-5 parts, alcohol 55-95 parts.
The gross weight number of above-mentioned substance is 100 parts by weight；
Wherein：Wherein described pure tobacco oil light component be by tobacco leaf through 10-20 times of concentration be 50%-70% alcohol in temperature
After spending to extract 1-3 hours under conditions of 50 DEG C -70 DEG C, it is 1.1-1.4 to be concentrated into relative density, obtains tobacco extract, then
It is to be filtered after 90%-99% alcohol mixes half an hour by 3-6 times of concentration of gained tobacco extract and its weight, takes clear liquid to concentrate
It is 0.9-1.2 to relative density, obtains pure tobacco oil, gained pure tobacco oil is distilled through molecular distillation equipment to obtain 40-60 DEG C
Cut is pure tobacco oil light component；The temperature concentrated twice is 50 DEG C -80 DEG C；The tobacco leaf can be all tobacco leaves, than
Such as flue-cured tobacco, suncured tabacco, air-curing of tobacco leaves；
The concentration of the alcohol is 90%-99%, preferably 95% alcohol (surplus is water).
The present invention preferably technical scheme, the additive for reducing cigarette bobbin paper xylon gas is by following parts by weight
Raw material forms：6 parts of pure tobacco oil light component, 0.05 part of cedar wood oil, 0.004 part of guaiacol, 0.6 part of β-damascone, two
Hydrogen coumarin 1 part, 2 parts of Ethyl vanillin, 90.346 parts of alcohol.
Preferably, the molecular distillation of the pure tobacco oil is divided into the scraper plate rotating speed of two-stage, wherein first order molecular distillation
For 20 rpms, pan feeding speed is 20 per minute, the vacuum 80pa of drop, under the conditions of temperature is 40 DEG C；Take first order molecule
The steaming excess of distillation carries out second level molecular distillation, and the temperature of second level molecular distillation is 60 DEG C, other conditions and the first fraction
The condition of son distillation is identical, collects the component that second level molecular distillation goes out, as described pure tobacco oil light component.
β-the damascone is called second position damascone, β-dihydro turkone, typically oxidized using β-ionol
Unsaturated dihydric alcohol is obtained, is then handled and got product with formic acid.
A kind of preparation method of additive for reducing cigarette bobbin paper xylon gas provided by the invention, it is characterised in that specific step
It is rapid as follows：
(1) by tobacco leaf through the alcohol that 10-20 times of concentration is 50%-70% be 50 DEG C -70 DEG C in temperature under conditions of extract
After 1-3 hours, it is 1.1-1.4 to be concentrated into relative density, obtains tobacco extract, then by gained tobacco extract and its weight 3-6
Times concentration is to be filtered after 90%-99% alcohol mixes half an hour, and it is 0.9-1.2 to take clear liquid to be concentrated into relative density, is obtained
Pure tobacco oil；The temperature concentrated twice is 50 DEG C -80 DEG C；
(2) pure tobacco oil of the preparation in step (1) is steamed into volatile light component by first order molecular distillation, then
The steaming excess of first order molecular distillation is subjected to second level molecular distillation, collects the component that second level molecular distillation goes out, as institute
State pure tobacco oil light component；Wherein the scraper plate rotating speed of first order molecular distillation and second level molecular distillation is 20 rpms, is entered
It is 20 per minute, the vacuum 80pa of drop to expect speed；The temperature of first order molecular distillation is 40 DEG C, the temperature of second level molecular distillation
Spend for 60 DEG C；
(3) additive raw material is prepared according to following parts by weight：The pure tobacco oil light component 5-15 prepared in step (2)
Part, cedar wood oil 0.05-0.2 parts, guaiacol 0.004-0.01 parts, β-damascone 0.3-0.7 parts, dihydrocoumarin 1-6
Part, Ethyl vanillin 2-5 parts, alcohol 55-95 parts；
(4) alcohol in above-mentioned raw materials is placed in blend tank, then remaining composition is accurately weighed and added by above-mentioned parts by weight
Enter blend tank, stand 24-48 hours after stirring 2-3 hours, be reduced the additive of cigarette bobbin paper xylon gas.
A kind of application of additive for reducing cigarette bobbin paper xylon gas provided by the invention, it is characterised in that：By above-mentioned drop
The additive of low cigarette bobbin paper xylon gas is sprayed on cigarette bobbin paper surface according to the 0.1-1%'s of cigarette bobbin paper gross weight；Specifically
It is that the spray process point of the additive in cigarette bobbin paper production process is sprayed.
Additive in the present invention is gone out using two kinds of natural perfume materials and four kinds of synthetic perfumes as material allocation, and by certain ratio
Example is sprayed at cigarette paper, and its specific advantage is as follows：
1. the additive raw material colourity is shallow, the additive modulated close to colourless, do not deposit by the cigarette bobbin paper after spraying
In the aberration problem caused by spraying inequality；
2. the fragrance matter contained in the additive, which has, covers and merges xylon gas caused by cigarette bobbin paper burning
Effect, so as to reach the effect for mitigating xylon gas；
3. the additive coating, compared to pipe tobacco is put on, has the characteristics of with strong points, to xylon gas in cigarette paper
Effect is covered to be better than putting on pipe tobacco；
After on heretofore described additive coating to cigarette paper, xylon gas caused by the cigarette bobbin paper burning
It is significantly less than regular-size cigarette obbbin, the cigarette that can assign cigarette pleasant smells perfume (or spice).
Embodiment
With reference to specific embodiment, the present invention is described in further detail, but embodiment is not to skill of the present invention
The restriction of art scheme.
The preparation process of pure tobacco oil light component in the embodiment：By tobacco leaf, through 15 times of 70% alcohol, (surplus is
Water) extracted 2 hours with 50 DEG C, it is 1.3 that extract solution is concentrated into relative density, and thickening temperature is 50 DEG C, obtains tobacco extract, so
(whipping temp is filtered after gained tobacco extract and 95% alcohol (surplus is water) of 5 times of its weight are mixed into half an hour afterwards
No requirement (NR)), it is 1.1 to take clear liquid to be concentrated into relative density at 50 DEG C, obtains pure tobacco oil；Pure tobacco oil is passed through into first order molecule
Volatile light component is steamed, then the steaming excess of first order molecular distillation is subjected to second level molecular distillation, collects second
The component that level molecule distills out, as described pure tobacco oil light component；Wherein first order molecular distillation and second level molecular distillation
Scraper plate rotating speed be 20 rpms, pan feeding speed be 20 drip per minute, vacuum 80pa；The temperature of first order molecular distillation
For 40 DEG C, the temperature of second level molecular distillation is 60 DEG C.
A kind of embodiment one, preparation method for the additive for reducing cigarette bobbin paper xylon gas, is comprised the following steps that：
(1) raw material is weighed according to following parts by weight：6 parts of pure tobacco oil light component, 0.05 part of cedar wood oil, guaiacol
0.004 part, 0.6 part of β-damascone, 1 part of dihydrocoumarin, 2 parts of Ethyl vanillin, 90.346 parts of alcohol；
(2) alcohol during above-mentioned raw materials are formulated is placed in blend tank, then remaining composition is accurately weighed by above-mentioned parts by weight
And blend tank is added, stir 2 hours, stand 24 hours, be reduced the additive of cigarette bobbin paper xylon gas.
By the additive for reducing cigarette bobbin paper xylon gas prepared in embodiment one in cigarette bobbin paper production additive spray
Process point is sprayed on cigarette bobbin paper surface with ratio of the weight than 0.1%, obtains the cigarette bobbin paper one.
A kind of embodiment two, preparation method for the additive for reducing cigarette bobbin paper xylon gas, is comprised the following steps that：
(1) raw material is weighed according to following parts by weight：8 parts of pure tobacco oil light component, 0.06 part of cedar wood oil, guaiacol
0.005 part, 0.5 part of β-damascone, 2 parts of dihydrocoumarin, 3 parts of Ethyl vanillin, 86.435 parts of alcohol；
(2) alcohol during above-mentioned raw materials are formulated is placed in blend tank, then remaining composition is accurately weighed by above-mentioned parts by weight
And blend tank is added, stir 2 hours, stand 24 hours, be reduced the additive of cigarette bobbin paper xylon gas.
By the additive for reducing cigarette bobbin paper xylon gas prepared in embodiment two in cigarette bobbin paper production additive spray
Process point is sprayed on cigarette bobbin paper surface with ratio of the weight than 0.15%, obtains the cigarette bobbin paper two.
A kind of embodiment three, preparation method for the additive for reducing cigarette bobbin paper xylon gas, is comprised the following steps that：
(1) raw material is weighed according to following parts by weight：7 parts of pure tobacco oil light component, 0.07 part of cedar wood oil, guaiacol
0.008 part, 0.3 part of β-damascone, 5 parts of dihydrocoumarin, 2 parts of Ethyl vanillin, 85.622 parts of alcohol；
(2) alcohol during above-mentioned raw materials are formulated is placed in blend tank, then remaining composition is accurately weighed by above-mentioned parts by weight
And blend tank is added, stir 3 hours, stand 48 hours, be reduced the additive of cigarette bobbin paper xylon gas.
By the additive for reducing cigarette bobbin paper xylon gas prepared in embodiment three in cigarette bobbin paper production additive spray
Process point is sprayed on cigarette bobbin paper surface with ratio of the weight than 0.5%, obtains the cigarette bobbin paper three.
A kind of embodiment four, preparation method for the additive for reducing cigarette bobbin paper xylon gas, is comprised the following steps that：
(1) raw material is weighed according to following parts by weight：6 parts of pure tobacco oil light component, 0.1 part of cedar wood oil, guaiacol
0.004 part, 0.3 part of β-damascone, 2 parts of dihydrocoumarin, 3 parts of Ethyl vanillin, 88.596 parts of alcohol；
(2) alcohol during above-mentioned raw materials are formulated is placed in blend tank, then remaining composition is accurately weighed by above-mentioned parts by weight
And blend tank is added, stir 2.5 hours, stand 24 hours, be reduced the additive of cigarette bobbin paper xylon gas.
By the additive for reducing cigarette bobbin paper xylon gas prepared in example IV in cigarette bobbin paper production additive spray
Process point is sprayed on cigarette bobbin paper surface with ratio of the weight than 0.1%, obtains the cigarette bobbin paper four.
The present invention on the index involved by the physical property and cigarette processing process of cigarette bobbin paper substantially without influence, completely
Technological requirement during Cigarette processing can be met.
Cigarette bobbin paper technic index is shown in Table 1.
The cigarette bobbin paper technic index of table 1
Cigarette bobbin paper involved in the present invention is significantly less than regular-size cigarette obbbin in xylon gas caused by burning, and its sense organ is commented
Inhale quality and be shown in Table 2.
The cigarette product sensory quality assessment of table 2
Claims (3)
1. a kind of preparation method for the additive for reducing cigarette bobbin paper xylon gas, it is characterised in that comprise the following steps that：
(1) by tobacco leaf through the alcohol that 10-20 times of concentration is 50%-70% be 50 DEG C -70 DEG C in temperature under conditions of extract 1-3 it is small
Shi Hou, it is 1.1-1.4 to be concentrated into relative density, obtains tobacco extract, then by gained tobacco extract and 3-6 times of concentration of its weight
Filtered after mixing half an hour for 90%-99% alcohol, it is 0.9-1.2 to take clear liquid to be concentrated into relative density, and it is net to obtain tobacco
Oil；The temperature concentrated twice is 50 DEG C -80 DEG C；
(2) pure tobacco oil of the preparation in step (1) is steamed into volatile light component by first order molecular distillation, then by
The steaming excess of first order molecular distillation carries out second level molecular distillation, collects the component that second level molecular distillation goes out, as described cigarette
Careless absolute oil light component；Wherein the scraper plate rotating speed of first order molecular distillation and second level molecular distillation is 20 rpms, pan feeding speed
Spend and drip per minute, vacuum 80pa for 20；The temperature of first order molecular distillation is 40 DEG C, and the temperature of second level molecular distillation is
60℃；
(3) additive raw material is prepared according to following parts by weight：The pure tobacco oil light component 5-15 parts prepared in step (1), cypress
Wood oil 0.05-0.2 parts, guaiacol 0.004-0.01 parts, β-damascone 0.3-0.7 parts, dihydrocoumarin 1-6 parts, second
Base vanillic aldehyde 2-5 parts, alcohol 55-95 parts；
(4) alcohol in above-mentioned raw materials is placed in blend tank, then remaining composition is accurately weighed by above-mentioned parts by weight and adds tune
Distribution tank, 24-48 hours are stood after stirring 2-3 hours, are reduced the additive of cigarette bobbin paper xylon gas.
2. a kind of application of the additive for reducing cigarette bobbin paper xylon gas prepared by method according in claim 1, its feature
It is：The additive of above-mentioned reduction cigarette bobbin paper xylon gas is sprayed on cigarette according to the 0.1-1% of cigarette bobbin paper gross weight
Obbbin surface.
A kind of 3. application of additive for reducing cigarette bobbin paper xylon gas according to claim 2, it is characterised in that：It is described
The additive for reducing cigarette bobbin paper xylon gas is the spray process point spraying of the additive in cigarette bobbin paper production process.
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| CN201610900959.XA CN106638160B (en) | 2016-10-14 | 2016-10-14 | A kind of additive for reducing cigarette bobbin paper xylon gas and its preparation method and application |
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| CN201610900959.XA CN106638160B (en) | 2016-10-14 | 2016-10-14 | A kind of additive for reducing cigarette bobbin paper xylon gas and its preparation method and application |
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| CN107510090B (en) * | 2017-08-16 | 2019-03-19 | 湖北中烟工业有限责任公司 | A kind of preparation method and applications for the additive inhibiting burley tobaccos bitter taste |
| CN108395932A (en) * | 2018-03-29 | 2018-08-14 | 武汉黄鹤楼香精香料有限公司 | A kind of preparation method of cigarette jasmine oil |
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| CN1181169C (en) * | 2002-09-13 | 2004-12-22 | 云南瑞升科技有限公司 | Method for preparing pure tobacco oil |
| CN102119784B (en) * | 2011-02-23 | 2013-05-01 | 红云红河烟草(集团)有限责任公司 | Spice extractum prepared by waste tobacco leaf, preparation method thereof and application thereof |
| CN102911789B (en) * | 2012-11-21 | 2014-03-26 | 红塔烟草(集团)有限责任公司 | Baked-smell tobacco essence and preparation method and application thereof |
| CN103923747B (en) * | 2014-04-24 | 2016-03-30 | 川渝中烟工业有限责任公司 | Essence on cigarette tissue |
| CN104856216A (en) * | 2015-05-31 | 2015-08-26 | 中国烟草总公司郑州烟草研究院 | Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette |
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