CN103181613A - Preparation method of electric dry distillation type tobacco sheet - Google Patents
Preparation method of electric dry distillation type tobacco sheet Download PDFInfo
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- CN103181613A CN103181613A CN2013101230504A CN201310123050A CN103181613A CN 103181613 A CN103181613 A CN 103181613A CN 2013101230504 A CN2013101230504 A CN 2013101230504A CN 201310123050 A CN201310123050 A CN 201310123050A CN 103181613 A CN103181613 A CN 103181613A
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- tobacco
- reconstituted tobacoo
- sheet base
- preparation
- extract
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 133
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 129
- 238000000197 pyrolysis Methods 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 239000000284 extract Substances 0.000 claims abstract description 68
- 239000007921 spray Substances 0.000 claims abstract description 31
- 239000002304 perfume Substances 0.000 claims abstract description 11
- 238000001035 drying Methods 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims abstract description 4
- 239000000419 plant extract Substances 0.000 claims abstract description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 55
- MDYZKJNTKZIUSK-UHFFFAOYSA-N tyloxapol Chemical compound O=C.C1CO1.CC(C)(C)CC(C)(C)C1=CC=C(O)C=C1 MDYZKJNTKZIUSK-UHFFFAOYSA-N 0.000 claims description 36
- 235000013599 spices Nutrition 0.000 claims description 35
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 20
- 235000011187 glycerol Nutrition 0.000 claims description 10
- 239000008367 deionised water Substances 0.000 claims description 9
- 229910021641 deionized water Inorganic materials 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 9
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 238000000605 extraction Methods 0.000 claims description 6
- 235000012054 meals Nutrition 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 235000019506 cigar Nutrition 0.000 claims description 4
- 238000010992 reflux Methods 0.000 claims description 4
- 239000011248 coating agent Substances 0.000 abstract description 13
- 238000000576 coating method Methods 0.000 abstract description 13
- 238000000034 method Methods 0.000 abstract description 13
- 235000019504 cigarettes Nutrition 0.000 abstract description 12
- 239000000126 substance Substances 0.000 abstract description 6
- 239000000796 flavoring agent Substances 0.000 abstract description 5
- 230000006378 damage Effects 0.000 abstract description 4
- 239000003205 fragrance Substances 0.000 abstract description 4
- 235000019634 flavors Nutrition 0.000 abstract description 3
- 238000002485 combustion reaction Methods 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000000779 smoke Substances 0.000 abstract 1
- 230000000391 smoking effect Effects 0.000 abstract 1
- 238000005507 spraying Methods 0.000 abstract 1
- 238000005303 weighing Methods 0.000 description 7
- 239000012141 concentrate Substances 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 5
- 102000011759 adducin Human genes 0.000 description 4
- 108010076723 adducin Proteins 0.000 description 4
- 238000009833 condensation Methods 0.000 description 4
- 230000005494 condensation Effects 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 3
- 230000008929 regeneration Effects 0.000 description 3
- 238000011069 regeneration method Methods 0.000 description 3
- 238000000889 atomisation Methods 0.000 description 2
- 235000013355 food flavoring agent Nutrition 0.000 description 2
- 210000000697 sensory organ Anatomy 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 150000002596 lactones Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
Abstract
The invention provides a preparation method of an electric dry distillation type tobacco sheet. The preparation method comprises the following steps of: (1) mixing one or more of a tobacco extract and a natural plant extract to obtain a sheet-based spray substance; (2) uniformly coating the sheet-based spray substance on a tobacco sheet base of which the weight is 1-10 times that of the sheet-based spray substance, and then drying the tobacco sheet base at 40-90 DEG C; (3) spraying an atomizing agent of which the weight is 2%-50% of that of the tobacco sheet base on the tobacco sheet base; and (4) drying the tobacco sheet base to obtain the electric dry distillation type tobacco sheet. The tobacco sheet prepared by the method disclosed by the invention can be combusted in an electric dry distilling device to generate smoke. The electric dry distillation way can dry-distill pure tobacco fragrance contained by a tobacco extract. The sheet prepared by the sheet preparation method integrates the pure fragrance of the tobacco with the tobacco flavor and perfume. The electric dry distillation type tobacco sheet satisfies the requirements of consumption, can be used for reducing the harm caused by combustion of cigarettes to consumers and preventing generation of passive smoking and has quite high practicability.
Description
Technical field
The present invention relates to a kind of preparation method of reconstituted tobacoo, specifically a kind of preparation method of electric destructive distillation type reconstituted tobacoo.
Background technology
Reconstituted tobacoo refers to that cigarette factory will comprise that tobacco dead meals such as tobacco dead meal in the cigarette manufacture process of beating the leaf operation such as offal, offal, tobacco leaf fragment, discarded tobacco leaf are as raw material, through reconfiguring the regeneration tobacco leaf that processes.The conventional regeneration reconstituted tobacoo is that the regeneration tobacco leaf is mixed the mode with addition of the worker through processing and tobacco, rolls into cigarette, can improve the utilization rate of raw tobacco material.Because the needed reconstituted tobacoo material of destructive distillation type cigarette will have certain thickness, can soak into the material of effumabilities such as certain density essence and flavoring agent and glycerine.And the reconstituted tobacoo that general technology is produced, the sheet base thickness of reconstituted tobacco sheet and the concentrate of interpolation all can not satisfy the demand of electric destructive distillation type cigarette,
Summary of the invention
The objective of the invention is to provide according to the deficiencies in the prior art a kind of preparation method of electric destructive distillation type reconstituted tobacoo, the electric destructive distillation type reconstituted tobacoo for preparing with this preparation method has certain thickness, can be under lower temperature, temperature destructive distillation by lower electric destructive distillation goes out essence and flavoring agent and some the volatile fragrance matters that add in the reconstituted tobacoo, satisfies the needs of electric destructive distillation type cigarette.
The present invention is achieved through the following technical solutions: a kind of preparation method of electric destructive distillation type reconstituted tobacoo, and its step comprises: (1) obtains sheet base spray with one or more mixing in tobacco extract and the natural plant extracts; (2) it is dry down at 40-90 ℃ then on the sheet base spray 1-10 reconstituted tobacoo sheet base doubly sheet base spray being uniformly coated on weight again; (3) be that the glycerine of propane diols, the 10-45% of 20-75%, the deionized water of 1-10%, the alcohol of 1-10%, the flavouring essence for tobacco of 1-10% and the tobacco extract of 1-10% mix atomized dose of spices according to percetage by weight then, the Alevaire spices of the 2-50% of reconstituted tobacoo sheet basic weight amount is sprayed on the dry good reconstituted tobacoo sheet base; This is because the temperature of electric destructive distillation cigarette is lower, do not reach more than 600 ℃ of cigarette burning, in suction, reconstituted tobacoo can not burn, need the fragrance matter destructive distillation in the tobacco product be come out by heating, for simulate the result of combustion of tobacco process haze effect, need auxiliary some Alevaire spices of interpolation, be convenient to produce visible smog; (4) obtain described electric destructive distillation type reconstituted tobacoo after at last reconstituted tobacoo sheet backbone is dry.
Preferably, described reconstituted tobacoo sheet base thickness is 0.1-0.5mm.
Preferred, described reconstituted tobacoo sheet base thickness is 0.2-0.4mm.
Described tobacco extract is one or more extracts in airing tobacco extract, Turkish tobaccos extract, flue-cured tobacco extract, burley tobaccos extract, cigar extract and the tobacco dead meal extract.Described tobacco extract can extract separately, mainly is the taste for the reconstituted tobacoo of coordinating to process, and concrete actual demand is allocated according to actual.
A kind of extraction of described tobacco extract in the following way: (1) is 95% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:2-5 mixes, be preferably 1:3, be immersed in 1 week of drying at room temperature place, refilter at the concentrated tobacco extract that obtains below 50 ℃, the composition that this method of this method soaks out is mainly some light components, keeps the suction flavor of tobacco light component; (2) be 75% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:2-5 mixes, be preferably 1:3, be immersed in 1 week of drying at room temperature place, refilter at the concentrated tobacco extract that obtains below 50 ℃, the composition that this method soaks out is mainly some light components, keeps the suction flavor of big polar substances in the tobacco light component; (3) be 95% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:1-4 mixes, be preferably 1:2, add hot reflux 1-4 hour, preferred 2 hours, refilter at the concentrated tobacco extract that obtains below 50 ℃, this method can be extracted the pure soluble substance in the tobacco largely, and higher temperature is extracted volatile material in the tobacco light component is caused damage; (4) be 75% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:1-4 mixes, be preferably 1:2, add hot reflux 1-4 hour, preferred 2 hours, refilter at the concentrated tobacco extract that obtains below 50 ℃, this method can be extracted the big polar substances in the tobacco largely, and higher temperature is extracted volatile material in the tobacco light component is caused damage.
In the described step (4) at last with reconstituted tobacoo sheet backbone dry refer to 25 ℃ down shady and cool dry place placed 2 hours.
The dry good basic spray content of reconstituted tobacoo sheet base last slice is 150-250g/m in the described step (1)
2, thickness is 0.3-0.4mm, the content of moisture is 10-12%.
Preferably, in the described step (1) sheet base spray being uniformly coated on weight is on the sheet base spray 2-8 reconstituted tobacoo sheet base doubly.
Preferably, be that Alevaire spices with the 5-45% of reconstituted tobacoo sheet basic weight amount is sprayed on the reconstituted tobacoo sheet base in the described step (3).
Flavouring essence for tobacco in the described step (3) comprises natural perfume material or artificial synthetic perfume.As: hydro carbons, alcohols, ethers, phenols, sulfur-containing compound, volatility amine, aldehydes, ketone, carboxylic acids, lactone or heterocycles.
A kind of preparation method's optimal technical scheme of electric destructive distillation type reconstituted tobacoo is: its step comprises: (1) obtains sheet base spray with one or more mixing in tobacco extract and the natural plant extracts; (2) it is dry under 50-70 ℃ then on the sheet base spray 2-8 reconstituted tobacoo sheet base doubly sheet base spray being uniformly coated on weight again, and the basic spray content of reconstituted tobacoo sheet base last slice that obtains is 150-250g/m
2, thickness is 0.3-0.4mm, the content of moisture is 10-12%; (3) be that the glycerine of propane diols, the 10-45% of 20-75%, the deionized water of 1-10%, the alcohol of 1-10%, the flavouring essence for tobacco of 1-10% and the tobacco extract of 1-10% mix atomized dose of spices according to percetage by weight then, the Alevaire spices of the 5-45% of reconstituted tobacoo sheet basic weight amount is sprayed on the dry good reconstituted tobacoo sheet base; (4) at last reconstituted tobacoo sheet base shady and cool dry place under 25 ℃ was placed 2 hours, obtain described electric destructive distillation type reconstituted tobacoo after the drying.
The reconstituted tobacoo that the preparation method of electric destructive distillation type reconstituted tobacoo provided by the invention prepares can burn in electric destructive distillation device and produces smog.The mode of electricity destructive distillation can destructive distillation go out this perfume (or spice) of tobacco that tobacco extract comprises.The thin slice of this kind thin sheet preparation technique preparation has this perfume of tobacco and essence spice for cigarette one integrated mass.Satisfy the demand of consumption, reduce cigarette burning to consumer's harm, avoid the generation of second-hand-cigarette, have very strong practicality.
The specific embodiment
Below further specify the present invention by specific embodiment:
Embodiment 1
(1) takes by weighing cured tobacco leaf 100g, add 95% ethanol 300g, be placed under the room temperature and soaked for 1 week.Filter out tobacco leaf then, concentrate below 50 ℃, obtain tobacco extract.
(2) tobacco extract after will extracting is coated on the reconstituted tobacoo sheet base that thickness is 0.2mm, every 100g tobacco extract coating reconstituted tobacoo sheet base 400g, 40 ℃ dry down, obtaining reconstituted tobacoo sheet base spray content is 200g/m
2, thickness is 0.35mm, moisture is 11%.
(3) percentage is by weight: propane diols 65%, and glycerine 15%, deionized water 3%, alcohol 5%, natural perfume material 6%, tobacco extract 6% mixes atomized dose of spices.Then Alevaire spices is sprayed on the reconstituted tobacoo sheet base that is coated with tobacco extract, coating weight is that the amount of 100g reconstituted tobacoo sheet base sprinkling Alevaire spices is 15g, i.e. the amount of 15% Alevaire spices.
(4) placed 2 hours at the reconstituted tobacoo sheet base shady and cool dry place under 25 ℃ that will spray Alevaire, can guarantee that Alevaire soaks in the reconstituted tobacoo preferably, obtains electric destructive distillation type reconstituted tobacoo 1.
Embodiment 2
(1) takes by weighing airing cigarette tobacco leaf 100g, add 75% ethanol 200g, be placed under the room temperature and soaked for 1 week.Filter out tobacco leaf then, concentrate below 50 ℃, obtain tobacco extract.
(2) tobacco extract after will extracting is coated on the reconstituted tobacoo sheet base that thickness is 0.1mm, every 100g tobacco extract coating reconstituted tobacoo sheet base 100g, 50 ℃ dry down, obtaining reconstituted tobacoo sheet base spray content is 250g/m
2, thickness is 0.3mm, moisture is 10%.
(3) percentage is by weight: propane diols 75%, and glycerine 10%, deionized water 1%, alcohol 10%, artificial synthetic perfume 1%, tobacco extract 5% mixes atomized dose of spices.Then Alevaire spices is sprayed on the reconstituted tobacoo sheet base that is coated with tobacco extract, coating weight is that the amount of 100g reconstituted tobacoo sheet base sprinkling Alevaire spices is 50g, i.e. the amount of 50% Alevaire spices.
(4) placed 2 hours at the reconstituted tobacoo sheet base shady and cool dry place under 25 ℃ that will spray Alevaire, can guarantee that Alevaire soaks in the reconstituted tobacoo preferably, obtains electric destructive distillation type reconstituted tobacoo 2.
Embodiment 3
(1) take by weighing burley tobaccos tobacco leaf 100g, add 95% ethanol 200g, extraction is 1-4 hour under the heating condensation counterflow condition.Filter out tobacco leaf then, concentrate below 50 ℃, obtain tobacco extract.
(2) tobacco extract after will extracting is coated on the reconstituted tobacoo sheet base that thickness is 0.4mm, every 100g tobacco extract coating reconstituted tobacoo sheet base 1000g, 70 ℃ dry down, obtaining reconstituted tobacoo sheet base spray content is 150g/m
2, thickness is 0.4mm, moisture is 12%.
(3) percentage is by weight: propane diols 20%, and glycerine 45%, deionized water 10%, alcohol 5%, natural perfume material 10%, tobacco extract 10% mixes atomized dose of spices.Then Alevaire spices is sprayed on the reconstituted tobacoo sheet base that is coated with tobacco extract, coating weight is that the amount of 100g reconstituted tobacoo sheet base sprinkling Alevaire spices is 2g, i.e. the amount of 2% Alevaire spices.
(4) placed 2 hours at the reconstituted tobacoo sheet base shady and cool dry place under 25 ℃ that will spray Alevaire, can guarantee that Alevaire soaks in the reconstituted tobacoo preferably, obtains electric destructive distillation type reconstituted tobacoo 3.
Embodiment 4
(1) take by weighing burley tobaccos tobacco leaf and Turkish tobaccos tobacco leaf 100g altogether, add 75% ethanol 200g, extraction is 1-4 hour under the heating condensation counterflow condition.Filter out tobacco leaf then, concentrate below 50 ℃, obtain tobacco extract.
(2) tobacco extract after will extracting is coated on the reconstituted tobacoo sheet base that thickness is 0.5mm, every 100g tobacco extract coating reconstituted tobacoo sheet base 200g, 90 ℃ dry down, obtaining reconstituted tobacoo sheet base spray content is 200g/m
2, thickness is 0.4mm, moisture is 12%.
(3) percentage is by weight: propane diols 58%, and glycerine 30%, deionized water 5%, alcohol 1%, artificial synthetic perfume 5%, tobacco extract 1% mixes atomized dose of spices.Then Alevaire spices is sprayed on the reconstituted tobacoo sheet base that is coated with tobacco extract, coating weight is that the amount of 100g reconstituted tobacoo sheet base sprinkling Alevaire spices is 45g, i.e. the amount of 45% Alevaire spices.
(4) placed 2 hours at the reconstituted tobacoo sheet base shady and cool dry place under 25 ℃ that will spray Alevaire, can guarantee that Alevaire soaks in the reconstituted tobacoo preferably, obtains electric destructive distillation type reconstituted tobacoo 4.
Embodiment 5
(1) take by weighing cigar tobacco leaf and tobacco dead meal 100g altogether, add 75% ethanol 200g, extraction is 1-4 hour under the heating condensation counterflow condition.Filter out tobacco leaf then, concentrate below 50 ℃, obtain tobacco extract.
(2) tobacco extract after will extracting is coated on the reconstituted tobacoo sheet base that thickness is 0.5mm, every 100g tobacco extract coating reconstituted tobacoo sheet base 200g, 90 ℃ dry down, obtaining reconstituted tobacoo sheet base spray content is 200g/m
2, thickness is 0.4mm, moisture is 12%.
(3) percentage is by weight: propane diols 58%, and glycerine 30%, deionized water 5%, alcohol 1%, flavouring essence for tobacco 5%, tobacco extract 1% mixes atomized dose of spices.Then Alevaire spices is sprayed on the reconstituted tobacoo sheet base that is coated with tobacco extract, coating weight is that the amount of 100g reconstituted tobacoo sheet base sprinkling Alevaire spices is 45g, i.e. the amount of 45% Alevaire spices.
(4) placed 2 hours at the reconstituted tobacoo sheet base shady and cool dry place under 25 ℃ that will spray Alevaire, can guarantee that Alevaire soaks in the reconstituted tobacoo preferably, obtains electric destructive distillation type reconstituted tobacoo 5.
Embodiment 6
(1) takes by weighing cured tobacco leaf 100g, add 95% ethanol 300g, be placed under the room temperature and soaked for 1 week.Filter out tobacco leaf then, concentrating below 50 ℃, obtain tobacco extract
Take by weighing cigar tobacco leaf 100g, add 95% ethanol 200g, extraction is 2 hours under the heating condensation counterflow condition, cools off, filters out tobacco leaf, concentrating below 50 ℃, obtains certain density immersion flue-cured tobacco tobacco extract, and is standby.
(2) after the ratio allotment of tobacco extract according to 1:1 with two kinds of extracting methods, be coated on the reconstituted tobacoo sheet base, every 100g tobacco extract coating reconstituted tobacoo 400g, dry under 70 ℃, obtaining reconstituted tobacoo sheet base spray content is 200g/m
2, thickness is 0.4mm, moisture is 11%.
(3) percentage is by weight: propane diols 58%, and glycerine 30%, deionized water 5%, alcohol 1%, flavouring essence for tobacco 5%, tobacco extract 1% mixes atomized dose of spices.Then Alevaire spices is sprayed on the reconstituted tobacoo sheet base that is coated with tobacco extract, coating weight is that the amount of 100g reconstituted tobacoo sheet base sprinkling Alevaire spices is 45g, i.e. the amount of 45% Alevaire spices.
(4) placed 2 hours at the reconstituted tobacoo sheet base shady and cool dry place under 25 ℃ that will spray Alevaire, can guarantee that Alevaire soaks in the reconstituted tobacoo preferably, obtains electric destructive distillation type reconstituted tobacoo 6.
Carry out sense organ and atomization quantity evaluation in the electric destructive distillation device with being placed on after the above-mentioned reconstituted tobacoo chopping, the result who obtains is as shown in table 1.
Sense organ and the atomization quantity evaluation of table 1 reconstituted tobacoo in electric destructive distillation device
From above-mentioned evaluation as can be seen, the electric destructive distillation type reconstituted tobacoo sensory effects for preparing of the inventive method is good.
Claims (10)
1. the preparation method of an electric destructive distillation type reconstituted tobacoo, its step comprises: (1) obtains sheet base spray with one or more mixing in tobacco extract and the natural plant extracts; (2) it is dry down at 40-90 ℃ then on the sheet base spray 1-10 reconstituted tobacoo sheet base doubly sheet base spray being uniformly coated on weight again; (3) be that the glycerine of propane diols, the 10-45% of 20-75%, the deionized water of 1-10%, the alcohol of 1-10%, the flavouring essence for tobacco of 1-10% and the tobacco extract of 1-10% mix atomized dose of spices according to percetage by weight then, the Alevaire spices of the 2-50% of reconstituted tobacoo sheet basic weight amount is sprayed on the dry good reconstituted tobacoo sheet base; (4) obtain described electric destructive distillation type reconstituted tobacoo after at last reconstituted tobacoo sheet backbone is dry.
2. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: described reconstituted tobacoo sheet base thickness is 0.1-0.5mm.
3. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 2, it is characterized in that: described reconstituted tobacoo sheet base thickness is 0.2-0.4mm.
4. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: described tobacco extract is one or more extracts in airing tobacco extract, Turkish tobaccos extract, flue-cured tobacco extract, burley tobaccos extract, cigar extract and the tobacco dead meal extract.
5. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: a kind of extraction of described tobacco extract in the following way: (1) is 95% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:2-5 mixes, be immersed in 1 week of drying at room temperature place, refilter at the concentrated tobacco extract that obtains below 50 ℃; (2) be 75% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:2-5 mixes, and is immersed in 1 week of drying at room temperature place, refilters concentrating below 50 ℃ and obtains tobacco extract; (3) be 95% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:1-4 mixes, and adds hot reflux 1-4 hour, refilters concentrating below 50 ℃ and obtains tobacco extract; (4) be 75% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:1-4 mixes, and adds hot reflux 1-4 hour, refilters concentrating below 50 ℃ and obtains tobacco extract.
6. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: in the described step (4) at last with reconstituted tobacoo sheet backbone dry refer to 25 ℃ down shady and cool dry place placed 2 hours.
7. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: the dry good basic spray content of reconstituted tobacoo sheet base last slice is 150-250g/m in the described step (1)
2, thickness is 0.3-0.4mm, the content of moisture is 10-12%.
8. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: in the described step (1) sheet base spray being uniformly coated on weight is on the sheet base spray 2-8 reconstituted tobacoo sheet base doubly.
9. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: be that Alevaire spices with the 5-45% of reconstituted tobacoo sheet basic weight amount is sprayed on the reconstituted tobacoo sheet base in the described step (3).
10. the preparation method of the described electric destructive distillation type reconstituted tobacoo of described claim 1 is characterized in that: the flavouring essence for tobacco in the described step (3) comprises natural perfume material or artificial synthetic perfume.
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| CN201310123050.4A CN103181613B (en) | 2013-04-10 | 2013-04-10 | A kind of preparation method of electric destructive distillation type reconstituted tobacoo |
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| CN201310123050.4A CN103181613B (en) | 2013-04-10 | 2013-04-10 | A kind of preparation method of electric destructive distillation type reconstituted tobacoo |
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| CN103181613B CN103181613B (en) | 2015-10-21 |
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| CN103919268A (en) * | 2014-03-28 | 2014-07-16 | 广东中烟工业有限责任公司 | Cigarette without generating secondhand smoke |
| CN103919270A (en) * | 2014-03-28 | 2014-07-16 | 广东中烟工业有限责任公司 | Tobacco product |
| CN105219530A (en) * | 2015-10-08 | 2016-01-06 | 中烟施伟策（云南）再造烟叶有限公司 | A kind of tobacco spice preparation method reinforced for reconstituted tobacco |
| CN105996111A (en) * | 2016-07-20 | 2016-10-12 | 湖北中烟工业有限责任公司 | Fragrance-keeping method for increasing quality of tobacco leaves reprocessed through paper-making process |
| WO2017181685A1 (en) | 2016-04-20 | 2017-10-26 | 贵州中烟工业有限责任公司 | Method for manufacturing heat-not-burn tobacco substrate containing activated carbon |
| CN107319641A (en) * | 2017-07-21 | 2017-11-07 | 上海烟草集团有限责任公司 | A kind of tobacco fuming liquids for heating the tobacco product that do not burn and its production and use |
| CN109875096A (en) * | 2017-12-06 | 2019-06-14 | 湖北中烟工业有限责任公司 | A kind of reconstituted tobacoo charging technology of new tobacco products |
| AU2018204476A1 (en) * | 2018-05-12 | 2019-11-28 | Shenzhen Dakavape Tech Co., Ltd. | Dual-use cigarette and tobacco filler thereof |
| CN110679984A (en) * | 2019-11-15 | 2020-01-14 | 湖北中烟工业有限责任公司 | Preparation method of special slice for heating cigarettes |
| CN111096472A (en) * | 2018-10-10 | 2020-05-05 | 云南巴菰生物科技有限公司 | A synthetic tobacco shred containing Chinese herbal materials and its preparation method |
| JP2022510056A (en) * | 2019-11-20 | 2022-01-26 | ケーティー・アンド・ジー・コーポレーション | Aerosol-producing articles comprising a method and an apparatus for manufacturing an aerosol-producing rod and an aerosol-producing rod produced by the method and the apparatus. |
| ES2898232R1 (en) * | 2019-01-28 | 2022-03-09 | Broadfar Shanghai Man Consulting Co Ltd | HEATING CIGARETTE WITHOUT COMBUSTION AND METHOD OF MANUFACTURING THE SAME |
| CN114532573A (en) * | 2022-02-18 | 2022-05-27 | 上海烟草集团有限责任公司 | Auxiliary material spraying system and coating method for improving utilization rate of auxiliary materials of reconstituted tobacco |
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| CN103919270A (en) * | 2014-03-28 | 2014-07-16 | 广东中烟工业有限责任公司 | Tobacco product |
| CN103919268B (en) * | 2014-03-28 | 2016-03-30 | 广东中烟工业有限责任公司 | A kind of cigarette not producing second-hand-cigarette |
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| EP3263276A4 (en) * | 2016-04-20 | 2018-12-05 | China Tobacco Guizhou Industrial Co., Ltd. | Method for manufacturing heat-not-burn tobacco substrate containing activated carbon |
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| CN105996111A (en) * | 2016-07-20 | 2016-10-12 | 湖北中烟工业有限责任公司 | Fragrance-keeping method for increasing quality of tobacco leaves reprocessed through paper-making process |
| CN107319641A (en) * | 2017-07-21 | 2017-11-07 | 上海烟草集团有限责任公司 | A kind of tobacco fuming liquids for heating the tobacco product that do not burn and its production and use |
| CN109875096A (en) * | 2017-12-06 | 2019-06-14 | 湖北中烟工业有限责任公司 | A kind of reconstituted tobacoo charging technology of new tobacco products |
| AU2018204476A1 (en) * | 2018-05-12 | 2019-11-28 | Shenzhen Dakavape Tech Co., Ltd. | Dual-use cigarette and tobacco filler thereof |
| CN111096472A (en) * | 2018-10-10 | 2020-05-05 | 云南巴菰生物科技有限公司 | A synthetic tobacco shred containing Chinese herbal materials and its preparation method |
| ES2898232R1 (en) * | 2019-01-28 | 2022-03-09 | Broadfar Shanghai Man Consulting Co Ltd | HEATING CIGARETTE WITHOUT COMBUSTION AND METHOD OF MANUFACTURING THE SAME |
| CN110679984A (en) * | 2019-11-15 | 2020-01-14 | 湖北中烟工业有限责任公司 | Preparation method of special slice for heating cigarettes |
| JP2022510056A (en) * | 2019-11-20 | 2022-01-26 | ケーティー・アンド・ジー・コーポレーション | Aerosol-producing articles comprising a method and an apparatus for manufacturing an aerosol-producing rod and an aerosol-producing rod produced by the method and the apparatus. |
| JP7164269B2 (en) | 2019-11-20 | 2022-11-01 | ケーティー アンド ジー コーポレイション | Aerosol-generating articles and methods of making aerosol-generating rods |
| CN114532573A (en) * | 2022-02-18 | 2022-05-27 | 上海烟草集团有限责任公司 | Auxiliary material spraying system and coating method for improving utilization rate of auxiliary materials of reconstituted tobacco |
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