CN106617285B - A kind of discoloration tobacco aromaticss pearl and preparation method thereof - Google Patents
A kind of discoloration tobacco aromaticss pearl and preparation method thereof Download PDFInfo
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- CN106617285B CN106617285B CN201610854701.0A CN201610854701A CN106617285B CN 106617285 B CN106617285 B CN 106617285B CN 201610854701 A CN201610854701 A CN 201610854701A CN 106617285 B CN106617285 B CN 106617285B
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- 238000002845 discoloration Methods 0.000 title claims abstract description 47
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 241000208125 Nicotiana Species 0.000 title abstract description 20
- 239000000853 adhesive Substances 0.000 claims abstract description 54
- 230000001070 adhesive effect Effects 0.000 claims abstract description 54
- 239000003205 fragrance Substances 0.000 claims abstract description 37
- 239000007787 solid Substances 0.000 claims abstract description 32
- 239000000843 powder Substances 0.000 claims abstract description 30
- 239000011812 mixed powder Substances 0.000 claims abstract description 29
- 239000000686 essence Substances 0.000 claims abstract description 28
- 241000196324 Embryophyta Species 0.000 claims abstract description 25
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- 239000000049 pigment Substances 0.000 claims abstract description 23
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- 238000000576 coating method Methods 0.000 claims abstract description 14
- 238000005119 centrifugation Methods 0.000 claims abstract description 12
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- SEBIKDIMAPSUBY-ARYZWOCPSA-N Crocin Chemical compound C([C@H]1O[C@H]([C@@H]([C@@H](O)[C@@H]1O)O)OC(=O)C(C)=CC=CC(C)=C\C=C\C=C(/C)\C=C\C=C(C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)O1)O)O[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O SEBIKDIMAPSUBY-ARYZWOCPSA-N 0.000 claims description 3
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- 244000008991 Curcuma longa Species 0.000 claims description 3
- 240000000950 Hippophae rhamnoides Species 0.000 claims description 3
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- 235000017858 Laurus nobilis Nutrition 0.000 claims description 3
- 244000246386 Mentha pulegium Species 0.000 claims description 3
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 3
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 3
- 241000228347 Monascus <ascomycete fungus> Species 0.000 claims description 3
- 235000008708 Morus alba Nutrition 0.000 claims description 3
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- 235000007189 Oryza longistaminata Nutrition 0.000 claims description 3
- 240000007594 Oryza sativa Species 0.000 claims description 3
- 235000007164 Oryza sativa Nutrition 0.000 claims description 3
- 235000011751 Pogostemon cablin Nutrition 0.000 claims description 3
- 240000002505 Pogostemon cablin Species 0.000 claims description 3
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- 244000046109 Sorghum vulgare var. nervosum Species 0.000 claims description 3
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- 244000125380 Terminalia tomentosa Species 0.000 claims description 3
- 244000269722 Thea sinensis Species 0.000 claims description 3
- 244000299461 Theobroma cacao Species 0.000 claims description 3
- 235000007303 Thymus vulgaris Nutrition 0.000 claims description 3
- 240000002657 Thymus vulgaris Species 0.000 claims description 3
- 235000009754 Vitis X bourquina Nutrition 0.000 claims description 3
- 235000012333 Vitis X labruscana Nutrition 0.000 claims description 3
- 235000014787 Vitis vinifera Nutrition 0.000 claims description 3
- 240000006365 Vitis vinifera Species 0.000 claims description 3
- WRANYHFEXGNSND-LOFNIBRQSA-N capsanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CCC(O)C2(C)C WRANYHFEXGNSND-LOFNIBRQSA-N 0.000 claims description 3
- 235000018889 capsanthin Nutrition 0.000 claims description 3
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- 235000003373 curcuma longa Nutrition 0.000 claims description 3
- 239000000284 extract Substances 0.000 claims description 3
- 239000009627 gardenia yellow Substances 0.000 claims description 3
- 239000001056 green pigment Substances 0.000 claims description 3
- 235000001050 hortel pimenta Nutrition 0.000 claims description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 3
- 235000012658 paprika extract Nutrition 0.000 claims description 3
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- KINGXFAMZNIVNL-SXQDSXCISA-N safflor yellow A Natural products OC[C@@H]1O[C@H]2[C@H](OC3=C2C(=O)C(=C(O)C=Cc4ccc(O)cc4)C(=O)[C@]3(O)[C@@H]5O[C@H](CO)[C@@H](O)[C@H](O)[C@H]5O)[C@@H](O)[C@H]1O KINGXFAMZNIVNL-SXQDSXCISA-N 0.000 claims description 3
- 229910052594 sapphire Inorganic materials 0.000 claims description 3
- 239000010980 sapphire Substances 0.000 claims description 3
- 239000001585 thymus vulgaris Substances 0.000 claims description 3
- 235000013976 turmeric Nutrition 0.000 claims description 3
- 235000017060 Arachis glabrata Nutrition 0.000 claims description 2
- 244000105624 Arachis hypogaea Species 0.000 claims description 2
- 235000010777 Arachis hypogaea Nutrition 0.000 claims description 2
- 235000018262 Arachis monticola Nutrition 0.000 claims description 2
- 241000723366 Coreopsis Species 0.000 claims description 2
- 240000001972 Gardenia jasminoides Species 0.000 claims description 2
- 235000001018 Hibiscus sabdariffa Nutrition 0.000 claims description 2
- 240000004153 Hibiscus sabdariffa Species 0.000 claims description 2
- 241000233855 Orchidaceae Species 0.000 claims description 2
- 240000008042 Zea mays Species 0.000 claims description 2
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 claims description 2
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims description 2
- 235000009973 maize Nutrition 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 235000020232 peanut Nutrition 0.000 claims description 2
- 235000013599 spices Nutrition 0.000 claims description 2
- 229940071676 hydroxypropylcellulose Drugs 0.000 claims 2
- 235000016357 Mirtillo rosso Nutrition 0.000 claims 1
- 235000009470 Theobroma cacao Nutrition 0.000 claims 1
- 235000017606 Vaccinium vitis idaea Nutrition 0.000 claims 1
- 244000077923 Vaccinium vitis idaea Species 0.000 claims 1
- 239000003610 charcoal Substances 0.000 claims 1
- 239000002131 composite material Substances 0.000 claims 1
- 239000011324 bead Substances 0.000 abstract description 13
- 239000011230 binding agent Substances 0.000 abstract description 7
- 230000009977 dual effect Effects 0.000 abstract description 3
- 230000014860 sensory perception of taste Effects 0.000 abstract description 3
- 238000005096 rolling process Methods 0.000 abstract description 2
- 235000019504 cigarettes Nutrition 0.000 description 24
- 239000000203 mixture Substances 0.000 description 11
- 238000000034 method Methods 0.000 description 8
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- 239000003546 flue gas Substances 0.000 description 6
- 230000002441 reversible effect Effects 0.000 description 5
- 239000011257 shell material Substances 0.000 description 4
- 230000000391 smoking effect Effects 0.000 description 4
- 239000000835 fiber Substances 0.000 description 3
- 239000011259 mixed solution Substances 0.000 description 3
- 239000002304 perfume Substances 0.000 description 3
- 238000012216 screening Methods 0.000 description 3
- 235000005764 Theobroma cacao ssp. cacao Nutrition 0.000 description 2
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- 235000001046 cacaotero Nutrition 0.000 description 2
- 239000006229 carbon black Substances 0.000 description 2
- MYSWGUAQZAJSOK-UHFFFAOYSA-N ciprofloxacin Chemical compound C12=CC(N3CCNCC3)=C(F)C=C2C(=O)C(C(=O)O)=CN1C1CC1 MYSWGUAQZAJSOK-UHFFFAOYSA-N 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 239000007968 orange flavor Substances 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 241001236788 Frangula rubra Species 0.000 description 1
- 244000111489 Gardenia augusta Species 0.000 description 1
- VAYOSLLFUXYJDT-RDTXWAMCSA-N Lysergic acid diethylamide Chemical compound C1=CC(C=2[C@H](N(C)C[C@@H](C=2)C(=O)N(CC)CC)C2)=C3C2=CNC3=C1 VAYOSLLFUXYJDT-RDTXWAMCSA-N 0.000 description 1
- 235000002597 Solanum melongena Nutrition 0.000 description 1
- 244000061458 Solanum melongena Species 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 description 1
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- -1 hydroxypropyl Chemical group 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention provides a kind of discoloration tobacco aromaticss pearl and preparation method.The perfumed beads preparation is that solid mixed powder is placed in centrifugation coating granulator first; and it is sprayed binder solution as slurry; powder rotates in centrifuge forms parent nucleus; then parent nucleus is continued to be placed in centrifugation coating granulator; and it is sprayed using color fragrance adhesive solution as slurry; solid mixed powder is added during sprinkling, continuing amplification pill makes its partial size increase to form changeable colour tobacco aromaticss pearl；Wherein solid powder is uniformly mixed and is formed by natural plant powder, starch, chitosan, microcrystalline cellulose；The fragrance adhesive solution that changes colour is mixed by adhesive, pigment, essence, color shifting ink and water.The present invention not only can be improved the fragrance of suction quality to tobacco rolling belt, moreover it is possible to be intuitive to see very much the color change of particle pearl in suction, consumer is made to experience the dual experience of vision and the sense of taste.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to one kind is used in filter stick for cigarettes, and the cigarette that can change colour is fragrant
Expect pearl and preparation method thereof.
Background technique
Essence is added in cigarette, mainly there are several ways at present: 1. direct flavoring and casings in the tobacco；2. in filter stick
It is brought into a manner of fragrant line；It is added 3. being wrapped up in the form of capsule in filter stick；4. being added in a manner of microcapsules in filter stick
Enter.The these types of multiple cigarette brands of mode are using, and consumer is difficult to find that more novel consumption experience.
Color shifting ink is a kind of by a kind of special ink to change colour by property substance, can be used in anti-fake industry, toy row
Industry, gift industry, apparel industry, craftwork industry etc..Color shifting ink is largely divided into several major class: 1. heat discoloration ink；2.
Ultraviolet photosensitive color-changing ink；3. Ultraluminescence color shifting ink；4. infrared excitation color shifting ink；5. meeting water color shifting ink；6. light
Learn color shifting ink；7. noctilucence color shifting ink.In these types of classification, since it is considered that the application in cigarette, is in cigarette
Portion, it is difficult to directly contact and react with ultraviolet light, fluorescence, infrared ray, noctilucence, water etc., it is contemplated that utilizing heat discoloration
Principle is applied in cigarette by color shifting ink in conjunction with carrier for essence, improves the novelty that essence uses.
Heat discoloration ink can must become color with the up and down of temperature repeatedly.(by taking 31 DEG C of red as an example, change colour shape
Formula is 31 DEG C of presented above colourless, 31 DEG C of red presented below).There are three major class for heat discoloration ink: showing certain under 1. room temperature
Kind particular color, heated rear color disappearance become colorless, and original color are recovered immediately after cooling, because its change procedure can
It is inverse, referred to as " Reversible temperature becomes colour killing ink "；2. showing at normal temperature colourless, become another color after heated, after cooling
Revert to again it is original colourless, because its change procedure is reversible, referred to as " Reversible temperature becomes color development ink "；3. ink is shown at normal temperature
Color becomes another color after heating, " Reversible temperature becomes annesl ink " is known as because its change procedure is reversible.
Summary of the invention
For the above-mentioned deficiency of the prior art, the technical problem to be solved in the present invention is to provide the cigarette use that one kind can change colour
Perfumed beads and preparation method thereof, the perfumed beads use heat discoloration ink in the preparation process of perfumed beads, and manufactured coloured silk pearl is not
The only fragrance matter suitable with gay colours, loading, moreover it is possible to which there is color changeable effect.It is added to the transparent filter stick of cigarette
In, flue-gas temperature caused by cigarette smoking heats color pearl, and color pearl color of being heated changes, while flue gas is taken out of
Aroma component in bead makes consumer experience the dual experience of vision and the sense of taste.
The technical scheme is that a kind of discoloration tobacco aromaticss pearl, it is characterised in that the perfumed beads are by mother
Core and discoloration fragrance shell composition diameter be 1.0~4.0mm colour-changeable perfumed beads, wherein the partial size of parent nucleus be 250~
450 μm, the discoloration fragrance shell is wrapped in parent nucleus surface by way of coating；
The parent nucleus raw material include the solid mixed powder that mass percent is 50~90% and mass percent be 10~
50% binder solution, wherein binder solution is to be mixed by mass percent for 1~20% adhesive and 80~99% water
Conjunction is formulated；
The discoloration fragrance shell material includes the solid mixed powder and quality percentage that mass percent is 70~90%
Than the discoloration fragrance adhesive solution for 10~30%, wherein the discoloration fragrance adhesive solution be by adhesive, pigment, essence,
Color shifting ink and water are mixed than 1~20:0.1~10:0.1~10:0.1~20:50~90 ratio according to parts by weight；
In above-mentioned formula, the solid mixed powder be by natural plant powder, starch, chitosan, microcrystalline cellulose by
It is mixed according to 1~30:1 of weight fraction ratio~50:1~50:1~20 ratio；
Described adhesive is one of povidone, hydroxypropyl cellulose, hydroxypropyl methyl cellulose, carboxymethyl cellulose
Or it is a variety of；
The pigment is water-soluble edible pigment；The essence is soluble perfume；The color shifting ink is heat discoloration
Water-based ink, discoloration cardinal temperature are 5 DEG C~60 DEG C.
The present invention preferably technical solution: wherein natural plant powder be 30 mesh of partial size~80 mesh powders, specifically by
Tobacco leaf, anise, Semen Cuscutae, lavender, peppermint, thyme, laurel, cortex cinnamomi, Radix Glycyrrhizae, dried orange peel, cloves, Chinese ilex, Pogostemon cablin, jasmine
The powder that any one or more plant in jasmine is formed after crushing.
The present invention preferably technical solution: discoloration fragrance shell pigment include natural bata-carotene, beet red, turmeric,
Safflower yellow, lac be red, more Exocarpium Citri Rubrum, capsanthin, chilli orange, burnt sugar coloring, red rice be red, coreopsis yellow extract, semen sojae atricolor are red, Kaoliang red, jade
Cream colour, cacao pigment, red yeast rice, Monascus color, falls that certain herbaceous plants with big flowers is red, Hei Jialun is red, Gardenia Yellow, gardenia blue at radish red, and sea-buckthorn is yellow, rose
Eggplant is red, acorn cup is brown, more favour Ke palm fibre, and mulberry fruit is red, natural leaf mustard is red, the fruit of Cherokee rose is brown, curcumin, peanut agriculture is red, Grape Skin is red, blue
Ingot arnotto, algae orchid, plant carbon black, Mi Menghuang, Asian puccoon is red, tea uranidin, Tea Green Pigment, citrus is yellow, relation by marriage rouge tree is orange, in famille rose
One or more；The essence is water-soluble flavouring essence for tobacco or water-soluble edible essence；The color of the color shifting ink includes
Bright red, rhodo, it is pink, bright red, orange red, sapphire blue, dark blue, sea blue, grass green, blackish green, in green, peacock green, golden yellow, black.
The preparation method of a kind of tobacco aromaticss pearl that changes colour provided by the invention, which is characterized in that specific step is as follows:
(1) it takes natural plants as raw material, is crushed, is sieved, obtaining partial size is 30 mesh~80 mesh natural vegetable powder
End, then by obtained natural plant powder, starch, chitosan, microcrystalline cellulose according to parts by weight than 1~30:1~50:1
The ratio of~50:1~20 is uniformly mixed the solid mixed powder for forming parent nucleus raw material；
(2) after the adhesive that mass percent is 1~20% being mixed with the pure water that mass percent is 80~99%
It is configured to binder solution；Wherein described adhesive is povidone, hydroxypropyl cellulose, hydroxypropyl methyl cellulose, carboxymethyl
One of cellulose is a variety of；
(3) solid mixed powder in step (1) is placed in centrifugation coating granulator, and viscous by what is prepared in step (2)
Mixture solution is sprayed as slurry, and powder rotates in centrifuge forms parent nucleus；And parent nucleus is sieved, particle size range
Control is at 250~450 μm；
(4) raw material of discoloration spice solution: adhesive 1~20 is weighed according to following parts by weight, pigment 0.1~10 is fragrant
Essence 0.1~10, color shifting ink 0.1~20, water 50~90；Whole adhesives, pigment, essence are first dissolved into 10~30 parts by weight
Water in be configured to mixed aqueous solution, then color shifting ink is dissolved into the water of 40~60 parts by weight, stirring 1~2 hour it is molten
Solution is configured to color shifting ink aqueous solution completely, then by prepared color shifting ink aqueous solution and adhesive, pigment, essence aqueous solution
It is stirred 1~2 hour after mixing, until dissolution forms discoloration fragrance adhesive solution completely；Described adhesive is povidone, hydroxypropyl fibre
Tie up one of element, hydroxypropyl methyl cellulose, carboxymethyl cellulose or a variety of；
(5) parent nucleus made of being granulated in step (3) continues to be placed in centrifugation coating granulator, and will match in step 4)
The discoloration fragrance adhesive solution of system is sprayed as slurry, and it is mixed that the solid prepared in step (1) is added during sprinkling
Powder is closed, continuing amplification pill makes its partial size rise to 1.0~4.0mm, forms changeable colour tobacco aromaticss pearl；Wherein slurry and solid
The mass ratio of body mixed powder is 10~30:70~90；
The present invention preferably technical solution: the natural plants in the step (1) are tobacco leaf, anise, Semen Cuscutae, smoke clothing
Grass, peppermint, thyme, laurel, cortex cinnamomi, Radix Glycyrrhizae, dried orange peel, cloves, Chinese ilex, Pogostemon cablin, any one or more in jasmine.
The present invention preferably technical solution: in step (4), the pigment is water-soluble edible pigment；Recklessly including natural β
Radish element, beet red, turmeric, safflower yellow, lac are red, it is red to get over Exocarpium Citri Rubrum, capsanthin, chilli orange, burnt sugar coloring, red rice, Chrysan Yellow leaching
Cream, semen sojae atricolor be red, Kaoliang red, maize, radish red, cacao pigment, red yeast rice, Monascus color, fall certain herbaceous plants with big flowers is red, Hei Jialun is red, Gardenia Yellow,
Gardenia blue, sea-buckthorn is yellow, roselle is red, acorn cup is brown, more favour Ke palm fibre, and mulberry fruit is red, natural leaf mustard is red, the fruit of Cherokee rose is brown, curcumin, flower
Raw agriculture is red, Grape Skin is red, blue ingot arnotto, algae are blue, plant carbon black, Mi Menghuang, and Asian puccoon is red, tea uranidin, Tea Green Pigment, citrus
One or more of yellow, relation by marriage rouge tree orange, famille rose；The essence is water-soluble flavouring essence for tobacco or water-soluble edible essence；Institute
Stating color shifting ink is heat discoloration water-based ink, and discoloration cardinal temperature is 5 DEG C~60 DEG C, and color is including but not limited to big
Red, rhodo, it is pink, bright red, orange red, sapphire blue, dark blue, sea blue, grass green, blackish green, in green, peacock green, golden yellow, black.
Pelletizer in the step (3) and step (5) is that BZJ type is centrifuged coating granulator.
Advantages of the present invention: the present invention uses heat discoloration ink in the preparation process of perfumed beads, manufactured perfumed beads
The not only fragrance matter suitable with gay colours, loading, moreover it is possible to there is color changeable effect, imparted to color grains pearl new
Version；It is added in the transparent filter stick of cigarette, cigarette generated flue-gas temperature in aspiration procedure carries out color pearl
Heating, the heated color of color pearl changes, while flue gas takes the aroma component in particle pearl out of, can not only mention to tobacco rolling belt
The fragrance of high suction quality, moreover it is possible to be intuitive to see very much the color change of particle pearl in suction, consumer is made to experience vision
With the dual experience of the sense of taste.
Specific embodiment
A specific embodiment of the invention is described in further detail below with reference to embodiment.Following embodiment is
Laboratory data.
A kind of embodiment 1: preparation method of tobacco aromaticss pearl, the specific steps are as follows:
(1) it takes tobacco leaf, anise as raw material, is crushed, is sieved in the ratio of 1:1, obtain required natural plants
Powder, powder diameter are 30 mesh.Plant powder and starch, chitosan, microcrystalline cellulose are filled according to the ratio in table 1-1
Divide and is hybridly prepared into solid mixed-powder；
Table 1-1 solid mixed-powder composition of raw materials
| Type | Parts by weight |
| Plant powder (tobacco leaf, anise) | 10 |
| Starch | 40 |
| Chitosan | 30 |
| Microcrystalline cellulose | 20 |
(2) it takes the solid mixed-powder prepared in step (1) to be placed in BZJ type centrifugation coating granulator, then prepares matter
The hydroxypropyl cellulose aqueous solution that amount percentage is 5% is sprayed as binder solution, powder rotary in centrifuge
At parent nucleus；Wherein the mass ratio of solid mixed-powder and hydroxypropyl cellulose aqueous solution is 60:40；
(3) it will be granulated in step (2) into parent nucleus and sieve, particle size range is controlled at 250 μm, then continues parent nucleus
It is placed in BZJ type centrifugation coating granulator, is sprayed using discoloration fragrance adhesive solution as slurry, and in sprinkling process
Middle that the solid mixed powder prepared in step (1) is added, continuing amplification pill makes its partial size rise to target zone；Aimed dia
For 1.2mm, the orange flavor pearl that partial size is 1.2mm is obtained by screening, wherein discoloration fragrance adhesive solution and solid mixed powder
The mass ratio of material is 10:90；The composition of raw materials such as table 2-1 of the discoloration fragrance adhesive solution；
The composition of raw materials of table 2-1 discoloration fragrance adhesive solution
The specific preparation of discoloration fragrance adhesive solution: first that whole hydroxypropyl celluloses, curcumin and fragrant chrysanthemum medicinal extract is molten
Solution is configured to mixed solution into the water of 20 parts by weight, is then dissolved into color shifting ink in the water of 56 parts by weight, stirs 1 hour
Color shifting ink aqueous solution is prepared in dissolution completely, then adhesive, pigment and essence mixed aqueous solution and color shifting ink aqueous solution are mixed
It closes, stirs dissolution in 1 hour and be configured to discoloration fragrance adhesive solution completely.
The orange flavor pearl for being 1.2mm by the diameter obtained in embodiment 1, is applied in the transparent filter stick of cigarette.Cigarette exists
It can be appreciated that color pearl color is turned yellow by orange during room temperature, when cigarette smoking can experience stronger pungent fragrance
Road is relatively coordinated with flue gas cigarette perfume.
A kind of embodiment 2: preparation method of tobacco aromaticss pearl, the specific steps are as follows:
(1) it takes tobacco leaf, lavender as raw material, is crushed, is sieved in the ratio of 2:1, obtain required natural plants
Powder, powder diameter are 60 mesh.Plant powder and starch, chitosan, microcrystalline cellulose are filled according to the ratio in table 1-2
Divide and is hybridly prepared into solid mixed-powder；
Table 1-2 solid mixed-powder composition of raw materials
| Type | Parts by weight |
| Plant powder (tobacco leaf, lavender) | 20 |
| Starch | 30 |
| Chitosan | 40 |
| Microcrystalline cellulose | 10 |
(2) the solid mixed-powder prepared in step (1) is placed in BZJ type centrifugation coating granulator, then prepares matter
The hydroxypropyl methyl cellulose aqueous solution that amount percentage is 10% is sprayed as binder solution, and powder revolves in centrifuge
Turn to form parent nucleus, wherein the mass ratio of solid mixed-powder and hydroxypropyl methyl cellulose aqueous solution is 70:30；
(3) it will be granulated in step (2) into parent nucleus and sieve, particle size range is controlled at 350 μm, then continues parent nucleus
It is placed in BZJ type centrifugation coating granulator, is sprayed using discoloration fragrance adhesive solution as slurry, and in sprinkling process
Middle that the solid mixed powder prepared in step (1) is added, continuing amplification pill makes its partial size rise to target zone；Aimed dia
For 1.6mm, the purple perfumed beads that partial size is 1.6mm are obtained by screening, wherein discoloration fragrance adhesive solution and solid mixed powder
The mass ratio of material is 20:80；The composition of raw materials such as table 2-2 of the discoloration fragrance adhesive solution；
The composition of raw materials of table 2-2 discoloration fragrance adhesive solution
| Type | Parts by weight |
| Adhesive (hydroxypropyl methyl cellulose) | 10 |
| Pigment (famille rose) | 0.5 |
| Color shifting ink (water-based ink, the variable white of royalblue, 30 DEG C of discoloring temperature) | 10 |
| Essence (flavoring rose essence) | 5 |
| Water | 74.5 |
The specific preparation of discoloration fragrance adhesive solution: first adhesive, pigment, essence are dissolved into the water of 20 parts by weight and are matched
Mixed solution is made, is then dissolved into color shifting ink in the water of 54.5 parts by weight, stirs dissolution in 2 hours and is configured to change colour completely
Ink aqueous solution, then the mixed aqueous solution of adhesive, pigment and essence is mixed with color shifting ink aqueous solution, stirring 2 hours are molten
Solution is configured to discoloration fragrance adhesive solution completely.
Diameter will be obtained in embodiment 2 in the purple perfumed beads of 1.6mm, be applied in the transparent filter stick of cigarette.Cigarette is being taken out
It can be appreciated that color pearl color becomes red by purple after inhaling 3 mouthfuls, when cigarette smoking can experience stronger fragrance of a flower taste, with flue gas
Cigarette perfume is relatively coordinated.
A kind of embodiment 3: preparation method of tobacco aromaticss pearl, the specific steps are as follows:
(1) it takes cloves, jasmine as raw material, is crushed, is sieved in the ratio of 4:3, obtain required natural vegetable powder
End, powder diameter are 80 mesh.Plant powder and starch, chitosan, microcrystalline cellulose are carried out sufficiently according to the ratio in table 1-3
It is hybridly prepared into solid mixed-powder；
Table 1-3 solid mixed-powder composition of raw materials
| Type | Parts by weight |
| Plant powder (cloves, jasmine) | 30 |
| Starch | 30 |
| Chitosan | 20 |
| Microcrystalline cellulose | 20 |
(2) the solid mixed-powder prepared in step (1) is placed in BZJ type centrifugation coating granulator, then by poly- dimension
Mixed adhesive, is then dissolved in by the ratio mixed preparing mixed adhesive of ketone and hydroxypropyl methyl cellulose 1:2 in mass ratio
In pure water, it is configured to the mixed adhesive aqueous solution that binder concn is 10% and is sprayed, powder rotates in centrifuge
Parent nucleus is formed, wherein the mass ratio of solid mixed-powder and mixed adhesive aqueous solution is 80:20；
(3) it will be granulated in step (2) into parent nucleus and sieve, particle size range is controlled at 450 μm, then continues parent nucleus
It is placed in BZJ type centrifugation coating granulator, is sprayed using discoloration fragrance adhesive solution as slurry, and in sprinkling process
Middle that the solid mixed powder prepared in step (1) is added, continuing amplification pill makes its partial size rise to target zone；Aimed dia
For 3.0mm, the brown perfumed beads that partial size is 3.0mm are obtained by screening, wherein discoloration fragrance adhesive solution and solid mixed powder
The mass ratio of material is 30:70；The composition of raw materials such as table 2-3 of the discoloration fragrance adhesive solution；
The composition of raw materials of table 2-3 discoloration fragrance adhesive solution
The specific preparation of discoloration fragrance adhesive solution: first adhesive, pigment, essence are dissolved into the water of 30 parts by weight and are matched
Mixed solution is made, is then dissolved into color shifting ink in the water of 35 parts by weight, stirs dissolution in 2 hours and is configured to discoloration oil completely
Ink solution, then the mixed aqueous solution of adhesive, pigment and essence is mixed with color shifting ink aqueous solution, it stirs 2 hours and dissolves
It is configured to discoloration fragrance adhesive solution completely.
Diameter will be obtained in embodiment 3 in the brown perfumed beads of 3.0mm, be applied in the transparent filter stick of cigarette.Cigarette is being taken out
It can be appreciated that color pearl color becomes cyan by brown after inhaling 5 mouthfuls, when cigarette smoking can experience very strong fragrance of a flower taste.
Claims (2)
1. a kind of preparation method for the tobacco aromaticss pearl that changes colour, which is characterized in that specific step is as follows:
(1) it takes natural plants as raw material, is crushed, is sieved, obtaining partial size is 30 mesh~80 mesh natural plant powder, so
Afterwards by obtained natural plant powder, starch, chitosan, microcrystalline cellulose according to parts by weight than 1~30:1~50:1~50:
1~20 ratio is uniformly mixed the solid mixed powder for forming parent nucleus raw material；The natural plants are tobacco leaf, anise, Tu
Son, lavender, peppermint, thyme, laurel, cortex cinnamomi, Radix Glycyrrhizae, dried orange peel, cloves, Chinese ilex, Pogostemon cablin, in jasmine any one or
It is a variety of；
(2) it is prepared after mixing the adhesive that mass percent is 1~20% with the pure water that mass percent is 80~99%
Composite adhesives solution；Wherein described adhesive is povidone, hydroxypropyl cellulose, hydroxypropyl methyl cellulose, carboxymethyl cellulose
One of element is a variety of；
(3) solid mixed powder in step (1) is placed in centrifugation coating granulator, and the adhesive that will be prepared in step (2)
Solution is sprayed as slurry, and powder rotates in centrifuge forms parent nucleus；And parent nucleus is sieved, particle size range control
At 250~450 μm；
(4) raw material of discoloration spice solution: adhesive 1~20, pigment 0.1~10, essence 0.1 is weighed according to following parts by weight
~10, color shifting ink 0.1~20, water 50~90；Whole adhesives, pigment, essence are first dissolved into the water of 10~30 parts by weight
In be configured to mixed aqueous solution, then color shifting ink is dissolved into the water of 40~60 parts by weight, stirring has been dissolved for 1~2 hour
It is configured to color shifting ink aqueous solution entirely, then prepared color shifting ink aqueous solution is mixed with adhesive, pigment, essence aqueous solution
It stirs 1~2 hour afterwards, until dissolution forms discoloration fragrance adhesive solution completely；Described adhesive is povidone, hydroxy propyl cellulose
One of element, hydroxypropyl methyl cellulose, carboxymethyl cellulose are a variety of；
(5) parent nucleus made of being granulated in step (3) continues to be placed in centrifugation coating granulator, and will prepare in step 4)
Discoloration fragrance adhesive solution is sprayed as slurry, and the solid mixed powder prepared in step (1) is added during sprinkling
Material, continuing amplification pill makes its partial size rise to 1.0~4.0mm, forms changeable colour tobacco aromaticss pearl；Wherein slurry and solid are mixed
The mass ratio for closing powder is 10~30:70~90.
2. a kind of preparation method of tobacco aromaticss pearl that changes colour according to claim 1, it is characterised in that: in step (4)
In, the pigment is water-soluble edible pigment；Including natural bata-carotene, beet red, turmeric, safflower yellow, lac be red, cowberry
Red, capsanthin, chilli orange, burnt sugar coloring, red rice be red, coreopsis yellow extract, semen sojae atricolor are red, Kaoliang red, maize, radish red, cocoa shell
Color, Monascus color, falls that certain herbaceous plants with big flowers is red, Hei Jialun is red, Gardenia Yellow, gardenia blue at red yeast rice, and sea-buckthorn is yellow, roselle is red, acorn cup is brown, more favours
Ke Zong, mulberry fruit is red, natural leaf mustard is red, the fruit of Cherokee rose is brown, curcumin, peanut agriculture is red, Grape Skin is red, blue ingot arnotto, algae orchid, plant charcoal
Black, Mi Menghuang, Asian puccoon is red, tea uranidin, Tea Green Pigment, citrus are yellow, relation by marriage rouge tree is orange, one or more of famille rose；It is described
Essence is water-soluble flavouring essence for tobacco or water-soluble edible essence；The color shifting ink is heat discoloration water-based ink, discoloration
Cardinal temperature is 5 DEG C~60 DEG C, and color is including but not limited to bright red, rhodo, pink, bright red, orange red, sapphire blue, dark blue, extra large
It is blue, grass green, blackish green, in green, peacock green, golden yellow, black.
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