CN107556940A - The cigarette adhesive that a kind of microencapsulation natural extract is modified - Google Patents
The cigarette adhesive that a kind of microencapsulation natural extract is modified Download PDFInfo
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- CN107556940A CN107556940A CN201710647631.6A CN201710647631A CN107556940A CN 107556940 A CN107556940 A CN 107556940A CN 201710647631 A CN201710647631 A CN 201710647631A CN 107556940 A CN107556940 A CN 107556940A
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- cigarette
- microencapsulation
- natural extract
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- extract
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Abstract
The invention provides the cigarette adhesive that a kind of microencapsulation natural extract is modified, using polymer wrapped microencapsulation natural extract, as cigarette adhesive modifying agent, for improving cigarette smoking organoleptic quality, cigarette suction comfort is improved, lift the fragrance of cigarette smoke or mitigates the excitant of cigarette smoke or miscellaneous gas.Natural extract, which is included from extractions such as natural traditional Chinese medicine plant, tealeaves, fruit and plant roots and stems, has fragrance or the liquid or solid material of pharmacological action, then using interfacial polymerization, phase separation or spray drying the methods of, particle diameter is formed between 100nm 100um, the microencapsulation natural extract of polymer wrapped.The microcapsules can be added to cigarette overlapping glue and connect in the cigarette adhesive such as mouth glue, discharge extract when cigarette is lighted, and reach the purpose of lifting cigarette taste and drop evil.
Description
Technical field
A kind of preparation method and its usage for the cigarette adhesive being modified the present invention relates to microencapsulation natural extract, category
In cigarette adhesive technical field.
Background technology
At present, adhesive used is that do not have dulcet in tobacco business, and adhesive primarily serves bonding cigarette in cigarette
Paper material, there is provided overlap and ensure the effect of enough intensity and processability.State's inner wrap strip adhesive mainly includes taking mouth
Glue, connect mouth glue and packaging glue.With the rise of smoking material functionalization and differentiation in industry, added using natural extract
It is added in smoking material, turns into development trend so as to assign pure and fresh graceful, the harm reduction health care of cigarette product.
Patent CN201110182609.1 discloses a kind of Momordica grosvenori, chrysanthemum, honeysuckle, lophatherum gracile, the sterculia seed and lemon
Deng the method through pure water extract flavouring filter stick shaping paper.Patent CN201010138393.4 discloses a kind of natural plants and carried
Thing is taken to be added to cigaratte filter, to reduce the harmful components in cigarette smoke.Patent CN200410022723.8 is disclosed Portugal
The extract of grape seed is added in cigarette shreds or filter tip, the scavenger as caused free radical in tobacco product smoking process
Method.Patent CN201310044250.0 discloses a kind of alkali metal salt, marine algae extract, amino acid and polyalcohol, application
In the method for pipe tobacco, paper-making method reconstructed tobacco, cigarette paper and mouth rod and other tobacco products as tobacco humectant.Patent
CN201310445798.6 discloses a kind of method of tea tree fragrance of a flower composition coating inner lining paper of cigarette inner wrapper.
Up to the present, document and patent report natural extract there is no to be added to the report of cigarette adhesive, in addition, such as
Natural extract is directly added in cigarette adhesive by fruit, because it changes adhesive composition, often influences technological parameter
And adhesive property.
To make up existing blending and adhesive technological deficiency, the present invention provides the controllable cigarette of a kind of natural safety, technique and used
Adhesive flavouring harm reduction technology.It is added to using microencapsulation natural extract in cigarette adhesive, it is pure and fresh assigns cigarette product
The advantages of gracefulness, harm reduction health care.
The content of the invention
In view of the above-mentioned problems existing in the prior art, an object of the present invention is to prepare a kind of encapsulation natural
The method of extract.
The preparation method for the cigarette adhesive that a kind of microencapsulation natural extract is modified, using polymer wrapped microcapsules
Change natural extract, as cigarette adhesive modifying agent.
Polymer capsule material includes thermoset synthetic resin, thermoplastic synthetic resin, natural sex macromolecule.
The thermoset synthetic resin includes urine aldehyde, phenolic aldehyde；The thermoplastic synthetic resin polymethyl methacrylate, gather
Styrene, polyvinyl butyral resin, vinyl-vinyl acetate copolymer, the natural sex macromolecule include Arabic gum, bright
Glue, agar-agar, sodium alginate, chitosan.
The natural extract includes having perfume from extractions such as natural traditional Chinese medicine plant, tealeaves, fruit and plant roots and stems
Gas or the liquid or solid material of pharmacological action.
Specifically, the natural extract include asparagus juice and Aloe Vera Gel, American Ginseng, rattletop, pepper extract, pine nut
Chrysanthemum essence oil from plant, extractive of flax seed, ginger and ginkgo biloba p.e, jujube, banana, pineapple, Fragaia ananassa Duchesne extract, oil of bay,
Shiu oil, cedar wood oil, tangerine oil and peppermint oil, ephedrine, licorice, grape seed extract, isoflavones and tea
Leaf extract.
The parcel of the liquid substance of the natural extract passes through polymer phase separation method and interfacial polymerization method etc.
Method obtains：By 1~1.5 part of natural extract, 1~2 part of capsule material, 0.01~2 part of surfactant, mixing and emulsifying heating obtains
The microcapsules of synthetic polymer parcel.
The parcel of the solid matter of the natural extract can be prepared by the following：By natural extract 1~1.5
Part, 1~2 part of natural sex macromolecule, it is well mixed, the microcapsules of polymer wrapped is obtained using spray drying process.
The cigarette adhesive includes starch base and acetate emulsion type overlapping glue and connects the adhesives such as mouth glue.
Described microencapsulation natural extract particle diameter is between 100 nanometers to 100 microns.
The specific steps that the microencapsulation natural extract is added to cigarette adhesive are included：Microcapsules are pressed 1%
It is added to 20% weight ratio in cigarette adhesive, 10-30min is stirred under the conditions of 20-40 DEG C, makes microcapsules fully dispersed.
The present invention also aims to provide concrete application of the microencapsulation natural extract in cigarette adhesive.
The purposes for the cigarette adhesive that microencapsulation natural extract is modified, for improving cigarette smoking organoleptic quality.Tool
Body, for improving cigarette suction comfort, lifting the fragrance of cigarette smoke or mitigating the excitant or miscellaneous of cigarette smoke
Gas.
Compared with prior art, the active ingredient extracted from natural plants makes microcapsules to the present invention, by this micro- glue
Capsule is added in cigarette adhesive, in smoking process, can be enriched cigarette perfume, be increased cigarette smoke quality and harmony, there is choosing
Selecting property reduces the oxious component in cigarette, protects the health of smoker.
Brief description of the drawings
Fig. 1 is ESEM (SEM) picture of encapsulation natural extract.
Fig. 2 is the section SEM pictures of the adhesive of addition microcapsules.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is described in further detail.It is appreciated that specific embodiment described herein is only used for explaining for this area researcher
The present invention, the protection domain being not intended to limit the present invention.
Embodiment 1：
By polymethyl methacrylate (PMMA) 20g, Sweet Almond Oil (production of Jiangxi middle ring new material Co., Ltd) 30g,
It is dissolved in dichloromethane 40g, is made into oil phase.The oil phase is added dissolved with the 100g water of 1% polyvinylpyrrolidone, with a high speed
Stirring and emulsifying machine emulsifies, and oil-in-water emulsion is made.Emulsion is heated to 40 DEG C, the solvent in oil-in-water emulsion drop is gradually waved
Hair, microcapsules are obtained using polymer phase partition method.Filtering, 60 DEG C dry 12 hours, so as to obtain the dessert almond of PMMA parcels
Oily ball type microcapsules.
The microcapsules are added in overlapping glue by 4% weight ratio, 20min is stirred under the conditions of 25 DEG C, makes microcapsules
It is fully dispersed, used as cigarette overlapping glue, and routinely cigarette is made in cigarette process.
Embodiment 2：
By green-tea extract powder 120g (Hubei Yuancheng Pharmaceutical Co., Ltd.), chitosan 60g, Arabic gum 30g 10L
The aqueous solution, after being well mixed, then microcapsules being prepared by spray drying process, feeding temperature is 50 DEG C, and EAT is 200 DEG C,
Leaving air temp is 110 DEG C, and microcapsules are made, microcapsules are added in overlapping glue by 2% weight ratio, stirred under the conditions of 25 DEG C
30min, make microcapsules fully dispersed, used as cigarette overlapping glue, and routinely cigarette is made in cigarette process.
Embodiment 3：
By cream jasmin france 20mL, 2% gelatin and 2% Arabic gum 1L solution, adjustment pH value are to heat to stir at 4.5,55 DEG C
Mix, obtain micro-capsule dispersion liquid.Microcapsule solution is cooled to 5 DEG C or so, adds 36% formaldehyde 10ml to solidify, continues to stir
20min, pH=9 is adjusted, placed 2 hours.Filtering, 60 DEG C dry 12 hours, micro- so as to obtain the jasmine sesame oil ball-type of gelatin coatings
Capsule.
The microcapsules are added in overlapping glue by 6% weight ratio, 15min is stirred under the conditions of 25 DEG C, makes microcapsules
It is fully dispersed, used as cigarette overlapping glue, and routinely cigarette is made in cigarette process.
As a result show, it is sweet using the more soft exquisiteness of cigarette smoke of addition microencapsulation natural extract overlapping glue
The obvious increase of sense, aroma quality have been lifted, and full weight is more preferable, and the miscellaneous gas and excitant in flue gas are decreased obviously, cigarette quality
It is obviously improved.
Claims (12)
1. the preparation method for the cigarette adhesive that a kind of microencapsulation natural extract is modified, it is characterised in that using polymer
Microencapsulation natural extract is wrapped up, as cigarette adhesive modifying agent.
2. the preparation method for the cigarette adhesive that microencapsulation natural extract is modified, its feature exist according to claim 1
In polymer capsule material includes thermoset synthetic resin, thermoplastic synthetic resin, natural sex macromolecule.
3. the preparation method for the cigarette adhesive that microencapsulation natural extract is modified, its feature exist according to claim 1
In the thermoset synthetic resin includes urine aldehyde, phenolic aldehyde；The thermoplastic synthetic resin polymethyl methacrylate, polyphenyl second
Alkene, polyvinyl butyral resin, vinyl-vinyl acetate copolymer, the natural sex macromolecule include Arabic gum, gelatin, fine jade
Glue, sodium alginate, chitosan.
4. the preparation method for the cigarette adhesive being modified according to microencapsulation natural extract described in letter of authorization 1, it is characterised in that
The natural extract includes having fragrance or pharmacology from extractions such as natural traditional Chinese medicine plant, tealeaves, fruit and plant roots and stems
The liquid or solid material of effect.
5. the preparation method for the cigarette adhesive being modified according to microencapsulation natural extract described in letter of authorization 4, it is characterised in that
The natural extract include asparagus juice and Aloe Vera Gel, American Ginseng, rattletop, pepper extract, Echinacea purpurea essence oil from plant, Asia
Numb seed extract, ginger and ginkgo biloba p.e, jujube, banana, pineapple, Fragaia ananassa Duchesne extract, oil of bay, shiu oil, cedar wood oil, mandarin orange
Mandarin oil and peppermint oil, ephedrine, licorice, grape seed extract, isoflavones and tea extract.
6. the preparation method for the cigarette adhesive being modified according to microencapsulation natural extract described in letter of authorization 4, it is characterised in that
The parcel of the liquid substance of the natural extract is obtained by the methods of polymer phase separation method and interfacial polymerization method：
By natural extract 1-1.5 parts, capsule material 1-2 parts, surfactant 0.01-2 parts, mixing and emulsifying heating obtains synthetic polymer bag
The microcapsules wrapped up in.
7. the preparation method for the cigarette adhesive being modified according to microencapsulation natural extract described in letter of authorization 4, it is characterised in that
The parcel of the solid matter of the natural extract can be prepared by the following：By natural extract 1-1.5 parts, natural sex
Macromolecule 1-2 parts, it is well mixed, the microcapsules of polymer wrapped is obtained using spray drying process.
8. the preparation method for the cigarette adhesive being modified according to any microencapsulation natural extracts of letter of authorization 1-7, it is special
Sign is that the cigarette adhesive includes starch base and acetate emulsion type overlapping glue and connects the adhesives such as mouth glue.
9. the preparation method for the cigarette adhesive being modified according to any microencapsulation natural extracts of letter of authorization 1-7, it is special
Sign is that described microencapsulation natural extract particle diameter is between 100nm-100um.
10. the preparation method for the cigarette adhesive being modified according to microencapsulation natural extract described in letter of authorization 1, its feature exist
In the specific steps that the microencapsulation natural extract is added to cigarette adhesive are included：Microcapsules are pressed into 1%-20%
Weight ratio is added in cigarette adhesive, and 10-30min is stirred under the conditions of 20-40 DEG C, makes microcapsules fully dispersed.
11. the purposes for the cigarette adhesive that microencapsulation natural extract is modified, for improving cigarette smoking organoleptic quality.
12. the purposes for the cigarette adhesive being modified according to microencapsulation natural extract described in letter of authorization 11, it is characterised in that use
In raising cigarette suction comfort, lift the fragrance of cigarette smoke or mitigate the excitant of cigarette smoke or miscellaneous gas.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710647631.6A CN107556940A (en) | 2017-08-01 | 2017-08-01 | The cigarette adhesive that a kind of microencapsulation natural extract is modified |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710647631.6A CN107556940A (en) | 2017-08-01 | 2017-08-01 | The cigarette adhesive that a kind of microencapsulation natural extract is modified |
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| CN107556940A true CN107556940A (en) | 2018-01-09 |
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| CN201710647631.6A Pending CN107556940A (en) | 2017-08-01 | 2017-08-01 | The cigarette adhesive that a kind of microencapsulation natural extract is modified |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110761112A (en) * | 2019-10-25 | 2020-02-07 | 武汉红金龙印务股份有限公司 | Method for preparing high-performance novel cigarette paper by using raw paper for cigarettes and improved equipment thereof |
| CN112625651A (en) * | 2020-11-28 | 2021-04-09 | 湖北中烟工业有限责任公司 | Special environment-friendly water-based glue for tobacco packaging and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1030926A (en) * | 1987-07-29 | 1989-02-08 | 湖南维尼纶厂 | Technique for cigarette package with high speed tackiness agent and manufacture method |
| CN101215805A (en) * | 2008-01-07 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Cigarette perfuming agent and its preparation method and application |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
| CN103504465A (en) * | 2013-09-27 | 2014-01-15 | 广东中烟工业有限责任公司 | Microcapsule humectant for cigarettes, preparation method of microcapsule humectant and application of microcapsule humectant |
| CN103923579A (en) * | 2014-04-24 | 2014-07-16 | 川渝中烟工业有限责任公司 | Essence used in vanilla-scented holder adhesive for cigarettes |
| CN104312497A (en) * | 2014-10-13 | 2015-01-28 | 湖北中烟工业有限责任公司 | Efficient cigarette connection adhesive with loading of mint essence and preparation process of efficient cigarette connection adhesive |
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2017
- 2017-08-01 CN CN201710647631.6A patent/CN107556940A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1030926A (en) * | 1987-07-29 | 1989-02-08 | 湖南维尼纶厂 | Technique for cigarette package with high speed tackiness agent and manufacture method |
| CN101215805A (en) * | 2008-01-07 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Cigarette perfuming agent and its preparation method and application |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
| CN103504465A (en) * | 2013-09-27 | 2014-01-15 | 广东中烟工业有限责任公司 | Microcapsule humectant for cigarettes, preparation method of microcapsule humectant and application of microcapsule humectant |
| CN103923579A (en) * | 2014-04-24 | 2014-07-16 | 川渝中烟工业有限责任公司 | Essence used in vanilla-scented holder adhesive for cigarettes |
| CN104312497A (en) * | 2014-10-13 | 2015-01-28 | 湖北中烟工业有限责任公司 | Efficient cigarette connection adhesive with loading of mint essence and preparation process of efficient cigarette connection adhesive |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110761112A (en) * | 2019-10-25 | 2020-02-07 | 武汉红金龙印务股份有限公司 | Method for preparing high-performance novel cigarette paper by using raw paper for cigarettes and improved equipment thereof |
| CN110761112B (en) * | 2019-10-25 | 2024-04-05 | 武汉红金龙印务股份有限公司 | Method for preparing high-performance novel cigarette paper by using base paper for cigarettes and improved equipment thereof |
| CN112625651A (en) * | 2020-11-28 | 2021-04-09 | 湖北中烟工业有限责任公司 | Special environment-friendly water-based glue for tobacco packaging and preparation method thereof |
| CN112625651B (en) * | 2020-11-28 | 2022-07-26 | 湖北中烟工业有限责任公司 | Special environment-friendly water-based glue for tobacco packaging and preparation method thereof |
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Application publication date: 20180109 |
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