CN106520411A - Preparation method of pure-biomass leather cleaner - Google Patents
Preparation method of pure-biomass leather cleaner Download PDFInfo
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- CN106520411A CN106520411A CN201610945527.0A CN201610945527A CN106520411A CN 106520411 A CN106520411 A CN 106520411A CN 201610945527 A CN201610945527 A CN 201610945527A CN 106520411 A CN106520411 A CN 106520411A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/265—Carboxylic acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/267—Heterocyclic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/46—Animal products
-
- C—CHEMISTRY; METALLURGY
- C14—SKINS; HIDES; PELTS; LEATHER
- C14C—CHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
- C14C11/00—Surface finishing of leather
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Zoology (AREA)
- General Chemical & Material Sciences (AREA)
- Treatment And Processing Of Natural Fur Or Leather (AREA)
Abstract
The invention relates to a preparation method of a pure-biomass leather cleaner and belongs to the technical field of leather cleaners. The preparation method comprises the steps that firstly, fresh milk is fermented to obtain raw yogurt, then tannin rich liquid is extracted from banana peels, egg white and washing water of rice are mixed, finally, the three substances are mixed and fermented, a natural preservative component is added, and the leather cleaner is obtained after concentration. According to the preparation method, lactic acid in the raw yogurt serves as a natural decontaminant, crude fibers in the washing water of rice serve as a friction agent to remove stains in leather, after cleaning is finished, tannin in the banana peel extracts and proteins in the leather are combined, hide which is compact, tough and not prone to decaying is formed on the surface of the leather, finally, the yogurt as well as proteins and lipid contained in the egg white can serve as a substitute of paraffin, a protective film is formed on the surface of the leather, the gloss of the leather can be maintained easily, no undesirable odor is generated, safety and environmental friendliness are achieved, and the preparation method has broad application prospects.
Description
Technical field
The present invention relates to a kind of preparation method of pure biomass leather cleaning agent, belongs to leather cleaning agent technical field.
Background technology
Oils and fatss are introduced the inside of animal skins in leather making process by leather, are formed
Oil film, so reduces the frictional force moved between leather internal fiber, makes the very soft of leather change.However, making in leather
With during, volatilization that this layer of oil film can be slowly, consume, or other reasonses cause oil film to be destroyed, now, inside leather
Fiber between will phase mutual friction, mutually bond, so as to being hardened, becoming fragile.Therefore, it is right to need during leatherware use
Leather is maintained.
Common leather cleaning agent composition includes：Surfactant, fatting agent, wetting agent, glazing agent etc..Surfactant
Emulsifying removal can be carried out to the pollutant of leather surface, also with preferable permeability and emulsibility, be conducive to the steady of product
Fixed, fatting agent is usually various oil substances, the oils and fatss of leather inside disappearance can be supplemented, keep its flexibility,
Common oils and fatss have：Mineral oil and oils and fatss, sulfonated oil, sulphation oils, higher alcohols, the higher alcohol lipid of higher fatty acids
Deng glazing agent can give leather gloss, commonly use Wax, such as paraffin, palm wax etc..But, existing leather cleaning agent
In the surfactant that contains and soap base, using remaining on leather after complete, not only degradability is poor for surfactant, and
And easily floating in atmosphere, is reunited with the pollutant such as dust, pollutes environment, and leather polishing not enough, can be produced after cleaning
, there is certain potential safety hazard in the substantial amounts of penetrating odor of life, therefore, develop that a kind of natural pollution-free and cleaning performance is splendid
Leather cleaning agent it is very urgent.
The content of the invention
The invention mainly solves the technical problem of：The present invention is for containing substantial amounts of chemical classes in conventional leather abluent
Surfactant and soap base, are easily remained on leather using rear, chemical classes surfactant difficult degradation, and easily pollute environment,
After cleaning, leather polishing not enough, can produce the defect of substantial amounts of penetrating odor, there is provided a kind of pure biomass leather cleaning
The preparation method of agent, the present invention are obtained raw Yoghourt with fresh milk fermentation first, then tannin pregnant solution is extracted from Pericarpium Musae, by egg
Cleer and peaceful washing water of rice mixing, finally by three's mixed fermentation, adds natural anticorrosion composition, leather cleaning agent is obtained final product after concentration.This
Used as natural detergent, the crude fibre in washing water of rice makees abrasivuss to be carried out the bright lactic acid by the use of in raw Yoghourt to the spot in leather
Cleaning, the protein in tannin and skin after cleaning in recycling pericarp of Fructus Musae extract combine, and are formed epidermis face fine and close soft
Tough and non-perishable leather, the protein contained in last Yoghourt and Ovum Gallus domesticus album and lipid can be as the substitutes of paraffin, in leather
Surface forms layer protecting film, is conducive to leather to keep gloss, and will not produce abnormal flavour, safety and environmental protection, with wide application
Prospect.
In order to solve above-mentioned technical problem, the technical solution adopted in the present invention is：
（1）The freshly extruded fresh milks of 3～5L are collected from dairy cow farm, with diameter being poured into after gauze repeatedly filter 23～5 time
30cm, in the wooden barrel of deep 1m, stands 30～40min, will swim in the butter on fresh milk surface with ferrum spoon after being stirred with waddy up and down
Scooping out, obtaining pure fresh-milk and proceed in fermentation tank, at a temperature of 17～19 DEG C being placed on after sealing tank mouth, natural fermentation 5～7 days, obtains
It is standby to raw Yoghourt；
（2）It is put in high-speed homogenization machine after weighing 400～500g Pericarpium Musae and the mixing of 1～2L deionized waters, with 8000～
9000r/min rotating speed 15～20min of homogenized, will obtain filtrate after the Pericarpium Musae homogenate filtered through gauze for obtaining, then with from
Scheming is by filtrate with 3000～4000r/min rotating speed 10～15min of centrifugal treating, isolated supernatant, i.e. Pericarpium Musae tannin
Pregnant solution, it is standby；
（3）Homogenizer is used with 700～800r/min after collecting 100～200g Ovum Gallus domesticus album and the mixing of 800～900g distilled water
Rotating speed stirring 5～8min of mixing, obtains Ovum Gallus domesticus album diluent, then is 1 in mass ratio:Ovum Gallus domesticus album diluent and washing water of rice mixing are stirred by 1
Mixed liquor is obtained after mixing uniformly；
（4）Count by weight, weigh 30～40 parts of steps（1）Standby raw Yoghourt, 20～30 parts of steps（2）Standby Fructus Musae
Skin tannin pregnant solution, 15～20 portions of above-mentioned mixed liquors are put in reactor jointly, and 10～15min is mixed at 18～20 DEG C
Afterwards, 1～2 part of vitamin C and 2～3 parts of sodium lactates are added then in reactor, stand after continuing stirring 20～30min of mixing from
So ferment 2～3 days；
（5）After above-mentioned fermentation ends, filter fermented product and obtain fermentation liquid, fermentation liquid is moved in Rotary Evaporators, is rotated dense
The 1/3 of its original volume is reduced to, concentrated solution is obtained, then concentrated solution is sterilized into 5 at 120～130 DEG C with high temperature sterilize tank～
10min, packs after which naturally cools to room temperature, obtains final product pure biomass leather cleaning agent.
The application process of the present invention：By the pure biomass leather cleaning agent obtained by the present invention and water in mass ratio 1:20～1:
Obtain cleaning medicinal liquid after 30 mixed dilutings, cleaning medicinal liquid is sprayed on into leather surface, after standing 3～5s, use clean soft cloth
It is uniform to wipe.After testing, after being cleaned using leather cleaning agent prepared by the present invention, leather surface is bright and clean, and can form one layer
Protecting film, reaches waterproof, the effect of mothproof, fixation, 20～25 days sustainable to the anti-fouling effect of leather.
The invention has the beneficial effects as follows：
（1）Preparation method of the present invention is simple, with low cost, and cleaning speed is fast, while forming protecting film in leather surface, is conducive to
Leather keeps gloss, and will not produce abnormal flavour, and safety and environmental protection has broad application prospects；
（2）Pure biomass leather cleaning agent prepared by the present invention has decontamination, sterilization, the effect of protection leather, and has assisting-dyeing concurrently
And tint retention, leather color clear can be made firmly, and harm is not resulted in environment.
Specific embodiment
The freshly extruded fresh milks of 3～5L are collected from dairy cow farm, with diameter being poured into after gauze repeatedly filter 23～5 time
30cm, in the wooden barrel of deep 1m, stands 30～40min, will swim in the butter on fresh milk surface with ferrum spoon after being stirred with waddy up and down
Scooping out, obtaining pure fresh-milk and proceed in fermentation tank, at a temperature of 17～19 DEG C being placed on after sealing tank mouth, natural fermentation 5～7 days, obtains
To raw Yoghourt；It is put in high-speed homogenization machine after weighing 400～500g Pericarpium Musae and the mixing of 1～2L deionized waters, with 8000～
9000r/min rotating speed 15～20min of homogenized, will obtain filtrate after the Pericarpium Musae homogenate filtered through gauze for obtaining, then with from
Scheming is by filtrate with 3000～4000r/min rotating speed 10～15min of centrifugal treating, isolated supernatant, i.e. Pericarpium Musae tannin
Pregnant solution；Homogenizer is used with 700～800r/min after collecting 100～200g Ovum Gallus domesticus album and the mixing of 800～900g distilled water
Rotating speed stirring 5～8min of mixing, obtains Ovum Gallus domesticus album diluent, then is 1 in mass ratio:Ovum Gallus domesticus album diluent and washing water of rice mixing are stirred by 1
Mixed liquor is obtained after mixing uniformly；Count by weight, weigh 30～40 parts of raw Yoghourt, 20～30 parts of Pericarpium Musae tannin and be enriched with
Liquid, 15～20 portions of above-mentioned mixed liquors are put in reactor jointly, after mixing 10～15min at 18～20 DEG C, then to anti-
1～2 part of vitamin C and 2～3 parts of sodium lactates are added in answering kettle, after continuing stirring 20～30min of mixing, natural fermentation 2～3 is stood
My god；After above-mentioned fermentation ends, filter fermented product and obtain fermentation liquid, fermentation liquid is moved in Rotary Evaporators, concentrated by rotary evaporation is extremely
The 1/3 of its original volume, obtains concentrated solution, then concentrated solution is sterilized at 120～130 DEG C 5～10min with high temperature sterilize tank, treats
Which is packed after naturally cooling to room temperature, obtains final product pure biomass leather cleaning agent.
Example 1
The freshly extruded fresh milks of 3L are collected from dairy cow farm, with diameter 30cm, the wood of deep 1m being poured into after gauze repeatedly filter 23 time
In bucket, 30min is stood after being stirred with waddy up and down, the butter for swimming in fresh milk surface is scooped out with ferrum spoon, obtain pure fresh-milk simultaneously
Proceed in fermentation tank, at a temperature of being placed on 17 DEG C after sealing tank mouth, natural fermentation 5 days, obtains raw Yoghourt；Weigh 400g Pericarpium Musae
It is put in high-speed homogenization machine after mixing with 1L deionized waters, with 8000r/min rotating speed homogenizeds 15min, by the Fructus Musae for obtaining
Obtain filtrate after skin homogenate filtered through gauze, then with centrifuge by filtrate with 3000r/min rotating speed centrifugal treating 10min, separate
Obtain supernatant, i.e. Pericarpium Musae tannin pregnant solution；Collect 100g Ovum Gallus domesticus album and 800g distilled water mixing after with homogenizer with
700r/min rotating speeds stirring mixing 5min, obtains Ovum Gallus domesticus album diluent, then is 1 in mass ratio:Ovum Gallus domesticus album diluent and washing water of rice are mixed by 1
Conjunction obtains mixed liquor after stirring；Count by weight, weigh 30 parts raw Yoghourt, 20 parts of Pericarpium Musae tannin pregnant solution,
15 portions of above-mentioned mixed liquors are put in reactor jointly, after mixing 10min, then 1 part of dimension are added in reactor at 18 DEG C
C and 2 part of sodium lactate of raw element, stands natural fermentation 2 days after continuing stirring mixing 20min；After above-mentioned fermentation ends, fermentation is filtered
Thing obtains fermentation liquid, fermentation liquid is moved in Rotary Evaporators, the 1/3 of concentrated by rotary evaporation to its original volume, obtains concentrated solution, then will
Concentrated solution high temperature sterilize tank sterilizes at 120 DEG C 5min, packs, obtain final product pure biomass leather after which naturally cools to room temperature
Cleaning agent.
By the pure biomass leather cleaning agent obtained by the present invention and water in mass ratio 1:Obtain cleaning medicine after 20 mixed dilutings
Cleaning medicinal liquid is sprayed on leather surface by liquid, is uniformly wiped with clean soft cloth after standing 3s.After testing, use
After leather cleaning agent cleaning prepared by the present invention, leather surface is bright and clean, and can form layer protecting film, reaches waterproof, mothproof, solid
The effect of color, 20 days sustainable to the anti-fouling effect of leather.
Example 2
The freshly extruded fresh milks of 5L are collected from dairy cow farm, pour diameter 30cm, the wood of deep 1m after 5 times being filtered repeatedly with gauze into
In bucket, 40min is stood after being stirred with waddy up and down, the butter for swimming in fresh milk surface is scooped out with ferrum spoon, obtain pure fresh-milk simultaneously
Proceed in fermentation tank, at a temperature of being placed on 19 DEG C after sealing tank mouth, natural fermentation 7 days, obtains raw Yoghourt；Weigh 500g Pericarpium Musae
It is put in high-speed homogenization machine after mixing with 2L deionized waters, with 9000r/min rotating speed homogenizeds 20min, by the Fructus Musae for obtaining
Obtain filtrate after skin homogenate filtered through gauze, then with centrifuge by filtrate with 4000r/min rotating speed centrifugal treating 15min, separate
Obtain supernatant, i.e. Pericarpium Musae tannin pregnant solution；Collect 200g Ovum Gallus domesticus album and 900g distilled water mixing after with homogenizer with
800r/min rotating speeds stirring mixing 8min, obtains Ovum Gallus domesticus album diluent, then is 1 in mass ratio:Ovum Gallus domesticus album diluent and washing water of rice are mixed by 1
Conjunction obtains mixed liquor after stirring；Count by weight, weigh 40 parts raw Yoghourt, 30 parts of Pericarpium Musae tannin pregnant solution,
20 portions of above-mentioned mixed liquors are put in reactor jointly, after mixing 15min, then 2 parts of dimensions are added in reactor at 20 DEG C
C and 3 part of sodium lactate of raw element, stands natural fermentation 3 days after continuing stirring mixing 30min；After above-mentioned fermentation ends, fermentation is filtered
Thing obtains fermentation liquid, fermentation liquid is moved in Rotary Evaporators, the 1/3 of concentrated by rotary evaporation to its original volume, obtains concentrated solution, then will
Concentrated solution high temperature sterilize tank sterilizes at 130 DEG C 10min, packs, obtain final product pure biomass skin after which naturally cools to room temperature
Leather cleaning agent.
By the pure biomass leather cleaning agent obtained by the present invention and water in mass ratio 1:Obtain cleaning medicine after 25 mixed dilutings
Cleaning medicinal liquid is sprayed on leather surface by liquid, is uniformly wiped with clean soft cloth after standing 4s.After testing, use
After leather cleaning agent cleaning prepared by the present invention, leather surface is bright and clean, and can form layer protecting film, reaches waterproof, mothproof, solid
The effect of color, 23 days sustainable to the anti-fouling effect of leather.
Example 3
The freshly extruded fresh milks of 4L are collected from dairy cow farm, pour diameter 30cm, the wood of deep 1m after 4 times being filtered repeatedly with gauze into
In bucket, 35min is stood after being stirred with waddy up and down, the butter for swimming in fresh milk surface is scooped out with ferrum spoon, obtain pure fresh-milk simultaneously
Proceed in fermentation tank, at a temperature of being placed on 18 DEG C after sealing tank mouth, natural fermentation 6 days, obtains raw Yoghourt；Weigh 450g Pericarpium Musae
It is put in high-speed homogenization machine after mixing with 2L deionized waters, with 8500r/min rotating speed homogenizeds 18min, by the Fructus Musae for obtaining
Obtain filtrate after skin homogenate filtered through gauze, then with centrifuge by filtrate with 3500r/min rotating speed centrifugal treating 13min, separate
Obtain supernatant, i.e. Pericarpium Musae tannin pregnant solution；Collect 150g Ovum Gallus domesticus album and 850g distilled water mixing after with homogenizer with
750r/min rotating speeds stirring mixing 7min, obtains Ovum Gallus domesticus album diluent, then is 1 in mass ratio:Ovum Gallus domesticus album diluent and washing water of rice are mixed by 1
Conjunction obtains mixed liquor after stirring；Count by weight, weigh 35 parts raw Yoghourt, 25 parts of Pericarpium Musae tannin pregnant solution,
18 portions of above-mentioned mixed liquors are put in reactor jointly, after mixing 13min, then 2 parts of dimensions are added in reactor at 19 DEG C
C and 3 part of sodium lactate of raw element, stands natural fermentation 3 days after continuing stirring mixing 25min；After above-mentioned fermentation ends, fermentation is filtered
Thing obtains fermentation liquid, fermentation liquid is moved in Rotary Evaporators, the 1/3 of concentrated by rotary evaporation to its original volume, obtains concentrated solution, then will
Concentrated solution high temperature sterilize tank sterilizes at 125 DEG C 8min, packs, obtain final product pure biomass leather after which naturally cools to room temperature
Cleaning agent.
By the pure biomass leather cleaning agent obtained by the present invention and water in mass ratio 1:Obtain cleaning medicine after 30 mixed dilutings
Cleaning medicinal liquid is sprayed on leather surface by liquid, is uniformly wiped with clean soft cloth after standing 5s.After testing, use
After leather cleaning agent cleaning prepared by the present invention, leather surface is bright and clean, and can form layer protecting film, reaches waterproof, mothproof, solid
The effect of color, 25 days sustainable to the anti-fouling effect of leather.
Claims (1)
1. a kind of preparation method of pure biomass leather cleaning agent, it is characterised in that concrete preparation process is：
（1）The freshly extruded fresh milks of 3～5L are collected from dairy cow farm, with diameter being poured into after gauze repeatedly filter 23～5 time
30cm, in the wooden barrel of deep 1m, stands 30～40min, will swim in the butter on fresh milk surface with ferrum spoon after being stirred with waddy up and down
Scooping out, obtaining pure fresh-milk and proceed in fermentation tank, at a temperature of 17～19 DEG C being placed on after sealing tank mouth, natural fermentation 5～7 days, obtains
It is standby to raw Yoghourt；
（2）It is put in high-speed homogenization machine after weighing 400～500g Pericarpium Musae and the mixing of 1～2L deionized waters, with 8000～
9000r/min rotating speed 15～20min of homogenized, will obtain filtrate after the Pericarpium Musae homogenate filtered through gauze for obtaining, then with from
Scheming is by filtrate with 3000～4000r/min rotating speed 10～15min of centrifugal treating, isolated supernatant, i.e. Pericarpium Musae tannin
Pregnant solution, it is standby；
（3）Homogenizer is used with 700～800r/min after collecting 100～200g Ovum Gallus domesticus album and the mixing of 800～900g distilled water
Rotating speed stirring 5～8min of mixing, obtains Ovum Gallus domesticus album diluent, then is 1 in mass ratio:Ovum Gallus domesticus album diluent and washing water of rice mixing are stirred by 1
Mixed liquor is obtained after mixing uniformly；
（4）Count by weight, weigh 30～40 parts of steps（1）Standby raw Yoghourt, 20～30 parts of steps（2）Standby Fructus Musae
Skin tannin pregnant solution, 15～20 portions of above-mentioned mixed liquors are put in reactor jointly, and 10～15min is mixed at 18～20 DEG C
Afterwards, 1～2 part of vitamin C and 2～3 parts of sodium lactates are added then in reactor, stand after continuing stirring 20～30min of mixing from
So ferment 2～3 days；
（5）After above-mentioned fermentation ends, filter fermented product and obtain fermentation liquid, fermentation liquid is moved in Rotary Evaporators, is rotated dense
The 1/3 of its original volume is reduced to, concentrated solution is obtained, then concentrated solution is sterilized into 5 at 120～130 DEG C with high temperature sterilize tank～
10min, packs after which naturally cools to room temperature, obtains final product pure biomass leather cleaning agent.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107669045A (en) * | 2017-08-23 | 2018-02-09 | 安徽楚艾农业科技有限公司 | A kind of wormwood pillow pillow inorganic agent and preparation method thereof |
| CN107739662A (en) * | 2017-11-30 | 2018-02-27 | 苏州龙腾万里化工科技有限公司 | Multiple-effect leather cleaning care agent |
| CN108085180A (en) * | 2017-12-20 | 2018-05-29 | 湖南润农生态茶油有限公司 | A kind of withered natural cleaning powder of oil tea and preparation method |
| CN108467679A (en) * | 2018-03-31 | 2018-08-31 | 裴文韬 | A kind of preparation method of high-durability solid wood maintenance wax |
| CN112159610A (en) * | 2020-09-14 | 2021-01-01 | 刘坚 | Antirust coating and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107669045A (en) * | 2017-08-23 | 2018-02-09 | 安徽楚艾农业科技有限公司 | A kind of wormwood pillow pillow inorganic agent and preparation method thereof |
| CN107739662A (en) * | 2017-11-30 | 2018-02-27 | 苏州龙腾万里化工科技有限公司 | Multiple-effect leather cleaning care agent |
| CN108085180A (en) * | 2017-12-20 | 2018-05-29 | 湖南润农生态茶油有限公司 | A kind of withered natural cleaning powder of oil tea and preparation method |
| CN108467679A (en) * | 2018-03-31 | 2018-08-31 | 裴文韬 | A kind of preparation method of high-durability solid wood maintenance wax |
| CN112159610A (en) * | 2020-09-14 | 2021-01-01 | 刘坚 | Antirust coating and preparation method thereof |
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