CN108158971A - A kind of ginseng U.S. face film and preparation method - Google Patents
A kind of ginseng U.S. face film and preparation method Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/00—Preparations for care of the skin
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
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Abstract
The present invention provides a kind of ginseng U.S. face film and preparation methods.Specific preparation process:1st, ginseng extract(1)Ginseng raw material is handled(2)It crushes(3)Extraction(4)It is concentrated under reduced pressure.2nd, the preparation 3 of deionized water, the preparation 4 of composite factor, the proportioning 5 of facial mask essence, sterilizing 6, filling system patch and envelope.Its process for integrally manufacturing is simple, and raw material is naturally easy to get, and the product good absorbing of preparation, effect is good, without side-effects, provide one it is simple for process, using simplicity, the facial mask for the features such as nutrition is comprehensive, with obvious effects, is a kind of beauty and skin care good merchantable brand of bright U.S. flesh.
Description
Technical field
The invention belongs to cosmetic mask preparing technical fields, are related to a kind of ginseng U.S. face film and preparation method.
Background technology
In the prior art, facial mask is a kind of cleaning, nurses, the cosmetics and skincare product of nutrition skin of face.The facial mask short time
Interior energy air-isolation and pollutant promote the surface temperature of skin of face, expand pore, promote sweat gland secretion, accelerate new old generation
It thanks, help excludes facial oil and metabolin, the effects that so as to reach tender skin, skin lightening.As facial mask market reaches its maturity, consumption
Person also gradually tends to the consumption demand of facial mask rationality, and product function subdivision and product safety environmental protection are the hairs in facial mask market future
Exhibition trend, abstraction function active material will be as facial mask future development importance as raw material from natural materials.
Ginseng principle active component saponin(e can enhance the metabolism of human body, have moist and trophism to skin, can promote skin blood
Liquid recycles, and skin dehydration, corrugation is prevented, so as to enhance skin elasticity delay skin aging.Ginsenoside also has stronger junket
Propylhomoserin enzyme inhibition activity, can whitening, nti-freckle, inhibition melanin generation.Baicalin is the principle active component of medicinal radix scutellariae, tool
There are antiallergy, anti-inflammatory, antiultraviolet, anti-oxidant and other effects, natural addition of the Chinese traditional herbs radix scutellariae as whitening day cream
Agent and it is widely used.With social progress and development, the increasingly raising of living standards of the people, cosmetics have more and more become existing
An indispensable part in living for life.At the same time, people are also higher and higher for the quality and performance requirement of cosmetics.
For this purpose, the present invention, based on ginseng, the herbal raw materials such as additional radix scutellariae develop ginseng U.S. face film, have adapted to people and have pursued peace
Entirely, the hope of natural beauty, has a vast market prospect, contributes to improve people’s lives quality.
Invention content
The present invention is to provide a kind of good absorbing under above-mentioned background, and delay skin aging, nutrition is comprehensive, and effect is good, work
The rational ginseng U.S. face film of skill and preparation method.
The technical scheme is that:A kind of ginseng U.S. face film, it is characterised in that be made of following raw material:Deionized water
85-120 parts, 0.01-0.03 parts of EDETATE SODIUM, 0.05-0.10 parts of dipotassium glycyrrhizinate, 0.1-0.2 parts of Chlorphenesin, niacinamide
0.1-5.0 parts, double 0.5-0.1 parts of-PEG-18 methyl ethers dimethylsilanes, glycerin polyether -26 be 1.0-2.0%, glycerine 6~8
Part, 6-8 parts of butanediol, 0.2~0.3 part of PEG-60 rilanit specials, 0.01 part~0.1 part of essence, acrylic acid(Ester)Class/C10-
30 0.11-0.13 parts of alkylol acrylamide acid esters cross-linked polymers, 0.02-0.04 parts of xanthans, Sodium Hyaluronate 0.01 part~0.05
Part, 0.15-0.20 parts of arginine, 0.1-0.3 parts of Phenoxyethanol, 1.0-3.0 parts of panthenol, 1,2- 0.1-0.2 parts of pentanediol, lactic acid
Bacillus/0.3-0.5 parts of soya-bean milk tunning filtrate, 0.001-0.003 parts of aaron's beard extract, peony root extractive
0.001-0.003 parts, radix scutellariae is with 0.001-0.003 parts of extract, 0.003-0.005 parts of ursin, citric acid 0.005-0.007
Part, 0.001-0.003 parts of Acetyl Tyrosine, glutathione 0.000, adds in sodium sulfite 0.005-0.006 by 5-0.0006 parts
Part, 0.4-0.8 parts of butanediol, 0.0005-0.0008 parts of aminopropanol ascorbic acid phosphoric acid esters, ginseng extract 0.05-0.10
Part.
Main component of the present invention is ginsenoside, and water logging extraction method is taken to extract, this method is easy, easy, safe, nontoxic,
Environmental protection, active constituent extraction is abundant, and raw material availability is high.The ginsenoside that the present invention is taken full advantage of in ginseng can improve skin
The antioxygenic activity of cell reduces the photooxidation as caused by irradiating ultraviolet light;Enhance the Scavenging activity of Skin Cell free radical, to brown
Spot, freckle and butterfly macules etc. are significant in efficacy, promote the blood circulation and metabolism of capillary in skin, increase the battalion of skin
Support supply, delay skin aging.The natural antibacterial ingredients such as radix scutellariae are added to, fungistatic effect protrudes, while mildly stingless to skin
Swash.Peony extract is added, intracellular O2- free radicals can be inhibited to generate, make skin brightening, fossil pigments in skin are restored
It fades.Containing a large amount of vitamin As in the aaron's beard extract of use, there is the work(for adjusting epidermis and cuticula metabolism
Effect can remove wrinkle with anti-aging, reduce seborrhea, make skin flexible.From ginseng, radix scutellariae, tree peony root, aaron's beard
The active material extracted in a variety of natural plants, has the advantages that natural environmental-protective.Employ ursin, citric acid, sodium sulfite,
A variety of skin conditioning agents such as Acetyl Tyrosine, aminopropanol ascorbic acid phosphoric acid esters, glutathione.Using natural surfactant
Bacillus acidi lactici/soya-bean milk tunning filtrate(LACTOBACILLUS/SOYMILK FERMENT FILTRATE), skin conditioning agent,
Rich in multivitamin and protein and active constituent, there is protection, releive, moisturizing, repair and whitening effect.Acrylic acid
(Ester)Class/C10-30 alkylol acrylamide acid esters cross-linked polymers(Acrylates C10-30 Alkyl Acrylate Cross
Polymer)It is used as thickener and stabilizer for film forming agent, water lock function is provided to product.
A kind of preparation method of ginseng U.S. face film, it is characterised in that step is as follows:
(1)Ginseng extract
(a)Ginseng raw material is handled:The middle ten days and the last ten days in September selects the fresh ginsengs of 4-6, scrubs, obtains fresh ginseng, dry, obtains dry people
Ginseng.
(b)It crushes:Fine powder is ground into, after crossing 200-300 mesh sieve, obtains Ginseng Root Powder.
(c)Extraction:Ginseng Root Powder with water by 1: 8-10 times is measured and extracts secondary, immersion 1.0-1.5 before extracting for the first time
H, temperature are maintained at 80~90 DEG C, and boiling extraction 2-2.5h, filtration separates extracting solution;Again in solid-liquid ratio be 6-8: 1 ratio with
Water mixes, and temperature is maintained at 80~90 DEG C, and boiling extraction 1.5-2.0h separates extracting solution, No. 2 extracting solutions are merged, are carried out dense
Contracting.
(d)It is concentrated under reduced pressure:By the extracting solution of merging, control temperature is at 65-75 DEG C, and pressure is in -0.06~-0.08MPa items
Under part, it is 1.0~1.20 to be concentrated under reduced pressure into relative density.
(2) preparation of deionized water
Using reverse osmose pure-water equipment, using tap water as raw water, at room temperature in the condition that reverse osmosis pressure is 0.2~0.6Mpa
It is lower to prepare deionized sterile water.
(3) preparation of composite factor
Step 1:In the emulsion tank of mulser, parts by weight of deionized water is added in, it is 0~40 DEG C to adjust temperature, is then being stirred
In the case of sequentially add 0.01-0.03 parts of parts by weight EDETATE SODIUM, 0.05-0.10 parts of dipotassium glycyrrhizinate, Chlorphenesin 0.1-
0.2 part, 0.1-5.0 parts of niacinamide, double 0.5-0.1 parts of-PEG-18 methyl ethers dimethylsilanes, glycerin polyether -26 is 1.0-
2.0%, emulsification machine scraper speed of agitator is adjusted to 25RPM by 6~8 parts of glycerine, 6-8 parts of butanediol at room temperature, after uniform dissolution,
Stop stirring, obtain mixed solution A phase, A phases are imported in material pot, it is spare.
Step 2:In the case of stirring successively into emulsion tank by parts by weight PEG-60 rilanit specials 0.2~0.3
Part, 0.01 part~0.1 part of essence is slowly launched in emulsion tank, under conditions of emulsification machine scraper speed of agitator is adjusted to 25RPM
Stirring can discharge after 3 minutes, obtain mixed solution B phases, B phases are imported in another material pot, spare.
Step 3:20-30 parts of parts by weight of deionized water is first added in into emulsion tank, adjusts temperature at 30-40 DEG C, then stirring
It is slowly arrived successively in the case of mixing and adds in acrylic acid(Ester)Class/C10-30 alkylol acrylamide acid esters cross-linked polymers 0.11-0.13
Part, 0.02-0.04 parts of xanthans, 0.01 part~0.05 part of Sodium Hyaluronate makes it be adjusted in emulsification machine scraper speed of agitator
Under conditions of 25RPM, after stirring 3 minutes, make its fully dispersed and uniform dissolution is to transparent, stop stirring, obtain mixed solution C
Phase imports C phases in another material pot, spare.
Step 4:20-30 parts of parts by weight of deionized water is first added in into emulsion tank, adjusts temperature at 30-40 DEG C, then stirring
It adds in 0.15-0.20 parts of arginine in the case of mixing into emulsion tank successively, machine scraper speed of agitator is emulsified in lift type vacuum
Be adjusted under conditions of 25RPM, stirring 3 minutes after, it is fully dispersed and be dissolved to it is transparent, stop stirring, obtain mixed solution D phases, will
D phases are imported in another material pot, spare.
Step 5:Add in 0.1-0.3 parts of parts by weight Phenoxyethanol, panthenol into emulsion tank successively in the case of stirring
1.0-3.0 parts, 1,2- 0.1-0.2 parts of pentanediol, Bacillus acidi lactici/0.3-0.5 parts of soya-bean milk tunning filtrate, aaron's beard carries
0.001-0.003 parts of object, 0.001-0.003 parts of peony root extractive, radix scutellariae are taken with 0.001-0.003 parts of extract, ursin
0.003-0.005 parts, 0.005-0.007 parts of citric acid, 0.001-0.003 parts of Acetyl Tyrosine, glutathione 0.000,5-
0.0006 part, add in 0.005-0.006 parts of sodium sulfite, 0.4-0.8 parts of butanediol, aminopropanol ascorbic acid phosphoric acid esters
0.0005-0.0008 parts, after 0.05-0.10 parts of ginseng extract, being transferred to scraper plate speed of agitator in lift type vacuum mulser is
It under conditions of 25RPM, is stirred 1 minute, makes its fully dispersed and uniform dissolution, stopping stirring obtaining mixed solution E phases, by E
It mutually imports in another material pot, it is spare.
(4) preparation of facial mask essence
First mixed solution A is mutually injected in the emulsion tank of mulser, it is 0~40 DEG C to adjust temperature, then in the case of stirring
Mixed solution B phases are slowly added to, emulsification machine scraper speed of agitator is adjusted to 25RPM at room temperature, after stirring 3 minutes, reaches and fills
Point dispersion and uniform dissolution, by above-mentioned same process again successively by mixed solution C phase, D phases, that E phases inject lift is true
In the emulsion tank of empty mulser, facial mask essence is obtained.
(5) sterilizing
It is placed on after carrying out ozone sterilization 1-1.5h in ozone disinfection cabinet and uses before non-woven fabrics Face film towel is filling, each raw material of facial mask
It mutually puts and preserves between sterilizing state in the UV lamp, meet very rigorous sanitary regulations.
(6) filling system patch and envelope.
Compared with prior art, main advantages of the present invention are:
1st, main component of the present invention is ginsenoside, water logging extraction method is taken to extract, this method is easy, easy, safe, nontoxic, ring
It protects, active constituent extraction is abundant, and raw material availability is high.It is thin that the ginsenoside that the present invention is taken full advantage of in ginseng can improve skin
The antioxygenic activity of born of the same parents reduces the photooxidation as caused by irradiating ultraviolet light;Enhance the Scavenging activity of Skin Cell free radical, to brown
Spot, freckle and butterfly macules etc. are significant in efficacy, promote the blood circulation and metabolism of capillary in skin, increase the battalion of skin
Support supply, delay skin aging.
2nd, the problem of colonizing skin for microorganism, the present invention are added to the natural antibacterial ingredients such as radix scutellariae in facial mask, press down
Bacterium effect protrudes, while mildly non-stimulated to skin;Present invention adds peony extracts, can inhibit intracellular O2- free radicals
It generates, makes skin brightening, by fossil pigments Reduction fading in skin;Containing big in the aaron's beard extract that the present invention uses
Vitamin A is measured, has effects that adjust epidermis and cuticula is metabolic, can wrinkle be gone with anti-aging, reduce seborrhea,
Make skin flexible.
3rd, inventive formulation is scientific and reasonable, and basic ingredient is from ginseng, radix scutellariae, tree peony root, a variety of days of aaron's beard
The active material extracted in right plant, has the advantages that natural environmental-protective.Present invention employs ursin, citric acid, sulfurous simultaneously
A variety of skin conditioning agents such as sour sodium, Acetyl Tyrosine, aminopropanol ascorbic acid phosphoric acid esters, glutathione, each raw material
Dosage and physicochemical property generate synergistic effect.It is rich simultaneously using natural surfactant Bacillus acidi lactici/soya-bean milk tunning filtrate
Containing multivitamin and protein and active constituent, there is protection, releive, moisturizing, repair and whitening effect.
4th, the present invention takes the process that split-phase is configured, respectively the pre- stirring and dissolving in different material pots, first by face
Film is dissolved in principal component such as EDTA disodiums, dipotassium glycyrrhizinate, Chlorphenesin, niacinamide, the double-PEG-18 methyl ethers dimethyl of water
Fully water phase is made in dissolving in material pot for silane, glycerin polyether -26 etc.(A phases), then by main oil-phase component such as PEG-60 hydrogen
Change the dissolvings such as castor oil and oil phase is made(B phases), the agent such as xanthans, Sodium Hyaluronate of facial mask support facial mask is configured to C
Phase, by nutrition U.S. face additive such as arginine, Bacillus acidi lactici/soya-bean milk tunning filtrate, aaron's beard extract, tree peony root
Extract, radix scutellariae are classified again with extract, ursin, citric acid, Acetyl Tyrosine, glutathione, ginseng extract etc. to be made
D, E phases.The water phase A phase materials being stirred are imported into emulsion tank, then oil phase tank is slowly added into water phase when Essence is configured, are made
Material is sufficiently mixed uniformly, and all kinds of nourishing additive agents then are made C, D, E phase again is slowly added into respectively, carries out emulsifying,
So configuration process makes formula system more stable, ensure that Essence production quality.
5th, the invention belongs to multifunction strengthened face paste cloth type facial masks, use molding class facial mask of the non-woven fabrics face paste for matrix,
Non-woven fabrics face paste has soft sticking nature, gas permeability and comfort, enhances absorption property, whitening effect is made to reach more preferably.Together
When contribute to facial mask liquid to skin carry out persistently and the moisturizing of deep layer, it is more obvious to the improvement of skin.
6th, facial mask preparation method method of the invention, Mechanization Level are high so that filling system patch is with envelope in full-automation
It is completed in facial mask production equipment, solves in facial mask production that packaging effect is poor, bad product rate is high, it is impossible to be automatically performed facial mask life
Production, it is difficult to ensure the work problem of the facial mask quality of production.The present invention uses independent non-returnable container, and convenient and health prevents two
Secondary pollution, realize mechanization, scale industrial production.
Specific embodiment
Embodiment 1
A kind of preparation method of ginseng U.S. face film, it is characterised in that step is as follows:
1st, ginseng extract
(1)Ginseng raw material is handled:The middle ten days and the last ten days in September, the fresh ginseng of the disease-free scars of 4-6 of selection ginseng ground harvesting, and to selected ginseng
Input, which is washed in ginseng machine, after progress impurity elimination is scrubbed, then the fresh ginseng that human assistance scrub, acquisition are cleaned.Fresh people after scrubbing
Ginseng is dried or alternating temperature is dried in hothouse, obtains dry ginseng.
(2)It crushes:Dry ginseng is crushed using ultralow temperature wall-broken grinder, is ground into fine powder, crosses 200-300
After mesh sieve, Ginseng Root Powder is obtained.
(3)Extraction:Ginseng Root Powder and water (W/V=1: 8-10 times is measured) extraction is secondary, impregnate 1.0- before extracting for the first time
1.5 h, temperature are maintained at 80~90 DEG C, and boiling extraction 2-2.5h, filtration separates extracting solution.Again by the ratio that solid-liquid ratio is 6-8: 1
Example is mixed with water, and temperature is maintained at 80~90 DEG C, and boiling extraction 1.5-2.0h separates extracting solution, No. 2 extracting solutions are merged, into
Row concentration.
(4)It is concentrated under reduced pressure:By the extracting solution of merging, control temperature is at 65-75 DEG C, and pressure is in -0.06~-0.08MPa items
Under part, it is 1.0~1.20 to be concentrated under reduced pressure into relative density.
2nd, the preparation of deionized water
Using reverse osmose pure-water equipment, using tap water as raw water, at room temperature in the condition that reverse osmosis pressure is 0.2~0.6Mpa
It is lower to prepare deionized sterile water.
3rd, the preparation of composite factor
Step 1:In the emulsion tank of lift type vacuum mulser, parts by weight of deionized water is added in, it is 0~40 DEG C to adjust temperature,
Then 0.01-0.03 parts of parts by weight EDETATE SODIUM, 0.05-0.10 parts of dipotassium glycyrrhizinate, chlorine are sequentially added in the case of stirring
Sweet ether 0.1-0.2 parts of benzene, 0.1-5.0 parts of niacinamide, double 0.5-0.1 parts of-PEG-18 methyl ethers dimethylsilanes, glycerin polyether-
26 be 1.0-2.0%, 6~8 parts of glycerine, 6-8 parts of butanediol;Emulsification machine scraper speed of agitator is adjusted to 25RPM at room temperature, is stirred
Mixing material in emulsion tank makes its fully dispersed and after uniform dissolution, stops stirring, obtains mixed solution A phase, A phases are imported material pot
It is interior, it is spare.
Step 2:In the case of stirring successively into emulsion tank by parts by weight PEG-60 rilanit specials 0.2~0.3
Part, 0.01 part~0.1 part of (daily) essence is slowly launched in emulsion tank, is adjusted to 25RPM's in emulsification machine scraper speed of agitator
Under the conditions of stir 3 minutes after, make its fully dispersed and uniform dissolution be to transparent, stop stirring, you can discharging obtains mixed solution B
Phase imports B phases in another material pot, spare.
Step 3:20-30 parts of parts by weight of deionized water is first added in into emulsion tank, adjusts temperature at 30-40 DEG C, then stirring
It is slowly arrived successively in the case of mixing and adds in acrylic acid(Ester)Class/C10-30 alkylol acrylamide acid esters cross-linked polymers 0.11-0.13
Part, 0.02-0.04 parts of xanthans, 0.01 part~0.05 part of Sodium Hyaluronate makes it be adjusted in emulsification machine scraper speed of agitator
Under conditions of 25RPM, after stirring 3 minutes, make its fully dispersed and uniform dissolution is to transparent, stop stirring, obtain mixed solution C
Phase imports C phases in another material pot, spare.
Step 4:20-30 parts of parts by weight of deionized water is first added in into emulsion tank, adjusts temperature at 30-40 DEG C, then stirring
It adds in 0.15-0.20 parts of arginine in the case of mixing into emulsion tank successively, machine scraper speed of agitator is emulsified in lift type vacuum
Be adjusted under conditions of 25RPM, stirring 3 minutes after, it is fully dispersed and be dissolved to it is transparent, stop stirring, obtain mixed solution D phases, will
D phases are imported in another material pot, spare.
Step 5:Add in 0.1-0.3 parts of parts by weight Phenoxyethanol, panthenol into emulsion tank successively in the case of stirring
1.0-3.0 parts, 1,2- 0.1-0.2 parts of pentanediol, Bacillus acidi lactici/0.3-0.5 parts of soya-bean milk tunning filtrate, aaron's beard carries
0.001-0.003 parts of object, 0.001-0.003 parts of peony root extractive, radix scutellariae are taken with 0.001-0.003 parts of extract, ursin
0.003-0.005 parts, 0.005-0.007 parts of citric acid, 0.001-0.003 parts of Acetyl Tyrosine, glutathione 0.000,5-
0.0006 part, add in 0.005-0.006 parts of sodium sulfite, 0.4-0.8 parts of butanediol, aminopropanol ascorbic acid phosphoric acid esters
0.0005-0.0008 parts, after 0.05-0.10 parts of ginseng extract, being transferred to scraper plate speed of agitator in lift type vacuum mulser is
It under conditions of 25RPM, is stirred 1 minute, makes its fully dispersed and uniform dissolution, stopping stirring obtaining mixed solution E phases, by E
It mutually imports in another material pot, it is spare.
4th, the preparation of facial mask essence
First mixed solution A is mutually injected in the emulsion tank of lift type vacuum mulser, it is 0~40 DEG C to adjust temperature, is then being stirred
Mixed solution B phases are slowly added in the case of mixing, emulsification machine scraper speed of agitator is adjusted to 25RPM at room temperature, are stirred 3 minutes
Afterwards, reach fully dispersed and uniform dissolution, again successively inject mixed solution C phase, D phases, E phases by above-mentioned same process
In the emulsion tank of lift type vacuum mulser, facial mask essence is obtained.
5th, sterilizing
Facial mask produces under stringent asepsis requirements, and 100,000 grades of gmp standards should be reached by producing filling preparation process.Non-woven fabrics Face film towel
It is placed on after carrying out ozone sterilization 1-1.5h in ozone disinfection cabinet and uses before filling, each raw material of facial mask is mutually put to go out in the UV lamp
It is preserved between bacterium state, meets very rigorous sanitary regulations.
6th, filling system patch and envelope
Filling system patch is completed with envelope in full-automatic facial mask production equipment, and facial mask cloth repeatedly fold and should by equipment
The facial mask cloth of folding is fitted into packaging bag, receives the packaging bag equipped with facial mask cloth by equipment device for filling, Essence is quantified
It is filled into packaging bag, the facial mask cloth in it is made to be infiltrated by Essence;Then the closing device of equipment is by the sack of the packaging bag
Sealing;The printing equipment of equipment completes the printing of product information in the sealing and packaging bag of sack.
Embodiment 2
Production engineering table, is shown in Table 1.
Table 1
Record of production book, is shown in Table 2
Table 2
Claims (2)
1. a kind of ginseng U.S. face film, it is characterised in that be made of following raw material:85-120 parts of deionized water, EDETATE SODIUM
0.01-0.03 parts, 0.05-0.10 parts of dipotassium glycyrrhizinate, 0.1-0.2 parts of Chlorphenesin, 0.1-5.0 parts of niacinamide, double-PEG-18
0.5-0.1 parts of methyl ether dimethylsilane, glycerin polyether -26 be 1.0-2.0%, 6~8 parts of glycerine, 6-8 parts of butanediol, PEG-
60 0.2~0.3 part of rilanit specials, 0.01 part~0.1 part of essence, acrylic acid(Ester)Class/C10-30 alkylol acrylamides acid esters crosslinking
0.11-0.13 parts of polymer, 0.02-0.04 parts of xanthans, 0.01 part~0.05 part of Sodium Hyaluronate, arginine 0.15-0.20
Part, 0.1-0.3 parts of Phenoxyethanol, 1.0-3.0 parts of panthenol, 1,2- 0.1-0.2 parts of pentanediol, Bacillus acidi lactici/soya-bean milk tunning
0.3-0.5 parts of filtrate, 0.001-0.003 parts of aaron's beard extract, 0.001-0.003 parts of peony root extractive, radix scutellariae with
0.001-0.003 parts of extract, 0.003-0.005 parts of ursin, 0.005-0.007 parts of citric acid, Acetyl Tyrosine 0.001-
0.003 part, glutathione 0.000, adds in 0.005-0.006 parts of sodium sulfite, 0.4-0.8 parts of butanediol, ammonia by 5-0.0006 parts
0.0005-0.0008 parts of base propyl alcohol ascorbic acid phosphoric acid esters, 0.05-0.10 parts of ginseng extract.
2. the preparation method of ginseng U.S. face film as described in claim 1, it is characterised in that step is as follows:
(1)Ginseng extract
(a)Ginseng raw material is handled:The middle ten days and the last ten days in September selects the fresh ginsengs of 4-6, scrubs, obtains fresh ginseng, dry, obtains dry people
Ginseng;
(b)It crushes:Fine powder is ground into, after crossing 200-300 mesh sieve, obtains Ginseng Root Powder;
(c)Extraction:It is secondary that Ginseng Root Powder and water by 1: 8-10 times are measured into extraction, 1.0-1.5 h are impregnated before extracting for the first time, it is warm
Degree is maintained at 80~90 DEG C, and boiling extraction 2-2.5h, filtration separates extracting solution;It is mixed again in the ratio that solid-liquid ratio is 6-8: 1 with water
It closes, temperature is maintained at 80~90 DEG C, and boiling extraction 1.5-2.0h separates extracting solution, No. 2 extracting solutions are merged, are concentrated;
(d)It is concentrated under reduced pressure:By the extracting solution of merging, control temperature is at 65-75 DEG C, and pressure is in -0.06~-0.08MPa conditions
Under, it is 1.0~1.20 to be concentrated under reduced pressure into relative density;
(2) preparation of deionized water
Using reverse osmose pure-water equipment, using tap water as raw water, at room temperature in the condition that reverse osmosis pressure is 0.2~0.6Mpa
It is lower to prepare deionized sterile water;
(3) preparation of composite factor
Step 1:In the emulsion tank of mulser, parts by weight of deionized water is added in, it is 0~40 DEG C to adjust temperature, is then being stirred
In the case of sequentially add 0.01-0.03 parts of parts by weight EDETATE SODIUM, 0.05-0.10 parts of dipotassium glycyrrhizinate, Chlorphenesin 0.1-
0.2 part, 0.1-5.0 parts of niacinamide, double 0.5-0.1 parts of-PEG-18 methyl ethers dimethylsilanes, glycerin polyether -26 is 1.0-
2.0%, emulsification machine scraper speed of agitator is adjusted to 25RPM by 6~8 parts of glycerine, 6-8 parts of butanediol at room temperature, after uniform dissolution,
Stop stirring, obtain mixed solution A phase, A phases are imported in material pot, it is spare;
Step 2:It is fragrant in the case of stirring successively into emulsion tank by 0.2~0.3 part of parts by weight PEG-60 rilanit specials
0.01 part~0.1 part of essence is slowly launched in emulsion tank, and 3 are stirred under conditions of emulsification machine scraper speed of agitator is adjusted to 25RPM
It can discharge after minute, obtain mixed solution B phases, B phases are imported in another material pot, it is spare;
Step 3:20-30 parts of parts by weight of deionized water is first added in into emulsion tank, adjusts temperature at 30-40 DEG C, then in stirring
In the case of slowly arrive successively add in acrylic acid(Ester)Class/0.11-0.13 parts of C10-30 alkylol acrylamides acid esters cross-linked polymer, it is yellow
0.02-0.04 parts of virgin rubber, 0.01 part~0.05 part of Sodium Hyaluronate make it be adjusted to 25RPM's in emulsification machine scraper speed of agitator
Under the conditions of, after stirring 3 minutes, make its fully dispersed and uniform dissolution is to transparent, stop stirring, mixed solution C phase is obtained, by C phases
It imports in another material pot, it is spare;
Step 4:20-30 parts of parts by weight of deionized water is first added in into emulsion tank, adjusts temperature at 30-40 DEG C, then in stirring
In the case of successively into emulsion tank add in 0.15-0.20 part of arginine, lift type vacuum emulsify machine scraper speed of agitator be adjusted to
Under conditions of 25RPM, stirring 3 minutes after, it is fully dispersed and be dissolved to it is transparent, stop stirring, mixed solution D phases are obtained, by D phases
It imports in another material pot, it is spare;
Step 5:Add in 0.1-0.3 parts of parts by weight Phenoxyethanol, panthenol 1.0- into emulsion tank successively in the case of stirring
3.0 parts, 1,2- 0.1-0.2 parts of pentanediol, Bacillus acidi lactici/0.3-0.5 parts of soya-bean milk tunning filtrate, aaron's beard extract
0.001-0.003 parts, 0.001-0.003 parts of peony root extractive, radix scutellariae is with 0.001-0.003 parts of extract, ursin
0.003-0.005 parts, 0.005-0.007 parts of citric acid, 0.001-0.003 parts of Acetyl Tyrosine, glutathione 0.000,5-
0.0006 part, add in 0.005-0.006 parts of sodium sulfite, 0.4-0.8 parts of butanediol, aminopropanol ascorbic acid phosphoric acid esters
0.0005-0.0008 parts, after 0.05-0.10 parts of ginseng extract, being transferred to scraper plate speed of agitator in lift type vacuum mulser is
It under conditions of 25RPM, is stirred 1 minute, makes its fully dispersed and uniform dissolution, stopping stirring obtaining mixed solution E phases, by E
It mutually imports in another material pot, it is spare;
(4) preparation of facial mask essence
First mixed solution A is mutually injected in the emulsion tank of mulser, it is 0~40 DEG C to adjust temperature, then in the case of stirring
Mixed solution B phases are slowly added to, emulsification machine scraper speed of agitator is adjusted to 25RPM at room temperature, after stirring 3 minutes, reaches and fills
Point dispersion and uniform dissolution, by above-mentioned same process again successively by mixed solution C phase, D phases, that E phases inject lift is true
In the emulsion tank of empty mulser, facial mask essence is obtained;
(5) sterilizing
It is placed on after carrying out ozone sterilization 1-1.5h in ozone disinfection cabinet and uses before non-woven fabrics Face film towel is filling, each raw material of facial mask
It mutually puts and preserves between sterilizing state in the UV lamp, meet very rigorous sanitary regulations;
(6) filling system patch and envelope.
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Cited By (5)
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CN108542793A (en) * | 2018-07-11 | 2018-09-18 | 南京汇因美化妆品有限公司 | Water moistens maintenance beautifying facial mask and its preparation method and application |
CN108542833A (en) * | 2018-07-11 | 2018-09-18 | 南京汇因美化妆品有限公司 | Water moistens moisturizing beautifying facial mask and its preparation method and application |
CN110179717A (en) * | 2019-07-03 | 2019-08-30 | 吉林省诚仁达医疗技术发展有限公司 | A kind of ginseng vesica cleaning pack and preparation method thereof |
CN110917092A (en) * | 2019-12-10 | 2020-03-27 | 士齐生物研发中心(苏州工业园区)有限公司 | Antioxidant composition and application thereof |
CN113975199A (en) * | 2021-11-03 | 2022-01-28 | 胡昌山 | Skin-firming wrinkle-removing anti-aging essence and preparation process thereof |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108542793A (en) * | 2018-07-11 | 2018-09-18 | 南京汇因美化妆品有限公司 | Water moistens maintenance beautifying facial mask and its preparation method and application |
CN108542833A (en) * | 2018-07-11 | 2018-09-18 | 南京汇因美化妆品有限公司 | Water moistens moisturizing beautifying facial mask and its preparation method and application |
CN110179717A (en) * | 2019-07-03 | 2019-08-30 | 吉林省诚仁达医疗技术发展有限公司 | A kind of ginseng vesica cleaning pack and preparation method thereof |
CN110917092A (en) * | 2019-12-10 | 2020-03-27 | 士齐生物研发中心(苏州工业园区)有限公司 | Antioxidant composition and application thereof |
CN113975199A (en) * | 2021-11-03 | 2022-01-28 | 胡昌山 | Skin-firming wrinkle-removing anti-aging essence and preparation process thereof |
CN113975199B (en) * | 2021-11-03 | 2024-04-16 | 胡昌山 | Preparation process of skin tightening, wrinkle removing and anti-aging essence |
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