CN105560129B - A kind of preparation method of pure natural draft pasteurization towelette - Google Patents
A kind of preparation method of pure natural draft pasteurization towelette Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses a kind of preparation methods of pure natural draft pasteurization towelette, belong to wet tissue preparation technical field.Using the moso bamboo blueness thin bamboo strip as raw material, fermented, charing is made bamboo charcoal fiber, and extracts tea tree ethereal oil and make natural disinfectant agent the present invention, most afterwards through gelatinized starch adhesion, hydrogen peroxide foaming, antiseptic-soaked, to obtain the preparation method of pure natural draft pasteurization towelette.Example proves, operation of the present invention is easy, using the natural moso bamboo blueness thin bamboo strip as raw material, instead of traditional non-woven cloth, can voluntarily degrade after, it is pollution-free, in addition during preparation, any chemical reagents, the addition of alcohol-free, essence and preservative are not added, with it is rear to skin without any harm, be a kind of efficient, nontoxic, degradable environmentally protective pasteurization towelette.
Description
Technical field
The invention discloses a kind of preparation methods of pure natural draft pasteurization towelette, belong to wet tissue preparation technical field.
Background technique
With the continuous improvement of social and economic level, people, which are no longer only satisfied with, to have enough to eat and wear, and more starts to focus on life
Taste, improves the quality of living.Increasingly severe pollution problem causes the enough attention of people, more focuses on safety therewith and defends
Raw, sterilizing, then there have been easy to carry, safety and sanitation Sanitary products based on pasteurization towelette.
Especially in recent years, the application of hygenic towelette and disinfection wet tissue gradually increases, however traditional wet tissue is mostly with poly-
Ethylene, polypropylene, polyester and polyamide are the non-woven cloth of material as matrix, although cheap, its is maximum
Disadvantage videlicet can not be biodegradable, and is difficult to recycle, and a large amount of uses will cause white pollution.In addition, functional wet for manufacture
Towel, it is also necessary to prepare the reagent comprising many chemical components, water source easy to pollute.
In addition, currently used disinfected paper napkin is typically all containing alcohol, essence and preservative, alcohol has volatilization
Property, it being easy after wiping so that skin surface water loss, essence has stimulation component, there is an injury to human skin, easy allergy, separately
Outer preservative also easily causes allergy, easily carcinogenic.
Therefore, one kind can either effectively cleaning-sterilizing will not generate stimulation again, and can voluntarily degrade, non-environmental-pollution
Pasteurization towelette be consumer there is an urgent need to.
Summary of the invention
Present invention mainly solves the technical issues of：It is mostly with non-woven cloth and tradition for current traditional disinfection wet tissue
Paper made from paper process is matrix, although cheap, easily biological-degradable, does not in addition contain in common pasteurization towelette big
The chemical reagent of amount makes skin surface moisture be easy to be lost containing alcohol, essence and preservative after using, easy allergy, easily
Carcinogenic status is provided using one kind using the moso bamboo blueness thin bamboo strip as raw material, and bamboo charcoal fiber is made in fermented, charing, and extracts tea tree essence
Oil makees natural disinfectant agent, most afterwards through gelatinized starch adhesion, hydrogen peroxide foaming, antiseptic-soaked, to obtain pure natural draft
The preparation method of pasteurization towelette.This method is easy to operate, using the natural moso bamboo blueness thin bamboo strip as raw material, instead of traditional non-woven cloth,
Can voluntarily degrade after, in addition during preparation, not add any chemical reagents, alcohol-free, essence and preservative plus
Enter, is a kind of efficient, nontoxic, degradable environmentally protective pasteurization towelette for skin also without any harm after.
In order to solve the above-mentioned technical problem, the technical scheme adopted by the invention is that：
（1）Weigh the segment that 900~1000g moso bamboo blueness thin bamboo strip is cut into 3~5cm with chopper, place in an oven in 100~
Manually extract bamboo fiber crops at 105 DEG C after dry 1~2h, then by obtained bamboo fiber crops be respectively put into concentration be 0.5mol/L hydrochloric acid solution and
2~4h is impregnated in 0.3mol/L soda bath, and bamboo fiber crops are taken out after immersion with deionized water and rinse 3~5 times and natural air drying；
（2）By it is above-mentioned air-dry after bamboo fiber crops and oil emulsion by solid-to-liquid ratio be 1:1 mixed after be put into fermentor, 35~
It is sealed by fermentation at 45 DEG C 1~2 week, takes out fermentation liquid after fermentation and be put into supercentrifuge with 7000~8000r/min rate
It is centrifugally separating to obtain bamboo fibre, then bamboo fibre will be obtained and move into retort, is warming up to 300~400 with 10 DEG C/min rate program
DEG C charing 40~50min, it is spare up to bamboo charcoal fiber after being cooled to room temperature；
（3）1~2kg tea free is weighed, rinses blade surface 3~5 times with deionized water to remove floating dust impurity, then will punching
Tea leaf after washing moves into agate mortar after being ground into 1~2cm fritter with airslide disintegrating mill, is fully ground 30~40min
Until blade fritter is at paste；
（4）500~600g paste obtained above is weighed to be put into the three-necked flask with air inlet pipe and condensing unit,
It is passed through 150~160 DEG C of vapor into flask by air inlet pipe with 10mL/min rate to be distilled, distillate is cold through condenser pipe
It instills in 100mL brown bottle and saves to get tea tree ethereal oil natural disinfectant agent dropwise after solidifying, it is spare；
（5）The spare bamboo charcoal fiber of 50~60g and 400~500mL distilled water is weighed to be uniformly mixed, with magnetic stirrer into
Row stirring, adds 30~40g starch during stirring, continues after 10~15min of stirring in 70~80 DEG C of water bath conditions
Lower gelatinization handles 2~3h, and mixture is put into concentration removing moisture in vacuum dehydration can after the completion of gelatinization；
（6）It is 10 by solid-to-liquid ratio:1 is uniformly mixed the hydrogen peroxide for shape object being mixed after above-mentioned dehydration and mass concentration is 30% simultaneously
It injects in 10cm × 10cm × 2mm glass mold, so that it is prolonged stream film forming naturally, use 100~105 DEG C of vapor after the completion of note film
20~30min of stifling curing makes its foaming form soft loose porous paper membrane, then by the paper membrane vacuum freeze-drying machine after curing
Freeze-drying makes wet tissue base-material by oneself after taking off film to obtain the final product；
（7）Above-mentioned self-control wet tissue base-material is laid in the container bottom of sonic oscillation instrument, spare tea is added into container
Tree the agent of essential oil natural disinfectant make its submerge wet tissue base-material, start shaker under 100~200W power ultrasonic immersing absorption 10~
12h impregnates and takes out wet tissue after the completion, up to pure natural draft pasteurization towelette after packaging.
Application method of the invention is：In use, taking out pasteurization towelette produced by the present invention, human body portion to be sterilized is wiped
Position.After use, it is not necessarily to special recycling, pasteurization towelette produced by the present invention starts voluntarily to degrade in the soil for 10~15 days,
General 25~40 days i.e. degradable to finish, environmentally protective, pollution-free, and feel refrigerant pleasant after human body use, does not have for skin
There is any harm, bacteriostasis rate reaches 98% or more.
The beneficial effects of the invention are as follows：
（1）The method of the present invention is unique novel, simple process；
（2）The present invention is that raw material can voluntarily degrade after instead of traditional non-woven cloth using the natural moso bamboo blueness thin bamboo strip,
General 25~40 days i.e. it is degradable finish, it is environmentally protective, it is pollution-free；
（3）During preparation, any chemical reagents are not added, the addition of alcohol-free, essence and preservative is right after
In skin also without any harm, bacteriostasis rate is up to 98% or more.
Specific embodiment
Weigh the segment that 900~1000g moso bamboo blueness thin bamboo strip is cut into 3~5cm with chopper first, place in an oven in 100~
Manually extract bamboo fiber crops at 105 DEG C after dry 1~2h, then by obtained bamboo fiber crops be respectively put into concentration be 0.5mol/L hydrochloric acid solution and
2~4h is impregnated in 0.3mol/L soda bath, and bamboo fiber crops are taken out after immersion with deionized water and rinse 3~5 times and natural air drying；
Then by it is above-mentioned air-dry after bamboo fiber crops and oil emulsion by solid-to-liquid ratio be 1:1 mixed after be put into fermentor, at 35~45 DEG C
It is sealed by fermentation 1~2 week, takes out fermentation liquid after fermentation and be put into supercentrifuge with the centrifugation point of 7000~8000r/min rate
From obtaining bamboo fibre, then bamboo fibre will be obtained and move into retort, 300~400 DEG C of charings are warming up to 10 DEG C/min rate program
40~50min, it is spare up to bamboo charcoal fiber after being cooled to room temperature；Next 1~2kg tea free is weighed, is rinsed with deionized water
1~2cm fritter is ground into airslide disintegrating mill to remove floating dust impurity, then by the tea leaf after flushing blade surface 3~5 times
It moves into agate mortar afterwards, is fully ground 30~40min until blade fritter is at paste；The above-mentioned system of 500~600g is weighed again
Paste be put into the three-necked flask with air inlet pipe and condensing unit, by air inlet pipe with 10mL/min rate to flask
In be passed through 150~160 DEG C of vapor and distilled, distillate is instilled in 100mL brown bottle dropwise after condensing tube condensation and is saved,
It is spare up to tea tree ethereal oil natural disinfectant agent；The spare bamboo charcoal fiber of 50~60g is weighed later and 400~500mL distilled water is mixed
It closes uniformly, is stirred with magnetic stirrer, 30~40g starch is added during stirring, continue 10~15min of stirring
Mixture is put into concentration in vacuum dehydration can after the completion of gelatinization and taken off by 2~3h of gelatinization processing under 70~80 DEG C of water bath conditions afterwards
Moisture removal；It is 10 by solid-to-liquid ratio:The hydrogen peroxide for shape object being mixed after above-mentioned dehydration and mass concentration is 30% is uniformly mixed and is injected by 1
In 10cm × 10cm × 2mm glass mold, so that it is prolonged stream film forming naturally, use 100~105 DEG C of vapor stifling after the completion of note film
20~30min of curing makes its foaming form soft loose porous paper membrane, then the paper membrane after curing is lyophilized with vacuum freeze-drying machine,
Wet tissue base-material is made by oneself to obtain the final product after taking off film；Above-mentioned self-control wet tissue base-material is finally laid in the container bottom of sonic oscillation instrument, Xiang Rong
Spare tea tree ethereal oil natural disinfectant agent is added in device makes it submerge wet tissue base-material, starts shaker under 100~200W power
10~12h is adsorbed in ultrasonic immersing, taking-up wet tissue after the completion of dipping, up to pure natural draft pasteurization towelette after packaging.
Example 1
The segment that the 900g moso bamboo blueness thin bamboo strip is cut into 3cm with chopper is weighed first, is placed in an oven at 100 DEG C after dry 1h
It is artificial to extract bamboo fiber crops, then it is in 0.5mol/L hydrochloric acid solution and 0.3mol/L soda bath that obtained bamboo fiber crops, which are respectively put into concentration,
2h is impregnated, bamboo fiber crops are taken out after immersion with deionized water and rinse 3 times and natural air drying；Then by it is above-mentioned air-dry after bamboo fiber crops and
Oil emulsion is 1 by solid-to-liquid ratio:1 mixed after be put into fermentor, be sealed by fermentation 1 week at 35 DEG C, take out hair after fermentation
Zymotic fluid is put into supercentrifuge and is centrifugally separating to obtain bamboo fibre with 7000r/min rate, then will obtain bamboo fibre and move into retort,
300 DEG C of charing 40min are warming up to 10 DEG C/min rate program, it is spare up to bamboo charcoal fiber after being cooled to room temperature；Next claim
1kg tea free is taken, rinses blade surface 3 times with deionized water to remove floating dust impurity, then by the tea leaf gas after flushing
Stream pulverizer moves into agate mortar after being ground into 1cm fritter, is fully ground 30min until blade fritter is at paste；Claim again
500g paste obtained above is taken to be put into the three-necked flask with air inlet pipe and condensing unit, by air inlet pipe with 10mL/
Min rate is passed through 150 DEG C of vapor into flask and is distilled, and distillate instills 100mL brown dropwise after condensing tube condensation
It is saved in bottle to get tea tree ethereal oil natural disinfectant agent, it is spare；The spare bamboo charcoal fiber of 50g is weighed later and 400mL distilled water is mixed
Close uniformly, be stirred with magnetic stirrer, 30g starch added during stirring, continue stir 10min after in 70 DEG C
Mixture is put into concentration removing moisture in vacuum dehydration can after the completion of gelatinization by gelatinization processing 2h under water bath condition；By solid-to-liquid ratio
It is 10:The hydrogen peroxide for shape object being mixed after above-mentioned dehydration and mass concentration is 30% is uniformly mixed and injects 10cm × 10cm × 2mm by 1
Glass mold in, so that it is prolonged stream film forming naturally, the stifling curing 20min of 100 DEG C of vapor used to make its shape that foams after the completion of note film
It is lyophilized at soft loose porous paper membrane, then by the paper membrane after curing with vacuum freeze-drying machine, makes wet tissue base-material by oneself to obtain the final product after taking off film；
Above-mentioned self-control wet tissue base-material is finally laid in the container bottom of sonic oscillation instrument, spare tea tree ethereal oil day is added into container
Right disinfectant makes it submerge wet tissue base-material, starts shaker ultrasonic immersing under 100W power and adsorbs 10h, takes out after the completion of dipping
Wet tissue, up to pure natural draft pasteurization towelette after packaging.
This example operation is simple and easy, in use, taking out pasteurization towelette produced by the present invention, wipes human body portion to be sterilized
Position.After use, it is not necessarily to special recycling, pasteurization towelette produced by the present invention starts voluntarily to degrade in the soil for 10 days, generally
25 days i.e. degradable to finish, environmentally protective, pollution-free, and feel refrigerant pleasant after human body use, does not have any danger for skin
Evil, bacteriostasis rate reach 98.5%.
Example 2
The segment that the 950g moso bamboo blueness thin bamboo strip is cut into 4cm with chopper is weighed first, places the dry 1.5h at 103 DEG C in an oven
Bamboo fiber crops are manually extracted afterwards, then it is 0.5mol/L hydrochloric acid solution and 0.3mol/L soda bath that obtained bamboo fiber crops, which are respectively put into concentration,
Middle immersion 3h takes out bamboo fiber crops with deionized water and rinses 4 times and natural air drying after immersion；Then by the bamboo fiber crops after above-mentioned air-dry
Pressing solid-to-liquid ratio with oil emulsion is 1:1 mixed after be put into fermentor, be sealed by fermentation 1.5 weeks at 40 DEG C, take after fermentation
Fermentation liquid is put into supercentrifuge and is centrifugally separating to obtain bamboo fibre with 7500r/min rate out, then will obtain bamboo fibre and move into charcoal
Change furnace, 350 DEG C of charing 45min are warming up to 10 DEG C/min rate program, it is spare up to bamboo charcoal fiber after being cooled to room temperature；It connects
Get off to weigh 1.5kg tea free, rinse blade surface 4 times with deionized water to remove floating dust impurity, then by the tea tree after flushing
Blade moves into agate mortar after being ground into 1.5cm fritter with airslide disintegrating mill, is fully ground 35min until blade fritter is at paste
Shape object；550g paste obtained above is weighed again to be put into the three-necked flask with air inlet pipe and condensing unit, passes through air inlet
Pipe is passed through 155 DEG C of vapor into flask with 10mL/min rate and is distilled, and distillate instills dropwise after condensing tube condensation
It is saved in 100mL brown bottle to get tea tree ethereal oil natural disinfectant agent, it is spare；Weigh later the spare bamboo charcoal fiber of 55g and
450mL distilled water is uniformly mixed, and is stirred with magnetic stirrer, 35g starch is added during stirring, continue to stir
Gelatinization handles 2.5h under 75 DEG C of water bath conditions after 13min, and mixture is put into concentration in vacuum dehydration can after the completion of gelatinization and is taken off
Moisture removal；It is 10 by solid-to-liquid ratio:The hydrogen peroxide for shape object being mixed after above-mentioned dehydration and mass concentration is 30% is uniformly mixed and is injected by 1
In 10cm × 10cm × 2mm glass mold, it is made to prolong stream film forming naturally, the stifling curing of 103 DEG C of vapor is used after the completion of note film
25min makes its foaming form soft loose porous paper membrane, then the paper membrane after curing is lyophilized with vacuum freeze-drying machine, takes off after film i.e.
Derived from wet tissue base-material processed；Above-mentioned self-control wet tissue base-material is finally laid in the container bottom of sonic oscillation instrument, is added into container
Spare tea tree ethereal oil natural disinfectant agent makes it submerge wet tissue base-material, starts shaker ultrasonic immersing under 150W power and adsorbs
11h impregnates and takes out wet tissue after the completion, up to pure natural draft pasteurization towelette after packaging.
This example operation is simple and easy, in use, taking out pasteurization towelette produced by the present invention, wipes human body portion to be sterilized
Position.After use, it is not necessarily to special recycling, pasteurization towelette produced by the present invention starts voluntarily to degrade in the soil for 13 days, generally
35 days i.e. degradable to finish, environmentally protective, pollution-free, and feel refrigerant pleasant after human body use, does not have any danger for skin
Evil, bacteriostasis rate reach 99%.
Example 3
The segment that the 1000g moso bamboo blueness thin bamboo strip is cut into 5cm with chopper is weighed first, places the dry 2h at 105 DEG C in an oven
Bamboo fiber crops are manually extracted afterwards, then it is 0.5mol/L hydrochloric acid solution and 0.3mol/L soda bath that obtained bamboo fiber crops, which are respectively put into concentration,
Middle immersion 4h takes out bamboo fiber crops with deionized water and rinses 5 times and natural air drying after immersion；Then by the bamboo fiber crops after above-mentioned air-dry
Pressing solid-to-liquid ratio with oil emulsion is 1:1 mixed after be put into fermentor, be sealed by fermentation 2 weeks at 45 DEG C, take out after fermentation
Fermentation liquid is put into supercentrifuge and is centrifugally separating to obtain bamboo fibre with 8000r/min rate, then will obtain bamboo fibre and move into charing
Furnace is warming up to 400 DEG C of charing 50min with 10 DEG C/min rate program, spare up to bamboo charcoal fiber after being cooled to room temperature；It connects down
2kg tea free is weighed, rinses blade surface 5 times with deionized water to remove floating dust impurity, then by tea leaf after flushing
It is moved into agate mortar after being ground into 2cm fritter with airslide disintegrating mill, is fully ground 40min until blade fritter is at paste；
600g paste obtained above is weighed again to be put into the three-necked flask with air inlet pipe and condensing unit, by air inlet pipe with
10mL/min rate is passed through 160 DEG C of vapor into flask and is distilled, and distillate instills 100mL dropwise after condensing tube condensation
It is saved in brown bottle to get tea tree ethereal oil natural disinfectant agent, it is spare；The spare bamboo charcoal fiber of 60g and 500mL distillation are weighed later
Water be uniformly mixed, be stirred with magnetic stirrer, 40g starch added during stirring, continue stir 15min after in
Mixture is put into concentration removing moisture in vacuum dehydration can after the completion of gelatinization by gelatinization processing 3h under 80 DEG C of water bath conditions；By solid
Liquor ratio is 10:1 will be mixed after above-mentioned dehydration the hydrogen peroxide that shape object and mass concentration are 30% be uniformly mixed and inject 10cm × 10cm ×
In the glass mold of 2mm, it is made to prolong stream film forming naturally, the stifling curing 30min of 105 DEG C of vapor is used to make its foaming after the completion of note film
Soft loose porous paper membrane is formed, then the paper membrane after curing is lyophilized with vacuum freeze-drying machine, makes wet tissue base by oneself to obtain the final product after taking off film
Material；Above-mentioned self-control wet tissue base-material is finally laid in the container bottom of sonic oscillation instrument, spare tea tree essence is added into container
Oily natural disinfectant agent makes its submerge wet tissue base-material, starts shaker ultrasonic immersing under 200W power and adsorbs 12h, after the completion of dipping
Wet tissue is taken out, up to pure natural draft pasteurization towelette after packaging.
This example operation is simple and easy, in use, taking out pasteurization towelette produced by the present invention, wipes human body portion to be sterilized
Position.After use, it is not necessarily to special recycling, pasteurization towelette produced by the present invention starts voluntarily to degrade in the soil for 15 days, generally
40 days i.e. degradable to finish, environmentally protective, pollution-free, and feel refrigerant pleasant after human body use, does not have any danger for skin
Evil, bacteriostasis rate reach 99.5%.
Claims (1)
1. a kind of preparation method of pure natural draft pasteurization towelette, it is characterised in that specifically preparation step is：
（1）The segment that 900~1000g moso bamboo blueness thin bamboo strip is cut into 3~5cm with chopper is weighed, is placed in an oven in 100~105 DEG C
Manually extracted after 1~2h of lower drying bamboo fiber crops, then by obtained bamboo fiber crops be respectively put into concentration be 0.5mol/L hydrochloric acid solution and
2~4h is impregnated in 0.3mol/L soda bath, and bamboo fiber crops are taken out after immersion with deionized water and rinse 3~5 times and natural air drying；
（2）By it is above-mentioned air-dry after bamboo fiber crops and oil emulsion by solid-to-liquid ratio be 1:1 mixed after be put into fermentor, at 35~45 DEG C
It is lower to be sealed by fermentation 1~2 week, fermentation liquid is taken out after fermentation is put into supercentrifuge with the centrifugation of 7000~8000r/min rate
Isolated bamboo fibre, then obtained bamboo fibre is moved into retort, 300~400 DEG C are warming up to 10 DEG C/min rate program
40~50min is carbonized, it is spare up to bamboo charcoal fiber after being cooled to room temperature；
（3）1~2kg tea free is weighed, rinses blade surface 3~5 times with deionized water to remove floating dust impurity, then will be after flushing
Tea leaf be ground into 1~2cm fritter with airslide disintegrating mill after move into agate mortar in, be fully ground 30~40min until
Blade fritter is at paste；
（4）It weighs 500~600g paste obtained above to be put into the three-necked flask with air inlet pipe and condensing unit, pass through
Air inlet pipe is passed through 150~160 DEG C of vapor into flask with 10mL/min rate and is distilled, and distillate is after condensing tube condensation
It instills in 100mL brown bottle and is saved to get tea tree ethereal oil natural disinfectant agent dropwise, it is spare；
（5）It weighs the spare bamboo charcoal fiber of 50~60g and 400~500mL distilled water is uniformly mixed, stirred with magnetic stirrer
It mixes, 30~40g starch is added during stirring, pasted under 70~80 DEG C of water bath conditions after continuing 10~15min of stirring
Change 2~3h of processing, mixture is put into concentration removing moisture in vacuum dehydration can after the completion of gelatinization；
（6）It is 10 by solid-to-liquid ratio:The hydrogen peroxide that mixture after above-mentioned dehydration and mass concentration are 30% is uniformly mixed and is injected by 1
In 10cm × 10cm × 2mm glass mold, so that it is prolonged stream film forming naturally, use 100~105 DEG C of vapor stifling after the completion of note film
20~30min of curing makes its foaming form soft loose porous paper membrane, then the paper membrane after curing is lyophilized with vacuum freeze-drying machine,
Wet tissue base-material is made by oneself to obtain the final product after taking off film；
（7）Above-mentioned self-control wet tissue base-material is laid in the container bottom of sonic oscillation instrument, spare tea tree essence is added into container
Oily natural disinfectant agent makes it submerge wet tissue base-material, starts shaker ultrasonic immersing under 100~200W power and adsorbs 10~12h,
It impregnates and takes out wet tissue after the completion, up to pure natural draft pasteurization towelette after packaging.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103407205A (en) * | 2013-07-16 | 2013-11-27 | 福建农林大学 | Konjac glucomannan fiber wet tissue and method for preparing same |
| CN105086943A (en) * | 2015-09-29 | 2015-11-25 | 江苏锦宇环境工程有限公司 | Preparation method for bamboo carbon fiber snow-melting agent |
Non-Patent Citations (1)
| Title |
|---|
| 全天然魔芋消毒湿纸巾的绿色制备工艺及性能研究;盛慧等;《中华纸业》;20030630;第24卷(第6期);第39-40、45页，尤其是第39页右栏第1.3节"工艺流程"、第39页右栏最后1行-第40页左栏第1行、第40页左栏第8-11行 * |
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| CN105560129A (en) | 2016-05-11 |
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