CN106511134B - A kind of astaxanthin facial mask nutrient solution and preparation method thereof - Google Patents
A kind of astaxanthin facial mask nutrient solution and preparation method thereof Download PDFInfo
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- CN106511134B CN106511134B CN201611144139.9A CN201611144139A CN106511134B CN 106511134 B CN106511134 B CN 106511134B CN 201611144139 A CN201611144139 A CN 201611144139A CN 106511134 B CN106511134 B CN 106511134B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses a kind of astaxanthin facial mask nutrient solutions, be prepared by the raw material of following percent mass proportioning: astaxanthin oil 0.1%~0.5%, Sodium Hyaluronate 0.2%~2.0%, beta- glucan 0.1%~1%, carbomer sodium 0.1%~0.3%, butanediol 1.0%~5.0%, glycerol 2.0%~5.0%, glycine betaine 0.5%~2.0%, methyl propanediol 0.1%~0.5%, allantoin 0.3%~1.0%, potassium sorbate 0.1%~0.5%, essence 0.05%~0.2%, vitamin E 0.1%~1.0% and surplus pure water are supplied.Compared with prior art, the present invention has stronger anti-oxidation function rich in ingredients such as astaxanthin oil, vitamin E and beta- glucans, can effectively remove facial oxygen radical, promotes cell metabolism, repairs skin damage cell.Meanwhile rich in glycerol, Sodium Hyaluronate etc., facial moisture of skin can be locked, the wet of skin is kept, plays crease-resistant beauty treatment.
Description
Technical field
The present invention relates to natural products applied technical fields, more particularly to a kind of astaxanthin facial mask nutrient solution and its preparation
Method.
Background technique
With the improvement of living standards, facial mask is an important beauty skin care product, people are also more next to the pursuit of beauty
Higher, wherein the facial mask of natural product active ingredient is more and more, for example, brown alga facial mask, algal polysaccharides facial mask, contain coreopsis tinctoria
The facial mask etc. of petal.
Astaxanthin is a kind of important carotenoid, anti-oxidation function with super strength.The antioxygenic property of astaxanthin
It is mainly shown as that singlet-oxygen quenching, scavenging activated oxygen prevent the functions such as lipid peroxidation in organism.Astaxanthin liposoluble
Property it is good, there is good affinity to cell membrane, can pass through cell membrane enter cell interior, participate in eliminating the oxygen generated in vivo certainly
By base, damaged cell can be effectively repaired, moreover it is possible to the generation of skin surface microgroove be effectively relieved, there is good beauty and skin care effect
Fruit.
Natural astaxanthin source is wider, can extract from shellfish, and microbial fermentation and microdisk electrode obtain.Its
In, haematococcus pluvialis is the highest microorganism of content astaxanthin in nature, is the best natural origin of astaxanthin.
Summary of the invention
In view of this, the purpose of the present invention is to provide a kind of with moisturizing, crease-resistant and whitening function natural astaxanthin
Facial mask nutrient solution, while the preparation method of the natural astaxanthin facial mask nutrient solution being provided.
In order to achieve the above objectives, the technical scheme is that
A kind of astaxanthin facial mask nutrient solution, is prepared by the raw material of following percent mass proportioning: mass fraction 0.5%
~2.0% astaxanthin oil 0.1%~0.5%, beta- glucan 0.1%~1%, is blocked Sodium Hyaluronate 0.2%~2.0%
Wave nurse sodium 0.1%~0.3%, butanediol 1.0%~5.0%, glycerol 2.0%~5.0%, glycine betaine 0.5%~2.0%, first
Base propylene glycol 0.1%~0.5%, allantoin 0.3%~1.0%, potassium sorbate 0.1%~0.5%, essence 0.05%~
0.2%, vitamin E 0.1%~1.0% and surplus pure water are supplied；
The astaxanthin oil is dissolved in vegetable oil by astaxanthin to be formulated, and the astaxanthin is mentioned from haematococcus pluvialis
Take gained, wherein vegetable oil is olive oil or grape seed oil；
When preparing astaxanthin oil, haematococcus pluvialis powder is first quantitatively weighed, by 1:(5~10) mass volume ratio be added to
In dehydrated alcohol, extraction repeatedly, merges gained leaching liquor repeatedly, removes solvent using being concentrated under reduced pressure, purified that shrimp is prepared
Astaxanthin, is then added in vegetable oil, in room temperature by green element in the ratio of the mass fraction 0.5%~2.0% of astaxanthin oil
Stirring to astaxanthin is completely dissolved, and forms astaxanthin oil.
A kind of preparation method of astaxanthin facial mask nutrient solution, comprising the following steps:
1) prepare astaxanthin oil, Sodium Hyaluronate, beta- dextran solution, carbomer sodium, butanediol, glycerol, beet
Alkali, methyl propanediol, allantoin, potassium sorbate, essence and vitamin E and appropriate amount of purified water；
Wherein, the astaxanthin oil is dissolved in vegetable oil by astaxanthin is formulated, and the astaxanthin gives birth to red ball from rain
Gained is extracted in algae, wherein vegetable oil is olive oil or grape seed oil；
When preparing astaxanthin oil, haematococcus pluvialis powder is first quantitatively weighed, by 1:(5~10) mass volume ratio be added to
In dehydrated alcohol, extraction repeatedly, merges gained leaching liquor repeatedly, removes solvent using being concentrated under reduced pressure, purified that shrimp is prepared
Astaxanthin, is then added in vegetable oil, in room temperature by green element in the ratio of the mass fraction 0.5%~2.0% of astaxanthin oil
Stirring to astaxanthin is completely dissolved, and forms astaxanthin oil；
2) the part pure water is taken, the carbomer sodium and the Sodium Hyaluronate are pressed into facial mask nutrient solution total amount respectively
The ratio of mass fraction 0.1%~0.3% and 0.2%~2.0% be added in this pure water, stirring is sufficiently dissolved to solid
Afterwards, solution is cooled to room temperature to get hyaluronic acid solution；
3) into the hyaluronic acid solution of step 2) successively addition by facial mask nutrient solution total amount mass fraction 1.0%~
5.0% butanediol, 2.0%~5.0% glycerol, 0.5%~2.0% glycine betaine, 0.1%~
0.5% methyl propanediol, 0.3%~1.0% allantoin and 0.1%~0.5% the potassium sorbate, shape
At mixed liquor, which is stirred at room temperature to after completely dissolution, being cooled to 10 DEG C -15 DEG C；
4) the beta- dextran solution is added in mixed liquor after cooling into step 3), the beta- glucan is molten
The additional amount of liquid accounts for the mass fraction 20%~50% of facial mask nutrient solution total amount, and the quality of the beta- dextran solution
Concentration is 0.5%~2.0%, and stirring is sufficiently mixed solution uniformly, and mixed liquor is cooled to 10 DEG C -15 DEG C to get facial mask basis
Nutrient solution；
5) mass fraction by facial mask nutrient solution total amount is sequentially added in the facial mask basic nutrient solution in obtained by step 4)
0.05%~0.2% essence and 0.1%~1.0% the vitamin E, stirring is sufficiently mixed solution uniformly, mixed
It closes liquid and is cooled to 10 DEG C -15 DEG C；
6) astaxanthin oil is added into the resulting mixed liquor of step 5), the additional amount of the astaxanthin oil accounts for facial mask battalion
The 0.1%~0.5% of the mass fraction of nutrient solution total amount, after at the uniform velocity stirring, gained mixed liquor is astaxanthin facial mask nutrient solution.
Further, the beta- dextran solution takes the part pure water, beta- glucan is pressed in configuration
0.5%~2.0% ratio of the mass fraction of the beta- dextran solution is added in this pure water, stirs to described
Beta- glucan after completely dissolution, is cooled to 10 DEG C~15 DEG C to get the beta- dextran solution.
Further, it is at the uniform velocity stirred in step 2) using blender, 200~500rpm of speed of agitator, whipping temp
50~80 DEG C；It is at the uniform velocity stirred in step 6) using blender, 200~500rpm of speed of agitator, 4~15 DEG C of whipping temp.
Further, obtained by the beta- dextran solution is at the uniform velocity stirred as blender, speed of agitator 200~
500rpm, 50~80 DEG C of whipping temp.
Compared with prior art, the beneficial effects of the present invention are:
Astaxanthin facial mask nutrient solution prepared by the present invention has rich in astaxanthin oil, vitamin E and beta- glucan etc.
Stronger inoxidizability can effectively remove facial oxygen radical, slow down skin aging, promote cell metabolism, repair
Skin damage cell.Meanwhile rich in glycerol, Sodium Hyaluronate and methyl propanediol etc., facial moisture of skin can be locked, is kept
Moistening for skin, plays crease-resistant beauty treatment.Containing glycine betaine, skin moisture activity can be improved, promote skin water balance, increase
Elasticity of skin.
The present invention uses pure natural raw material, non-stimulated to skin, guarantees the safety in utilization of skin care item, wide application of the crowd.
Specific embodiment
In order to further explain the technical solution of the present invention, being explained in detail below by specific embodiment the present invention
It states.
Embodiment one
A kind of preparation method of astaxanthin facial mask nutrient solution, is achieved by the steps of:
(1) configuration of astaxanthin oil
1) preparation of natural astaxanthin: haematococcus pluvialis powder is quantitatively weighed, by 1:(5~10) mass volume ratio be added to
In dehydrated alcohol, extraction repeatedly, merges gained leaching liquor repeatedly, removes solvent using being concentrated under reduced pressure, purified that day is prepared
Right astaxanthin, it is spare；
2) it configures astaxanthin oil: natural astaxanthin obtained in step 1) is pressed into the mass fraction 0.5% of astaxanthin oil
Ratio is added in olive oil, is stirred at room temperature to natural astaxanthin and is completely dissolved, and astaxanthin oil is formed, spare.
(2) preparation of astaxanthin facial mask nutrient solution
1) prepare astaxanthin oil, Sodium Hyaluronate, beta- glucan, carbomer sodium, butanediol, glycerol, glycine betaine, first
Base propylene glycol, allantoin, potassium sorbate, essence and vitamin and appropriate amount of purified water；
2) part pure water is taken, beta- glucan is added in the ratio of the mass fraction 0.5% of beta- dextran solution
It is added in this pure water, the solution for being mixed with beta- glucan to be dissolved is put into blender and is at the uniform velocity stirred, setting is stirred
Mix the revolving speed 200rpm of machine, 50~80 DEG C of whipping temp；When stirring to beta- glucan after completely dissolution, solution is cooled to 15
DEG C to get arrive beta- dextran solution, it is spare；
3) part pure water is taken, carbomer sodium and Sodium Hyaluronate are pressed to the mass fraction of facial mask nutrient solution total amount respectively
0.2% and 1.0% ratio is added in this pure water, which is put into blender and is at the uniform velocity stirred, setting stirring
The revolving speed 200rpm of machine, 50~80 DEG C of whipping temp；When stirring to carbomer sodium and Sodium Hyaluronate solid after completely dissolution, it is molten
Liquid is cooled to room temperature to get hyaluronic acid solution, spare；
4) butanediol, glycerol, glycine betaine, methyl propanediol, allantois are successively added into the hyaluronic acid solution of step 3)
Element, potassium sorbate, the amount of addition is corresponding in turn to by the mass fraction of facial mask nutrient solution total amount are as follows: 3.0%, 2.0%, 0.5%,
0.5%, 0.3%, 0.1%, the mixed liquor for being mixed with many kinds of solids is obtained, which is stirred by glass bar to mixed in room temperature
The solid of conjunction after completely dissolution, is cooled to 15 DEG C；
5) it is molten that beta- glucan obtained in step 2) is added into the mixed liquor obtained in step 4) after completely dissolution
Liquid, the mass fraction of addition are the 40% of facial mask nutrient solution total amount, after being sufficiently mixed solution uniformly by glass bar stirring, are mixed
It closes liquid and is cooled to 15 DEG C to get facial mask basic nutrient solution；
6) essence and vitamin E, the quality point of addition are sequentially added into facial mask basic nutrient solution obtained in step 5)
Number is respectively 0.05% and 0.2%, is sufficiently mixed mixed liquor uniformly by glass bar stirring, uniformly mixed mixed liquor is cooling
To 10 DEG C or less；
7) mass fraction 0.1% of facial mask nutrient solution total amount is pressed into the mixed liquor obtained in step 6) after mixing
Astaxanthin oil obtained in the step 2) of the configuration of (one) astaxanthin oil is added, mixed liquor is put into blender and is at the uniform velocity stirred
It mixes, the revolving speed 200rpm of blender is set, and 4~15 DEG C of whipping temp, gained mixed liquor is astaxanthin facial mask after mixing evenly
Nutrient solution.In the step, it can be carried out supplying adjusting with the pure water of surplus, be settled to specified amount, so that astaxanthin facial mask is sought
The nutrient solution total amount of nutrient solution is stirred operation after constant volume up to 100% again.
Astaxanthin facial mask in order to obtain can further carry out following steps:
8) by the facial mask for being cut into facial mask size with non-woven fabrics be immersed in step 7) obtained in astaxanthin facial mask nutrient solution,
Wherein the mass volume ratio of facial mask non-woven fabrics and astaxanthin facial mask nutrient solution is 1g:30mL, and soaking time is 30 minutes, is impregnated
Astaxanthin facial mask is obtained afterwards.
Embodiment two
The difference between this embodiment and the first embodiment lies in the preparation of (two) astaxanthin facial mask nutrient solution.In the present embodiment, shrimp
The preparation of green vegetarian noodles film nutrient solution the following steps are included:
1) prepare astaxanthin oil, Sodium Hyaluronate, beta- glucan, carbomer sodium, butanediol, glycerol, glycine betaine, first
Base propylene glycol, allantoin, potassium sorbate, essence and vitamin and appropriate amount of purified water；
2) part pure water is taken, beta- glucan is added in the ratio of the mass fraction 1.0% of beta- dextran solution
It is added in this pure water, the solution for being mixed with beta- glucan to be dissolved is put into blender and is at the uniform velocity stirred, setting is stirred
Mix the revolving speed 500rpm of machine, 50~80 DEG C of temperature；When stirring to beta- glucan solid after completely dissolution, solution is cooled to 10
It is spare DEG C to get beta- dextran solution；
3) part pure water is taken, carbomer sodium and Sodium Hyaluronate are pressed to the mass fraction of facial mask nutrient solution total amount respectively
0.3% and 1.0% ratio is added in this pure water, and the pure water for being mixed with carbomer sodium and Sodium Hyaluronate solid is put into
It is at the uniform velocity stirred in blender, the revolving speed 200rpm of blender is set, 50~80 DEG C of whipping temp；When stirring to carbomer sodium
After completely dissolution with Sodium Hyaluronate solid, solution is cooled to room temperature to get hyaluronic acid solution, spare；
4) successively added into the transparent acid solution of step 3) butanediol, glycerol, glycine betaine, methyl propanediol, allantoin,
The amount of potassium sorbate, addition is corresponding in turn to by the mass fraction of facial mask nutrient solution total amount are as follows: 1.0%, 3.0%, 1.5%,
0.2%, 0.5%, 0.3%, the mixed liquor for being mixed with many kinds of solids is obtained, which is stirred by glass bar to mixing in room temperature
Solid after completely dissolution, be cooled to 10 DEG C；
5) it is molten that beta- glucan obtained in step 2) is added into the mixed liquor obtained in step 4) after completely dissolution
Liquid, the mass fraction of addition are the 50% of facial mask nutrient solution total amount, after being sufficiently mixed solution uniformly by glass bar stirring, are mixed
It closes liquid and is cooled to 10 DEG C to get facial mask basic nutrient solution；
6) essence and vitamin E, the quality point of addition are sequentially added into facial mask basic nutrient solution obtained in step 5)
Number is respectively 0.2% and 0.8%, is sufficiently mixed mixed liquor uniformly by glass bar stirring, uniformly mixed mixed liquor is cooling
To 10 DEG C or less；
7) embodiment one (one) is added by mass fraction 0.5% into the mixed liquor obtained in step 6) after mixing
Astaxanthin oil obtained in the step 2) of the configuration of astaxanthin oil, mixed liquor are put into blender and are at the uniform velocity stirred, and setting is stirred
The revolving speed 500rpm of machine is mixed, 4~10 DEG C of whipping temp, gained mixed liquor is astaxanthin facial mask nutrient solution after mixing evenly.It should
In step, it can be carried out supplying adjusting with the pure water of surplus, be settled to specified amount, so that the nutrition of astaxanthin facial mask nutrient solution
Liquid total amount is stirred operation after constant volume up to 100% again；
Astaxanthin facial mask in order to obtain can further carry out following steps:
8) by the facial mask for being cut into facial mask size with non-woven fabrics be immersed in step 7) obtained in astaxanthin facial mask nutrient solution；
Wherein the mass volume ratio of facial mask non-woven fabrics and astaxanthin facial mask nutrient solution is 1g:30mL, and soaking time is 30 minutes, is impregnated
Astaxanthin facial mask is obtained afterwards.
Embodiment three
A kind of preparation method of astaxanthin facial mask nutrient solution, is achieved by the steps of:
(1) configuration of astaxanthin oil
1) preparation of astaxanthin: quantitative weighed haematococcus pluvialis powder, by 1:(5~10) mass volume ratio be added to nothing
In water-ethanol, extraction is multiple repeatedly, merges gained leaching liquor, removes solvent using being concentrated under reduced pressure, purified to be prepared naturally
Astaxanthin, it is spare；
2) it configures astaxanthin oil: natural astaxanthin obtained in step 1) is pressed into the mass fraction 0.5% of astaxanthin oil
Ratio is added in glucose seed oil, is stirred at room temperature to natural astaxanthin and is completely dissolved, and astaxanthin oil is formed, spare.
(2) preparation of astaxanthin facial mask nutrient solution
1) prepare astaxanthin oil, Sodium Hyaluronate, beta- glucan, carbomer sodium, butanediol, glycerol, glycine betaine, first
Base propylene glycol, allantoin, potassium sorbate, essence and vitamin and appropriate amount of purified water；
2) part pure water is taken, beta- glucan is added in the ratio of the mass fraction 1.0% of beta- dextran solution
It is added in this pure water, the solution for being mixed with beta- glucan to be dissolved is put into blender and is at the uniform velocity stirred, setting is stirred
Mix the revolving speed 500rpm of machine, 50~80 DEG C of temperature；When stirring to beta- glucan after completely dissolution, solution is cooled to 10 DEG C, i.e.,
Beta- dextran solution is obtained, it is spare；
3) part pure water is taken, carbomer sodium and Sodium Hyaluronate are pressed to the mass fraction of facial mask nutrient solution total amount respectively
0.1% and 2.0% ratio is added in this pure water, and the pure water for being mixed with carbomer sodium and Sodium Hyaluronate solid is put into
It is at the uniform velocity stirred in blender, the revolving speed 200rpm of blender is set, 50~80 DEG C of whipping temp；When stirring to carbomer sodium
After completely dissolution with Sodium Hyaluronate solid, solution is cooled to room temperature to get hyaluronic acid solution, spare；
4) butanediol, glycerol, glycine betaine, methyl propanediol, allantois are successively added into the hyaluronic acid solution of step 3)
Element, potassium sorbate, the amount of addition is corresponding in turn to by the mass fraction of facial mask nutrient solution total amount are as follows: 2.0%, 2.0%, 1.5%,
0.5%, 0.7%, 0.2%, the mixed liquor for being mixed with many kinds of solids is obtained, which is stirred by glass bar to mixing in room temperature
Solid after completely dissolution, be cooled to 10 DEG C；
5) it is molten that beta- glucan obtained in step 2) is added into the mixed liquor obtained in step 4) after completely dissolution
Liquid, the mass fraction of addition are the 50% of facial mask nutrient solution total amount, after being sufficiently mixed solution uniformly by glass bar stirring, are mixed
It closes liquid and is cooled to 10 DEG C to get facial mask basic nutrient solution；
6) essence and vitamin E, the quality point of addition are sequentially added into facial mask basic nutrient solution obtained in step 5)
Number is respectively 0.1% and 0.5%, is sufficiently mixed mixed liquor uniformly by glass bar stirring, uniformly mixed mixed liquor is cooling
To 10 DEG C or less；
7) mass fraction 0.2% of facial mask nutrient solution total amount is pressed into the mixed liquor obtained in step 6) after mixing
Astaxanthin oil obtained in the step 2) of the configuration of (one) astaxanthin oil is added, mixed liquor is put into blender and is at the uniform velocity stirred
It mixes, the revolving speed 500rpm of blender is set, and 4~10 DEG C of whipping temp, gained mixed liquor is astaxanthin facial mask after mixing evenly
Nutrient solution.In the step, it can be carried out supplying adjusting with the pure water of surplus, be settled to specified amount, so that astaxanthin facial mask is sought
The nutrient solution total amount of nutrient solution is stirred operation after constant volume up to 100% again.
Astaxanthin facial mask in order to obtain can further carry out following steps:
8) by the facial mask for being cut into facial mask size with non-woven fabrics be immersed in step 7) obtained in natural astaxanthin facial mask nutrition
In liquid；Wherein the mass volume ratio of facial mask non-woven fabrics and astaxanthin facial mask nutrient solution is 1g:25mL, and soaking time is 30 points
Clock obtains astaxanthin facial mask after immersion.
It should be noted that the modes such as natural cooling or water cooling can be used in the cooling means in the present invention, it is specific cold
But mode can comprehensively consider ambient temperature etc. and be selected.
Compared with prior art, the beneficial effects of the present invention are:
Astaxanthin facial mask nutrient solution prepared by the present invention has rich in astaxanthin oil, vitamin E and beta- glucan etc.
Stronger inoxidizability can effectively remove facial oxygen radical, slow down skin aging, promote cell metabolism, repair
Skin damage cell.Meanwhile rich in glycerol, Sodium Hyaluronate and methyl propanediol etc., facial moisture of skin can be locked, is kept
Moistening for skin, plays crease-resistant beauty treatment.Containing glycine betaine, skin moisture activity can be improved, promote skin water balance, increase
Elasticity of skin.
The present invention uses pure natural raw material, non-stimulated to skin, guarantees the safety in utilization of skin care item, wide application of the crowd.
Skin care detection effect of the invention is as follows:
1) short run effect
Four groups of ages are selected to be tested for the female volunteers of 18~45 one full year of life, every group of 30 people.Volunteer cleans good hand
It after arm, is positioned behind environmental balance 30 minutes of constant temperature and humidity (22~26 DEG C of room temperature, humidity 40~60%), measures skin
Basic data.Sample in embodiment 1,2,3 is applied respectively by positioning in corresponding region, is applying measurement after twenty minutes respectively
Use the data (blank control group is not dealt with) on the area skin surface after facial mask.Experimental result is shown in Table 1.
1 astaxanthin facial mask nutrient solution short-period used effect of table
| Effect (number) | Embodiment one | Embodiment two | Embodiment three | Control group |
| Humidity increases | 25 | 27 | 28 | 7 |
| Elasticity increases | 7 | 8 | 11 | 4 |
| Microgroove is reduced | 4 | 5 | 8 | 3 |
| Melanin reduces | 5 | 3 | 4 | 0 |
It can be seen that there is apparent moisture-keeping efficacy in a short time using facial mask of the present invention, but to the increase of skin elasticity, microgroove
It reduces and the functions such as whitening does not embody temporarily.
2) long-term effect
Select the age for the female volunteers of 18~45 one full year of life, every group of 30 people carry out test in 28 days by a definite date.Volunteer is clear
It after washed arm, positions, surveys behind environmental balance 30 minutes of constant temperature and humidity (22~25 DEG C of room temperature, humidity 40~60%)
Determine skin (including moisture, brilliant white degree, melanin, elasticity), and is marked in test position.Four groups of volunteers continuously make respectively
With a kind of embodiment sample totally 28 days, skin data, test method and time were measured in the same position of test after using 4 weeks
Ibid.Compare the situation of change of each parameter in use front and back.
2 astaxanthin facial mask nutrient solution permanence operation of table
| Effect (number) | Embodiment one | Embodiment two | Embodiment three | Control group |
| Humidity increases | 24 | 29 | 28 | 8 |
| Elasticity increases | 23 | 27 | 25 | 5 |
| Microgroove is reduced | 19 | 26 | 25 | 3 |
| Melanin reduces | 21 | 27 | 24 | 2 |
The test result shows continuous use one 28 days period of facial mask of the present invention, not only acts as the function of moisturizing, also
Microgroove can effectively be desalinated, increase skin elasticity, and also there is apparent white-skinned face function.
3) preservative challenge testing
Facial mask enfeoffment made from embodiment 1-3 is entered into packaging bag respectively, after sealed package, is placed in 40 DEG C of environment temperature, phase
In the environment of humidity 40-60%RH, continuous observation is as a result as follows:
The preservative challenge testing result of 3 astaxanthin facial mask nutrient solution of table
| Case | Phenomenon |
| Embodiment one | No abnormality seen after 90 days；After packaging is opened, microorganism is not detected in pure in smell. |
| Embodiment two | No abnormality seen after 90 days, after packaging is opened, microorganism is not detected in pure in smell. |
| Embodiment three | No abnormality seen after 90 days, after packaging is opened, microorganism is not detected in pure in smell. |
Above-described embodiment and non-limiting product of the invention, any person of an ordinary skill in the technical field do it
Appropriate changes or modifications, all should be regarded as not departing from patent category of the invention.
Claims (5)
1. a kind of astaxanthin facial mask nutrient solution, which is characterized in that be prepared by the raw material of following percent mass proportioning: quality point
Count the astaxanthin oil 0.1%~0.5% for 0.5%~2.0%, Sodium Hyaluronate 0.2%~2.0%, beta- glucan
0.1%~1%, carbomer sodium 0.1%~0.3%, butanediol 1.0%~5.0%, glycerol 2.0%~5.0%, glycine betaine
0.5%~2.0%, methyl propanediol 0.1%~0.5%, allantoin 0.3%~1.0%, potassium sorbate 0.1%~0.5%,
Essence 0.05%~0.2%, vitamin E 0.1%~1.0% and surplus pure water are supplied；
The astaxanthin oil is dissolved in vegetable oil by astaxanthin to be formulated, and the astaxanthin extracts institute from haematococcus pluvialis
, wherein vegetable oil is olive oil or grape seed oil；
When preparing astaxanthin oil, haematococcus pluvialis powder is first quantitatively weighed, by 1:(5~10) mass volume ratio be added to it is anhydrous
In ethyl alcohol, extraction repeatedly, merges gained leaching liquor repeatedly, removes solvent using being concentrated under reduced pressure, purified that astaxanthin is prepared,
Then astaxanthin is added in vegetable oil in the ratio of the mass fraction 0.5%~2.0% of astaxanthin oil, be stirred at room temperature to
Astaxanthin is completely dissolved, and forms astaxanthin oil.
2. a kind of preparation method of astaxanthin facial mask nutrient solution, which comprises the following steps:
1) prepare astaxanthin oil, Sodium Hyaluronate, beta- dextran solution, carbomer sodium, butanediol, glycerol, glycine betaine, first
Base propylene glycol, allantoin, potassium sorbate, essence and vitamin E and appropriate amount of purified water；
Wherein, the astaxanthin oil is dissolved in vegetable oil by astaxanthin is formulated, and the astaxanthin is from haematococcus pluvialis
Extract gained, wherein vegetable oil is olive oil or grape seed oil；
When preparing astaxanthin oil, haematococcus pluvialis powder is first quantitatively weighed, by 1:(5~10) mass volume ratio be added to it is anhydrous
In ethyl alcohol, extraction repeatedly, merges gained leaching liquor repeatedly, removes solvent using being concentrated under reduced pressure, purified that astaxanthin is prepared,
Then astaxanthin is added in vegetable oil in the ratio of the mass fraction 0.5%~2.0% of astaxanthin oil, be stirred at room temperature to
Astaxanthin is completely dissolved, and forms astaxanthin oil；
2) the part pure water is taken, the carbomer sodium and the Sodium Hyaluronate are pressed to the matter of facial mask nutrient solution total amount respectively
The ratio of amount score 0.1%~0.3% and 0.2%~2.0% is added in this pure water, stirs to solid after completely dissolution,
Solution is cooled to room temperature to get hyaluronic acid solution；
3) into the hyaluronic acid solution of step 2), successively the mass fraction 1.0%~5.0% of facial mask nutrient solution total amount is pressed in addition
The butanediol, 2.0%~5.0% glycerol, 0.5%~2.0% glycine betaine, 0.1%~0.5% institute
Methyl propanediol, 0.3%~1.0% allantoin and 0.1%~0.5% potassium sorbate are stated, mixed liquor is formed,
The mixed liquor is stirred at room temperature to after completely dissolution, being cooled to 10 DEG C -15 DEG C；
4) the beta- dextran solution is added in mixed liquor after cooling into step 3), the beta- dextran solution
Additional amount accounts for the mass fraction 20%~50% of facial mask nutrient solution total amount, and the mass concentration of the beta- dextran solution
It is 0.5%~2.0%, stirring is sufficiently mixed solution uniformly, and mixed liquor is cooled to 10 DEG C -15 DEG C to get facial mask basal nutrient
Liquid；
5) mass fraction by facial mask nutrient solution total amount is sequentially added in the facial mask basic nutrient solution in obtained by step 4)
0.05%~0.2% essence and 0.1%~1.0% the vitamin E, stirring is sufficiently mixed solution uniformly, mixed
It closes liquid and is cooled to 10 DEG C -15 DEG C；
6) astaxanthin oil is added into the resulting mixed liquor of step 5), the additional amount of the astaxanthin oil accounts for facial mask nutrient solution
The 0.1%~0.5% of the mass fraction of total amount, after at the uniform velocity stirring, gained mixed liquor is astaxanthin facial mask nutrient solution.
3. a kind of preparation method of astaxanthin facial mask nutrient solution according to claim 2, it is characterised in that: the beta-
Dextran solution takes the part pure water in configuration, and beta- glucan is pressed to the quality of the beta- dextran solution
0.5%~2.0% ratio of score is added in this pure water, stirs to the beta- glucan after completely dissolution, cooling
To 10 DEG C~15 DEG C to get the beta- dextran solution.
4. a kind of preparation method of astaxanthin facial mask nutrient solution according to claim 2, it is characterised in that: make in step 2)
It is at the uniform velocity stirred with blender, 200~500rpm of speed of agitator, 50~80 DEG C of whipping temp；Blender is used in step 6)
It is at the uniform velocity stirred, 200~500rpm of speed of agitator, 4~15 DEG C of whipping temp.
5. a kind of preparation method of astaxanthin facial mask nutrient solution according to claim 3, it is characterised in that: the beta-
Obtained by dextran solution is at the uniform velocity stirred as blender, 200~500rpm of speed of agitator, 50~80 DEG C of whipping temp.
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| CN105434319A (en) * | 2015-12-07 | 2016-03-30 | 华南理工大学 | Cosmetics based on phaffia rhodozyma raw materials and preparation method thereof |
| CN106074200A (en) * | 2016-08-02 | 2016-11-09 | 深圳大学 | A kind of biodiesel extracts natural astaxanthin and the formula of facial film thereof and preparation method |
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| CN105434319A (en) * | 2015-12-07 | 2016-03-30 | 华南理工大学 | Cosmetics based on phaffia rhodozyma raw materials and preparation method thereof |
| CN106074200A (en) * | 2016-08-02 | 2016-11-09 | 深圳大学 | A kind of biodiesel extracts natural astaxanthin and the formula of facial film thereof and preparation method |
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