CN106074200A - A kind of biodiesel extracts natural astaxanthin and the formula of facial film thereof and preparation method - Google Patents
A kind of biodiesel extracts natural astaxanthin and the formula of facial film thereof and preparation method Download PDFInfo
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- CN106074200A CN106074200A CN201610620997.XA CN201610620997A CN106074200A CN 106074200 A CN106074200 A CN 106074200A CN 201610620997 A CN201610620997 A CN 201610620997A CN 106074200 A CN106074200 A CN 106074200A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
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- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/08—Anti-ageing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
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Abstract
A kind of biodiesel extracts natural astaxanthin and the formula of facial film thereof and preparation method, the present invention relates to the manufacture technology field of cosmetic health product, the present invention is for providing a kind of facial film containing natural astaxanthin, the formula of a kind of natural astaxanthin facial film is, glycerol 2 3%, sodium lactate 0.8 2%, butanediol 1 3%, acrylic acid (or ester) class/C10 30 alcohol acrylate crosspolymers potassium salt 0.2 0.7%, trehalose 0.2 1%, hyaluronate sodium 0.01 0.2%, phenoxyethanol 0.1 0.3%, EDETATE DISODIUM 0.01 0.03%g, natural oil astaxanthin extract 5 10%, deionized water 81 90%.The present invention compared with prior art, has the aging effect of more strong anti-oxidation, whitening and alleviation, can avoid the phenomenons such as the mottle, the wrinkle that bring because cell is oxidized.
Description
Technical field
The present invention relates to the manufacture technology field of cosmetic health product, particularly to extraction and the biodiesel of natural astaxanthin
Facial film and preparation method thereof.
Background technology
Reactivity keto is the by-product of human body aerobic metabolism, including oxonium ion, peroxide and oxygen-derived free radicals etc..Reaction
The character of active oxygen is enlivened, and has the strongest chemical reactivity, participates in multiple body physiological biochemical process.But too much activity
Oxygen has serious side effect, causes human normal cell and disorganization, causes multiple disease.Reactivity keto can be at ring
Border and increase under the influence of the time.Such as smoking, air pollution, water are polluted, lonizing radiation (x line, ultraviolet), insecticide, life
Pressure is big, hyperkinesia etc., number of free radical all can be made to increase, referred to as oxidative pressure.Oxidative pressure is the biggest, interior free yl
Concentration the highest.Research display antioxidation is pre-anti-aging important step, if it is possible to eliminate too much oxyradical,
Cause for many free radicals and aging-related disease can prevent.
Antioxidant can capture and neutralize reactivity keto, thus the infringement that Scavenging active oxygen is to human body, prevent carefully
Born of the same parents cause aging, delay health catagen speed.Natural astaxanthin has superpower antioxidation, can be effectively in scavenger cell
Active oxygen, strengthens cell regeneration ability, maintains organism balance and reduces the accumulation of senile cell, thus protecting skin health, promoting
Enter hair growth, defying age, alleviate exercise fatigue, invigorate.Research shows that natural astaxanthin antioxidant activity is vitamin C
6000 times of effect, 1000 times of vitamin E, 800 times of coenzyme Q10,700 times of anthocyanidin, be beta-carotene effect
100 times.The more important thing is, natural astaxanthin is uniquely all to be had in multiple fields by a Carotenoids of blood brain barrier
Important application.
Animal self cannot synthesizing astaxanthin, can only by food chain from the external world take in.Microalgae and yeast energy in nature
Synthesizing astaxanthin, the most only microalgae synthesis astaxanthin be 100% left-handed, there is higher biological activity.Its thing of astaxanthin
The absorption peak of matter is exactly about 470nm, and with ultraviolet wavelength is close, therefore the astaxanthin of trace just can absorb substantial amounts of
UVA, can ultraviolet radiation preventing, the UV-induced free radical of cancellation efficiently, reduce ultraviolet and the injury of skin prevented.
In addition, it also can restore the skin destroyed by ultraviolet burn rapidly.Due to the non-oxidizability that it is powerful, the whole world is very
Many cosmetics brand with the addition of the natural astaxanthin composition as its superpower antioxidant, including Estee Lauder, DermaE, height
Silk, Fang Kai and Mentholatum etc. are proposed special astaxanthin flesh and grind series moisturiser, anti-wrinkle eye cream, lipstick etc..
Up to the present, astaxanthin composition for cosmetics a lot, but the research of domestic natural astaxanthin application and also
At the early-stage, natural astaxanthin application in cosmetic industry is the most little.
Summary of the invention
The object of the invention, for the deficiencies in the prior art, develops a kind of facial film containing natural astaxanthin, rise have higher
Aging effect of antioxidation, whitening and alleviation, it is to avoid the phenomenon such as the mottle that brings because cell is oxidized, wrinkle.
The object of the invention can be achieved through the following technical solutions, and a kind of biodiesel extracts the method for natural astaxanthin,
Its described method includes: by food stage Haematocoocus Pluvialls dry powder or food stage red phaffia rhodozyma powder or thin rich in astaxanthin
Bacterium dry mycelium, adds biodiesel in the ratio of 1:10-1:2, and in anaerobism, temperature is 5-15 degree Celsius, and pressure is 35Mpa-
Under conditions of 45Mpa, high pressure homogenize 3-5 time, each 10-30 minute, i.e. can get natural oil astaxanthin extract.
Described biodiesel be olive oil, Camellia oil, bathypelagic fish oil, safflower oil one or more.
The formula of a kind of natural astaxanthin facial film is, when its facial film is liquid, its ingredient percentage by weight is: glycerol
2-3%, sodium lactate 0.8-2%, butanediol 1-3%, acrylic acid (or ester) class/C10-30 alcohol acrylate crosspolymers potassium salt
0.2-0.7%, trehalose 0.2-1%, hyaluronate sodium 0.01-0.2%, phenoxyethanol 0.1-0.3%, EDETATE DISODIUM 0.01-
0.03%g, natural oil astaxanthin extract 5-10%, deionized water 81-90%.
A kind of preparation method of natural astaxanthin facial film, when its facial film is liquid, concrete step play into:
(1), in the ratio in the formula of natural astaxanthin facial film by acrylic acid (ester) class/acrylate cross linked polymerization of C10-30 alcohol
Thing potassium salt, glycerol, EDETATE DISODIUM, butanediol and deionized water mixing, stirring, to being completely dispersed, adds after the most swelling 12 hours
Heat, to 80 degrees Celsius, is incubated 20-30 minute;
(2), when it is cooled to 50 degrees Celsius, the sodium lactate of formula ratio, trehalose, hyaluronate sodium and phenoxyethanol are added,
Being thoroughly mixed, vacuum is placed, and treats that it is cooled to 5-10 degree Celsius；
(3), when being cooled to 5-10 degree Celsius, adding natural oil astaxanthin extract, vacuum stirring is uniform；
(4), taking a small amount of sample, by QB/T2872 standard test, 300 mesh filter the most under nitrogen protection, and vacuum is divided
It is loaded on opaque containers, obtains liquid natural astaxanthin facial film.
The preparation method of described natural astaxanthin facial film, its liquid natural astaxanthin facial film, it is coated uniformly at the bottom of facial film
On material.
The preparation method of described natural astaxanthin facial film, described facial film ground is non-woven fabrics, silkworm silk or biological fiber
In one.
The present invention compared with prior art, has the aging effect of more strong anti-oxidation, whitening and alleviation, can avoid because of cell quilt
Oxidation and bring mottle, the phenomenon such as wrinkle.
Specific embodiments
A kind of facial film containing natural astaxanthin Yu biodiesel of the present invention, natural astaxanthin essentially from rain
Raw Haematococcus Pluvialis, also includes from various antibacterial, yeast, plant and animal materials containing astaxanthin.
Embodiment 1: the preparation of the olive oil extract of natural astaxanthin:
Selected biodiesel is olive oil, and itself is rich in unsaturated fatty acid, multivitamin and polyphenoils etc., energy
It is effectively prevented from the phenomenons such as cell senescence that is that occur is brought because fat is oxidized mottle, wrinkle.With olive oil as solvent
Extract natural oil astaxanthin extract, can fully dissolve astaxanthin and can promote again the absorption of skin, and astaxanthin can be made
Anti-oxidation characteristics obtains and more preferably plays.
The extraction step of natural oil astaxanthin extract is: every 40-200g food stage Haematocoocus Pluvialls dry powder or food
Grade red phaffia rhodozyma powder or the antibacterial dry mycelium rich in astaxanthin, add 400g olive oil, in anaerobism, 5-15 degree Celsius,
Under conditions of pressure 35Mpa-45Mpa, high pressure homogenize 3-5 time, obtain natural oil astaxanthin extract, vacuum and low temperature preserves；
In this extract, the content of natural astaxanthin is between 0.1%-10%.
Embodiment 2: the preparation method of natural astaxanthin facial film (liquid):
The preparation method of natural astaxanthin facial film: choose following components, glycerol 3%, sodium lactate 2%, butanediol 3%, acrylic acid (ester)
Class/C10-30 alcohol acrylate crosspolymers potassium salt 0.7%, trehalose 1%, hyaluronate sodium 0.2%, phenoxyethanol 0.3%,
EDETATE DISODIUM 0.03%g, natural oil astaxanthin extract 6%, deionized water 83.77%.Carry out by the component chosen:
(1), by acrylic acid (ester) class/C10-30 alcohol acrylate crosspolymers potassium salt, glycerol, EDETATE DISODIUM, butanediol
Mix with deionized water, stir to being completely dispersed, the most swelling 12 hours post-heating to 80 degree, be incubated 230 minutes;
(2), when it is cooled to 50 degree, add sodium lactate, trehalose, hyaluronate sodium and phenoxyethanol, be thoroughly mixed,
Vacuum is placed, and treats that it cools down；
(3), when being cooled to 5 degree, adding natural oil astaxanthin extract, vacuum stirring is uniform；
(4), a small amount of sample is taken, by QB/T2872 standard test.300 mesh filter the most under nitrogen protection, and vacuum is divided
It is loaded on opaque containers, obtains natural astaxanthin facial film (liquid).During use, this natural astaxanthin facial film (liquid) can be smeared or sprayed
On the face.
Embodiment 3: the preparation method of natural astaxanthin facial film:
Astaxanthin facial film is made up of face-mask material dough-making powder coating solution.Facial film ground is in non-woven fabrics, silkworm silk or biological fiber
Kind, wherein non-woven fabrics is preferred.
The raw material of facial film solution makes astaxanthin facial mask liquid according to following ratio: every 100g facial film solution 2g Han glycerol, newborn
Acid sodium 2g, butanediol 1g, acrylic acid (ester) class/C10-30 alcohol acrylate crosspolymers potassium salt 0.5g, trehalose 1g are transparent
Matter acid sodium 0.2g, phenoxyethanol 0.3g, EDETATE DISODIUM 0.03g, astaxanthin extract 8g of olive oil, deionized water
84.97g.By obtained liquid natural astaxanthin facial film, it is coated uniformly on facial film ground.
Claims (6)
1. the method that a biodiesel extracts natural astaxanthin, it is characterised in that described method includes: by raw for food stage rain red
Ball algae dry powder or food stage red phaffia rhodozyma powder or the antibacterial dry mycelium of astaxanthin-containing, add merit in the ratio of 1:10-1:2
Energy oils and fats, in anaerobism, temperature is 5-15 degree Celsius, under conditions of pressure is 35Mpa-45Mpa, high pressure homogenize 3-5 time, every time
10-30 minute, i.e. can get natural oil astaxanthin extract.
2. biodiesel as claimed in claim 1 extracts the extracting method of natural astaxanthin, it is characterised in that described function oil
Fat be olive oil, Camellia oil, bathypelagic fish oil, safflower oil one or more.
3. the formula of a natural astaxanthin facial film, it is characterised in that when described facial film is liquid, its ingredient weight percent
Ratio is: glycerol 2-3%, sodium lactate 0.8-2%, butanediol 1-3%, and acrylic compounds or propylene esters or C10-30 alcohol acrylate are handed over
Linked polymer potassium salt 0.2-0.7%, trehalose 0.2-1%, hyaluronate sodium 0.01-0.2%, phenoxyethanol 0.1-0.3%, EDTA bis-
Sodium salt 0.01-0.03%g, natural oil astaxanthin extract 5-10%, deionized water 81-90%.
4. the preparation method of a natural astaxanthin facial film, it is characterised in that when described facial film is liquid, concretely comprise the following steps:
(1), in the ratio in the formula of natural astaxanthin facial film by acrylic acid (ester) class/acrylate cross linked polymerization of C10-30 alcohol
Thing potassium salt, glycerol, EDETATE DISODIUM, butanediol and deionized water mixing, stirring, to being completely dispersed, adds after the most swelling 12 hours
Heat, to 80 degrees Celsius, is incubated 20-30 minute;
(2), when it is cooled to 50 degrees Celsius, the sodium lactate of formula ratio, trehalose, hyaluronate sodium and phenoxyethanol are added,
Being thoroughly mixed, vacuum is placed, and treats that it is cooled to 5-10 degree Celsius；
(3), when being cooled to 5-10 degree Celsius, adding natural oil astaxanthin extract, vacuum stirring is uniform；
(4), taking a small amount of sample, by QB/T2872 standard test, 300 mesh filter the most under nitrogen protection, and vacuum is divided
It is loaded on opaque containers, obtains liquid natural astaxanthin facial film.
5. the preparation method of natural astaxanthin facial film as claimed in claim 4, it is characterised in that by described liquid natural shrimp
Blue or green vegetarian noodles film, is coated uniformly on facial film ground.
6. the preparation method of natural astaxanthin facial film as claimed in claim 5, it is characterised in that be by described facial film ground
One in non-woven fabrics, silkworm silk or biological fiber.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610620997.XA CN106074200A (en) | 2016-08-02 | 2016-08-02 | A kind of biodiesel extracts natural astaxanthin and the formula of facial film thereof and preparation method |
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| CN201610620997.XA CN106074200A (en) | 2016-08-02 | 2016-08-02 | A kind of biodiesel extracts natural astaxanthin and the formula of facial film thereof and preparation method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511134A (en) * | 2016-12-13 | 2017-03-22 | 泉州师范学院 | Astaxanthin mask nutrient solution and preparation method thereof |
| CN106963670A (en) * | 2017-04-19 | 2017-07-21 | 北京赛尔佳人化妆品有限公司 | A kind of marine alga moisture saver mask liquid and preparation method thereof |
| CN113491651A (en) * | 2020-04-07 | 2021-10-12 | 中国科学院青岛生物能源与过程研究所 | Soothing and repairing mask essence containing camellia extract and preparation method and application thereof |
| CN113491650A (en) * | 2020-04-07 | 2021-10-12 | 中国科学院青岛生物能源与过程研究所 | Multi-effect nourishing facial mask essence containing camellia extract and preparation method and application thereof |
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| US20100080762A1 (en) * | 2006-09-08 | 2010-04-01 | Regina Goralczyk | Skin care composition |
| CN104945297A (en) * | 2015-05-18 | 2015-09-30 | 万庆家 | Method for extracting astaxanthin from haematococcus pluvialis |
| CN105434319A (en) * | 2015-12-07 | 2016-03-30 | 华南理工大学 | Cosmetics based on phaffia rhodozyma raw materials and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100080762A1 (en) * | 2006-09-08 | 2010-04-01 | Regina Goralczyk | Skin care composition |
| CN104945297A (en) * | 2015-05-18 | 2015-09-30 | 万庆家 | Method for extracting astaxanthin from haematococcus pluvialis |
| CN105434319A (en) * | 2015-12-07 | 2016-03-30 | 华南理工大学 | Cosmetics based on phaffia rhodozyma raw materials and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511134A (en) * | 2016-12-13 | 2017-03-22 | 泉州师范学院 | Astaxanthin mask nutrient solution and preparation method thereof |
| CN106511134B (en) * | 2016-12-13 | 2019-09-17 | 泉州师范学院 | A kind of astaxanthin facial mask nutrient solution and preparation method thereof |
| CN106963670A (en) * | 2017-04-19 | 2017-07-21 | 北京赛尔佳人化妆品有限公司 | A kind of marine alga moisture saver mask liquid and preparation method thereof |
| CN113491651A (en) * | 2020-04-07 | 2021-10-12 | 中国科学院青岛生物能源与过程研究所 | Soothing and repairing mask essence containing camellia extract and preparation method and application thereof |
| CN113491650A (en) * | 2020-04-07 | 2021-10-12 | 中国科学院青岛生物能源与过程研究所 | Multi-effect nourishing facial mask essence containing camellia extract and preparation method and application thereof |
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