CN106509353A - Sonchus oleraceus purple flower extract and preparation method thereof - Google Patents

Sonchus oleraceus purple flower extract and preparation method thereof Download PDF

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Publication number
CN106509353A
CN106509353A CN201610971885.9A CN201610971885A CN106509353A CN 106509353 A CN106509353 A CN 106509353A CN 201610971885 A CN201610971885 A CN 201610971885A CN 106509353 A CN106509353 A CN 106509353A
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CN
China
Prior art keywords
preparation
ixeris denticulata
water
drying
liquid phase
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CN201610971885.9A
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Chinese (zh)
Inventor
雷国俊
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Bole City Yutian Biotechnology Co Ltd
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Bole City Yutian Biotechnology Co Ltd
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Priority to CN201610971885.9A priority Critical patent/CN106509353A/en
Publication of CN106509353A publication Critical patent/CN106509353A/en
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Abstract

The present invention relates to a sonchus oleraceus purple flower extract and a preparation method thereof. Sonchus oleraceus purple flowers are dried to a water content of less than or equal to 30%. The sonchus oleraceus purple flower extract is obtained by stacking, fermenting, drying, crushing, water extracting and concentrating and drying. Compared with the prior art, the preparation method is simple in consumption, especially the water extraction is conducted after the fermentation is carried out, and the preparation method can effectively improve the active ingredients, and greatly improves the utilization of the active ingredients in the sonchus oleraceus purple flowers.

Description

The preparation method of Ixeris denticulata extract and the extract
Technical field
The present invention relates to the preparation method of a kind of Ixeris denticulata extract and the extract.
Background technology
Ixeris denticulata also referred to as sets flourish Herba Sonchi Oleracei, is annual herb plant, gains the name because opening purple flower, its chronic gallbladder for the treatment of The chronic diseases such as inflammation, gastritis, hypertension, cerebral thrombosiss, heart disease have extraordinary effect.Ixeris denticulata is planted for annual Compositae The herb or root of thing.Early spring harvests, and cleans, using fresh herb or dries.For cholecystitis, gastritis have good curative effect.Because open it is pale reddish brown and Gain the name, which is grown in limes marginis, hillside, in bulk integrated distribution, pluck opportunity difference, its drug effect is different, and general early spring excavates medicine Effect is preferable.
Current record, which is grown in limes marginis, hillside, in bulk integrated distribution, plucks opportunity difference, and its drug effect is different, Excavation in good time just can guarantee that drug effect.Ixeris denticulata is typically chosen early spring, the Ching Ming Festival such as before and after harvest, it is after cleaning, in addition to using fresh herb, main Want processing method to be or dry, then mainly brew later or it is to boil water drink, one is to take inconvenience, and two is utilization rate of active components It is low.
The also simply general water extraction of existing some researchs, such as decocting in water or boiled water brew, composition contained therein are not had Effectively lifted.
Therefore, a kind of taking convenience, particularly preferably can be lifted to effective ingredient and Ixeris denticulata that utilization rate is high The preparation method of extract and the extract is just arisen at the historic moment.
The content of the invention
The technical problem to be solved is:A kind of taking convenience is provided, particularly can be preferable to effective ingredient Lifting and the preparation method of the high Ixeris denticulata extract of utilization rate and the extract.
For achieving the above object, the present invention provides following technical scheme:
It is dried:Take fresh Ixeris denticulata and be dried to water content≤30%, preferably 25~30%.
Further, the preferably first dry in the sun of the Ixeris denticulata is to water content≤50%, then inserts drier to water Part content≤30%.
Fermentation:Pile up, in 25~30 DEG C of bottom fermentations 5~10 days.0.5~3% addition yeast of weight of material is pressed preferably Plant and fermented.
Drying:Dry water content≤13%, preferably≤5%.
Crush:It is ground into 500 μm of particles below, preferably 250~380 μm.
Water extraction:Preferably by the granule after above-mentioned crushing in the water of 5~10 times of weight, recirculation water at 90~120 DEG C of temperature Carry 30~90 minutes, mistake≤180 μm sieve, respectively obtains liquid phase and solid phase by preferably 38~150 μm.
By solid phase drying to moisture≤10%, can be used as feed additive.
Concentrate drying:By above-mentioned gained liquid phase concentrate drying to moisture≤10%, Ixeris denticulata extract is obtained.
Compared with prior art, invention formulation taking convenience, especially with carrying out water extraction after fermentation again, to effectively into Divide and effectively can be lifted, substantially increase Ixeris denticulata utilization rate of active components.
Specific embodiment
The following detailed description of the preferred embodiment of the present invention.
Embodiment 1:Fresh Ixeris denticulata is taken, and dry in the sun is to water content 50%, then drier is inserted to water content 30%, in 25~30 DEG C of bottom fermentations 5~10 days, insert drying machine drying to water content 10%, be ground into less than 500 μm Grain, by the granule after the crushing in the water of 5~10 times of weight, at 90~120 DEG C of temperature, recirculation water carries 30~90 minutes, mistake 180 μm of sieves, respectively obtain liquid phase and solid phase.
By gained liquid phase concentrate drying to moisture 10%, Ixeris denticulata extract is obtained.By solid phase drying to moisture Content 10%, then be obtained feed additive.
Embodiment 2:Fresh Ixeris denticulata is taken, and dry in the sun is to water content 45%, then drier is inserted to water content 30%, pile up, in 25~30 DEG C of bottom fermentations 5~10 days, insert drying machine drying to water content 10%, be ground into 500 μm with Under granule, by the granule after crushing in the water of 5~10 times of weight, at 90~120 DEG C of temperature, recirculation water is carried 30~90 minutes, 150 μm of sieves are crossed, liquid phase and solid phase is respectively obtained.
By gained liquid phase concentrate drying to moisture 8%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 10%, then be obtained feed additive.
Embodiment 3:Take fresh Ixeris denticulata, insert drier to water content 25%, by weight of material 0.5~ 3% adds barmses, piles up, and in 25~30 DEG C of bottom fermentations 5~10 days, inserts drying machine drying to water content 8%, crushing Into 300 μm of particles below, by the granule after crushing in the water of 5~10 times of weight, at 90~120 DEG C of temperature, recirculation water carries 30 ~90 minutes, 150 μm of sieves are crossed, liquid phase and solid phase is respectively obtained.
By gained liquid phase concentrate drying to moisture 5%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 8%, then be obtained feed additive.
Embodiment 4:Fresh Ixeris denticulata is taken, and dry in the sun is to water content 40%, then drier is inserted to water content 25%, by 1% addition barmses of weight of material, pile up, in 25~30 DEG C of bottom fermentations 5~10 days.Dehydrator baking is inserted again Water content 8% is done, 250 μm of particles below, by the granule after crushing in the water of 5~10 times of weight, temperature are ground into At 90~120 DEG C, recirculation water is carried 60 minutes, is crossed 150 μm of sieves, is respectively obtained liquid phase and solid phase.
By gained liquid phase concentrate drying to moisture 6%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 10%, then be obtained feed additive.
Embodiment 5:Fresh Ixeris denticulata is taken, and drier is inserted to water content 30%, is piled up, at 25~30 DEG C Natural fermentation 5~10 days, then drying machine drying is inserted to water content 10%, 280 μm of particles below are ground into, by above-mentioned powder In the water of 5~10 times of weight, at 90~120 DEG C of temperature, recirculation water is carried 30~90 minutes granule after broken, crosses 120 μm of sieves, point Liquid phase and solid phase are not obtained.
By gained liquid phase concentrate drying to moisture 7%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 10%, then be obtained feed additive.
Embodiment 6:Fresh Ixeris denticulata is taken, and drier is inserted to water content 28%, is added by the 3% of weight of material Enter barmses, pile up, in 25~30 DEG C of bottom fermentations 5~10 days, then drying machine drying is inserted to water content 10%, be ground into 250 μm of particles below, by the granule after above-mentioned crushing in the water of 5~10 times of weight, at 90~120 DEG C of temperature, recirculation water is carried 30~90 minutes, 75 μm of sieves are crossed, liquid phase and solid phase is respectively obtained.
By gained liquid phase concentrate drying to moisture 5%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 8%, then be obtained feed additive.
Embodiment 7:Fresh Ixeris denticulata is taken, and dry in the sun is to water content 48%, then drier is inserted to water content 25%, by 2% addition barmses of weight of material, pile up, in 25~30 DEG C of bottom fermentations 5~10 days.Dehydrator baking is inserted again Water content 8% is done, 150 μm of particles below, by the granule after crushing in the water of 5~10 times of weight, temperature are ground into At 90~120 DEG C, recirculation water is carried 30~90 minutes, is crossed 38 μm of sieves, is respectively obtained liquid phase and solid phase.
By gained liquid phase concentrate drying to moisture 7%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 10%, then be obtained feed additive.
Embodiment 8:Fresh Ixeris denticulata is taken, and dry in the sun is to water content 45%, then drier is inserted to water content 30%, by 1% addition barmses of weight of material, pile up, in 25~30 DEG C of bottom fermentations 5~10 days.Dehydrator baking is inserted again Water content 10% is done, is crushed:Be ground into 250 μm of particles below, by the granule after crushing 5~10 times of weight water In, at 90~120 DEG C of temperature, recirculation water is carried 30~90 minutes, is crossed 150 μm of sieves, is respectively obtained liquid phase and solid phase.
By gained liquid phase concentrate drying to moisture 6%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 8%, then be obtained feed additive.
Embodiment 9:By fresh Ixeris denticulata, first dry in the sun is to water content 50%, then inserts drier and contain to moisture content Amount 30%, by 1.5% addition barmses of weight of material, piles up, in 25~30 DEG C of bottom fermentations 5~10 days.Drying is inserted again Machine drying is ground into 180 μm of particles below to water content 8%, by the granule after crushing in the water of 5~10 times of weight, At 90~120 DEG C of temperature, recirculation water is carried 30~90 minutes, is crossed 100 μm of sieves, is respectively obtained liquid phase and solid phase.
By gained liquid phase concentrate drying to moisture 5%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 9%, then be obtained feed additive.
Embodiment 10:Take fresh Ixeris denticulata, dry in the sun to water content 30%, by 3% addition yeast of weight of material Kind, pile up, in 25~30 DEG C of bottom fermentations 5~10 days.Drying machine drying is inserted again to water content 5%, is ground into less than 180 μm Granule, by the granule after crushing in the water of 5~10 times of weight, at 90~120 DEG C of temperature, recirculation water carries 30~90 minutes, mistake 75 μm of sieves, respectively obtain liquid phase and solid phase.
By gained liquid phase concentrate drying to moisture 4%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 8%, then be obtained feed additive.
Embodiment 11:Take fresh Ixeris denticulata, dry in the sun to water content 26%, by 2% addition yeast of weight of material Kind, pile up, in 25~30 DEG C of bottom fermentations 5~10 days, then drying machine drying is inserted to water content 5%, be ground into less than 150 μm Granule, by the granule after crushing in the water of 5~10 times of weight, at 90~120 DEG C of temperature, recirculation water carries 30~90 minutes, mistake 100 μm of sieves, respectively obtain liquid phase and solid phase.
By gained liquid phase concentrate drying to moisture 6%, Ixeris denticulata extract is obtained.Solid phase drying is contained to moisture Amount 8%, then be obtained feed additive.
Embodiment 12:Take fresh Ixeris denticulata, dry in the sun to water content 28%, by 0.5~3% addition ferment of weight of material Female strain, piled up, in 25~30 DEG C of bottom fermentations 5~10 days.Drying machine drying is inserted again to water content 8%, is ground into 250 μm Particles below, by the granule after crushing in the water of 5~10 times of weight, at 90~120 DEG C of temperature, recirculation water carries 30~90 points Clock, crosses 100 μm of sieves, respectively obtains liquid phase and solid phase,.
By gained liquid phase concentrate drying to moisture 10%, Ixeris denticulata extract is obtained.By solid phase drying to moisture Content 10%, then be obtained feed additive.
Above-described is only the preferred embodiment of the present invention, it is noted that for one of ordinary skill in the art For, without departing from the concept of the premise of the invention, some changes and improvements can also be made, these belong to the present invention Protection domain.

Claims (10)

1. a kind of preparation method of Ixeris denticulata extract, it is characterised in that the extract is mainly by following technical process Prepare:
It is dried:Take fresh Ixeris denticulata and be dried to water content≤30%;
Fermentation:Pile up, in 25~30 DEG C of bottom fermentations 5~10 days;
Drying:Dry water content≤13%;
Crush:It is ground into 500 μm of particles below.
Water extraction:Preferably by the granule after above-mentioned crushing in the water of 5~10 times of weight, at 90~120 DEG C of temperature, recirculation water carries 30 ~90 minutes, mistake≤180 μm sieve, respectively obtained liquid phase and solid phase by preferably 38~150 μm;
Concentrate drying:By above-mentioned gained liquid phase concentrate drying to moisture≤10%, Ixeris denticulata extract is obtained.
2. the preparation method of Ixeris denticulata extract according to claim 1, it is characterised in that the fermentation, by material 0.5~3% addition barmses of weight are fermented.
3. the preparation method of Ixeris denticulata extract according to claim 1 and 2, it is characterised in that the Ixeris denticulata First dry in the sun is to water content≤50%, then inserts drier to water content≤30%.
4. the preparation method of Ixeris denticulata extract according to claim 1 and 2, it is characterised in that the crushing:Crush Into the granule of 250~380 μ.
5. the preparation method of Ixeris denticulata extract according to claim 3, it is characterised in that the crushing:It is ground into The granule of 250~380 μ.
6. the preparation method of Ixeris denticulata extract according to claim 1 and 2, it is characterised in that the water extraction:Cross 38 ~150 μm of sieves, respectively obtain liquid phase and solid phase.
7. the preparation method of Ixeris denticulata extract according to claim 3, it is characterised in that the water extraction:Cross 38~ 150 μm of sieves, respectively obtain liquid phase and solid phase.
8. the preparation method of Ixeris denticulata extract according to claim 4, it is characterised in that the water extraction:Cross 38~ 150 μm of sieves, respectively obtain liquid phase and solid phase.
9. the preparation method of Ixeris denticulata extract according to claim 5, it is characterised in that the water extraction:Cross 38~ 150 μm of sieves, respectively obtain liquid phase and solid phase.
10. the preparation method of the Ixeris denticulata extract according to any one of claim 1~9, it is characterised in that will be described Solid phase drying to moisture≤10%, as feed additive.
CN201610971885.9A 2016-11-07 2016-11-07 Sonchus oleraceus purple flower extract and preparation method thereof Pending CN106509353A (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102835704A (en) * 2012-08-23 2012-12-26 杨钠 Fermented common sowthistle herb beverage and preparation method thereof
CN103416561A (en) * 2013-08-15 2013-12-04 杨景山 Dahurian patrinia herb tea and starter culture thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102835704A (en) * 2012-08-23 2012-12-26 杨钠 Fermented common sowthistle herb beverage and preparation method thereof
CN103416561A (en) * 2013-08-15 2013-12-04 杨景山 Dahurian patrinia herb tea and starter culture thereof

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Application publication date: 20170322

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