CN106496355A - 一种果胶的制备方法 - Google Patents
一种果胶的制备方法 Download PDFInfo
- Publication number
- CN106496355A CN106496355A CN201610975835.8A CN201610975835A CN106496355A CN 106496355 A CN106496355 A CN 106496355A CN 201610975835 A CN201610975835 A CN 201610975835A CN 106496355 A CN106496355 A CN 106496355A
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- Prior art keywords
- pectin
- preparation
- solvent
- temperature
- dialysis
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- Granted
Links
- 239000001814 pectin Substances 0.000 title claims abstract description 68
- 235000010987 pectin Nutrition 0.000 title claims abstract description 68
- 229920001277 pectin Polymers 0.000 title claims abstract description 68
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 102000004190 Enzymes Human genes 0.000 claims abstract description 25
- 108090000790 Enzymes Proteins 0.000 claims abstract description 25
- 239000002904 solvent Substances 0.000 claims abstract description 24
- 238000000605 extraction Methods 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 22
- 238000000502 dialysis Methods 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 17
- 238000000265 homogenisation Methods 0.000 claims abstract description 16
- 239000000463 material Substances 0.000 claims abstract description 10
- 238000001694 spray drying Methods 0.000 claims abstract description 8
- 238000000638 solvent extraction Methods 0.000 claims abstract description 6
- 239000012530 fluid Substances 0.000 claims abstract description 5
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 239000012467 final product Substances 0.000 claims abstract 2
- 238000010298 pulverizing process Methods 0.000 claims abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 8
- 230000008569 process Effects 0.000 claims description 7
- 235000013399 edible fruits Nutrition 0.000 claims description 6
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 4
- 239000000284 extract Substances 0.000 claims description 4
- 241000207199 Citrus Species 0.000 claims description 3
- 240000000716 Durio zibethinus Species 0.000 claims description 3
- 235000006025 Durio zibethinus Nutrition 0.000 claims description 3
- 244000294611 Punica granatum Species 0.000 claims description 3
- 235000014360 Punica granatum Nutrition 0.000 claims description 3
- 235000020971 citrus fruits Nutrition 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 238000005507 spraying Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 8
- 239000002253 acid Substances 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 235000013305 food Nutrition 0.000 description 5
- 239000002699 waste material Substances 0.000 description 5
- 235000012000 cholesterol Nutrition 0.000 description 4
- IAJILQKETJEXLJ-UHFFFAOYSA-N Galacturonsaeure Natural products O=CC(O)C(O)C(O)C(O)C(O)=O IAJILQKETJEXLJ-UHFFFAOYSA-N 0.000 description 3
- IAJILQKETJEXLJ-RSJOWCBRSA-N aldehydo-D-galacturonic acid Chemical compound O=C[C@H](O)[C@@H](O)[C@@H](O)[C@H](O)C(O)=O IAJILQKETJEXLJ-RSJOWCBRSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001879 gelation Methods 0.000 description 3
- 229910001385 heavy metal Inorganic materials 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000004042 decolorization Methods 0.000 description 2
- 230000002440 hepatic effect Effects 0.000 description 2
- 150000002772 monosaccharides Chemical class 0.000 description 2
- 230000008520 organization Effects 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- PYMYPHUHKUWMLA-UHFFFAOYSA-N 2,3,4,5-tetrahydroxypentanal Chemical compound OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 description 1
- 206010008190 Cerebrovascular accident Diseases 0.000 description 1
- 244000276331 Citrus maxima Species 0.000 description 1
- 235000001759 Citrus maxima Nutrition 0.000 description 1
- 208000032843 Hemorrhage Diseases 0.000 description 1
- 241001299723 Limonia <Rutaceae> Species 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 208000006011 Stroke Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 239000000729 antidote Substances 0.000 description 1
- 235000013405 beer Nutrition 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 231100000357 carcinogen Toxicity 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 230000029142 excretion Effects 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000003058 plasma substitute Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 238000004078 waterproofing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0045—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid alpha-D-Galacturonans, e.g. methyl ester of (alpha-1,4)-linked D-galacturonic acid units, i.e. pectin, or hydrolysis product of methyl ester of alpha-1,4-linked D-galacturonic acid units, i.e. pectinic acid; Derivatives thereof
- C08B37/0048—Processes of extraction from organic materials
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610975835.8A CN106496355B (zh) | 2016-11-07 | 2016-11-07 | 一种果胶的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610975835.8A CN106496355B (zh) | 2016-11-07 | 2016-11-07 | 一种果胶的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN106496355A true CN106496355A (zh) | 2017-03-15 |
CN106496355B CN106496355B (zh) | 2018-11-20 |
Family
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CN201610975835.8A Active CN106496355B (zh) | 2016-11-07 | 2016-11-07 | 一种果胶的制备方法 |
Country Status (1)
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CN (1) | CN106496355B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106866840A (zh) * | 2017-04-08 | 2017-06-20 | 桂林理工大学 | 一种表面活性剂增效微波辐射提取百香果皮中果胶的方法 |
CN107266609A (zh) * | 2017-07-31 | 2017-10-20 | 湖北工业大学 | 电解水提取石榴皮渣果胶的方法 |
CN109134675A (zh) * | 2018-07-10 | 2019-01-04 | 吴海萍 | 一种苹果皮渣多糖的提取方法 |
CN110229248A (zh) * | 2019-06-26 | 2019-09-13 | 广州三广生物科技有限公司 | 一种具有祛眼袋功效的天然提取物 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1749379A (zh) * | 2005-10-18 | 2006-03-22 | 中南大学 | 从柑桔类果皮中提取桔子油和果胶的方法 |
CN104592324A (zh) * | 2015-02-05 | 2015-05-06 | 西安艾克瑞科贸有限公司 | 一种天麻素的提取纯化方法 |
CN105440155A (zh) * | 2015-12-28 | 2016-03-30 | 西北农林科技大学 | 一种果胶提取方法 |
-
2016
- 2016-11-07 CN CN201610975835.8A patent/CN106496355B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1749379A (zh) * | 2005-10-18 | 2006-03-22 | 中南大学 | 从柑桔类果皮中提取桔子油和果胶的方法 |
CN104592324A (zh) * | 2015-02-05 | 2015-05-06 | 西安艾克瑞科贸有限公司 | 一种天麻素的提取纯化方法 |
CN105440155A (zh) * | 2015-12-28 | 2016-03-30 | 西北农林科技大学 | 一种果胶提取方法 |
Non-Patent Citations (1)
Title |
---|
汪海波等: ""柑橘皮果胶的改进提取工艺研究"", 《食品科学》 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106866840A (zh) * | 2017-04-08 | 2017-06-20 | 桂林理工大学 | 一种表面活性剂增效微波辐射提取百香果皮中果胶的方法 |
CN107266609A (zh) * | 2017-07-31 | 2017-10-20 | 湖北工业大学 | 电解水提取石榴皮渣果胶的方法 |
CN109134675A (zh) * | 2018-07-10 | 2019-01-04 | 吴海萍 | 一种苹果皮渣多糖的提取方法 |
CN110229248A (zh) * | 2019-06-26 | 2019-09-13 | 广州三广生物科技有限公司 | 一种具有祛眼袋功效的天然提取物 |
Also Published As
Publication number | Publication date |
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CN106496355B (zh) | 2018-11-20 |
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Application publication date: 20170315 Assignee: Hunan kangliyuan pectin Technology Co.,Ltd. Assignor: LIANYUAN KANGBIOTECH CO.,LTD. Contract record no.: X2023980053693 Denomination of invention: A method for preparing pectin Granted publication date: 20181120 License type: Common License Record date: 20231225 Application publication date: 20170315 Assignee: Lianyuan Orange Sweet Biotechnology Co.,Ltd. Assignor: LIANYUAN KANGBIOTECH CO.,LTD. Contract record no.: X2023980053571 Denomination of invention: A method for preparing pectin Granted publication date: 20181120 License type: Common License Record date: 20231225 |