CN106345389A - Reactor with cooling function - Google Patents
Reactor with cooling function Download PDFInfo
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- CN106345389A CN106345389A CN201610956059.7A CN201610956059A CN106345389A CN 106345389 A CN106345389 A CN 106345389A CN 201610956059 A CN201610956059 A CN 201610956059A CN 106345389 A CN106345389 A CN 106345389A
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- pipe
- tube
- reactor
- dust removing
- flange
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/248—Reactors comprising multiple separated flow channels
- B01J19/249—Plate-type reactors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B9/00—General methods of preparing halides
- C01B9/08—Fluorides
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/24—Stationary reactors without moving elements inside
- B01J2219/2401—Reactors comprising multiple separate flow channels
- B01J2219/245—Plate-type reactors
- B01J2219/2451—Geometry of the reactor
- B01J2219/2456—Geometry of the plates
- B01J2219/2458—Flat plates, i.e. plates which are not corrugated or otherwise structured, e.g. plates with cylindrical shape
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Inorganic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
A reactor with a cooling function comprises a silo tube, a preheating tube, a reaction tube and a cooling tank, wherein a flared capacity-expansion tube is arranged at the bottom of the silo tube, and is gradually inwardly narrowed from the upper end opening to the lower end opening of the capacity-expansion tube; the silo tube, the capacity-expansion tube and the preheating tube are all vertically arranged, and the reaction tube is transversely arranged; the upper end of the preheating tube is connected with the opening at the lower end of the capacity-expansion tube, and the lower end of the preheating tube is communicated with the reaction tube; a first air inlet is arranged at each end of the reaction tube; the silo tube is provided with a first air outlet tube which is communicated with the interior and the exterior of the silo tube; and the reaction tube is arranged inside the cooling tank, and the two ends of the reaction tube protrudes from the cooling tank. The reactor provided by the invention has a cooling function, and has the advantages of long service life, high capacity, and high reaction efficiency.
Description
Technical field
The present invention relates to consersion unit field, more particularly, to a kind of reactor with refrigerating function.
Background technology
Carbon tetrafluoride is important plasma etching gas in current microelectronics industry, be widely used in silicon, silicon dioxide,
The etching of the thin-film materials such as silicon nitride, phosphorosilicate glass and tungsten, in electronic device surface clean, the production of solaode, laser
Technology, cryogenic refrigeration, gas-insulated, leak detectants, printed circuit produce in detergent, the aspect such as lubricant and brake fluid
Also there is extensive application.Carbon tetrafluoride synthetic method is a lot, include hydrofluorocarbons and fluorine gas, cfc in the presence of a catalyst with
Fluohydric acid gas and fluorine gas prepare carbon tetrafluoride etc. with carbon source directly contact reaction.Wherein, current maturation process adopt hydrofluorocarbons,
Cfc does carbon source and prepares carbon tetrafluoride, and the prices of raw materials are expensive, easily explode, and has in synthetic product and be difficult removal
Impurity；Fluorine carbon directly contact reaction method prepares carbon tetrafluoride, and the method, through continuous development and perfection, can prepare height
Pure carbon tetrafluoride.
But, the capacity of existing cylindrical reactor is little, easily blocks, and reaction efficiency is low, needs repeatedly to add reactant, behaviour
Make personnel labor intensity big, and there is no refrigerating function, the service life of reactor is low, and reaction efficiency is low, is unfavorable for carbon tetrafluoride
Preparation.
Content of the invention
It is an object of the invention to propose a kind of reactor with refrigerating function, can overcome of the prior art not
Foot, it has, and refrigerating function, the long service life of reactor, and capacity are big, and reaction efficiency is high.
For reaching this purpose, the present invention employs the following technical solutions:
A kind of reactor with refrigerating function, including feed bin pipe, economizer bank, reaction tube and cooler bin；Described feed bin pipe
Bottom be provided with trumpet-shaped dilatation pipe, the opening of described dilatation Guan Youqi upper end gradually inwardly narrows to the opening of its lower end；
Described feed bin pipe, dilatation pipe and economizer bank be vertically arranged, described reaction tube be horizontally set；
The upper end of described economizer bank is connected with the opening of described dilatation pipe lower end, and the lower end of described economizer bank is communicated in described
Reaction tube；
The two ends of described reaction tube are provided with the first air inlet；
Described feed bin pipe is provided with downtake pipe, and it connects the inside and outside of described feed bin pipe；
In described cooler bin, the two ends of described reaction tube protrude from the outside of described cooler bin to described reaction tube.
Further, the top of described feed bin pipe is provided with charge pipe and blow-down pipe；
One end of one end of described charge pipe and blow-down pipe is respectively communicated with the top of described feed bin pipe；
The two ends of the other end of described charge pipe and described reaction tube are equipped with flange and blind flange, and described blind flange is installed
In described flange.
Further, described cooler bin is rectangular box, and its top is provided with opening.
Further, the bottom outer wall of the wherein side wall of described cooler bin is at least provided with a water inlet pipe；
Outer wall at the top proximal of wherein side wall of described cooler bin is at least provided with an overflow pipe.
Further, described reactor also includes cleaner unit, and it includes dust removing tube and dividing plate；
Described dividing plate includes upper spacer and lower clapboard, the quantity all at least one of described upper spacer and lower clapboard；
Described upper spacer and lower clapboard are equally spacedly welded in described dust removing tube；
Adjacent described upper spacer and lower clapboard form dedusting gas circuit；
The outer wall of described dust removing tube is communicated with the second air inlet pipe and the second exhaust pipe within described dust removing tube, described
Downtake pipe is connected with described second air inlet pipe.
Further, the two ends of described dust removing tube are equipped with blind flange and flange, described blind flange be installed on described flange with
Seal described dust removing tube；
Fitted with the lower surface of the described blind flange on described dust removing tube top in the top of described upper spacer, described lower clapboard
Fitted with the upper surface of the described blind flange of described dust removing tube bottom in bottom.
Further, described cleaner unit also includes multiple baffle plates；
Described baffle plate is individually fixed in the blind flange at described dust removing tube two ends, and respectively be located at described upper spacer or under every
The both sides of the weld of plate.
Further, the bottom of described dust removing tube is provided with trumpet-shaped seal pipe；
The described blind flange of the bottom of described dust removing tube is communicated with the blow-off pipe within described dust removing tube, described blowdown
Pipe is provided with valve.
Further, described reaction tube be respectively arranged at two ends with flange and blind flange, described blind flange is installed on described flange
To seal described reaction tube；
Described first air inlet is located at described blind flange.
Further, described downtake pipe is laterally at described feed bin pipe top proximal.
The present invention proposes a kind of reactor with refrigerating function according to the above, and it has refrigerating function, Neng Gouzeng
Plus the service life of reactor, and capacity is big, reaction efficiency is high.
Described reactor is used for fluorine gas and carbon reaction generates carbon tetrafluoride, and carbon is placed on described feed bin pipe, economizer bank and anti-
In should managing, described first air inlet, located at the two ends of reaction tube, on the one hand can increase fluorine gas in the unit interval and be passed through to described
The amount of reaction tube, makes more fluorine gas and carbon be fully contacted, and increases the efficiency of reaction；Fluorine gas and carbon occur to release during chemical reaction
Heat, because the lower end of described economizer bank is communicated in described reaction tube, substantial amounts of heat can be transmitted by product carbon tetrafluoride
These carbon are preheated by the carbon to described economizer bank, keep reaction temperature stable, make the reaction efficiency of follow-up carbon and fluorine gas
Higher.
Fluorine gas and carbon reaction when can release substantial amounts of heat, described cooler bin built with cooling water, to reduce described reaction tube
Temperature, thus increasing its service life.The two ends of described reaction tube protrude from the outside of described cooler bin, are easily installed in it
The dismounting of the blind flange at two ends, it is to avoid cooling water enters in described reaction tube.
With the carrying out of reaction, the carbon of described reaction tube is gradually consumed, due to described feed bin pipe, dilatation pipe and economizer bank
It is vertically arranged, under gravity, the carbon in described economizer bank will fall to described reaction tube to ensure reaction
Persistently carry out, improve stability and the persistence of its work；Similarly, the carbon in described feed bin pipe can fall to described economizer bank
The interior carbon ensureing question response is preheated, ready for follow-up reaction.
Trumpet-shaped described dilatation pipe has the effect that the described feed bin tube capacity of expansion amasss, due to described dilatation Guan Youqi upper end
Opening gradually inwardly narrow to the opening of its lower end, so being connected to the cross section of the feed bin pipe of described dilatation pipe upper end open
The long-pending cross-sectional area of the economizer bank being connected to described dilatation pipe lower ending opening that can be more than is it is assumed that described feed bin pipe and economizer bank are in phase
Under same length, the volume of described feed bin pipe can greatly increase, thus reducing the addition number of times of carbon, improves described reactor work
Persistence.
So speed when described dilatation pipe falls to described economizer bank for the carbon can slow down, the carbon tetrafluoride gas that reaction generates
Know from experience and discharge from described downtake pipe.
Brief description
Fig. 1 is the part sectioned view in the front of the one of embodiment of the present invention.
Fig. 2 is the part sectioned view of the side of the one of embodiment of the present invention.
Fig. 3 is the part sectioned view in the front of cleaner unit of the one of embodiment of the present invention.
Fig. 4 is the partial enlarged drawing at the c of Fig. 3.
Wherein: feed bin pipe 21, dilatation pipe 211, downtake pipe 212, charge pipe 213, blow-down pipe 214, support base 215,
Economizer bank 22, reaction tube 23, the first air inlet 231, thermometer boss 232, flange 261, blind flange 262, cooler bin 24, water inlet
Pipe 241, overflow pipe 242, cleaner unit 25, dust removing tube 251, seal pipe 2511, dividing plate 252, upper spacer 2521, lower clapboard 2522,
Dedusting gas circuit 253, the second air inlet pipe 254, second exhaust pipe 255, baffle plate 256, blow-off pipe 257.
Specific embodiment
Further illustrate technical scheme below in conjunction with the accompanying drawings and by specific embodiment.
A kind of reactor with refrigerating function, including feed bin pipe 21, economizer bank 22, reaction tube 23 and cooler bin 24；
The bottom of described feed bin pipe 21 is provided with trumpet-shaped dilatation pipe 211, described dilatation pipe 211 from its upper end opening to
The opening of its lower end gradually inwardly narrows；
Described feed bin pipe 21, dilatation pipe 211 and economizer bank 22 be vertically arranged, described reaction tube 23 be horizontally set；
The upper end of described economizer bank 22 is connected with the opening of described dilatation pipe 211 lower end, and the lower end of described economizer bank 22 is even
Lead in described reaction tube 23；
The two ends of described reaction tube 23 are provided with the first air inlet 231；
Described feed bin pipe 21 is provided with downtake pipe 212, and it connects the inside and outside of described feed bin pipe 21；
In described cooler bin 24, the two ends of described reaction tube 23 protrude from described cooler bin 24 to described reaction tube 23
Outside.
As Fig. 1, the described reactor of the present embodiment is used for fluorine gas and carbon reaction generates carbon tetrafluoride, and carbon is placed on described material
In storekeeper 21, economizer bank 22 and reaction tube 23, described first air inlet 231, located at the two ends of reaction tube 23, on the one hand can increase
Plus fluorine gas is passed through to the amount of described reaction tube 23 in the unit interval, so that more fluorine gas and carbon is fully contacted, increase the effect of reaction
Rate；There is to release heat during chemical reaction in fluorine gas and carbon, because the lower end of described economizer bank 22 is communicated in described reaction tube 23, greatly
The heat of amount can be transferred to the carbon in described economizer bank 22 by product carbon tetrafluoride, and these carbon are preheated, and keeps anti-
Answer temperature stabilization, make the reaction efficiency of follow-up carbon and fluorine gas higher.
Fluorine gas and carbon reaction when can release substantial amounts of heat, described cooler bin 24 built with cooling water, to reduce described reaction
The temperature of pipe 23, thus increase its service life.The two ends of described reaction tube 23 protrude from the outside of described cooler bin 24, convenient
It is arranged on the dismounting of the blind flange 262 at its two ends, it is to avoid cooling water enters in described reaction tube 23.
With the carrying out of reaction, the carbon of described reaction tube 23 is gradually consumed, due to described feed bin pipe 21, dilatation pipe 211
It is vertically arranged with economizer bank 22, under gravity, the carbon in described economizer bank 22 will fall to described reaction tube
23 are persistently carried out with ensureing react, improve stability and the persistence of its work；Similarly, the carbon meeting in described feed bin pipe 21
Fall in described economizer bank 22 and ensure that the carbon of question response is preheated, ready for follow-up reaction.
Trumpet-shaped described dilatation pipe 211 has the effect expanding described feed bin pipe 21 volume, due to described dilatation pipe 211
Gradually inwardly narrowed from the opening of its upper end to the opening of its lower end, so being connected to the material of described dilatation pipe 211 upper end open
The cross-sectional area of storekeeper 21 can be more than the cross-sectional area of the economizer bank 22 being connected to described dilatation pipe 211 lower ending opening it is assumed that institute
State feed bin pipe 21 and economizer bank 22 under identical length, the volume of described feed bin pipe 21 can greatly increase, thus reducing carbon
Add number of times, improve the persistence of described reactor work.
So speed when described dilatation pipe 211 falls to described economizer bank 22 for the carbon can slow down, the tetrafluoro that reaction generates
Change carbon gas to discharge from described downtake pipe 212.
Further, the top of described feed bin pipe 21 is provided with charge pipe 213 and blow-down pipe 214；
One end of one end of described charge pipe 213 and blow-down pipe 214 is respectively communicated with the top of described feed bin pipe 21；
The two ends of the other end of described charge pipe 213 and described reaction tube 23 are equipped with flange 261 and blind flange 262, institute
State blind flange 262 and be installed on described flange 261.
Carbon in described reactor, after reaction consumes, adds from the charge pipe 213 located at described feed bin pipe 21 top
Carbon, operates simpler convenience directly, because one end of one end of described charge pipe 213 and blow-down pipe 214 is respectively communicated with institute
State the top of feed bin pipe 21, so carbon can fall to feed bin pipe 21, dilatation pipe 211, economizer bank 22 and anti-under gravity
Should pipe 23, with ensure react persistently carry out；Because the two ends of the other end of described charge pipe 213 and described reaction tube 23 are all provided with
There are flange 261 and blind flange 262, described blind flange 262 is installed on described flange 261, so only need to dismantle described in charging
Blind flange 262, just can carry out feeding operation to described reactor.
The other end of described blow-down pipe 214 is communicated to exhaust gas treating tower, and only need to open emptying valve during operation can be to enter
The emptying of circulation of qi promoting body.
Further, described cooler bin 24 is rectangular box, and its top is provided with opening.
The casing of rectangle easily produces, and the cooling water that can load is also more, the opening that its top is provided with play observation and
Check the effect of described reactor behaviour in service.
Further, the bottom outer wall of the wherein side wall of described cooler bin 24 is at least provided with a water inlet pipe 241；
Outer wall at the top proximal of wherein side wall of described cooler bin 24 is at least provided with an overflow pipe 242.
As Fig. 2, the quantity of the described water inlet pipe 241 of the present embodiment is one, and the quantity of described overflow pipe 242 is two, described
Water inlet pipe 241 and overflow pipe 242, all located at the side wall of described cooler bin 24, are more convenient its installation；Described cooler bin 24 is wherein
The bottom outer wall of side wall, when passing through the water inlet of described water inlet pipe 241 when cooling water, cooling water is passed through to described cooler bin
Can more slowly stablize when 24；Described overflow pipe 242 is outer at the top proximal of the wherein side wall of described cooler bin 24
Wall it is ensured that the cooling water in described cooler bin 24 enough effectively to cool down described reaction tube 23, it is to avoid cooling water excess overflow
Go out.
Further, described reaction tube 23 is provided with least one thermometer boss 232；
The lower end closed of described thermometer boss 232 and be located at described reaction tube 23 in；
It is provided with temperature detector in described thermometer boss 232.
As Fig. 1, the quantity of the described thermometer boss 232 of the present embodiment is two, and is symmetrically set in 22 liang of described economizer bank
On the described reaction tube 23 of side, it is possible to increase the precision to the temperature detection in reaction tube 23 for the described temperature detector, described
The lower end closed of thermometer boss 232, can seal described reaction tube 23 and also can protect described temperature detector.
Further, described reactor also includes cleaner unit 25, and it includes dust removing tube 251 and dividing plate 252；
Described dividing plate 252 includes upper spacer 2521 and lower clapboard 2522, the number of described upper spacer 2521 and lower clapboard 2522
Amount all at least one；
Described upper spacer 2521 and lower clapboard 2522 are equally spacedly welded in described dust removing tube 251；
Adjacent described upper spacer 2521 and lower clapboard 2522 form dedusting gas circuit 253；
The outer wall of described dust removing tube 251 is communicated with the second air inlet pipe 254 and second row within described dust removing tube 251
Trachea 255, described downtake pipe 212 is connected with described second air inlet pipe 254.
As the insufficient carbon dust of some reactions, most carbon dust can be mixed in the carbon tetrafluoride gas that Fig. 3, reaction generate
Heavy collection can drop back into described reaction tube 23 when through carbon-coating, fraction carbon dust is with carbon tetrafluoride gas together from described first exhaust
Pipe 212 is discharged, when the carbon tetrafluoride gas being contaminated with carbon dust enter to described dust removing tube 251 through described second air inlet pipe 254
Dedusting gas circuit 253 when, in the presence of the iris action and gravity of described upper spacer 2521 and lower clapboard 2522, carbon dust can sink
It is down to the bottom of described dust removing tube 251, be easy to follow-up cleaning, to improve the purity of carbon tetrafluoride gas, finally further
The carbon tetrafluoride gas of purification are discharged from described second exhaust pipe 255.
The quantity of the described upper spacer 2521 of the present embodiment is two, and the quantity of described lower clapboard 2522 is one, by welding,
Make described upper spacer 2521 and lower clapboard 2522 more firmly in described dust removing tube 251.
Further, the two ends of described dust removing tube 251 are equipped with blind flange 262 and flange 261, and described blind flange 262 is installed
In described flange 261 to seal described dust removing tube 251；
Fitted with the lower surface of the described blind flange 262 on described dust removing tube 251 top in the top of described upper spacer 2521, institute
Fitted with the upper surface of the described blind flange 262 of described dust removing tube 251 bottom in the bottom stating lower clapboard 2522.
As Fig. 3, can rapidly clear up described dust removing tube 251, described upper spacer 2521 by dismounting described blind flange 262
Top fit with the lower surface of the described blind flange 262 on described dust removing tube 251 top, the bottom of described lower clapboard 2522 and institute
State the upper surface laminating of the described blind flange 262 of dust removing tube 251 bottom, so that the carbon tetrafluoride gas mixing is removed along described as far as possible
Moving in dust and gas road 253, rather than directly directly wears from the joint place of described blind flange 262 and upper spacer 2521 and lower clapboard 2522
Cross, improve and remove the quality of carbon dust and the purity of carbon tetrafluoride gas.
Further, described cleaner unit 25 also includes multiple baffle plates 256；
Described baffle plate 256 is individually fixed in the blind flange 262 at described dust removing tube 251 two ends, and is located at respectively on described
The both sides of the weld of dividing plate 2521 or lower clapboard 2522.
As Fig. 4, improve further and remove the quality of carbon dust and the purity of carbon tetrafluoride gas, described baffle plate 256 can stop
The carbon tetrafluoride gas mixing directly directly are worn from the joint place of described blind flange 262 and upper spacer 2521 and lower clapboard 2522
Cross.
Further, the bottom of described dust removing tube 251 is provided with trumpet-shaped seal pipe 2511；
The described blind flange 262 of the bottom of described dust removing tube 251 is communicated with the blow-off pipe within described dust removing tube 251
257, described blow-off pipe 257 is provided with valve.
As Fig. 3, the described blind flange 262 of described dust removing tube 251 bottom need to periodically pull down discharge solid-state carbon dust, but described removes
The diameter of dirt pipe 251 bottom is bigger, is more difficult to seal, so described seal pipe 2511 is set to opening from its upper end to its lower end
The trumpet-shaped pipe that gradually inwardly narrows of opening, improve its seal degree.
The fluorine gas of the present embodiment is produced by electrolysis, so can be contaminated with hf gas in fluorine gas, at a temperature of it
Acid solution can be become after fall, in order to clear up safety during carbon dust, first open the valve on described blow-off pipe 257, clear acid solution, then tear open
Unload blind flange 262 cleaning dust.
Further, described reaction tube 23 be respectively arranged at two ends with flange 261 and blind flange 262, described blind flange 262 is installed
In described flange 261 to seal described reaction tube 23；
Described first air inlet 231 is located at described blind flange 262.
By installing described flange 261 in described blind flange 262, can effectively seal described reaction tube 23, it is to avoid gas
Body leaks, the such as leakage of reactant fluorine gas and the leakage of product carbon tetrafluoride gas；By dismantling described blind flange 262, energy
Enough rapidly clear up the waste residue that the reaction in described reaction tube 23 stays, simple to operation；Described first air inlet 231 located at
Described blind flange 262 is it is ensured that fluorine gas is passed through effectively to described reaction tube.
Further, the described downtake pipe 212 laterally radial position at described feed bin pipe 21 top proximal.
During reaction, the reaction of part carbon is insufficient, and the gas that the carbon dust of a residual part can be generated by reaction is taken away, and described the
The one exhaustor 212 laterally outer wall at described feed bin pipe 21 top proximal, can make the distance that gas rises increase, favorably
In the sedimentation under gravity of carbon dust, improve the purity of carbon tetrafluoride gas.
Further, described feed bin pipe 21 also includes at least two support bases 215；Described support base 215 is along described feed bin
The outer wall circumference of pipe 21 is equally spacedly arranged.
The quantity of the described support base 215 of the present embodiment be two, its along described feed bin pipe 21 outer wall circumference equally spacedly
Setting, can preferably support described feed bin pipe 21, being more uniformly stressed when making described feed bin pipe 21 be supported.
Describe the know-why of the present invention above in association with specific embodiment.These descriptions are intended merely to explain the present invention's
Principle, and limiting the scope of the invention can not be construed to by any way.Based on explanation herein, the technology of this area
Personnel do not need to pay other specific embodiments that performing creative labour can associate the present invention, and these modes fall within
Within protection scope of the present invention.
Claims (10)
1. a kind of reactor with refrigerating function, including feed bin pipe, economizer bank, reaction tube and cooler bin；It is characterized in that:
The bottom of described feed bin pipe is provided with trumpet-shaped dilatation pipe, and the opening of described dilatation Guan Youqi upper end is to the opening of its lower end
Gradually inwardly narrow；
Described feed bin pipe, dilatation pipe and economizer bank be vertically arranged, described reaction tube be horizontally set；
The upper end of described economizer bank is connected with the opening of described dilatation pipe lower end, and the lower end of described economizer bank is communicated in described reaction
Pipe；
The two ends of described reaction tube are provided with the first air inlet；
Described feed bin pipe is provided with downtake pipe, and it connects the inside and outside of described feed bin pipe；
In described cooler bin, the two ends of described reaction tube protrude from the outside of described cooler bin to described reaction tube.
2. a kind of reactor with refrigerating function according to claim 1 it is characterised in that: the top of described feed bin pipe
It is provided with charge pipe and blow-down pipe；
One end of one end of described charge pipe and blow-down pipe is respectively communicated with the top of described feed bin pipe；
The two ends of the other end of described charge pipe and described reaction tube are equipped with flange and blind flange, and described blind flange is installed on institute
State flange.
3. a kind of reactor with refrigerating function according to claim 1 it is characterised in that: described cooler bin be rectangle
Casing, its top is provided with opening.
4. a kind of reactor with refrigerating function according to claim 3 it is characterised in that: described cooler bin is wherein
The bottom outer wall of side wall is at least provided with a water inlet pipe；
Outer wall at the top proximal of wherein side wall of described cooler bin is at least provided with an overflow pipe.
5. a kind of reactor with refrigerating function according to claim 1 it is characterised in that: described reactor also includes
Cleaner unit, it includes dust removing tube and dividing plate；
Described dividing plate includes upper spacer and lower clapboard, the quantity all at least one of described upper spacer and lower clapboard；
Described upper spacer and lower clapboard are equally spacedly welded in described dust removing tube；
Adjacent described upper spacer and lower clapboard form dedusting gas circuit；
The outer wall of described dust removing tube is communicated with the second air inlet pipe and the second exhaust pipe within described dust removing tube, and described first
Exhaustor is connected with described second air inlet pipe.
6. a kind of reactor with refrigerating function according to claim 5 it is characterised in that:
The two ends of described dust removing tube are equipped with blind flange and flange, and described blind flange is installed on described flange to seal described dedusting
Pipe；
Fitted with the lower surface of the described blind flange on described dust removing tube top in the top of described upper spacer, the bottom of described lower clapboard
Fit with the upper surface of the described blind flange of described dust removing tube bottom.
7. a kind of reactor with refrigerating function according to claim 6 it is characterised in that: described cleaner unit also includes
Multiple baffle plates；
Described baffle plate is individually fixed in the blind flange at described dust removing tube two ends, and is located at described upper spacer or lower clapboard respectively
The both sides of weld.
8. a kind of reactor with refrigerating function according to claim 6 it is characterised in that: the bottom of described dust removing tube
It is provided with trumpet-shaped seal pipe；
The described blind flange of the bottom of described dust removing tube is communicated with the blow-off pipe within described dust removing tube, and described blow-off pipe sets
There is valve.
9. a kind of reactor with refrigerating function according to claim 1 it is characterised in that:
Described reaction tube be respectively arranged at two ends with flange and blind flange, it is described anti-to seal that described blind flange is installed on described flange
Ying Guan；
Described first air inlet is located at described blind flange.
10. a kind of reactor with refrigerating function according to claim 1 it is characterised in that: described downtake pipe
Laterally at described feed bin pipe top proximal.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610956059.7A CN106345389B (en) | 2016-10-27 | 2016-10-27 | A kind of reactor with refrigerating function |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610956059.7A CN106345389B (en) | 2016-10-27 | 2016-10-27 | A kind of reactor with refrigerating function |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112892410A (en) * | 2021-02-02 | 2021-06-04 | 福建德尔科技有限公司 | Reactor for preparing electronic-grade carbon tetrafluoride, uninterrupted reaction device and method |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5196629A (en) * | 1991-11-21 | 1993-03-23 | Mobil Oil Corporation | Isoparaffin:olefin alkylation process and reactor apparatus |
| CN1233971A (en) * | 1996-09-09 | 1999-11-03 | 普利茅斯产品公司 | Method and apparatus for continuous extrusion of block elements |
| CN2659530Y (en) * | 2003-11-28 | 2004-12-01 | 王志强 | Smoke purifier |
| CN201250097Y (en) * | 2008-06-24 | 2009-06-03 | 核工业理化工程研究院华核新技术开发公司 | Reactor for preparing carbon tetrafluoride gas |
| CN103088431A (en) * | 2013-01-17 | 2013-05-08 | 陈功 | Device for eliminating phosphorus oxychloride in phosphorus diffusion furnace |
| CN106390876A (en) * | 2016-10-27 | 2017-02-15 | 广东华特气体股份有限公司 | Large-capacity reactor |
| CN206435214U (en) * | 2016-10-27 | 2017-08-25 | 广东华特气体股份有限公司 | A kind of reactor with refrigerating function |
-
2016
- 2016-10-27 CN CN201610956059.7A patent/CN106345389B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5196629A (en) * | 1991-11-21 | 1993-03-23 | Mobil Oil Corporation | Isoparaffin:olefin alkylation process and reactor apparatus |
| CN1233971A (en) * | 1996-09-09 | 1999-11-03 | 普利茅斯产品公司 | Method and apparatus for continuous extrusion of block elements |
| CN2659530Y (en) * | 2003-11-28 | 2004-12-01 | 王志强 | Smoke purifier |
| CN201250097Y (en) * | 2008-06-24 | 2009-06-03 | 核工业理化工程研究院华核新技术开发公司 | Reactor for preparing carbon tetrafluoride gas |
| CN103088431A (en) * | 2013-01-17 | 2013-05-08 | 陈功 | Device for eliminating phosphorus oxychloride in phosphorus diffusion furnace |
| CN106390876A (en) * | 2016-10-27 | 2017-02-15 | 广东华特气体股份有限公司 | Large-capacity reactor |
| CN206435214U (en) * | 2016-10-27 | 2017-08-25 | 广东华特气体股份有限公司 | A kind of reactor with refrigerating function |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112892410A (en) * | 2021-02-02 | 2021-06-04 | 福建德尔科技有限公司 | Reactor for preparing electronic-grade carbon tetrafluoride, uninterrupted reaction device and method |
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Application publication date: 20170125 Assignee: XIANGNENG SEMIGAS (CHENZHOU) Co.,Ltd. Assignor: GUANGDONG HUATE GASES Co.,Ltd. Contract record no.: X2021440000088 Denomination of invention: A reactor with cooling function Granted publication date: 20190322 License type: Common License Record date: 20210315 |