CN106336969A - Atractylodes lancea volatile oil-containing antibacterial perfumed soap, and making method and application thereof - Google Patents
Atractylodes lancea volatile oil-containing antibacterial perfumed soap, and making method and application thereof Download PDFInfo
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- CN106336969A CN106336969A CN201610603490.3A CN201610603490A CN106336969A CN 106336969 A CN106336969 A CN 106336969A CN 201610603490 A CN201610603490 A CN 201610603490A CN 106336969 A CN106336969 A CN 106336969A
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- Prior art keywords
- oil
- volatile oil
- antibacterial
- atractylodis lanceae
- rhzoma atractylodis
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses an Atractylodes lancea volatile oil-containing antibacterial perfumed soap, and a making method and an application thereof. The making method of the above product is simple and safe, and antibacterial active substances and soap base raw materials used in the invention are natural products, so the product is safe and nontoxic, and has no side effects. The use amount of effective components is determined in the invention. Too large content of the natural antibacterial active components influences the emulsification effect of the perfumed soap, and too small content of the natural antibacterial active components does not reach the antibacterial effect. The Atractylodes lancea volatile oil-containing antibacterial perfumed soap overcomes the defects of chemically synthesized antiseptics, can inhibit growth of common bacteria on skins cuticles, has a certain treatment effect on manus and tinea pedis, also has certain nourishing and moisture retention effects on skins, and is suitable for most people. Volatile substances in Atractylodes lancea volatile oil have an inhibition effect on pathogenic microorganisms in air, and have fragrant smell, so the Atractylodes lancea volatile oil-containing antibacterial perfumed soap can clean skins, can purify air, and keeps pleasant home environment.
Description
Technical field
The present invention relates to a kind of novel toilet soap is and in particular to a kind of Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil and preparation method thereof
And application.
Background technology
We live around, there is substantial amounts of malignant bacteria and fungi, and they are the main sources of infection.Skin is
The parasitic main portions of pathogenic bacteria, are one of pre- aseptic good measures using the perfumed soap with antibacterial action.Go out on market
The perfumed soap major part sold is that its security needs to be probed into, and makes for a long time using the chemical substance antibacterial such as triclocarban, triclosan
This bacterium can be led to produce drug resistance with certain chemical substance bacteria growing inhibiting.With the material of plant origin and bioactivator
Make perfumed soap for primary raw material, its ph value is relatively low, the acceptance that human skin can be long-term.Some plant extracts of existing discovery
In the natural high-efficiency antimicrobial active material that contains, bad reaction and side effect will not be produced to human body, without compromising on user
Health.But the active substance of plant that can maturely be applied to perfumed soap in prior art is less or relatively costly.
Content of the invention
In order to solve the deficiencies in the prior art, the invention provides a kind of Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil and its preparation
Methods and applications.
The technical scheme is that a kind of Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil, the antibacterial in described Antibacterial soaps is lived
Property and fragrance ingredient be Rhzoma Atractylodis Lanceae volatile oil.
Another object of the present invention is to providing a kind of Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil, include rhizoma atractylodis according to mass parts
Volatile oil 0.05-5 part, palm oil 10-12 part, castor oil 20-23 part, olive oil 20-35 part, NaOH 8.5-9 part and water
20-25 part.
Further improvement of the present invention includes:
According to mass parts by Rhzoma Atractylodis Lanceae volatile oil 0.05-5 part, palm oil 10-12 part, castor oil 20-23 part, olive oil 20-
35 parts, NaOH 8.5-9 part and water 20-25 part composition.
Present invention also offers a kind of preparation method of the Antibacterial soaps as containing Rhzoma Atractylodis Lanceae volatile oil, its step includes: to soap
Add Rhzoma Atractylodis Lanceae volatile oil in base, then stir, obtain mixing soap lye；Dip in a small amount of olive oil brushing die inside with brush,
Then the soap lye of mixing is poured into and with plastic sheeting, mould is covered after mould, 35 DEG C of incubators are placed 2～3 days, obtain perfumed soap.
The preparation method of described soap base includes: palm oil, castor oil, olive oil is put into by weight to scale heatproof container
Interior, heating makes the temperature of oil maintain 40 DEG C～50 DEG C；By the amount of required water and NaOH, water is poured slowly into and fills hydrogen-oxygen
Change in the glass container of sodium, side edged is quickly stirred with alkaline-resisting agitator, and NaOH is cooled to 40 DEG C after being dissolved completely in water
～50 DEG C, obtain aqueous slkali；The aqueous slkali preparing slowly is poured into the resistance to thermal capacitance that dress is mixed with palm oil, castor oil, olive oil
In device, side edged is constantly stirred with alkaline-resisting agitator, and stir about makes both saponifications in 40 minutes, until two kinds of solution are complete
Mixing obtains final product soap base, and adjusts ph to 7.5～8.
Invention further provides Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil are in suppression tubercle bacillus, Escherichia coli, golden yellow
Color staphylococcus, candida albicanses, pseudomonas aeruginosa, salmonella typhimurium, Trichophyton rubrum, acrothesium floccosum
And/or the application in Trichophyton mentagrophytes growth.And application in treatment tinea manuum and tinea pedis for the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil.
Advantages of the present invention:
The product that the present invention provides, its antibacterial activity is significantly improved, and can effectively suppress multiple pathogenetic bacterias and true
The growth of bacterium.
Production process is simple safety of the present invention, antibacterial substance used and soap base raw material are natural products, tool
Have the advantages that safe and nontoxic, have no side effect.Determine effective ingredient consumption.Because natural antibacterial active component content is excessive then
The emulsifying effectiveness of perfumed soap can be affected, and consumption is too small can not play antibacterial effect.Applicant through long research and
Substantial amounts of analysis of experimental data, it is determined that the Optimum of this active constituent content, is allowed to there is good antibacterial effect, simultaneously
Do not affect the shaping of perfumed soap again.
The present invention prepares Antibacterial soaps and its preparation method and application using Rhzoma Atractylodis Lanceae volatile oil, overcomes chemical synthesis antiseptic
Defect.The perfumed soap of the present invention can suppress the growth of epiderm skin common bacteria, has certain therapeutic action to tinea of feet and hands, also
There is certain nourishing moisture-keeping function to skin it is adaptable to most of crowd.Volatile materials in Rhzoma Atractylodis Lanceae volatile oil is for air
In pathogenic microorganism inhibited, and fragrant odour.Therefore, the perfumed soap containing Rhzoma Atractylodis Lanceae volatile oil composition can not only be clear
Clean skin, additionally it is possible to purify air, keeps pleasant domestic environment.
Specific embodiment
With reference to embodiment, the present invention is elaborated.
Embodiment 1: the preparation one of the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil
The first step: weigh 11 kilograms of palm oil, 20 kilograms of castor oil, 30 kilograms of olive oil, be sequentially placed in heatproof container,
Boiled with water proof mode of heating molten, make mixing oil temperature maintain 40 DEG C～50 DEG C.
Second step: weigh 20 kilograms of water, 9 kilograms of NaOH.First NaOH is put in glass container, then slowly
Add water, side edged is quickly stirred with alkaline-resisting agitator, and NaOH is cooled to 40 DEG C～50 DEG C after being dissolved completely in water, obtain alkali
Solution.
3rd step: the aqueous slkali of second step is slowly poured in the glass container equipped with miscella of the first step, leans to one side
While be stirred continuously about 40 minutes with alkaline-resisting agitator making both saponifications, obtain final product soap base until both solution are thoroughly mixed,
Then adjust ph to 7.5～8.
4th step: add 1 kilogram of Rhzoma Atractylodis Lanceae volatile oil toward in the soap base of the 3rd step while stirring, then stir, obtain
Mixing soap lye.
5th step: dip in a small amount of olive oil brushing die inside with brush, mould poured into by the soap lye then mixing the 4th step
With plastic sheeting, mould is covered afterwards, 35 DEG C of incubators are placed 2～3 days, obtain perfumed soap.
6th step: ready-made for the 5th step perfumed soap is removed from the molds, is put in ventilation and allows it to spontaneously dry, about 5 weeks left
The right side, obtains perfumed soap finished product.
Embodiment 2: the preparation two of the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil
The first step: weigh 12 kilograms of palm oil, 21 kilograms of castor oil, 25.5 kilograms of olive oil, be sequentially placed into heatproof container
Interior, boiled with water proof mode of heating molten, make mixing oil temperature maintain 40 DEG C～50 DEG C.
Second step: weigh 21 kilograms of water, 9 kilograms of NaOH.First NaOH is put in glass container, then slowly
Add water, side edged is quickly stirred with alkaline-resisting agitator, and NaOH is cooled to 40 DEG C～50 DEG C after being dissolved completely in water, obtain alkali
Solution.
3rd step: the aqueous slkali of second step is slowly poured in the glass container equipped with miscella of the first step, leans to one side
While be stirred continuously about 40 minutes with alkaline-resisting agitator making both saponifications, obtain final product soap base until both solution are thoroughly mixed,
Then adjust ph to 7.5～8.
4th step: add 1.5 kilograms of Rhzoma Atractylodis Lanceae volatile oils toward in the soap base of the 3rd step while stirring, then stir, obtain
To mixing soap lye.
5th step: dip in a small amount of olive oil brushing die inside with brush, mould poured into by the soap lye then mixing the 4th step
With plastic sheeting, mould is covered afterwards, 35 DEG C of incubators are placed 2～3 days, obtain perfumed soap.
6th step: ready-made for the 5th step perfumed soap is removed from the molds, is put in ventilation and allows it to spontaneously dry, about 5 weeks left
The right side, obtains perfumed soap finished product.
Embodiment 3: the preparation three of the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil
The first step: weigh 10 kilograms of palm oil, 22 kilograms of castor oil, 23 kilograms of olive oil, be sequentially placed in heatproof container,
Boiled with water proof mode of heating molten, make mixing oil temperature maintain 40 DEG C～50 DEG C.
Second step: weigh 20 kilograms of water, 8.8 kilograms of NaOH.First NaOH is put in glass container, then slowly
Slow addition water, side edged is quickly stirred with alkaline-resisting agitator, and NaOH is cooled to 40 DEG C～50 DEG C after being dissolved completely in water, obtain
Aqueous slkali.
3rd step: the aqueous slkali of second step is slowly poured in the glass container equipped with miscella of the first step, leans to one side
While be stirred continuously about 40 minutes with alkaline-resisting agitator making both saponifications, obtain final product soap base until both solution are thoroughly mixed,
Then adjust ph to 7.5～8.
4th step: add 2 kilograms of Rhzoma Atractylodis Lanceae volatile oils toward in the soap base of the 3rd step while stirring, then stir, obtain
Mixing soap lye.
5th step: dip in a small amount of olive oil brushing die inside with brush, mould poured into by the soap lye then mixing the 4th step
With plastic sheeting, mould is covered afterwards, 35 DEG C of incubators are placed 2～3 days, obtain perfumed soap.
6th step: ready-made for the 5th step perfumed soap is removed from the molds, is put in ventilation and allows it to spontaneously dry, about 5 weeks left
The right side, obtains perfumed soap finished product.
Embodiment 4: the preparation four of the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil
The first step: weigh 12 kilograms of palm oil, 23 kilograms of castor oil, 35 kilograms of olive oil, be sequentially placed in heatproof container,
Boiled with water proof mode of heating molten, make mixing oil temperature maintain 40 DEG C～50 DEG C.
Second step: weigh 25 kilograms of water, 9 kilograms of NaOH.First NaOH is put in glass container, then slowly
Add water, side edged is quickly stirred with alkaline-resisting agitator, and NaOH is cooled to 40 DEG C～50 DEG C after being dissolved completely in water, obtain alkali
Solution.
3rd step: the aqueous slkali of second step is slowly poured in the glass container equipped with miscella of the first step, leans to one side
While be stirred continuously about 40 minutes with alkaline-resisting agitator making both saponifications, obtain final product soap base until both solution are thoroughly mixed,
Then adjust ph to 7.5～8.
4th step: add 10 kilograms of Rhzoma Atractylodis Lanceae volatile oils toward in the soap base of the 3rd step while stirring, then stir, obtain
Mixing soap lye.
5th step: dip in a small amount of olive oil brushing die inside with brush, mould poured into by the soap lye then mixing the 4th step
With plastic sheeting, mould is covered afterwards, 35 DEG C of incubators are placed 2～3 days, obtain perfumed soap.
6th step: ready-made for the 5th step perfumed soap is removed from the molds, is put in ventilation and allows it to spontaneously dry, about 5 weeks left
The right side, obtains perfumed soap finished product.
Embodiment 5:
Carry out antibacterial experiment with the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil for the embodiment 3:
(1) preparation of antiseptic solution: the Antibacterial soaps made containing Rhzoma Atractylodis Lanceae volatile oil are configured to the solution of 1:10.
(2) experimental strain is: Escherichia coli, staphylococcus aureus, candida albicanses, pseudomonas aeruginosa, mouse wound
Cold salmonella, Trichophyton rubrum, acrothesium floccosum, Trichophyton mentagrophytes.Test strain after activity is inoculated in mh meat soup
In culture medium, at 37 DEG C, cultivate 24h, being diluted to concentration with mh culture medium is 1 × 105～1 × 108The bacteria suspension of cfu/ml.
(3) mic measures: adopts micro-dilution method, adds the solution that (1) prepares in first hole in 96 hole elisa Plates
100μl；The solution 100 μ l that in secondary series hole, addition (1) prepares and 100 μ l mh nutrient solutions mix；Add in 3rd row hole
Solution in 100 μ l secondary series holes and 100 μ l mh nutrient solutions mix；100 μ l the 3rd is added to arrange the solution in hole in 4th row hole
Mix with 100 μ lmh nutrient solutions；100 μ l the 4th is added to arrange the solution in hole and the mixing of 100 μ l mh nutrient solutions in 5th row hole,
Obtain a series of drug concentrations by that analogy.After medicament interpolation finishes, add the cultured bacteria suspension (medicine of 100 μ l in every hole
Final concentration of 50,25,12.5,6.25,3.13,1.56,0.78, the 0.39 μ l/ml of agent).
The ELISA Plate of above-mentioned process is placed in 37 DEG C of incubators culture 24h, in every hole, then adds 20 μ l with aseptic
The new 0.2mg/ml preparing is purple to iodonitrotetrazolium for water, covers ELISA Plate lid and continues to cultivate 1h, Ran Houguan in 37 DEG C of incubators
Examine each hole color change.Color is changed into pink, shows that cell has a metabolic activity, minimum there is not color change concentration be
For mic.The anti-bacterial result is shown in Table 1.
(4) mensure of mbc: the culture that bacterium does not grow hole (>=mic) successively dilutes 20 times with SPSS,
Draw 0.05ml dibbling respectively in agar plate, put 37 DEG C of standard incubator, 24h cultivates, no bacterial growth inoculation region institute is right
The minimum drug concentration answered is MBC (mbc).
Table 1 antimicrobial is to several minimum antimicrobial concentration for examination bacterium and MBC
Result shows, the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil are all had to a certain degree with fungi to the malignant bacteria participating in test
Antibacterial effect, especially for Escherichia coli, staphylococcus aureus, pseudomonas aeruginosa, Trichophyton rubrum, Epidermophvton
Tinea bacterium and Trichophyton mentagrophytes, have preferable antibacterial effect.
Embodiment 6
(1) acquisition of Atractylis lancea powder:
The rhizoma atractylodis root of fresh collection is cleaned up, after drying, pulverized 60 mesh sieves.
(2) extraction of Atractylis lancea volatile oil:
Accurately weigh 50g rhizoma atractylodis sample in three-neck flask, add 50ml distilled water immersion 30min, be then placed in xh-
The combination of 300ul computer microwave ultrasonic wave ultraviolet light catalyzes and synthesizes in instrument and extracts 60min with firm power 500w.
(3) acquisition of Atractylis lancea volatile oil:
Extraction collects volatile oil with glue head dropper after terminating, and then cleans the sample on glue head dropper with ether.Add grey
The anhydrous sodium sulfate of art example weight 1/5～1/4, is dried overnight in 4 DEG C of refrigerators and Rhzoma Atractylodis Lanceae volatile oil is obtained.
General principle and principal character and the advantages of the present invention of the present invention have been shown and described above.The technology of the industry
, it should be appreciated that the present invention is not restricted to the described embodiments, the simply explanation described in above-described embodiment and specification is originally for personnel
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes
Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and its
Equivalent thereof.
Claims (7)
1. a kind of Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil are it is characterised in that the antibacterial activity in described Antibacterial soaps and fragrance become
It is divided into Rhzoma Atractylodis Lanceae volatile oil.
2. a kind of Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil it is characterised in that according to mass parts include Rhzoma Atractylodis Lanceae volatile oil 0.05-5 part,
Palm oil 10-12 part, castor oil 20-23 part, olive oil 20-35 part, NaOH 8.5-9 part and water 20-25 part.
3. a kind of Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil according to claim 2 are it is characterised in that according to mass parts by grey
Art volatile oil 0.05-5 part, palm oil 10-12 part, castor oil 20-23 part, olive oil 20-35 part, NaOH 8.5-9 part and
Water 20-25 part forms.
4. a kind of preparation method as the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil is it is characterised in that its step includes: adds in soap base
Enter Rhzoma Atractylodis Lanceae volatile oil, then stir, obtain mixing soap lye；Dip in a small amount of olive oil brushing die inside with brush, then will
Mould is covered after pouring mould into by the soap lye mixing with plastic sheeting, and 35 DEG C of incubators are placed 2～3 days, obtain perfumed soap.
5. a kind of preparation method as the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil according to claim 4 is it is characterised in that institute
The preparation method stating soap base includes: palm oil, castor oil, olive oil is put in heatproof container by weight to scale, heating makes
The temperature of oil maintains 40 DEG C～50 DEG C；By the amount of required water and NaOH, water is poured slowly into the glass filling NaOH
In glass container, side edged is quickly stirred with alkaline-resisting agitator, and NaOH is cooled to 40 DEG C～50 DEG C after being dissolved completely in water, obtain
Aqueous slkali；The aqueous slkali preparing slowly is poured in the heatproof container that dress is mixed with palm oil, castor oil, olive oil, Bian Jia
While constantly being stirred with alkaline-resisting agitator, stir about makes both saponifications in 40 minutes, obtains final product until two kinds of solution are thoroughly mixed
Soap base, and adjust ph to 7.5～8.
6. the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil are in suppression tubercle bacillus, Escherichia coli, staphylococcus aureus, Candida albicans ball
In bacterium, pseudomonas aeruginosa, salmonella typhimurium, Trichophyton rubrum, acrothesium floccosum and/or Trichophyton mentagrophytes growth
Application.
7. application in treatment tinea manuum and tinea pedis for the Antibacterial soaps containing Rhzoma Atractylodis Lanceae volatile oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610603490.3A CN106336969A (en) | 2016-07-28 | 2016-07-28 | Atractylodes lancea volatile oil-containing antibacterial perfumed soap, and making method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610603490.3A CN106336969A (en) | 2016-07-28 | 2016-07-28 | Atractylodes lancea volatile oil-containing antibacterial perfumed soap, and making method and application thereof |
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| CN106336969A true CN106336969A (en) | 2017-01-18 |
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ID=57824664
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|---|---|---|---|
| CN201610603490.3A Pending CN106336969A (en) | 2016-07-28 | 2016-07-28 | Atractylodes lancea volatile oil-containing antibacterial perfumed soap, and making method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107012029A (en) * | 2017-03-24 | 2017-08-04 | 广东医科大学 | A kind of antimicrobial soap and preparation method thereof |
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|---|---|---|---|---|
| CN102397412A (en) * | 2011-11-19 | 2012-04-04 | 大连得达科技发展有限公司 | Foot bath liquid for treating tinea pedis |
| CN102415975A (en) * | 2011-12-12 | 2012-04-18 | 大连创达技术交易市场有限公司 | Chinese medicine deodorizing foot bath salt |
| CN104342323A (en) * | 2013-08-01 | 2015-02-11 | 徐州金牌药业有限公司 | Smell-removing bacteriostatic soap |
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2016
- 2016-07-28 CN CN201610603490.3A patent/CN106336969A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102397412A (en) * | 2011-11-19 | 2012-04-04 | 大连得达科技发展有限公司 | Foot bath liquid for treating tinea pedis |
| CN102415975A (en) * | 2011-12-12 | 2012-04-18 | 大连创达技术交易市场有限公司 | Chinese medicine deodorizing foot bath salt |
| CN104342323A (en) * | 2013-08-01 | 2015-02-11 | 徐州金牌药业有限公司 | Smell-removing bacteriostatic soap |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107012029A (en) * | 2017-03-24 | 2017-08-04 | 广东医科大学 | A kind of antimicrobial soap and preparation method thereof |
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Application publication date: 20170118 |