CN114149878B - Goat milk sand sagebrush mixture, preparation method and application thereof - Google Patents

Goat milk sand sagebrush mixture, preparation method and application thereof Download PDF

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CN114149878B
CN114149878B CN202111497927.7A CN202111497927A CN114149878B CN 114149878 B CN114149878 B CN 114149878B CN 202111497927 A CN202111497927 A CN 202111497927A CN 114149878 B CN114149878 B CN 114149878B
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sand sagebrush
goat milk
oil
mixture
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CN114149878A (en
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贾博然
郝志伟
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14—Shaping
    • C11D13/16—Shaping in moulds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Dermatology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a goat milk sand sagebrush mixture, a preparation method and application thereof, wherein the raw material proportion of the goat milk sand sagebrush mixture comprises the following raw materials in parts by weight: 40-45 parts of plant extract, 25-30 parts of hump oil, 10-20 parts of goat milk, 5-10 parts of sand sagebrush concentrated solution, 4-8 parts of oat protein and 4-8 parts of hyaluronic acid; the method for preparing the goat milk sand sagebrush mixture comprises the following steps: firstly preparing ointment, preparing sodium hydroxide according to the mass of the ointment, then adding goat milk and artemisia desertorum extract, and mixing with the ointment at the same temperature; the goat milk sand sagebrush mixture is used for preparing perfumed soap, soap powder and soap liquid; the goat milk sand sagebrush mixture prepared by the invention is suitable for various skin types, the skin is moist and elastic after face cleaning, the moisturizing effect is better, and the additive sand sagebrush has stronger antibacterial effect; the preparation method is simple and is suitable for industrial production.

Description

Goat milk sand sagebrush mixture, preparation method and application thereof
Technical Field
The invention relates to the field of cosmetics, in particular to a goat milk sand sagebrush mixture, a preparation method and application thereof.
Background
The soap is used as a skin cleaner to remove dirt adhering to the skin surface and keep the skin clean. Keep the skin healthy and beautiful, and can make the physiological function of the skin full of vitality. The soap is used for washing hands, faces, bathing, etc. unlike the washing soap, it is generally aimed at the skin of human body. With the improvement of living standard of people, the skin-cleaning agent is required to have a skin-cleaning function, and also has new functions of sterilization, beauty treatment, moisture preservation and the like.
The Artemisia sphaerocephala, also known as Artemisia sphaerocephala, is a plant of Compositae. The root system of the Artemisia sphaerocephala is thick and long, the stem is woody, the branches are many and long, and the Artemisia sphaerocephala is pressure-resistant and buried; the fruit wall contains colloid matters, and the fruit wall can absorb moisture and expand to lock soil and promote seed germination, so that the fruit wall is one of good sand-fixing plants. The plant growth regulator is distributed on movable and semi-movable sand dunes or fixed sand dunes in desert and semi-desert areas with the altitude of 1500 meters or below, and also grows on dry grasslands and arid sloping fields. The sand sagebrush seeds, namely the sand sagebrush seeds contain a large amount of colloid, and can be widely used as thickening agents, gelling agents, stabilizing agents and the like in the fields of food, textile, papermaking, medicine, petroleum, coal mines and the like.
The Chinese patent with publication number of CN108619026A discloses moisturizing facial cleanser containing sand sagebrush seed extract and a preparation method thereof, wherein the moisturizing facial cleanser comprises sand sagebrush extract, folium sennae, fructus cannabis, chinese toon head, trichosanthes bark and sodium alginate according to a certain proportion.
The prior art can supplement water and preserve moisture when the artemisia desertorum extract is applied to the facial cleanser, but still has some disadvantages: 1. at present, the demand of people on perfumed soap is far greater than the demand of facial cleanser; 2. the facial cleanser has no antibacterial effect and low cleaning strength.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide goat milk sand sagebrush soap for solving the problems in the background art.
In order to achieve the above purpose, the present invention provides the following technical solutions:
the invention provides a goat milk sand sagebrush mixture, which comprises the following raw materials in parts by weight: 40-45 parts of plant extract, 25-30 parts of hump oil, 10-20 parts of goat milk, 5-10 parts of sand sagebrush concentrated solution, 4-8 parts of oat protein and 4-8 parts of hyaluronic acid.
The plant extract comprises 50-60 parts of sunflower cold-pressed oil, 12-16 parts of coconut oil, 8-12 parts of castor oil, 10-15 parts of shea butter and 10-15 parts of cold-pressed sweet almond oil.
As a further preferable scheme of the invention, the goat milk sand sagebrush mixture comprises the following raw materials in parts by weight: 40 parts of plant extract, 25 parts of hump oil, 10 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid, wherein the plant extract comprises 50 parts of sunflower cold-pressed oil, 16 parts of coconut oil, 8 parts of castor oil, 15 parts of shea butter and 10 parts of cold-pressed sweet almond oil.
As a further preferable scheme of the invention, the goat milk sand sagebrush mixture comprises the following raw materials in parts by weight: 40 parts of plant extract, 30 parts of hump oil, 20 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid, wherein the plant extract comprises 50 parts of sunflower cold-pressed oil, 12 parts of coconut oil, 8 parts of castor oil, 10 parts of shea butter and 10 parts of cold-pressed sweet almond oil.
As a further preferable scheme of the invention, the goat milk sand sagebrush mixture comprises the following raw materials in parts by weight: 40 parts of plant extract, 25 parts of hump oil, 10 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid, wherein the plant extract comprises 60 parts of sunflower cold-pressed oil, 16 parts of coconut oil, 12 parts of castor oil, 15 parts of shea butter and 15 parts of cold-pressed sweet almond oil.
As a further scheme of the invention, the preparation method of the artemisia annua concentrated solution comprises the following steps: shearing Sha Haoshe stems with scissors, stirring in a stirrer to obtain sand sagebrush tissue powder particles with particle diameter of about 1-1.5mm, adding 60% ethanol solution with weight 10 times that of sand sagebrush tissue powder particles, ultrasonic treating for 1 hr, oscillating for 30 min, pouring ethanol solution, repeating the above extraction process for three times, mixing extractive solutions, and concentrating to solid state by distillation under reduced pressure at 38deg.C.
A preparation method of goat milk sand sagebrush mixture comprises the following steps:
(1) Cutting the whole hump into strips, mincing with a meat mincer, and heating and decocting to obtain oil paste; pouring the plant extract and hump ointment into a stainless steel pot, heating and stirring;
(2) Weighing the mass of sodium hydroxide according to the following formula:
sodium hydroxide mass (g) =ointment mass (g) × 0.1362 (0.1362 is saponification value);
(3) After the sodium hydroxide is weighed, pouring goat milk and artemisia sauce into a container for containing the sodium hydroxide, and stirring, wherein the adding weight of the goat milk is 1.5 times of that of the sodium hydroxide, and the adding weight of the artemisia sauce concentrated solution is the same as that of the sodium hydroxide;
(4) And (3) placing sodium hydroxide and oil at the same temperature, mixing at 40-50 ℃, continuously stirring to a yogurt state, pouring the mixture into a mold, standing for 3-5 days, demolding, and drying in the shade for about 60 days in a natural environment to obtain the solid perfumed soap.
According to the proportion of the raw materials, soap powder, soap and soap liquid are prepared according to the conventional technical means.
Compared with the prior art, the invention has the beneficial effects that:
according to the goat milk sand sagebrush mixture, the goat milk and the oat protein are added, so that redundant grease of skin can be absorbed, melanin generation is reduced, spots are lightened, the skin is whitened, and pores are refined. More importantly, the sand sagebrush concentrated solution is added on the basis, so that the skin is improved, meanwhile, the regeneration of germs can be further inhibited, and the sand sagebrush concentrated solution is especially suitable for dry, sensitive and itchy skin.
Detailed Description
The technical solution of the present patent will be described in further detail with reference to the specific embodiments, and it should be noted that the following specific embodiments are described in detail as to the preferred embodiments of the present patent, but the present patent is not limited to the above embodiments, and various changes may be made within the knowledge of those skilled in the art without departing from the technical scope of the present patent, and the following components are calculated according to parts by weight unless specifically noted.
The invention provides a goat milk sand sagebrush mixture, which comprises the following raw materials in parts by weight: 40-45 parts of plant extract, 25-30 parts of hump oil, 10-20 parts of goat milk, 5-10 parts of sand sagebrush concentrated solution, 4-8 parts of oat protein and 4-8 parts of hyaluronic acid.
The plant extract comprises 50-60 parts of sunflower cold-pressed oil, 12-16 parts of coconut oil, 8-12 parts of castor oil, 10-15 parts of shea butter and 10-15 parts of cold-pressed sweet almond oil.
As a further preferable scheme of the invention, the goat milk sand sagebrush mixture comprises the following raw materials in parts by weight: 40 parts of plant extract, 25 parts of hump oil, 10 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid, wherein the plant extract comprises 50 parts of sunflower cold-pressed oil, 16 parts of coconut oil, 8 parts of castor oil, 15 parts of shea butter and 10 parts of cold-pressed sweet almond oil.
As a further preferable scheme of the invention, the goat milk sand sagebrush mixture comprises the following raw materials in parts by weight: 40 parts of plant extract, 30 parts of hump oil, 20 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid, wherein the plant extract comprises 50 parts of sunflower cold-pressed oil, 12 parts of coconut oil, 8 parts of castor oil, 10 parts of shea butter and 10 parts of cold-pressed sweet almond oil.
As a further preferable scheme of the invention, the goat milk sand sagebrush mixture comprises the following raw materials in parts by weight: 40 parts of plant extract, 25 parts of hump oil, 10 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid, wherein the plant extract comprises 60 parts of sunflower cold-pressed oil, 16 parts of coconut oil, 12 parts of castor oil, 15 parts of shea butter and 15 parts of cold-pressed sweet almond oil.
As a further scheme of the invention, the preparation method of the artemisia annua concentrated solution comprises the following steps: shearing Sha Haoshe stems with scissors, stirring in a stirrer to obtain sand sagebrush tissue powder particles with particle diameter of about 1-1.5mm, adding 60% ethanol solution with weight 10 times that of sand sagebrush tissue powder particles, ultrasonic treating for 1 hr, oscillating for 30 min, pouring ethanol solution, repeating the above extraction process for three times, mixing extractive solutions, and concentrating to solid state by distillation under reduced pressure at 38deg.C.
A preparation method of goat milk sand sagebrush mixture comprises the following steps:
(1) Cutting the whole hump into strips, mincing with a meat mincer, and heating and decocting to obtain oil paste; pouring the plant extract and hump ointment into a stainless steel pot, heating and stirring;
(2) Weighing the mass of sodium hydroxide according to the following formula:
sodium hydroxide mass (g) =ointment mass (g) × 0.1362 (0.1362 is saponification value);
(3) After the sodium hydroxide is weighed, pouring goat milk and artemisia sauce into a container for containing the sodium hydroxide, and stirring, wherein the adding weight of the goat milk is 1.5 times of that of the sodium hydroxide, and the adding weight of the artemisia sauce concentrated solution is the same as that of the sodium hydroxide;
(4) And (3) placing sodium hydroxide and oil at the same temperature, mixing at 40-50 ℃, continuously stirring to a yogurt state, pouring the mixture into a mold, standing for 3-5 days, demolding, and drying in the shade for about 60 days in a natural environment to obtain the solid perfumed soap.
According to the proportion of the raw materials, soap powder, soap and soap liquid are prepared according to the conventional technical means.
Example 1:
the goat milk sand sagebrush mixture comprises the following raw materials in parts by weight: 40 parts of plant extract, 25 parts of hump oil, 10 parts of goat milk, 5 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid, wherein the plant extract comprises 50 parts of sunflower cold-pressed oil, 16 parts of coconut oil, 8 parts of castor oil, 15 parts of shea butter and 10 parts of cold-pressed sweet almond oil.
The preparation method of the sand sagebrush concentrated solution comprises the following steps: crushing Sha Haoshe stems with scissors, placing into a stirrer, stirring to obtain particle size of about 1-1.5mm, drying to obtain sand sagebrush tissue powder particles, adding 60% ethanol solution with weight 10 times that of sand sagebrush tissue powder particles, performing ultrasonic treatment for 1 hr, oscillating for 30 min, pouring ethanol solution, repeating the above extraction process for three times, mixing extractive solutions, and concentrating to solid state by distillation under reduced pressure at 38deg.C.
The preparation method of the goat milk sand sagebrush mixture comprises the following steps:
(1) Cutting the whole hump into strips, mincing with a meat mincer, and heating and decocting to obtain oil paste; pouring the plant extract and hump ointment into a stainless steel pot, heating and stirring.
(2) Weighing the mass of sodium hydroxide according to the following formula:
sodium hydroxide mass (g) =ointment mass (g) × 0.1362 (0.1362 is saponification value)
(3) After the sodium hydroxide is weighed, the goat milk and the artemisia juice are poured into a container for containing the sodium hydroxide and stirred.
(4) And (3) placing sodium hydroxide and oil at the same temperature, mixing at 40-50 ℃, continuously stirring to be in a yogurt state, pouring the mixture into a mold, standing for 3-5 days, demolding, and drying in the shade for about 60 days in a natural environment to obtain the goat milk artemisia sphaerocephala soap A.
Example 2:
the goat milk sand sagebrush mixture comprises the following raw materials in parts by weight: 40 parts of plant extract, 25 parts of hump oil, 20 parts of goat milk, 5 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid, wherein the plant extract comprises 50 parts of sunflower cold-pressed oil, 16 parts of coconut oil, 8 parts of castor oil, 15 parts of shea butter and 10 parts of cold-pressed sweet almond oil.
The preparation method of the sand sagebrush concentrated solution comprises the following steps: crushing Sha Haoshe stems with scissors, placing into a stirrer, stirring to obtain particle size of about 1-1.5mm, drying to obtain sand sagebrush tissue powder particles, adding 60% ethanol solution with weight 10 times that of sand sagebrush tissue powder particles, performing ultrasonic treatment for 1 hr, oscillating for 30 min, pouring ethanol solution, repeating the above extraction process for three times, mixing extractive solutions, and concentrating to solid state by distillation under reduced pressure at 38deg.C.
The preparation method of the goat milk sand sagebrush mixture comprises the following steps:
(1) Cutting the whole hump into strips, mincing with a meat mincer, and heating and decocting to obtain oil paste; pouring the plant extract and hump ointment into a stainless steel pot, heating and stirring.
(2) Weighing the mass of sodium hydroxide according to the following formula:
sodium hydroxide mass (g) =ointment mass (g) × 0.1362 (0.1362 is saponification value)
(3) After the sodium hydroxide is weighed, the goat milk and the artemisia juice are poured into a container for containing the sodium hydroxide and stirred.
(4) And (3) placing sodium hydroxide and oil at the same temperature, mixing at 40-50 ℃, continuously stirring to be in a yogurt state, pouring the mixture into a mold, standing for 3-5 days, demolding, and drying in the shade for about 60 days in a natural environment to obtain the goat milk artemisia sphaerocephala soap B.
Example 3:
the goat milk sand sagebrush soap comprises the following raw materials in parts by weight: 40 parts of plant extract, 25 parts of hump oil, 10 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid, wherein the plant extract comprises 50 parts of sunflower cold-pressed oil, 16 parts of coconut oil, 8 parts of castor oil, 15 parts of shea butter and 10 parts of cold-pressed sweet almond oil.
The preparation method of the sand sagebrush concentrated solution comprises the following steps: crushing Sha Haoshe stems with scissors, placing into a stirrer, stirring to obtain particle size of about 1-1.5mm, drying to obtain sand sagebrush tissue powder particles, adding 60% ethanol solution with weight 10 times that of sand sagebrush tissue powder particles, performing ultrasonic treatment for 1 hr, oscillating for 30 min, pouring ethanol solution, repeating the above extraction process for three times, mixing extractive solutions, and concentrating to solid state by distillation under reduced pressure at 38deg.C.
The preparation method of the goat milk sand sagebrush mixture comprises the following steps:
(1) Cutting the whole hump into strips, mincing with a meat mincer, and heating and decocting to obtain oil paste; pouring the plant extract and hump ointment into a stainless steel pot, heating and stirring.
(2) Weighing the mass of sodium hydroxide according to the following formula:
sodium hydroxide mass (g) =ointment mass (g) × 0.1362 (0.1362 is saponification value)
(3) After the sodium hydroxide is weighed, the goat milk and the artemisia juice are poured into a container for containing the sodium hydroxide and stirred.
(4) And (3) placing sodium hydroxide and oil at the same temperature, mixing at 40-50 ℃, continuously stirring to be in a yogurt state, pouring the mixture into a mold, standing for 3-5 days, demolding, and drying in the shade for about 60 days in a natural environment to obtain the goat milk artemisia sphaerocephala soap C.
Example 4:
the goat milk sand sagebrush soap comprises the following raw materials in parts by weight: 40 parts of plant extract, 25 parts of hump oil, 20 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 8 parts of hyaluronic acid, wherein the plant extract comprises 60 parts of sunflower cold-pressed oil, 16 parts of coconut oil, 8 parts of castor oil, 15 parts of shea butter and 10 parts of cold-pressed sweet almond oil.
The preparation method of the sand sagebrush concentrated solution comprises the following steps: crushing Sha Haoshe stems with scissors, placing into a stirrer, stirring to obtain particle size of about 1-1.5mm, drying to obtain sand sagebrush tissue powder particles, adding 60% ethanol solution with weight 10 times that of sand sagebrush tissue powder particles, performing ultrasonic treatment for 1 hr, oscillating for 30 min, pouring ethanol solution, repeating the above extraction process for three times, mixing extractive solutions, and concentrating to solid state by distillation under reduced pressure at 38deg.C.
The preparation method of the goat milk sand sagebrush mixture comprises the following steps:
(1) Cutting the whole hump into strips, mincing with a meat mincer, and heating and decocting to obtain oil paste; pouring the plant extract and hump ointment into a stainless steel pot, heating and stirring.
(2) Weighing the mass of sodium hydroxide according to the following formula:
sodium hydroxide mass (g) =ointment mass (g) × 0.1362 (0.1362 is saponification value)
(3) After the sodium hydroxide is weighed, the goat milk and the artemisia juice are poured into a container for containing the sodium hydroxide and stirred.
(4) And (3) placing sodium hydroxide and oil at the same temperature, mixing at 40-50 ℃, continuously stirring to be in a yogurt state, pouring the mixture into a mold, standing for 3-5 days, demolding, and drying in the shade for about 60 days in a natural environment to obtain the goat milk artemisia sphaerocephala soap D.
Example 5:
the goat milk sand sagebrush soap comprises the following raw materials in parts by weight: 40 parts of plant extract, 30 parts of hump oil, 20 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 8 parts of hyaluronic acid, wherein the plant extract comprises 60 parts of sunflower cold-pressed oil, 16 parts of coconut oil, 12 parts of castor oil, 15 parts of shea butter and 15 parts of cold-pressed sweet almond oil.
The preparation method of the sand sagebrush concentrated solution comprises the following steps: crushing Sha Haoshe stems with scissors, placing into a stirrer, stirring to obtain particle size of about 1-1.5mm, drying to obtain sand sagebrush tissue powder particles, adding 60% ethanol solution with weight 10 times that of sand sagebrush tissue powder particles, performing ultrasonic treatment for 1 hr, oscillating for 30 min, pouring ethanol solution, repeating the above extraction process for three times, mixing extractive solutions, and concentrating to solid state by distillation under reduced pressure at 38deg.C.
The preparation method of the goat milk sand sagebrush mixture comprises the following steps:
(1) Cutting the whole hump into strips, mincing with a meat mincer, and heating and decocting to obtain oil paste; pouring the plant extract and hump ointment into a stainless steel pot, heating and stirring.
(2) Weighing the mass of sodium hydroxide according to the following formula:
sodium hydroxide mass (g) =ointment mass (g) × 0.1362 (0.1362 is saponification value)
(3) After the sodium hydroxide is weighed, the goat milk and the artemisia juice are poured into a container for containing the sodium hydroxide and stirred.
(4) And (3) placing sodium hydroxide and oil at the same temperature, mixing at 40-50 ℃, continuously stirring to be in a yogurt state, pouring the mixture into a mold, standing for 3-5 days, demolding, and drying in the shade for about 60 days in a natural environment to obtain the goat milk artemisia sphaerocephala soap E.
Comparative example 1:
the Artemisia annua concentrate in example 1 is replaced by vegetable glycerin on the market, and other component contents and preparation methods are the same as in example 1.
Comparative example 2:
the Artemisia annua concentrate in example 4 is replaced by vegetable glycerin on the market, and other component contents and preparation methods are the same as in example 4.
Bacteriostasis test:
the antibacterial effect of the soaps obtained in the above examples and comparative examples was measured using the dilution-coating flat-plate method. The operation method comprises the following steps: square pigskin with side length of 5cm is prepared, and gamma rays are used for irradiation sterilization of the pigskin.
Preparing beef extract peptone liquid culture medium, sterilizing with high pressure steam, inoculating Escherichia coli bacterial liquid into beef extract peptone liquid culture medium for enrichment culture, collecting enrichment liquid, and sequentially performing 10 times 5 After dilution, the samples were spread onto sterilized pigskin, incubated at 30℃for 12 hours with aeration, the samples were repeated three times and a blank control of E.coli was set.
After uniformly wiping the surface of the pig skin inoculated with escherichia coli using the goat artemisia soap prepared in examples 1 to 5 and comparative examples 1 to 2 for 20 seconds, washing soap foam on the pig skin with sterile water, then air-drying, controlling the washing time to 40 seconds, placing the pig skin on a sterilized beef extract peptone solid medium in an ultra clean bench, removing the pig skin after 10 minutes, pouring the flat plate into a 30 ℃ constant temperature incubator for cultivation, setting a blank control for washing the pig skin with only sterile water, observing the colony count of escherichia coli in four time periods of 0, 6, 12 and 24 hours, and calculating the bacteriostasis rate for 24 hours, wherein the specific detection results are shown in the following table 1 (data are average values of three repetitions), and the calculation formula of the bacteriostasis rate is as follows:
antibacterial ratio= (number of control colonies-number of treated colonies)/number of control colonies
Through detection, the average colony number of the pig skin coated with the escherichia coli after ventilation culture for 12 hours at 30 ℃ is 72, and the escherichia coli is not detected on the blank pig skin without the escherichia coli, namely the successful infection of the escherichia coli and the growth on the pig skin are proved.
TABLE 1
Goat milk Sha Haozao 0(h) 6(h) 12(h) 24(h) Bacteriostasis rate (%)
Example 1 0 3 9 21 74.07
Example 2 0 3 8 20 75.30
Example 3 0 0 2 9 88.89
Example 4 0 0 3 12 85.19
Example 5 0 0 1 11 86.42
Comparative example 1 0 11 20 49 39.51
Comparative example 2 0 9 17 52 35.80
Blank control 0 21 37 81 —
The inhibition rate of the embodiment is 74.07-88.89% in 24 hours, and the inhibition rate of the comparative example is 35.80-39.51% in 24 hours, and the inhibition rate of the embodiment is more than about 1 time of that of the comparative example in 24 hours, which shows that the inhibition effect of the soap on escherichia coli can be obviously improved by adding the sand sagebrush concentrate in the formula of the goat milk sand sagebrush soap; the antibacterial rate of the goat milk sand sagebrush soap of examples 1-2 for 24 hours is 74.07-75.30%, and the antibacterial rate of the goat milk sand sagebrush soap of examples 3-5 for 24 hours is 85.19-88.89%, which shows that the higher the fraction of the added sand sagebrush concentrate, the better the antibacterial effect, and indirectly proves that the sand sagebrush has a certain antibacterial effect on escherichia coli. Examples 4 and 5 changed the parts of plant extract and hump oil, but the antibacterial rate did not change significantly, indicating that the content of ointment did not affect the antibacterial effect of the soap.
Hardness test:
further, the hardness test is carried out on GOAT milk sand sagebrush soap C prepared according to the component of the embodiment 3 and the soap with the highest sales in the market, wherein the selected commercial soap is GOAT milk soap (model GOAT 952373), the hardness of the soap is tested by a texture analyzer (model Bohler femto CT 3), and the traditional puncturing method is adopted in the experimental method.
In view of the fact that soap softens or falls off when water is used for a period of time in daily life, the test method cuts the whole rectangular soap along the broadside direction at the center position, hardness of the three positions of the cross section is measured by a texture analyzer, the hardness is measured three times by each sample, the hardness is measured repeatedly, and the hardness measurement data are averaged, wherein the hardness is shown in the following table 2.
TABLE 2
Soap type Center hardness/g Intermediate hardness/g Edge hardness/g
Goat milk sand sagebrush soap C 2210.394 2425.872 2601.421
GOAT milk soap (GOAT 952373) 1968.254 2106.754 2338.471
From the hardness measurement data in the table, the hardness of the center, the middle and the edge of the GOAT milk sand sagebrush soap prepared by the preparation method is higher than that of all parts of the GOAT milk soap (GOAT 952373) sold in the market, and the commercial GOAT milk soap is taken as the commodity soap with the largest sales, and has no phenomenon of softening or deslagging when in use, so that the GOAT milk sand sagebrush soap prepared by the preparation method can not have the problems from the results of hardness test.
The specific embodiments are illustrative only and not intended to be limiting, as modifications would be required to the embodiments after reading the present specification without inventive contribution, but would be protected by the patent laws within the scope of the claims of the present application.

Claims (7)

1. The goat milk sand sagebrush mixture for preparing perfumed soap, soap powder, soap and soap liquid is characterized by comprising the following raw materials in parts by weight: 40-45 parts of plant extract, 25-30 parts of hump oil, 10-20 parts of goat milk, 5-10 parts of sand sagebrush concentrated solution, 4-8 parts of oat protein and 4-8 parts of hyaluronic acid;
the plant extract comprises 50-60 parts of sunflower cold-pressed oil, 12-16 parts of coconut oil, 8-12 parts of castor oil, 10-15 parts of shea butter and 10-15 parts of cold-pressed sweet almond oil.
2. The goat milk sand sagebrush mixture according to claim 1 is characterized by comprising the following raw materials in parts by weight: 40 parts of plant extract, 25 parts of hump oil, 10 parts of goat milk, 10 parts of sand sagebrush concentrated solution, 8 parts of oat protein and 4 parts of hyaluronic acid.
3. A goat milk sand sagebrush mixture according to claim 2 wherein the plant extract comprises 50 parts sunflower cold pressed oil, 16 parts coconut oil, 8 parts castor oil, 15 parts shea butter, 10 parts cold pressed sweet almond oil.
4. The preparation method of the goat milk sand sagebrush mixture is characterized by comprising the following steps of:
s101, cutting the whole hump into strips, mincing with a meat mincer, and heating and decocting to obtain an oil paste; pouring the plant extract and hump ointment into a stainless steel pot, heating and stirring;
s102, weighing the mass of sodium hydroxide according to the mass of the ointment;
s103, after weighing sodium hydroxide, pouring goat milk and sand sagebrush concentrated solution into a container for containing sodium hydroxide and stirring;
s104, placing sodium hydroxide and the stirred oil at the same temperature, mixing at 40-50 ℃, continuing stirring to be in a yogurt state, pouring the mixture into a mould, standing for 3-5 days, demolding, and drying in the shade for about 60 days in a natural environment.
5. The method for preparing a goat milk sand sagebrush mixture according to claim 4, wherein the weight ratio of sodium hydroxide to ointment is 0.1362:1.
6. The method for preparing the goat milk sand sagebrush mixture according to claim 4, wherein the method for preparing the sand sagebrush concentrate comprises the following steps:
s201, shearing Sha Haoshe and stems by scissors, stirring, and drying to obtain sand sagebrush tissue powder particles;
s202, soaking sand sagebrush tissue particles in 60% ethanol solution, and vibrating after ultrasonic treatment;
s203, pouring out the extraction solution, repeating the extraction process for three times, combining the extraction solutions, and concentrating to be solid by reduced pressure distillation at 38 ℃.
7. The method for preparing a goat milk sand sagebrush mixture according to claim 6, wherein the weight ratio of the ethanol solution to sand sagebrush tissue powder particles is 10:1.
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CN114958502A (en) * 2022-06-15 2022-08-30 内蒙古沙漠苁蓉科技有限公司 Manual cold soap based on hump oil and preparation method thereof
CN116121006A (en) * 2023-02-16 2023-05-16 塔里木大学 Method for preparing antibacterial transparent soap by using camel hump as raw material

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CN107397702A (en) * 2017-07-26 2017-11-28 北京健旭康技术有限公司 Purposes of the desert plant in cosmetics are prepared
CN110960565A (en) * 2018-09-28 2020-04-07 肖斌 Artemisia annua root extract and preparation method and application thereof
CN111317809A (en) * 2020-04-02 2020-06-23 新疆医科大学 Camel peak compound ointment and preparation method and application thereof

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Publication number Priority date Publication date Assignee Title
CN107397702A (en) * 2017-07-26 2017-11-28 北京健旭康技术有限公司 Purposes of the desert plant in cosmetics are prepared
CN110960565A (en) * 2018-09-28 2020-04-07 肖斌 Artemisia annua root extract and preparation method and application thereof
CN111317809A (en) * 2020-04-02 2020-06-23 新疆医科大学 Camel peak compound ointment and preparation method and application thereof

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