CN106336735A - Covering type textile inkjet printing pigment ink - Google Patents

Covering type textile inkjet printing pigment ink Download PDF

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Publication number
CN106336735A
CN106336735A CN201610723008.XA CN201610723008A CN106336735A CN 106336735 A CN106336735 A CN 106336735A CN 201610723008 A CN201610723008 A CN 201610723008A CN 106336735 A CN106336735 A CN 106336735A
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weight portion
essential oil
oil
weight
traditional chinese
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魏本武
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/30—Inkjet printing inks
    • C09D11/38—Inkjet printing inks characterised by non-macromolecular additives other than solvents, pigments or dyes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/30—Inkjet printing inks
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/30—Inkjet printing inks
    • C09D11/32—Inkjet printing inks characterised by colouring agents
    • C09D11/322—Pigment inks
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/645—Aliphatic, araliphatic or cycloaliphatic compounds containing amino groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/651—Compounds without nitrogen
    • D06P1/65106—Oxygen-containing compounds
    • D06P1/65118—Compounds containing hydroxyl groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D06P1/67333—Salts or hydroxides
    • D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/30—Ink jet printing
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a covering type textile inkjet printing pigment ink, which has effects of long-term air negative ion releasing, air purification, human health benefiting, and a certain inhibition and killing effect on Staphylococcus, Escherichia coli, gram-positive bacteria and a variety of pathogenic bacteria and fungi, has characteristics of fragrant odor, refreshing and pressure relieving, can leave long-lasting aroma after the use, further has health effects of refreshing and fatigue eliminating, is suitable for all ages of people, and has the wide application prospect.

Description

A kind of covering type textile inkjet printing pigment ink
Technical field
The present invention relates to a kind of ink, particularly to a kind of covering type textile inkjet printing pigment ink.
Background technology
Ink can be used for routine office work or textile printing field, but traditional general ink do not have refresh oneself and generation bear from The health-care effects such as son, user using with producing taediumvitae, due to the single function of traditional ink, can not meet people when long Multi-demandses.
Content of the invention
In view of the shortcomings of the prior art, the present invention provides a kind of smell pure and fresh for the user of ink, has and refreshes oneself Effect and the ink of negative ion health effect, it not only can discharge negative aeroion, purify air for a long time, is good for beneficial to human body Health；Also to staphylococcus, Escherichia coli, gram-positive bacteria etc., multiple germs and fungi have certain suppression, killing action；With When fragrant odour, pure and fresh soothe the spirit, pressure of releiving, also can expelling mosquito, will not to human body produce harmful effect, have widely Application prospect.
The purpose of the present invention is achieved by the following technical solution:
A kind of covering type textile inkjet printing pigment ink it is characterised in that: by following component by weight: face Material mill base 23 weight portion, bis-phenol a19 weight portion, glycerine 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight Amount part, triethylamine 3.3 weight portion, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 Weight portion, surfactant blend 1.2 weight portion, sustained release agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portions, the average grain diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanite, fluorite, tourmaline, zinc Spinelle is dravite and elbaite 5:3 by weight by weight the mixture of 2.5:3:3.7:2, wherein tourmaline Mixture, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is made by the steps and forms,
S1, take rhamnus crenata sieb.et zucc 35 weight portion to clean, naturally dry, be subsequently placed in 90 DEG C of frying pans and fry to savory effusion, then Air washer 17 weight portion, is placed in constant temperature oven less than 60 DEG C and dries, water content≤6.5%；
S2, selfheal 12.5 weight portion is cleaned, puts in salt solution and soak 3.5 hours, the salt water yield by immersion spice quality 3.7 times, put into and steam in pot thoroughly, take out, dry, the concentration of salt solution is 27%；
S3, by honeycomb 12 weight portion, lavender 15.5 weight portion, anemone vitifolia 4.5 weight portion, Moschus 4.5 weight portion, peppermint 1 weight portion, rosemary 1 weight portion, marjoram 0.75 weight portion, ambergris 0.65 weight portion decontamination, with step s1 and s2 Made bulk drug puts into together in micronizer and is crushed to 60 mesh, and prepared bulk drug powder is standby；
S4, by step s3 be obtained bulk drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, adjust extraction Pressure power 27.65mpa, 45.10 DEG C of extraction temperature, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, are directly separating Kettle outlet triangular flask collects volatile oil a, standby；
S5, by elm bark 8.5 weight portion, agalloch eaglewood 2.5 weight portion, camphorwood 35-40 weight portion, the Radix Astragali 1 weight portion is cleaned and is dried, Together put into micronizer in be crushed to 70 mesh, then plus deionized water soak 6 hours, amount of water is by being soaked bulk drug matter 6.5 times of amount, dispersed with stirring is mixed well, prepared Traditional Chinese drug mixture, standby；
S6, the Traditional Chinese drug mixture that step s5 is obtained decoct 2 hours in 80 DEG C, collect distillate, and add ether to extract, distillation Then plus anhydrous sodium sulfate drying the volume ratio of liquid and ether is 2:1, takes upper oil phase, that is, volatile oil b is obtained, standby；
S7, step s4 and s6 made volatile oil a and volatile oil b mixing are mixed well prepared miscella, then sequentially add while stirring Needle juniper essential oil, Moschus essential oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene, are sufficiently stirred for 35 minutes, stand 30 minutes, It is sufficiently stirred for mixing well, filtering and impurity removing, obtains final product essential oil of traditional Chinese medicine, wherein, described miscella and needle juniper essential oil, Moschus essential oil, fish pelargonium The mass ratio of essential oil, eucalyptus quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, also include origanum oil 1.3 weight portion in the bulk drug powder of step s3 and spend in vain Dalmatian chrysanthemum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step s5 also includes borneol 0.6 weight portion and lotus leaf 0.4 Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step s7 also includes eucalyptus oil 0.3 weight portion.
Equipment involved in the present invention, raw material and method, are the usual equipment using of the industry, raw material and method, This repeats no more.
Wherein each essential oil component must be sufficiently mixed with surfactant, sustained release agent, to reach slow release effect, each essential oil and The addition of anion natural mineral powder must be appropriate, and not only antibiotic and sterilizing is moreover it is possible to stable mood, so to the not normal heart Reason state has the effect in front, can purify, pacify soul, can mitigate angry and beaten sensation, and making one can be with the flat gas of the heart With ground to life, because its energy centre of equilibrium nerve, helpful to alarmed and dejected state, also have significantly flat Quiet with releive function, insomniac is had goodish relax to put console with spirit, for pacify hot-tempered enter or moody temper have Goodish effect, can improve operating efficiency.
The present invention with reference to modern Chinese medicine pharmacological research, verifies from the drug screening of existing Chinese medicine and repeatedly, gives full play to respectively Group weight portion synergy, wherein each traditional Chinese medicinal components are described as follows.
Rhamnus crenata sieb.et zucc:: machaka or dungarunga, root skin or complete stool are used as medicine, mild-natured, bitter, dry, sterilized, desinsection.
Selfheal: there is clearing heat and detoxicating, cooling blood and hemostasis, to staphylococcus aureus, beta hemolytic streptococcus, Escherichia coli, typhoid bacillus, shigella dysenteriae, corynebacterium diphtheriae, bacillus anthracis, Pseudomonas aeruginosa, shigella dysenteriae, typhoid bacillus, cholera Vibrios, Escherichia coli, Pseudomonas aeruginosa and staphylococcus, streptococcus and Bacillus tuberculosis all have certain inhibitory action.
Honeycomb: pick up from the lair of honeybee, effect: wind-dispelling, attack poison, desinsection, pain relieving, antiallergy, HBS is resisted Original deactivation, also to staphylococcus aureus, Pseudomonas aeruginosa, Escherichia coli, shigella dysenteriae, typhoid bacillus and common variation Bacillus etc. has very strong restraint；Also there is inhibitory action to fungies such as aspergillus fumigatus, aspergillus flavus, eggplant sickle bacterium, leukonids.
Lavender not only can replace camphor ball moreover it is possible to stay except ant, except roach, except mite when being placed under wardrobe, pillow The fragrance of one people that oozes lower, research finds, lavender has obvious antibacterial action, and the linalool containing in lavender is lavender The main component of antibacterial, it can suppress 17 kinds of bacteriums (including gram-negative bacteria and gram-positive bacteria), the life of 10 kinds of fungies Long.
Anemone vitifolia: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature, Slightly poisonous." removing toxic substances, apocenosis myogenic, scattered stasis detumescence, have and kill maggot, wriggler, change long-pending, detumescence, the scattered stasis of blood, control stubborn dermatitis, the favus of the scalp, malaria Disease, infantile malnutrition, dysentery, carbuncle furuncle sore swells, scrofula, traumatic injury.
Moschus: have and have one's ideas straightened out, ward off dirty, dredging collateral, effect of the scattered stasis of blood；Control apoplexy, coma due to blocking of the respiratory system, frightened epilepsy, middle evil unhappiness, Xin Fubao Bitterly, the lump in the abdomen hypochondriac lump, traumatic injury, swollen ulcer drug." this warp ": master wards off bad odor, a kind of malaria, epilepsy convulsion, goes three worms.
Peppermint: for the dry aerial parts of labiate peppermint, dispelling wind and heat from the body, the sharp clearly head, profit pharynx promoting eruption, soothing the liver row Gas.
Rosemary: there is tranquilizing and allaying excitement, restoring consciouness effect, all have certain curative effect to indigestion and stomachache, there is calmness, profit Urine acts on, and can also be used for treating multiple diseases such as insomnia, palpitaition, headache, indigestion, external application can treat wound and arthritis. Also there is strong heart, promote metabolism, promote the effect such as blood circulation of peripheral vessel.
Marjoram: can improve that mood is depressed and addictive disease, especially to liberal-mindedness and vigorous endurance stress symptom effectively, can expansion of blood vessels, Hypotensive, mitigate and burden, help eliminate palpitaition, have excellent nerve to pacify and calm function.
Ambergris: be lasting spices the most lasting, any spices all can not compare favourably therewith in the world, have " dragon The perfume of saliva and life coexist " saying.Compendium of Material Medica carries: can invigorate blood circulation, beneficial marrow, supporing yang road, promoting blood circulation, resolving sputum are put down Breathe heavily；A lump in the abdomen causing distension and pain；Trusted subordinate's pain；Coma；Liao Yongyan: promoting diuresis for stranguria, dissipating bind, knot of cooling down, by labor worm.
Elm bark: the dry bark for Ulmaceae or root skin, sweet, flat, nontoxic；Li Shui, treating stranguria, detumescence, for urine Obstructed, stranguria with turbid discharge, oedema, ulcer carbuncle on the back, erysipelas, mange.
Agalloch eaglewood: " Compendium of Materia Medica " record wood has strong antibacterial efficacy, fragrance enters spleen, god's qi-regulating, tonifying five zang organs, cough-relieving clearly Resolving sputum, warm stomach temperature spleen, ventilation analgesic therapy, can be used as medicine, be first-class medicinal material superfine product.
Camphorwood: aiphyllium, bark yellowish-brown, there is irregular longitudinal crack, on the south main product the Changjiang river and southwestern various places.Winter Cut down trees and split broken or be sawn into bulk, dry or air-dry.Timber bulk is not of uniform size, surface rufous to burgundy, and cross section is visible Annual ring.Matter is again hard.There is strong camphor fragrance, taste is refrigerant, have pungent sense, warm in nature, taste is pungent；Sensible can ward off dirty, middle benefit gas to stop Bitterly, dampness removing desinsection.
The Radix Astragali: also known as continuous stilbene.Perennial herb, the medicinal history having more than 2000 year so far of the Radix Astragali, it has enhancing machine Body immunity function, liver protection, diuresis, anti-aging, resisting stress, step-down and wide antibacterial action.
Needle juniper essential oil: there is purify air, mosquito-proof insect bite, antibacterial, antirheumatic, antitetanic effect, it may have calm Refresh oneself, encourage mood, purify the state of mind and the function of release soul, people's body and mind can be allowed relaxed and comfortable, it may have the effect promoted the sexual maturity；Separately Outward, the function of its toxin expelling is very famous, and it can discharge the toxin of accumulation, purifies intestinal mucosa.
Moschus essential oil: there is light fragrance, have and releive, calm, releasing melancholy and anti-depression effect, increase romance Mood, natural fragrance bring warm impression by body and mind.
Geranium Essential: there is hemostasis, vasoconstriction, asthma, liver and expelling toxin, gall stone, kidney toxin expelling, kidney stone, diuresis, flesh Carnic acid pain, Oily, aging skin activates, bleb, ochrodermia, fat-reducing, promotes to scab, eczema, sunburn of burning, tinea, the moon Through having some setbacks, engorgement of breasts inflammation, mitigate melancholy uneasy, there is deodorant, antibacterial, the effect of sterilization.
Eucalyptus quintessence oil has functions that anti-infective, antiviral, sterilized, desinsection, deodorant, antiviral effect, to breathing Tract disease is most effective, can relax inflammation phenomenon, makes schneiderian membrane comfortable；There is calm effect to mood simultaneously, sanity can be made, Focus on.
P-Cymene: to bacillus anthracis, Alpha-hemolytic streptococcus, b- Streptococcus hemolyticus, corynebacterium diphtheriae, bacillus pseudodiphthericus, lung 10 kinds of Gram-positives such as diplococcoid, staphylococcus aureus, Staphylococcus citreus, white Portugal Portugal coccus, hay bacillus Aerophil all has antibacterial action, also has bacteriostasis for multiple pathomycetes.
Origanum oil: the herb of Labiatae origanum wild marjoram origznum vul-garel., also known as only careless, the wild chaste tree of dysentery The ground such as mustard accord with name, have heat-clearing, dampness elimination, driving away summer heat, induce sweat, sterilization that qi-regulating is extremely strong, bacteriostasis, the volatilization extracted from wild marjoram Oil, cause enteritis bacterium common to 31 kinds and shigella flexneri, are the pure Chinese medicine additives of most broad-spectrum antiseptic.
Chrysanthemum cinesariaefolium: the general designation of chrysanthemum artemisia (tanacetum) several plants, removing dampness and destroying parasites, kill crab louse, head louse, body Lice, flea, the effect except mosquito desinsection.
Borneol: pungent, bitter, cool.There is inducing resuscitation of having one's ideas straightened out, heat-clearing dissipates poison, removing nebula.Cure mainly high fever apoplexy coma due to blocking of the respiratory system shies epilepsy, middle wind phlegm Faint frightened epilepsy, summer-heat and damp blinds clear key, larynx numbness is deaf, aphtha tooth swells, sore carbuncle infantile malnutrition due to digestive disturbances or intestinalparasites hemorrhoid, red eye, swell pain, pterygium.
Lotus leaf: for the leaf of nymphaeaceae plant lotus, play the role of clearing heat and detoxicating, cool blood, hemostasis.Have clearing summer-heat and damp, rise send out clear The effects such as sun, cooling blood and hemostasis.
Eucalyptus oil: one of most common and widest essential oil of purposes, there is good health-care effect, help focal attention Power.Sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory diseases can effectively be alleviated.There is good resisting Bacterium and sterilization idiocratic, in some certain food, eucalyptus oil is also as fragrance component.Carry this essential oil in travelling, permissible Effectively resist mosquito bite and insect bite, treat skin measles.It is good culicifuge.Mixing with water can become a kind of and simple and effective disappear Toxic agent.
Beneficial effects of the present invention:
The present invention provides a kind of smell pure and fresh for user, has stimulating effect and the ink of negative ion health effect, it is not only Negative aeroion can be discharged for a long time, purify air, beneficial to health；Also thin to staphylococcus, Escherichia coli, Grain-positive Multiple germ such as bacterium and fungi have certain suppression, killing action；Fragrant odour simultaneously, pure and fresh soothe the spirit, pressure of releiving, also can drive Catch up with mosquito, harmful effect will not be produced it is adaptable to each age groups to human body, its appropriate add other function ingredients after still Original effect and quality can be kept.
1st, tourmaline is a kind of silicate mineral, and its chemical formula is na (mg, fe, mn, li, al) 3al6 (si6o18) (bo3) 3 (oh, f) 4, it contacts under electrostatic field with hydrone, just hydrone can be ionized into hydrogen ion (h+) and hydrogen-oxygen Radical ion (oh-), hydroxide ion and water molecules form basic hydroxide group anion (h2o oh-), as " air bear from Son ", current scientific research proves: anion can not only facilitate human body synthesis and vitamin storage, the life of strengthening and human activin Reason activity, has highly important impact to the vital movement of human body and other biological, is referred to as " air vitamin ".Anion Effectively adsorb indoor harmful substance, the such as construction and decoration harmful substance such as formaldehyde, toluene, not only itself do not increase pollution, Er Qieqing Purifying room air, is inherently eliminated construction and decoration syndrome, ensures that health is unaffected.
2nd, the traditional Chinese medicine ingredients containing in the present invention, not only thin to staphylococcus, tubercle bacillus, Pseudomonas aeruginosa, Grain-negative Multiple germ such as bacterium and gram-positive bacteria and fungi have certain suppression, killing action；Fragrant odour simultaneously, property is gentle, Pure and fresh soothe the spirit, help hormone secretion, the effect of anxiety of releiving, also there is certain mosquito-repelling effect simultaneously, more it is essential that The Long-Time Service present invention will not produce harmful effect it is adaptable to each age groups to human body, before having application widely Scape.
Specific embodiment
Embodiment.
A kind of covering type textile inkjet printing pigment ink it is characterised in that: by following component according to weight portion array Become: dispersible pigment color paste 23 weight portion, bis-phenol a19 weight portion, glycerine 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portions, triethylamine 3.3 weight portion, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter Powder 1.7 weight portion, surfactant blend 1.2 weight portion, sustained release agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, goes Ionized water 62 weight portion, the average grain diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanite, fluorite, electricity Gas stone, gahnite by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and elbaite by weight The ratio mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is made by the steps Form,
S1, take rhamnus crenata sieb.et zucc 35 weight portion to clean, naturally dry, be subsequently placed in 90 DEG C of frying pans and fry to savory effusion, then Air washer 17 weight portion, is placed in constant temperature oven less than 60 DEG C and dries, water content≤6.5%；
S2, selfheal 12.5 weight portion is cleaned, puts in salt solution and soak 3.5 hours, the salt water yield by immersion spice quality 3.7 times, put into and steam in pot thoroughly, take out, dry, the concentration of salt solution is 27%；
S3, by honeycomb 12 weight portion, lavender 15.5 weight portion, anemone vitifolia 4.5 weight portion, Moschus 4.5 weight portion, peppermint 1 weight portion, rosemary 1 weight portion, marjoram 0.75 weight portion, ambergris 0.65 weight portion decontamination, with step s1 and s2 Made bulk drug puts into together in micronizer and is crushed to 60 mesh, and prepared bulk drug powder is standby；
S4, by step s3 be obtained bulk drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, adjust extraction Pressure power 27.65mpa, 45.10 DEG C of extraction temperature, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, are directly separating Kettle outlet triangular flask collects volatile oil a, standby；
S5, by elm bark 8.5 weight portion, agalloch eaglewood 2.5 weight portion, camphorwood 35-40 weight portion, the Radix Astragali 1 weight portion is cleaned and is dried, Together put into micronizer in be crushed to 70 mesh, then plus deionized water soak 6 hours, amount of water is by being soaked bulk drug matter 6.5 times of amount, dispersed with stirring is mixed well, prepared Traditional Chinese drug mixture, standby；
S6, the Traditional Chinese drug mixture that step s5 is obtained decoct 2 hours in 80 DEG C, collect distillate, and add ether to extract, distillation Then plus anhydrous sodium sulfate drying the volume ratio of liquid and ether is 2:1, takes upper oil phase, that is, volatile oil b is obtained, standby；
S7, step s4 and s6 made volatile oil a and volatile oil b mixing are mixed well prepared miscella, then sequentially add while stirring Needle juniper essential oil, Moschus essential oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene, are sufficiently stirred for 35 minutes, stand 30 minutes, It is sufficiently stirred for mixing well, filtering and impurity removing, obtains final product essential oil of traditional Chinese medicine, wherein, described miscella and needle juniper essential oil, Moschus essential oil, fish pelargonium The mass ratio of essential oil, eucalyptus quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, also include origanum oil 1.3 weight portion in the bulk drug powder of step s3 and spend in vain Dalmatian chrysanthemum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step s5 also includes borneol 0.6 weight portion and lotus leaf 0.4 Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step s7 also includes eucalyptus oil 0.3 weight portion.
Test the ink in this above-described embodiment using air ion static method of testing, anion burst size is in 430-650 Individual/m3, and sustained release negative aeroion, it is more beneficial for long-term purify air, reach the basic demand of health of people.
Reference examples.
Colour carbon black 20g, phenol 11g, glycerine 4g, BTA 3g, triethanolamine 1g, triethylamine 3g, sodium acid carbonate 5g, polyoxyethylene groups ethers nonionic fluorocarbon surfactant 1.5g, sustained release agent 0.4g, marjoram essential oil 0.6g, wheat Bud essential oil 0.5g, Lavender 0.5g, RADIX PAEONIAE ALBA essential oil 0.4g, cypress essential oil 0. 4g, eucalyptus quintessence oil 0.4g, tarragon essence Oily 0. 4g, Peppermint essential oil 0.4g, deionized water 75g.
Test the ink in this above-mentioned reference examples using air ion static method of testing, anion burst size is in 0/m3, There is no the function of release negative aeroion.
(1) acute toxicity test is carried out to obtained essential oil of traditional Chinese medicine, result is as follows:
1. Mouse oral acute toxicity test: the ld50 of Mouse oral essential oil of traditional Chinese medicine is 383.55g/kg, 95% credible is limited to 294.68g/kg～499.31g/kg.And the toxicity criterion of air freshener is: Mouse oral anxious poison ld50 >=5g/ Kg, is judged to nontoxic.The ld50 of this essential oil of traditional Chinese medicine is higher than 76 times of nontoxic standard, therefore, it is determined that being nontoxic.
2. chmice acute toxicity on inhalation test: the lc50 that chmice acute sucks essential oil of traditional Chinese medicine is 24863.99g/m3,95% Credible be limited to 16837.34g/m3～33387.46g/m3.And the toxicity criterion of air freshener is: chmice acute Suck (2h) lc50 ＞ 10000mg/m3, the nontoxic level in true border.The lc50 of this essential oil of traditional Chinese medicine is higher than the 2486 of nontoxic standard Times, therefore, it is determined that being nontoxic.
Through inspection, its fragrance, color and luster, refraction index, relative density, arsenic content, heavy metal contain obtained essential oil of traditional Chinese medicine Amount, ph value all meet the requirement of national standard.
(2) check above-mentioned ink anion burst size result such as table 1:
(3) to the test improving the state of mind.
Main method is that ink uses volunteer to test, and recruits 60 people, respectively using the ink in above-mentioned 2 kinds of embodiments, By scl-90 questionnaire (i.e. " Self-reporting inventory-scl90 ", be in the world one of foremost Mental health test scale), By continuous 1 week using following the tracks of, to judge that the present invention acts in the actual efficacy of aspect of refreshing oneself, wherein 6 people are noninductive to be subject to；9 people Impression is general；2 people think that this product is invalid for stimulating effect；There are 43 people to feed back this product and there is effect of preferably refreshing oneself, can make People's notice is concentrated, and efficient is 71.67%.
(4) repelling effect test.
Repelling effect according to common ink of the prior art and ink in above-described embodiment carries out contrast test, test Data is shown in Table 2.
Conclusion: the ink in the embodiment of the present invention has certain repelling effect.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, common for art For technical staff, can also make other changes in different forms on the basis of the above description, here need not All of embodiment cannot be exhaustive, all any modifications within the spirit and principles in the present invention, made, equivalent replace Change, improve, be still included within protection scope of the present invention.

Claims (1)

1. a kind of covering type textile inkjet printing pigment ink it is characterised in that: by following component by weight: Dispersible pigment color paste 23 weight portion, bis-phenol a19 weight portion, glycerine 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 Weight portion, triethylamine 3.3 weight portion, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portions, surfactant blend 1.2 weight portion, sustained release agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, go from Sub- water 62 weight portion, the average grain diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanite, fluorite, electrically Stone, gahnite by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and elbaite by weight The mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine be made by the steps and Become,
S1, take rhamnus crenata sieb.et zucc 35 weight portion to clean, naturally dry, be subsequently placed in 90 DEG C of frying pans and fry to savory effusion, then Air washer 17 weight portion, is placed in constant temperature oven less than 60 DEG C and dries, water content≤6.5%；
S2, selfheal 12.5 weight portion is cleaned, puts in salt solution and soak 3.5 hours, the salt water yield by immersion spice quality 3.7 times, put into and steam in pot thoroughly, take out, dry, the concentration of salt solution is 27%；
S3, by honeycomb 12 weight portion, lavender 15.5 weight portion, anemone vitifolia 4.5 weight portion, Moschus 4.5 weight portion, peppermint 1 weight portion, rosemary 1 weight portion, marjoram 0.75 weight portion, ambergris 0.65 weight portion decontamination, with step s1 and s2 Made bulk drug puts into together in micronizer and is crushed to 60 mesh, and prepared bulk drug powder is standby；
S4, by step s3 be obtained bulk drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, adjust extraction Pressure power 27.65mpa, 45.10 DEG C of extraction temperature, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, are directly separating Kettle outlet triangular flask collects volatile oil a, standby；
S5, by elm bark 8.5 weight portion, agalloch eaglewood 2.5 weight portion, camphorwood 35-40 weight portion, the Radix Astragali 1 weight portion is cleaned and is dried, Together put into micronizer in be crushed to 70 mesh, then plus deionized water soak 6 hours, amount of water is by being soaked bulk drug matter 6.5 times of amount, dispersed with stirring is mixed well, prepared Traditional Chinese drug mixture, standby；
S6, the Traditional Chinese drug mixture that step s5 is obtained decoct 2 hours in 80 DEG C, collect distillate, and add ether to extract, distillation Then plus anhydrous sodium sulfate drying the volume ratio of liquid and ether is 2:1, takes upper oil phase, that is, volatile oil b is obtained, standby；
S7, step s4 and s6 made volatile oil a and volatile oil b mixing are mixed well prepared miscella, then sequentially add while stirring Needle juniper essential oil, Moschus essential oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene, are sufficiently stirred for 35 minutes, stand 30 minutes, It is sufficiently stirred for mixing well, filtering and impurity removing, obtains final product essential oil of traditional Chinese medicine, wherein, described miscella and needle juniper essential oil, Moschus essential oil, fish pelargonium The mass ratio of essential oil, eucalyptus quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
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