CN106336731A - Prepared Chinese ink - Google Patents
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- CN106336731A CN106336731A CN201610735647.8A CN201610735647A CN106336731A CN 106336731 A CN106336731 A CN 106336731A CN 201610735647 A CN201610735647 A CN 201610735647A CN 106336731 A CN106336731 A CN 106336731A
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- 230000028327 secretion Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 229910052604 silicate mineral Inorganic materials 0.000 description 1
- 201000009890 sinusitis Diseases 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 229940031000 streptococcus pneumoniae Drugs 0.000 description 1
- 238000013268 sustained release Methods 0.000 description 1
- 239000012730 sustained-release form Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 230000035900 sweating Effects 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 208000011580 syndromic disease Diseases 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- CEIZFXOZIQNICU-UHFFFAOYSA-N tenuazonic acid Chemical compound CCC(C)C1NC(=O)C(C(C)=O)=C1O CEIZFXOZIQNICU-UHFFFAOYSA-N 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
- 231100000167 toxic agent Toxicity 0.000 description 1
- 231100000397 ulcer Toxicity 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
- 230000003639 vasoconstrictive effect Effects 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Plant Substances (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The ink comprises 23 parts by weight of pigment paste, 19 parts by weight of bisphenol A, 4.5 parts by weight of glycerol, 2.3 parts by weight of anhydrous sodium sulfate, 2.7 parts by weight of triethanolamine, 3.3 parts by weight of triethylamine, 3.6 parts by weight of acetone and 0.25 part by weight of dithiocarbamic acid ester, and not only can release negative ions in air for a long time, purify the air and be beneficial to human health; also has certain inhibiting and killing effects on staphylococcus, escherichia coli, gram-positive bacteria and other various germs and fungi; meanwhile, the fragrance is fragrant, the fragrance is fresh and refreshing, and the long-lasting fragrance can be left after the use, so that the fragrance type perfume has a very wide application prospect.
Description
The application is the Application No. 2016107230412 that 2016 applyings date August is submitted on the 25th, invention entitled " one
The divisional application of the Chinese invention patent application of kind calligraphy prepared Chinese ink ".
Technical field
The present invention relates to a kind of prepared Chinese ink, particularly to a kind of new offset lithography prepared Chinese ink.
Background technology
Prepared Chinese ink can be used for routine office work or textile printing field, but traditional general prepared Chinese ink do not have refresh oneself and generation bear from
The health-care effects such as son, user using with producing taediumvitae, due to the single function of traditional prepared Chinese ink, can not meet people when long
Multi-demandses.
Content of the invention
In view of the shortcomings of the prior art, the present invention provides a kind of abnormal smells from the patient pure and fresh for the user of prepared Chinese ink, has and refreshes oneself
Effect and the prepared Chinese ink of negative ion health effect, it not only can discharge negative aeroion, purify air for a long time, is good for beneficial to human body
Health；Also to staphylococcuses, escherichia coli, gram-positive bacteria etc., multiple pathogenic bacterias and funguses have certain suppression, killing action；With
When fragrant odour, pure and fresh soothe the spirit, pressure of releiving, also can expelling mosquito, will not to human body produce harmful effect, have widely
Application prospect.
The purpose of the present invention is achieved by the following technical solution:
A kind of prepared Chinese ink it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight portion, bis-phenol a19 weight
Amount part, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine 3.3 weight portion, acetone
3.6 weight portions, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surfactant blend
1.2 weight portions, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, the pigment of described mill base
For high-carbon black pigment, the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanite, fluorite, electrically
Stone, gahnite by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and elbaite by weight
The mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine be made by the steps and
Become,
S1, take Cortex Meliae 35 weight portion clean, naturally dry, be subsequently placed in 90 DEG C of frying pans and fry to savory effusion, then spray
Drench deionized water 17 weight portion, be placed in constant temperature oven less than 60 DEG C and dry, water content≤6.5%；
S2, lavandula angustifolia 17.5 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality
3.7 times, put into and steam in pot thoroughly, take out, dry, the concentration of saline is 27%；
S3, by Herba Anemones Hupehensiss 4.5 weight portion, Moschus 4.5 weight portion, Fructus Chebulae 1 weight portion, Cortex Phellodendri 1 weight portion, Origanum majorana
0.75 weight portion decontamination, is put into together with step s1 and the made crude drug of s2 and is crushed to 60 mesh in super micron mill, is obtained former
Material medicated powder end, standby；
S4, by step s3 be obtained crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, adjust extraction
Pressure power 27.65mpa, 45.10 DEG C of extraction temperature, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, are directly separating
Kettle outlet triangular flask collects volatile oil a, standby；
S5, by jujube nucleus 13 weight portion, Semen Torreyae 15.5 weight portion, Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae
Then plus deionization 15.5 weight portions, Rhizoma Acori Graminei 4.5 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 70 mesh,
Water soaks 6 hours, amount of water by 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, prepared Traditional Chinese drug mixture, standby；
S6, the Traditional Chinese drug mixture that step s5 is obtained decoct 2 hours in 80 DEG C, collect distillate, and add ether to extract, distillation
Then plus anhydrous sodium sulfate drying the volume ratio of liquid and ether is 2:1, takes upper oil phase, that is, volatile oil b is obtained, standby；
S7, step s4 and s6 made volatile oil a and volatile oil b mixing are mixed well prepared miscella, then sequentially add while stirring
Fructus Citri Limoniae quintessence oil, cypress quintessence oil, Geranium Essential, Fructus Tritici aestivi quintessence oil and Peppermint essential oil, are sufficiently stirred for 35 minutes, stand 30 minutes,
It is sufficiently stirred for mixing well, filtering and impurity removing, obtains final product essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Citri Limoniae quintessence oil, cypress quintessence oil, Flos Pelargonii
The mass ratio of quintessence oil, Fructus Tritici aestivi quintessence oil and Peppermint essential oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, also include Herba Origani oil 1.3 weight portion in the crude drug powder of step s3 and spend in vain
Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step s5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4
Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step s7 also includes Eucalyptus oil 0.3 weight portion.
Equipment involved in the present invention, raw material and method, are the usual equipment using of the industry, raw material and method,
This repeats no more.
Wherein each essential oil component must be sufficiently mixed with surfactant, slow releasing agent, to reach slow release effect, each quintessence oil and
The addition of anion natural mineral powder must be appropriate, and not only antibiotic and sterilizing is moreover it is possible to stable emotion, so to the not normal heart
Reason state has the effect in front, can purify, pacify soul, can mitigate angry and beaten sensation, and making one can be with the flat gas of the heart
With ground to life, because its energy centre of equilibrium nerve, helpful to alarmed and dejected state, also have significantly flat
Quiet with releive function, insomniac is had goodish relax to put console with spirit, for pacify hot-tempered enter or moody temper have
Goodish effect, can improve work efficiency.
The present invention with reference to modern Chinese medicine pharmacological research, verifies from the drug screening of existing Chinese medicine and repeatedly, gives full play to respectively
Group weight portion synergism, wherein each Chinese medicinal components are described as follows.
Cortex Meliae: can ascarifuge and ancylostome, but poisonous, the used time will sternly follow the doctor's advice, and root bark powder adjusts vinegar can control scabies, uses Melia azedarach L.
Son is made ointment and can be controlled tinea capitis.In addition, fruit nucleolus oil is available for lubricating oil processed and soap etc..
Lavandula angustifolia not only can replace camphor ball moreover it is possible to stay except ant, except roach, acaricide when being placed under wardrobe, medicated pillow
The fragrance of one people that oozes lower, research finds, lavandula angustifolia has obvious antibacterial action, and the linalool containing in lavandula angustifolia is lavandula angustifolia
The main component of antibacterial, it can suppress 17 kinds of antibacterials (including gram-negative bacteria and gram-positive bacteria), the life of 10 kinds of funguses
Long.
Herba Anemones Hupehensiss: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature,
Slightly poisonous." removing toxic substances, evacuation of pus granulation promoting, scattered stasis detumescence, have and kill maggot, wriggler, change long-pending, detumescence, dissipating blood stasis, control stubborn dermatitis, tinea alba, malaria
Disease, infantile malnutrition, dysentery, carbuncle furuncle swells, scrofula, traumatic injury.
Moschus: have and have one's ideas straightened out, ward off dirty, dredging collateral, effect of dissipating blood stasis；Control apoplexy, syncope due to accumulation of phlegm, infantile convulsion, middle evil unhappiness, Xin Fubao
Bitterly, the abdominal mass hypochondriac lump, traumatic injury, swollen ulcer drug." this warp ": master wards off bad odor, pyrexial malaria, epilepsy convulsion, goes three worms.
Fructus Chebulae: have and astringe the lung；Astringing intestine to stop diarrhea；The therapeutic method to keep the adverse QI flowing downwards；Sore-throat relieving；Convergence, antidiarrheal；Resisting pathogenic microbes；The effect of spasmolytic, to various
Dysentery bacterium is effectively outer, and relatively strong to bacillus pyocyaneus, diphtheria corynebacterium effect, to staphylococcus aureuses, escherichia coli, pneumonia ball
Bacterium, Hemolytic streptococcuss, Bacillus proteuss, bacillus typhi murium also have effect.
Cortex Phellodendri: to staphylococcus aureuses, streptococcus pneumoniae, diphtheria corynebacterium, Streptococcus viridanss, dysentery bacterium (Song Nei Shi
Except), Hemolytic streptococcuss, meningococcuss, vibrio cholera, anthrax bacillus all effectively or have stronger inhibitory action；To withered
Careless bacillus, bordetella pertussis, clostridium tetani also have inhibitory action.
Origanum majorana: can improve that mood is depressed and addictive disease, especially to liberal-mindedness and vigorous endurance stress symptom effectively, can expansion of blood vessels,
Blood pressure lowering, mitigation and burden, help eliminate cardiopalmus, have excellent nerve to pacify and calm function.
Jujube nucleus: described in Compendium of Material Medica: Semen Ziziphi Spinosae is ripe, and insomnia due to insufficiency of the gallbladder-qi with treating, the disease of excessive thirst sweating due to debility；Raw using treats gallbladder-heat
Good dormancy, all sufficient cloudy few sun medicine of fainting.There are calmness, hypnosis, analgesia, anticonvulsant action.
Semen Torreyae " this warp ": pathogen in main abdomen, go three worms, Serpentiss sting.
Cortex ulmi pumilae: the dry bark for Ulmaceae or root bark, sweet, flat, nontoxic；Diuretic, treating stranguria, detumescence, for urine
Obstructed, stranguria with turbid discharge, edema, carbuncle carbuncle on the back, erysipelas, scabies.
Lignum Aquilariae Resinatum: " Compendium of Materia Medica " record wood has strong antibacterial efficacy, fragrance enters spleen, god's qi-regulating, tonifying five ZANG-organses, cough-relieving clearly
Resolving sputum, warming the stomach warming the spleen, ventilation analgesic therapy, can be used as medicine, be first-class medical material superfine product.
Lignum cinnamomi camphorae: aiphyllium, bark yellowish-brown, there is irregular longitudinal crack, on the south main product the Changjiang river and southwestern various places.Winter
Cut down trees and split broken or be sawn into bulk, dry or air-dry.Timber bulk is not of uniform size, surface rufous to burgundy, and transverse section is visible
Annual ring.Matter is again hard.There is strong Camphora fragrance, taste is refrigerant, have pungent sense, warm in nature, acrid in the mouth；Sensible can ward off dirty, warming middle-JIAO to stop
Bitterly, dampness removing parasite killing.
Rhizoma Acori Graminei: its flower, stem aromatic flavor, have functions that to have one's ideas straightened out, eliminating the phlegm, dissipate wind, epidemic disease of can dispelling Fructus Alpiniae Oxyphyllae, building body, can
Make spice or mosquito dispersing.
Fructus Citri Limoniae quintessence oil: there are biocidal efficacies, be effective cardiac tonic, be generally used for reducing blood pressure.The characteristic energy of its antibacterial
Mitigate sore throat, cough, catch a cold and influenza, headache, migraine, gout and arthritis can be mitigated.Feel hot agitation
When, pure and fresh impression can be brought, help clarify the state of mind, effectively improve work efficiency.
Cypress quintessence oil: have a charming succinum taste as wooden and face cream, rheumatism, antibacterial, spasmolytic, suppression diaphoresis, convergence,
Promote to scab, except bromhidrosis, diuresis, bring down a fever, stop blooding, sharp liver, parasite killing, rehabilitation, calmness, astringing to arrest bleeding, benefit body, vasoconstrictive.Disappear
Except fatigue, angry emotion of releiving, alleviate heart anxiety and pressure, purification of the mind.
Fructus Tritici aestivi quintessence oil: have overpowering odor to contain abundant high unit vitamin e, the Natural antioxidant being famous is (anti-corrosion
Agent), the quintessence oil of each composition can be stablized, make the effect of perfume more lasting.There is overpowering odor to contain abundant high unit vitamin e, be
The famous Natural antioxidant (preservative), can stablize the quintessence oil of each composition, make the effect of perfume more lasting.
Peppermint essential oil: not only fragrance, moreover it is possible to driving away mosquito, has contraction blood capillary simultaneously, excludes vivotoxin, improves wet
Rash, tinea, releive itch, inflammation and burning, soft skin, eliminate blackhead, be beneficial to oily hair and skin quality, purify air
And the effect refreshed oneself.
Herba Origani oil: the herb of Labiatae origanum Adeps Bovis seu Bubali origznum vul-garel., also known as careless, the wild chaste tree of dysentery relieving
The ground such as mustard accord with name, have heat clearing away, removing dampness, driving away summer heat, induce sweat, sterilization that qi-regulating is extremely strong, bacteriostasis, the volatilization extracted from Adeps Bovis seu Bubali
Oil, cause enteritis antibacterial common to 31 kinds and shigella flexneri, are the pure Chinese medicine additives of most broad-spectrum antiseptic.
Herba et Flos Pyrethri Cinerariifolii: Tanacetum vulgare L belongs to the general designation of (tanacetum) several plants, removing dampness and killing parasites, kills pubic louse, head louse, body
Louse, flea, the effect except mosquito parasite killing.
Borneolum Syntheticum: pungent, bitter, cool.There is inducing resuscitation of having one's ideas straightened out, heat-clearing dissipates poison, improving acuity of vision and removing nebula.Cure mainly high fever apoplexy coma due to blocking of the respiratory system shies epilepsy, middle wind-phlegm
Faint infantile convulsion, summer-heat and damp blinds clear key, larynx numbness is deaf, aphtha tooth swells, sore carbuncle infantile malnutrition due to digestive disturbances or intestinalparasites hemorrhoid, conjunctival congestion and swelling pain, pterygium.
Folium Nelumbinis: for the leaf of nymphaeaceae plant lotus, play the role of heat-clearing and toxic substances removing, removing heat from blood, hemostasis.There is clearing away summer-heat and eliminating dampness, rise and send out clearly
The effects such as sun, cooling blood for hemostasis.
Eucalyptus oil: one of most common and widest quintessence oil of purposes, there is good health-care effect, help focused attention
Power.Sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory system diseases can effectively be alleviated.There is good resisting
Bacterium and sterilization idiocratic, in some certain food, Eucalyptus oil is also as fragrance component.Carry this quintessence oil in travelling, permissible
Effectively resist mosquito bite and insect bite, treat skin measles.It is good anophelifuge.Mixing with water can become a kind of and simple and effective disappear
Toxic agent.
Beneficial effects of the present invention:
The present invention provides a kind of abnormal smells from the patient pure and fresh for user, has stimulating effect and the prepared Chinese ink of negative ion health effect, it is not only
Negative aeroion can be discharged for a long time, purify air, beneficial to health；Also thin to staphylococcuses, escherichia coli, Grain-positive
Multiple pathogenic bacteria such as bacterium and funguses have certain suppression, killing action；Fragrant odour simultaneously, pure and fresh soothe the spirit, pressure of releiving, also can drive
Catch up with mosquito, harmful effect will not be produced it is adaptable to each age groups to human body, its appropriate add other function ingredients after still
Original effect and quality can be kept.
1st, tourmaline is a kind of silicate mineral, and its chemical formula is na (mg, fe, mn, li, al) 3al6 (si6o18)
(bo3) 3 (oh, f) 4, it contacts under electrostatic field with hydrone, just hydrone can be ionized into hydrion (h+) and hydrogen-oxygen
Radical ion (oh-), hydroxide ion and water molecules form basic hydroxide group anion (h2o oh-), as " air bear from
Son ", current scientific research proves: anion can not only facilitate human body synthesis and vitamin storage, the life of strengthening and human activin
Reason activity, has highly important impact to the vital movement of human body and other biological, is referred to as " air vitamin ".Anion
Active adsorption interior harmful substance, the such as construction and decoration harmful substance such as formaldehyde, toluene, not only itself do not increase pollution, Er Qieqing
Purifying room air, is inherently eliminated construction and decoration syndrome, ensures that health is unaffected.
2nd, the Chinese medicine ingredients containing in the present invention, not only thin to staphylococcuses, tubercule bacillus, bacillus pyocyaneus, Grain-negative
Multiple pathogenic bacteria such as bacterium and gram-positive bacteria and funguses have certain suppression, killing action；Fragrant odour simultaneously, property is gentle,
Pure and fresh soothe the spirit, help hormone secretion, the effect of anxiety of releiving, also there is certain mosquito-repelling effect simultaneously, more it is essential that
The life-time service present invention will not produce harmful effect it is adaptable to each age groups to human body, before having application widely
Scape.
Specific embodiment
Embodiment.
A kind of prepared Chinese ink it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight portion, bis-phenol
A19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine 3.3 weight
Part, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surfactant
Compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, described mill base
Pigment be high-carbon black pigment, the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanite, firefly
Stone, tourmaline, gahnite are dravite and elbaite by weight the mixture of 2.5:3:3.7:2, wherein tourmaline
By weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine passes through following walking
Suddenly it is prepared from,
S1, take Cortex Meliae 35 weight portion clean, naturally dry, be subsequently placed in 90 DEG C of frying pans and fry to savory effusion, then spray
Drench deionized water 17 weight portion, be placed in constant temperature oven less than 60 DEG C and dry, water content≤6.5%；
S2, lavandula angustifolia 17.5 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality
3.7 times, put into and steam in pot thoroughly, take out, dry, the concentration of saline is 27%；
S3, by Herba Anemones Hupehensiss 4.5 weight portion, Moschus 4.5 weight portion, Fructus Chebulae 1 weight portion, Cortex Phellodendri 1 weight portion, Origanum majorana
0.75 weight portion decontamination, is put into together with step s1 and the made crude drug of s2 and is crushed to 60 mesh in super micron mill, is obtained former
Material medicated powder end, standby；
S4, by step s3 be obtained crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, adjust extraction
Pressure power 27.65mpa, 45.10 DEG C of extraction temperature, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, are directly separating
Kettle outlet triangular flask collects volatile oil a, standby；
S5, by jujube nucleus 13 weight portion, Semen Torreyae 15.5 weight portion, Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae
Then plus deionization 15.5 weight portions, Rhizoma Acori Graminei 4.5 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 70 mesh,
Water soaks 6 hours, amount of water by 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, prepared Traditional Chinese drug mixture, standby；
S6, the Traditional Chinese drug mixture that step s5 is obtained decoct 2 hours in 80 DEG C, collect distillate, and add ether to extract, distillation
Then plus anhydrous sodium sulfate drying the volume ratio of liquid and ether is 2:1, takes upper oil phase, that is, volatile oil b is obtained, standby；
S7, step s4 and s6 made volatile oil a and volatile oil b mixing are mixed well prepared miscella, then sequentially add while stirring
Fructus Citri Limoniae quintessence oil, cypress quintessence oil, Geranium Essential, Fructus Tritici aestivi quintessence oil and Peppermint essential oil, are sufficiently stirred for 35 minutes, stand 30 minutes,
It is sufficiently stirred for mixing well, filtering and impurity removing, obtains final product essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Citri Limoniae quintessence oil, cypress quintessence oil, Flos Pelargonii
The mass ratio of quintessence oil, Fructus Tritici aestivi quintessence oil and Peppermint essential oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, also include Herba Origani oil 1.3 weight portion in the crude drug powder of step s3 and spend in vain
Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step s5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4
Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step s7 also includes Eucalyptus oil 0.3 weight portion.
Test the prepared Chinese ink in this above-described embodiment using air ion static method of testing, anion burst size is in 430-650
Individual/m3, and sustained release negative aeroion, it is more beneficial for long-term purify air, reach the basic demand of health of people.
Reference examples.
Colour carbon black 20g, phenol 11g, glycerol 4g, BTA 3g, triethanolamine 1g, triethylamine 3g, sodium bicarbonate
5g, polyoxyethylene groups ethers nonionic fluorocarbon surfactant 1.5g, slow releasing agent 0.4g, Origanum majorana quintessence oil 0.6g, Semen Tritici aestivi
Bud quintessence oil 0.5g, Herba Lysimachiae foenum-graeci quintessence oil 0.5g, Radix Paeoniae Alba quintessence oil 0.4g, cypress quintessence oil 0. 4g, eucalyptus quintessence oil 0.4g, Folium Artemisiae Argyi essence
Oily 0. 4g, Peppermint essential oil 0.4g, deionized water 75g.
Test the prepared Chinese ink in this above-mentioned reference examples using air ion static method of testing, anion burst size is in 0/m3,
There is no the function of release negative aeroion.
(1) acute toxicity test is carried out to obtained essential oil of traditional Chinese medicine, result is as follows:
1. Mouse oral acute toxicity test: the ld50 of Mouse oral essential oil of traditional Chinese medicine is 383.55g/kg, 95% credible is limited to
294.68g/kg～499.31g/kg.And the toxicity criterion of air freshener is: Mouse oral anxious poison ld50 >=5g/
Kg, is judged to nontoxic.The ld50 of this essential oil of traditional Chinese medicine is higher than 76 times of nontoxic standard, therefore, it is determined that being nontoxic.
2. chmice acute toxicity on inhalation test: the lc50 that chmice acute sucks essential oil of traditional Chinese medicine is 24863.99g/m3,95%
Credible be limited to 16837.34g/m3～33387.46g/m3.And the toxicity criterion of air freshener is: chmice acute
Suck (2h) lc50 ＞ 10000mg/m3, the nontoxic level in true border.The lc50 of this essential oil of traditional Chinese medicine is higher than the 2486 of nontoxic standard
Times, therefore, it is determined that being nontoxic.
Through inspection, its fragrance, color and luster, refraction index, relative density, arsenic content, heavy metal contain obtained essential oil of traditional Chinese medicine
Amount, ph value all meet the requirement of national standard.
(2) check above-mentioned ink anion burst size result such as table 1:
(3) repelling effect test.
Repelling effect according to common prepared Chinese ink of the prior art and prepared Chinese ink in above-described embodiment carries out contrast test, test
Data is shown in Table 2.
Conclusion: the prepared Chinese ink in the embodiment of the present invention has certain repelling effect.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, common for art
For technical staff, can also make other changes in different forms on the basis of the above description, here need not
All of embodiment cannot be exhaustive, all any modifications within the spirit and principles in the present invention, made, equivalent replace
Change, improve, be still included within protection scope of the present invention.
Claims (1)
1. a kind of prepared Chinese ink it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight portion, bis-phenol a19
Weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine 3.3 weight portion, third
Ketone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surfactant blend
1.2 weight portions, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, the pigment of described mill base
For high-carbon black pigment, the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanite, fluorite, electrically
Stone, gahnite by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and elbaite by weight
The mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine be made by the steps and
Become,
S1, take Cortex Meliae 35 weight portion clean, naturally dry, be subsequently placed in 90 DEG C of frying pans and fry to savory effusion, then spray
Drench deionized water 17 weight portion, be placed in constant temperature oven less than 60 DEG C and dry, water content≤6.5%；
S2, lavandula angustifolia 17.5 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality
3.7 times, put into and steam in pot thoroughly, take out, dry, the concentration of saline is 27%；
S3, by Herba Anemones Hupehensiss 4.5 weight portion, Moschus 4.5 weight portion, Fructus Chebulae 1 weight portion, Cortex Phellodendri 1 weight portion, Origanum majorana
0.75 weight portion, Herba Origani oil 1.3 weight portion and Herba et Flos Pyrethri Cinerariifolii 1.5 weight portion decontamination, with step s1 and the made crude drug of s2
Put into together in super micron mill and be crushed to 60 mesh, prepared crude drug powder, standby；
S4, by step s3 be obtained crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, adjust extraction
Pressure power 27.65mpa, 45.10 DEG C of extraction temperature, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, are directly separating
Kettle outlet triangular flask collects volatile oil a, standby；
S5, by jujube nucleus 13 weight portion, Semen Torreyae 15.5 weight portion, Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae
15.5 weight portions, Rhizoma Acori Graminei 4.5 weight portion, Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4 weight portion are cleaned and are dried, and put into superfine powder together
Be crushed to 70 mesh in broken machine, then plus deionized water soaks 6 hours, amount of water by 6.5 times of immersions crude drug quality, stir
Dispersion is mixed well, prepared Traditional Chinese drug mixture, standby；
S6, the Traditional Chinese drug mixture that step s5 is obtained decoct 2 hours in 80 DEG C, collect distillate, and add ether to extract, distillation
Then plus anhydrous sodium sulfate drying the volume ratio of liquid and ether is 2:1, takes upper oil phase, that is, volatile oil b is obtained, standby；
S7, step s4 and s6 made volatile oil a and volatile oil b mixing are mixed well prepared miscella, then sequentially add while stirring
Fructus Citri Limoniae quintessence oil, cypress quintessence oil, Geranium Essential, Fructus Tritici aestivi quintessence oil and Peppermint essential oil, are sufficiently stirred for 35 minutes, stand 30 minutes,
It is sufficiently stirred for mixing well, filtering and impurity removing, obtains final product essential oil of traditional Chinese medicine, wherein, described miscella and Fructus Citri Limoniae quintessence oil, cypress quintessence oil, Flos Pelargonii
The mass ratio of quintessence oil, Fructus Tritici aestivi quintessence oil and Peppermint essential oil is 1.3:0.4:0.75:0.6:0.5:0.3, in described essential oil of traditional Chinese medicine also
Include Eucalyptus oil 0.3 weight portion.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2016100937314 | 2016-02-19 | ||
| CN201610093731.4A CN105602338A (en) | 2016-02-19 | 2016-02-19 | Calligraphy ink |
| CN201610723041.2A CN106243832A (en) | 2016-02-19 | 2016-08-25 | A kind of calligraphy prepared Chinese ink |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610723041.2A Division CN106243832A (en) | 2016-02-19 | 2016-08-25 | A kind of calligraphy prepared Chinese ink |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106336731A true CN106336731A (en) | 2017-01-18 |
Family
ID=55982710
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610093731.4A Pending CN105602338A (en) | 2016-02-19 | 2016-02-19 | Calligraphy ink |
| CN201610735647.8A Withdrawn CN106336731A (en) | 2016-02-19 | 2016-08-25 | Prepared Chinese ink |
| CN201610723041.2A Withdrawn CN106243832A (en) | 2016-02-19 | 2016-08-25 | A kind of calligraphy prepared Chinese ink |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610093731.4A Pending CN105602338A (en) | 2016-02-19 | 2016-02-19 | Calligraphy ink |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610723041.2A Withdrawn CN106243832A (en) | 2016-02-19 | 2016-08-25 | A kind of calligraphy prepared Chinese ink |
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| CN (3) | CN105602338A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104212237A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Anion-releasing health type ink |
| CN104212236A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Fragrant ink with refreshing effect |
| CN104212240A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Ink prepared from compound plant extracts for ink-jet printer |
| CN104212238A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Antibacterial carbon black ink |
-
2016
- 2016-02-19 CN CN201610093731.4A patent/CN105602338A/en active Pending
- 2016-08-25 CN CN201610735647.8A patent/CN106336731A/en not_active Withdrawn
- 2016-08-25 CN CN201610723041.2A patent/CN106243832A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104212237A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Anion-releasing health type ink |
| CN104212236A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Fragrant ink with refreshing effect |
| CN104212240A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Ink prepared from compound plant extracts for ink-jet printer |
| CN104212238A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Antibacterial carbon black ink |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105602338A (en) | 2016-05-25 |
| CN106243832A (en) | 2016-12-21 |
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Application publication date: 20170118 |