CN106189513A - Covering type textile inkjet printing pigment ink - Google Patents
Covering type textile inkjet printing pigment ink Download PDFInfo
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- CN106189513A CN106189513A CN201610735659.0A CN201610735659A CN106189513A CN 106189513 A CN106189513 A CN 106189513A CN 201610735659 A CN201610735659 A CN 201610735659A CN 106189513 A CN106189513 A CN 106189513A
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- 230000001105 regulatory effect Effects 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- 210000003296 saliva Anatomy 0.000 description 1
- 208000005687 scabies Diseases 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 210000000582 semen Anatomy 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 229910052604 silicate mineral Inorganic materials 0.000 description 1
- 201000009890 sinusitis Diseases 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- PJANXHGTPQOBST-UHFFFAOYSA-N stilbene Chemical compound C=1C=CC=CC=1C=CC1=CC=CC=C1 PJANXHGTPQOBST-UHFFFAOYSA-N 0.000 description 1
- 235000021286 stilbenes Nutrition 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 238000013268 sustained release Methods 0.000 description 1
- 239000012730 sustained-release form Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 208000011580 syndromic disease Diseases 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
- 231100000167 toxic agent Toxicity 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 231100000397 ulcer Toxicity 0.000 description 1
- 230000003639 vasoconstrictive effect Effects 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
A covering type textile inkjet printing pigment ink comprises 23 parts by weight of pigment paste, 19 parts by weight of bisphenol A, 4.5 parts by weight of glycerol, 2.3 parts by weight of anhydrous sodium sulfate, 2.7 parts by weight of triethanolamine, 3.3 parts by weight of triethylamine, 3.6 parts by weight of acetone, 0.25 part by weight of dithiocarbamic acid ester, 1.7 parts by weight of active mineral powder, 1.2 parts by weight of surfactant complex and 0.55 part by weight of slow release agent, and not only can release negative ions of air for a long time, purify the air and be beneficial to human health; also has certain inhibiting and killing effects on staphylococcus, escherichia coli, gram-positive bacteria and other various germs and fungi; has wide application prospect.
Description
The application is Application No. 201610723008X submitted to August 25 2016 applying date, invention entitled " one
Kind of covering type textile inkjet printing pigment ink " the divisional application of Chinese invention patent application.
Technical field
The present invention relates to a kind of ink, particularly to one covering type textile inkjet printing pigment ink.
Background technology
Ink can be used for routine office work or textile printing field, but traditional general ink do not have refresh oneself and generation bear from
The health-care effects such as son, user use when long produces taediumvitae, due to the function singleness of tradition ink, can not meet people
Multi-demands.
Summary of the invention
The deficiency existed for prior art, the user that the present invention is ink provides a kind of abnormal smells from the patient pure and fresh, has and refresh oneself
Effect and the ink of negative ion health effect, it is possible not only to discharge for a long time negative aeroion, purifies air, beneficially human body strong
Health；Also the multiple pathogenic bacterias such as staphylococcus, escherichia coli, gram-positive bacteria and fungus are had certain suppression, killing action；With
Time fragrant odour, pure and fresh soothe the spirit, pressure of releiving, also can expelling mosquito, human body will not be produced harmful effect, have widely
Application prospect.
It is an object of the invention to be achieved through the following technical solutions:
A kind of covering type textile inkjet printing pigment ink, it is characterised in that: by following component by weight: face
Material mill base 23 weight portion, bisphenol-A 19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight
Amount part, triethylamine 3.3 weight portion, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7
Weight portion, surfactant blend 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water
62 weight portions, the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanite, fluorite, tourmaline, zinc
Spinelle is by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and elbaite 5:3 by weight
Mixture, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is made by the steps and forms,
S1, take rhamnus crenata sieb.et zucc. 35 weight portion and clean, naturally dry, be subsequently placed in 90 DEG C of frying pans stir-fry extremely savory effusion, then
Air washer 17 weight portion, is placed in less than 60 DEG C drying, water content≤6.5% in constant temperature oven；
S2, Spica Prunellae 12.5 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality
3.7 times, putting into and steam thoroughly in pot, take out, dry, the concentration of saline is 27%；
S3, by Nidus Vespae 12 weight portion, lavandula angustifolia 15.5 weight portion, Herba Anemones Hupehensis 4.5 weight portion, Moschus 4.5 weight portion, Herba Menthae
1 weight portion, Herba Rosmarini Officinalis 1 weight portion, Origanum majorana 0.75 weight portion, Ambra Grisea 0.65 weight portion decontamination, with step S1 and S2
Made crude drug puts into together in super micron mill and is crushed to 60 mesh, prepares crude drug powder, standby；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, directly separating
Still outlet triangular flask collects volatile oil A, standby；
S5, by Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 35-40 weight portion, the Radix Astragali 1 weight portion cleans and dries,
Putting in super micron mill together and be crushed to 70 mesh, then add deionized water and soak 6 hours, amount of water is by being soaked crude drug matter
6.5 times of amount, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S6, Traditional Chinese drug mixture step S5 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate and be dried, i.e. prepares volatile oil B, standby；
S7, made to step S4 and S6 volatile oil A and volatile oil B are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Juniperus rigida Sieb.et Zucc. quintessence oil, Moschus quintessence oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene, be sufficiently stirred for 35 minutes, stands 30 minutes,
It is sufficiently stirred for mixing well, filtering and impurity removing, obtains essential oil of traditional Chinese medicine, wherein, described miscella and Juniperus rigida Sieb.et Zucc. quintessence oil, Moschus quintessence oil, Flos Pelargonii
The mass ratio of quintessence oil, eucalyptus quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the crude drug powder of step S3, also include Herba Origani oil 1.3 weight portion and spend in vain
Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step S5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4
Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step S7 also includes Eucalyptus oil 0.3 weight portion.
Equipment, raw material and method involved in the present invention, is equipment, raw material and method that the industry usually uses,
This repeats no more.
The most each essential oil component must be sufficiently mixed with surfactant, slow releasing agent, to reach slow release effect, each quintessence oil and
The addition of anion natural mineral matter powder must be appropriate, not only antibiotic and sterilizing, moreover it is possible to stable emotion, so to the not normal heart
Reason state has the effect in front, can purify, pacify soul, can alleviate angry and beaten sensation, makes the people can be with the flat gas of the heart
With ground in the face of life, because its energy centre of equilibrium is neural, thus helpful to alarmed and dejected state, also have the most flat
Quiet with releive function, insomniac is had goodish relax to put console with spirit, for pacify hot-tempered enter or moody temper have
Goodish effect, can improve work efficiency.
The present invention with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine and repeatedly verifies, gives full play to respectively
Group weight portion synergism, the most each Chinese medicinal components brief introduction is as follows.
Rhamnus crenata sieb.et zucc.:: machaka or dungarunga, root bark or Herb are used as medicine, and property is flat, bitter in the mouth, dries, sterilizes, parasite killing.
Spica Prunellae: there is effect of heat-clearing and toxic substances removing, cooling blood for hemostasis, to staphylococcus aureus, beta hemolytic streptococcus,
Escherichia coli, Bacillus typhi, dysentery bacterium, diphtheria corynebacterium, anthrax bacillus, bacillus pyocyaneus, dysentery bacterium, Bacillus typhi, cholera
Vibrio, escherichia coli, bacillus pyocyaneus and staphylococcus, streptococcus and Bacillus tuberculosis all have certain inhibitory action.
Nidus Vespae: pick up from the lair of Apis, effect: dispel the wind, counteracting toxic substances, parasite killing, pain relieving, antiallergic, HBS is resisted
Original deactivation, also to staphylococcus aureus, bacillus pyocyaneus, escherichia coli, dysentery bacterium, Bacillus typhi and common variation
Bacillus etc. have the strongest restraint；The funguses such as Aspergillus fumigatus, Aspergillus flavus, eggplant sickle bacterium, leukonid also there is inhibitory action.
Lavandula angustifolia can remove ant, except roach, acaricide, the when of being placed under wardrobe, medicated pillow, not only can replace camphor ball, moreover it is possible to stay
The fragrance of one people that oozes lower, research finds, lavandula angustifolia has obvious antibacterial action, and the linalool contained in lavandula angustifolia is lavandula angustifolia
Antibacterial main component, it can suppress 17 kinds of antibacterials (including gram-negative bacteria and gram-positive bacteria), the life of 10 kinds of funguses
Long.
Herba Anemones Hupehensis: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature,
Slightly poisonous." removing toxic substances, evacuation of pus granulation promoting, dissipating blood stasis of subsiding a swelling, have and kill maggot, wriggler, change long-pending, detumescence, dissipating blood stasis, control stubborn dermatitis, tinea alba, malaria
Disease, infantile malnutrition, dysentery, carbuncle furuncle swells, scrofula, traumatic injury.
Moschus: have and have one's ideas straightened out, wards off dirty, dredging collateral, effect of dissipating blood stasis；Controlling apoplexy, syncope due to accumulation of phlegm, infantile convulsion, attacked by pestiferous factors is unhappy, Xin Fubao
Bitterly, the abdominal mass hypochondriac lump, traumatic injury, swollen ulcer drug." herbal classic ": master wards off bad odor, pyrexial malaria, epilepsy convulsion, goes three worms.
Herba Menthae: for the dry aerial parts of labiate Herba Menthae, dispelling wind and heat pathogens, the clear profit head, sore-throat relieving rash, soothing the liver row
Gas.
Herba Rosmarini Officinalis: have tranquillizing and allaying excitement, refreshment effect, all has certain curative effect to dyspepsia and stomachache, has calmness, profit
Urine effect, it is possible to being used for treating the multiple diseases such as insomnia, cardiopalmus, headache, dyspepsia, external can treat wound and arthritis.
Also there is strong heart, promote that metabolism, the blood circulation etc. of promotion peripheral vessel act on.
Origanum majorana: can improve that mood is depressed and addictive disease, especially effective to liberal-mindedness and vigorous endurance stress symptom, can expand blood vessel,
Blood pressure lowering, alleviate and burden, help to eliminate cardiopalmus, have the nerve of excellence to pacify and calm function.
Ambra Grisea: be the most lasting spice of lasting, any spice all can not compare favourably therewith in the world, have " dragon
The perfume of saliva and life coexist " saying.Compendium of Material Medica carry: can invigorate blood circulation, benefit marrow, supporing yang road, promoting blood circulation, reduce phlegm flat
Breathe heavily；Lump in the abdomen；Trusted subordinate's pain；Coma；Liao Yongyan: relieving stranguria by diuresis, eliminating stagnation, knot of cooling down, by labor worm.
Cortex ulmi pumilae: for dry bark or the root bark of Ulmaceae, sweet, flat, nontoxic；Diuretic, treating stranguria, detumescence, for urine
Obstructed, stranguria with turbid discharge, edema, carbuncle carbuncle on the back, erysipelas, scabies.
Lignum Aquilariae Resinatum: " Compendium of Materia Medica " record wood have strong antibacterial efficacy, fragrance enters spleen, clear god regulates the flow of vital energy, tonifying five ZANG-organs, cough-relieving
Reduce phlegm, warming the stomach warming the spleen, ventilation analgesic therapy, can be used as medicine, be first-class medical material superfine product.
Lignum cinnamomi camphorae: aiphyllium, bark yellowish-brown, there is irregular longitudinal crack, on the south main product the Changjiang river and various places, southwest.Winter
Cut down trees and split broken or be sawn into bulk, dry or air-dry.Timber bulk is not of uniform size, surface red brown to burgundy, and transverse section is visible
Annual ring.Matter is heavily hard.Having strong Camphora fragrance, taste is refrigerant, has pungent sense, warm in nature, acrid in the mouth；Only sensible can ward off dirty, warming middle-JIAO
Bitterly, dampness removing parasite killing.
The Radix Astragali: have another name called continuous stilbene.Perennial herb, the medicinal history having more than 2000 year so far of the Radix Astragali, it has enhancing machine
Body immunity function, protect the liver, diuresis, defying age, anti-stress, blood pressure lowering and wide antibacterial action.
Juniperus rigida Sieb.et Zucc. quintessence oil: there is purification air, mosquito-proof insect bite, antibacterial, rheumatism, antitetanic effect, it may have calm
Refresh oneself, encourage emotion, purify the state of mind and the function of release soul, it is possible to make people's body and mind relaxed and comfortable, it may have the effect promoted the sexual maturity；Separately
Outward, the function of its toxin expelling is the most famous, and it can discharge the toxin of accumulation, purifies intestinal mucosa.
Moschus quintessence oil: have light fragrance, has and releives, calms, releases the melancholy and effect of anti-depression, increases romantic
Mood, natural fragrance bring warm impression by body and mind.
Geranium Essential: there is hemostasis, vasoconstrictive, asthma, liver and expelling toxin, cholelithiasis, kidney toxin expelling, renal calculus, diuresis, flesh
Carnic acid pain, oily skin, aging skin activates, herpes, palor, and fat-reducing promotes to scab, eczema, sunburn of burning, tinea, the moon
Through having some setbacks, engorgement of breasts inflammation, alleviate melancholy uneasy, there is deodorization, antibacterial, the effect of sterilization.
Eucalyptus quintessence oil has effect of infection, antiviral, sterilization, parasite killing, deodorization, and the effect of antiviral, to breathing
Tract disease is most effective, can relax inflammation phenomenon, makes nasal mucosa comfortable；Emotion is had calm effect simultaneously, sanity can be made,
Focus on.
P-Cymene: to anthrax bacillus, Alpha-hemolytic streptococcus, B-Streptococcus hemolyticus, diphtheria corynebacterium, bacillus pseudodiphthericus, lung
10 kinds of Gram-positives such as diplococcoid, staphylococcus aureus, Staphylococcus citreus, white Portugal Portugal coccus, bacillus subtilis
Aerophil all has antibacterial action, also has bacteriostasis for multiple pathomycete.
Herba Origani oil: the herb of Labiatae origanum Adeps Bovis seu Bubali ORIGZNUM VUL-GAREL., has another name called dysentery relieving chaste tree careless, wild
The ground such as mustard symbol name, have heat clearing away, removing dampness, drive away summer heat, induce sweat, the sterilization of regulating the flow of vital energy extremely strong, bacteriostasis, the volatilization extracted from Adeps Bovis seu Bubali
Oil, to 31 kinds of common cause enteritis antibacterials and shigella flexneri, is the pure Chinese medicine additive most with broad-spectrum antiseptic.
Herba et Flos Pyrethri Cinerariifolii: Tanacetum vulgare L belongs to the general designation of (Tanacetum) several plants, removing dampness and killing parasites, kills pubic louse, head louse, body
Louse, flea, effect except mosquito parasite killing.
Borneolum Syntheticum: pungent, bitter, cool.Having refreshment of having one's ideas straightened out, heat clearing away dissipates poison, improving acuity of vision and removing nebula.Cure mainly calentura unconsciousness due to high fever, middle wind-phlegm
Fainting infantile convulsion, heat-damp in summer blinds clear key, and sore throat is deaf, and aphtha tooth swells, carbuncle sore infantile malnutrition hemorrhoid, conjunctival congestion and swelling pain, pterygium.
Folium Nelumbinis: for the leaf of nymphaeaceae plant lotus, have the effect of heat-clearing and toxic substances removing, removing heat from blood, hemostasis.There is clearing away summer-heat and eliminating dampness, rise and send out clearly
The effects such as sun, cooling blood for hemostasis.
Eucalyptus oil: one of most common and widest quintessence oil of purposes, has good health-care effect, helps focused attention
Power.Can effectively alleviate sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory system diseases.There is good resisting
Bacterium and sterilization idiocratic, in some certain food, Eucalyptus oil is also as fragrance component.This quintessence oil is carried at whilst on tour, permissible
Effectively resist mosquito bite and insect bite, treat skin measles.It it is good anophelifuge.Mixing with water can become a kind of and simple and effective disappear
Toxic agent.
Beneficial effects of the present invention:
The present invention provides a kind of abnormal smells from the patient pure and fresh for user, has stimulating effect and the ink of negative ion health effect, and it is not only
Negative aeroion can be discharged for a long time, purify air, beneficially health；Also thin to staphylococcus, escherichia coli, Grain-positive
The multiple pathogenic bacteria such as bacterium and fungus have certain suppression, killing action；Fragrant odour simultaneously, pure and fresh soothes the spirit, and pressure of releiving also can drive
Catch up with mosquito, human body will not be produced harmful effect, it is adaptable to each age groups, its appropriate add other function ingredients after still
Original effect and quality can be kept.
1, tourmaline is a kind of silicate mineral, and its chemical formula is Na (Mg, Fe, Mn, Li, Al) 3Al6 (Si6O18)
(Bo3) 3 (OH, F) 4, it contacts with hydrone under electrostatic field, and hydrone just can be ionized into hydrion (H+) and hydrogen-oxygen
Radical ion (OH-), hydroxide ion and water molecules form basic hydroxide group anion (H2O OH-), be " air bear from
Son ", current scientific research proves: anion can not only facilitate human body synthesis and vitamin storage, strengthening and the life of human activin
Reason activity, has highly important impact to the vital movement of human body and other biological, is referred to as " air vitamin ".Anion
Active adsorption indoor harmful substance, such as the construction and decoration harmful substance such as formaldehyde, toluene, not only self does not increase pollution, Er Qieqing
Purifying room air, is inherently eliminated construction and decoration syndrome, ensures that health is unaffected.
2, the Chinese medicine ingredients contained in the present invention, not only thin to staphylococcus, tubercule bacillus, bacillus pyocyaneus, Grain-negative
The multiple pathogenic bacteria such as bacterium and gram-positive bacteria and fungus have certain suppression, killing action；Fragrant odour simultaneously, character is gentle,
Pure and fresh soothe the spirit, help hormone secretion, the effect of anxiety of releiving, also there is certain mosquito-repelling effect simultaneously, more it is essential that
The life-time service present invention will not produce harmful effect to human body, it is adaptable to each age groups, before having application widely
Scape.
Detailed description of the invention
Embodiment.
A kind of covering type textile inkjet printing pigment ink, it is characterised in that: by following component according to weight portion array
Become: dispersible pigment color paste 23 weight portion, bisphenol-A 19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine
2.7 weight portions, triethylamine 3.3 weight portion, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter
Powder 1.7 weight portion, surfactant blend 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, goes
Ionized water 62 weight portion, the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanite, fluorite, electricity
Gas stone, gahnite by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and elbaite by weight
The ratio mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is made by the steps
Form,
S1, take rhamnus crenata sieb.et zucc. 35 weight portion and clean, naturally dry, be subsequently placed in 90 DEG C of frying pans stir-fry extremely savory effusion, then
Air washer 17 weight portion, is placed in less than 60 DEG C drying, water content≤6.5% in constant temperature oven；
S2, Spica Prunellae 12.5 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality
3.7 times, putting into and steam thoroughly in pot, take out, dry, the concentration of saline is 27%；
S3, by Nidus Vespae 12 weight portion, lavandula angustifolia 15.5 weight portion, Herba Anemones Hupehensis 4.5 weight portion, Moschus 4.5 weight portion, Herba Menthae
1 weight portion, Herba Rosmarini Officinalis 1 weight portion, Origanum majorana 0.75 weight portion, Ambra Grisea 0.65 weight portion decontamination, with step S1 and S2
Made crude drug puts into together in super micron mill and is crushed to 60 mesh, prepares crude drug powder, standby；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, directly separating
Still outlet triangular flask collects volatile oil A, standby；
S5, by Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 35-40 weight portion, the Radix Astragali 1 weight portion cleans and dries,
Putting in super micron mill together and be crushed to 70 mesh, then add deionized water and soak 6 hours, amount of water is by being soaked crude drug matter
6.5 times of amount, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S6, Traditional Chinese drug mixture step S5 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate and be dried, i.e. prepares volatile oil B, standby；
S7, made to step S4 and S6 volatile oil A and volatile oil B are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Juniperus rigida Sieb.et Zucc. quintessence oil, Moschus quintessence oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene, be sufficiently stirred for 35 minutes, stands 30 minutes,
It is sufficiently stirred for mixing well, filtering and impurity removing, obtains essential oil of traditional Chinese medicine, wherein, described miscella and Juniperus rigida Sieb.et Zucc. quintessence oil, Moschus quintessence oil, Flos Pelargonii
The mass ratio of quintessence oil, eucalyptus quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the crude drug powder of step S3, also include Herba Origani oil 1.3 weight portion and spend in vain
Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step S5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4
Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step S7 also includes Eucalyptus oil 0.3 weight portion.
Using air ion static method of testing to test the ink in this above-described embodiment, anion burst size is at 430-650
Individual/m3, and sustained release negative aeroion, it is more beneficial for purifying for a long time air, reaches the basic demand of health of people.
Reference examples.
Colour carbon black 20g, phenol 11g, glycerol 4g, BTA 3g, triethanolamine 1g, triethylamine 3g, sodium bicarbonate
5g, polyoxyethylene groups ethers nonionic fluorocarbon surfactant 1.5g, slow releasing agent 0.4g, Origanum majorana quintessence oil 0.6g, Semen Tritici aestivi
Bud quintessence oil 0.5g, Herba Lysimachiae foenum-graeci quintessence oil 0.5g, Radix Paeoniae Alba quintessence oil 0.4g, cypress quintessence oil 0. 4g, eucalyptus quintessence oil 0.4g, Folium Artemisiae Argyi essence
Oil 0. 4g, Peppermint essential oil 0.4g, deionized water 75g.
Using air ion static method of testing to test the ink in this above-mentioned reference examples, anion burst size is at 0/m3,
Not there is the function of release negative aeroion.
(1) obtained essential oil of traditional Chinese medicine being carried out acute toxicity test, result is as follows:
1. Mouse oral acute toxicity test: the LD50 of Mouse oral essential oil of traditional Chinese medicine is 383.55g/kg, 95% credible be limited to
294.68g/kg～499.31g/kg.And the toxicity criterion of air freshener is: Mouse oral anxious poison LD50 >=5g/
Kg, it is determined that for nontoxic.The LD50 of this essential oil of traditional Chinese medicine is higher than 76 times of nontoxic standard, therefore, it is determined that be nontoxic.
2. chmice acute toxicity on inhalation test: it is 24863.99g/m3 that chmice acute sucks the LC50 of essential oil of traditional Chinese medicine, 95%
Credible be limited to 16837.34g/m3～33387.46g/m3.And the toxicity criterion of air freshener is: chmice acute
Suck (2h) LC50 ＞ 10000mg/m3, the nontoxic level in true border.The LC50 of this essential oil of traditional Chinese medicine is higher than the 2486 of nontoxic standard
Times, therefore, it is determined that be nontoxic.
Obtained essential oil of traditional Chinese medicine is through inspection, and its fragrance, color and luster, refraction index, relative density, arsenic content, heavy metal contain
Amount, pH value all meet the requirement of national standard.
(2) above-mentioned ink anion burst size result such as table 1 is checked:
(3) to the test improving the mental status.
Main method is that ink uses volunteer's experiment, recruits 60 people, uses the ink in above-mentioned 2 kinds of embodiments respectively,
By SCL-90 questionnaire (i.e. " Self-reporting inventory-SCL90 ", be one of the most foremost Mental health test scale),
Being followed the tracks of by the use of continuous 1 week, judge the present invention actual efficacy effect at aspect of refreshing oneself, wherein 6 people are noninductive is subject to；9 people
Impression is general；2 people think that this product is invalid for stimulating effect；There are 43 people to feed back this product and there is effect of preferably refreshing oneself, can make
People's attention is concentrated, and effective percentage is 71.67%.
(4) repelling effect test.
Contrast test is carried out with the repelling effect of ink in above-described embodiment, test according to common ink of the prior art
Data are shown in Table 2.
Conclusion: the ink in the embodiment of the present invention has certain repelling effect.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, common for art
For technical staff, can also make other changes in different forms on the basis of the above description, here without also
Cannot all of embodiment be given exhaustive, all within the spirit and principles in the present invention, any amendment of being made, equivalent are replaced
Change, improvement etc., within being still included in protection scope of the present invention.
Claims (1)
1. a covering type textile inkjet printing pigment ink, it is characterised in that: by following component by weight:
Dispersible pigment color paste 23 weight portion, bisphenol-A 19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7
Weight portion, triethylamine 3.3 weight portion, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder
1.7 weight portions, surfactant blend 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, go from
Sub-water 62 weight portion, the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanite, fluorite, electrically
Stone, gahnite by weight the mixture of 2.5:3:3.7:2, wherein tourmaline be dravite and elbaite by weight
The mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine be made by the steps and
Become,
S1, take rhamnus crenata sieb.et zucc. 35 weight portion and clean, naturally dry, be subsequently placed in 90 DEG C of frying pans stir-fry extremely savory effusion, then
Air washer 17 weight portion, is placed in less than 60 DEG C drying, water content≤6.5% in constant temperature oven；
S2, Spica Prunellae 12.5 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality
3.7 times, putting into and steam thoroughly in pot, take out, dry, the concentration of saline is 27%；
S3, by Nidus Vespae 12 weight portion, lavandula angustifolia 15.5 weight portion, Herba Anemones Hupehensis 4.5 weight portion, Moschus 4.5 weight portion, Herba Menthae
1 weight portion, Herba Rosmarini Officinalis 1 weight portion, Origanum majorana 0.75 weight portion, Ambra Grisea 0.65 weight portion, Herba Origani oil 1.3 weight portion is with white
Spend Pyrethrum 1.5 weight portion decontamination, put into together with crude drug made with step S1 and S2 and super micron mill is crushed to 60 mesh,
Prepare crude drug powder, standby；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, directly separating
Still outlet triangular flask collects volatile oil A, standby；
S5, by Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 35-40 weight portion, the Radix Astragali 1 weight portion, Borneolum Syntheticum 0.6 weight
Amount part and Folium Nelumbinis 0.4 weight portion are cleaned and are dried, and put in super micron mill together and are crushed to 70 mesh, then add deionized water and soak
6 hours, amount of water by 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S6, Traditional Chinese drug mixture step S5 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate and be dried, i.e. prepares volatile oil B, standby；
S7, made to step S4 and S6 volatile oil A and volatile oil B are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Juniperus rigida Sieb.et Zucc. quintessence oil, Moschus quintessence oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene, be sufficiently stirred for 35 minutes, stands 30 minutes,
It is sufficiently stirred for mixing well, filtering and impurity removing, obtains essential oil of traditional Chinese medicine, wherein, described miscella and Juniperus rigida Sieb.et Zucc. quintessence oil, Moschus quintessence oil, Flos Pelargonii
The mass ratio of quintessence oil, eucalyptus quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3, in described essential oil of traditional Chinese medicine also
Include Eucalyptus oil 0.3 weight portion.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610093678.8A CN105504992A (en) | 2016-02-19 | 2016-02-19 | Covering type textile ink jet printing pigment ink |
| CN2016100936788 | 2016-02-19 | ||
| CN201610723008.XA CN106336735A (en) | 2016-02-19 | 2016-08-25 | Covering type textile inkjet printing pigment ink |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610723008.XA Division CN106336735A (en) | 2016-02-19 | 2016-08-25 | Covering type textile inkjet printing pigment ink |
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| Publication Number | Publication Date |
|---|---|
| CN106189513A true CN106189513A (en) | 2016-12-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610735659.0A Withdrawn CN106189513A (en) | 2016-02-19 | 2016-08-25 | Covering type textile inkjet printing pigment ink |
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| CN (1) | CN106189513A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107778960A (en) * | 2017-11-24 | 2018-03-09 | 天长市天翔包装有限公司 | A kind of fragrant pearl ink composition |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104212236A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Fragrant ink with refreshing effect |
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2016
- 2016-08-25 CN CN201610735659.0A patent/CN106189513A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104212236A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Fragrant ink with refreshing effect |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107778960A (en) * | 2017-11-24 | 2018-03-09 | 天长市天翔包装有限公司 | A kind of fragrant pearl ink composition |
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Application publication date: 20161207 |