CN106118220A - A kind of modified form printing-ink - Google Patents
A kind of modified form printing-ink Download PDFInfo
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- CN106118220A CN106118220A CN201610723029.1A CN201610723029A CN106118220A CN 106118220 A CN106118220 A CN 106118220A CN 201610723029 A CN201610723029 A CN 201610723029A CN 106118220 A CN106118220 A CN 106118220A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Abstract
A kind of modified form printing-ink, is possible not only to discharge for a long time negative aeroion, purifies air, beneficially health；Also the multiple pathogenic bacterias such as staphylococcus, escherichia coli, gram-positive bacteria and fungus are had certain suppression, killing action；Fragrant odour simultaneously, pure and fresh soothes the spirit, and pressure of releiving can leave lasting fragrance, have the health-care effect of refreshment, allaying tiredness, it is adaptable to each age groups, have application prospect widely after using.
Description
Technical field
The present invention relates to a kind of ink, particularly to a kind of modified form printing-ink.
Background technology
Ink can be used for routine office work or textile printing field, but traditional general ink do not have refresh oneself and generation bear from
The health-care effects such as son, user use when long produces taediumvitae, due to the function singleness of tradition ink, can not meet people
Multi-demands.
Summary of the invention
The deficiency existed for prior art, the user that the present invention is ink provides a kind of abnormal smells from the patient pure and fresh, has and refresh oneself
Effect and the ink of negative ion health effect, it is possible not only to discharge for a long time negative aeroion, purifies air, beneficially human body strong
Health；Also the multiple pathogenic bacterias such as staphylococcus, escherichia coli, gram-positive bacteria and fungus are had certain suppression, killing action；With
Time fragrant odour, pure and fresh soothe the spirit, pressure of releiving, also can expelling mosquito, human body will not be produced harmful effect, have widely
Application prospect.
It is an object of the invention to be achieved through the following technical solutions:
A kind of modified form printing-ink, it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight
Part, bisphenol-A 19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine
3.3 weight portions, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surface
Activating agent compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, institute
The pigment stating mill base is high-carbon black pigment, and the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanium
Stone, fluorite, tourmaline, gahnite are by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and lithium electricity
Gas stone is by weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, and wherein said essential oil of traditional Chinese medicine is by such as
Lower step is prepared from,
S1, take Fructus Quisqualis 35 weight portion and clean, naturally dry, be subsequently placed in 90 DEG C of frying pans stir-fry extremely savory effusion, then spray
Drench deionized water 17 weight portion, be placed in less than 60 DEG C drying, water content≤6.5% in constant temperature oven；
S2, Pericarpium Citri Reticulatae 18 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality 3.7
Times, to put into and pot steams thoroughly, take out, dry, the concentration of saline is 27%；
S3, by Aloe 15.5 weight portion, lavandula angustifolia 12 weight portion, Herba Anemones Hupehensis 4.5 weight portion, Fructus Schisandrae Chinensis 1 weight portion, sweet horse
Yu Lan 0.75 weight portion decontamination, puts into together with crude drug made with step S1 and S2 and is crushed to 60 mesh in super micron mill, system
Obtain crude drug powder, standby；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, directly separating
Still outlet triangular flask collects volatile oil A, standby；
S5, by Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 15.5 weight portion, Rhizoma Acori Graminei 4.5 weight portion, Herba Menthae 1 weight
Amount part, XIAONIE 1 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 70 mesh, and then adding deionized water, to soak 6 little
Time, amount of water by 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S6, Traditional Chinese drug mixture step S5 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate and be dried, i.e. prepares volatile oil B, standby；
S7, made to step S4 and S6 volatile oil A and volatile oil B are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Radix Paeoniae Alba quintessence oil, Juniperus rigida Sieb.et Zucc. quintessence oil, propolis quintessence oil, Peppermint essential oil and cypress quintessence oil, be sufficiently stirred for 35 minutes, stands 30 minutes, fills
Stirring is divided to mix well, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Radix Paeoniae Alba quintessence oil, Juniperus rigida Sieb.et Zucc. quintessence oil, propolis essence
The mass ratio of oil, Peppermint essential oil and cypress quintessence oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the crude drug powder of step S3, also include Herba Origani oil 1.3 weight portion and spend in vain
Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step S5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4
Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step S7 also includes Eucalyptus oil 0.3 weight portion.
Equipment, raw material and method involved in the present invention, is equipment, raw material and method that the industry usually uses,
This repeats no more.
The most each essential oil component must be sufficiently mixed with surfactant, slow releasing agent, to reach slow release effect, each quintessence oil and
The addition of anion natural mineral matter powder must be appropriate, not only antibiotic and sterilizing, moreover it is possible to stable emotion, so to the not normal heart
Reason state has the effect in front, can purify, pacify soul, can alleviate angry and beaten sensation, makes the people can be with the flat gas of the heart
With ground in the face of life, because its energy centre of equilibrium is neural, thus helpful to alarmed and dejected state, also have the most flat
Quiet with releive function, insomniac is had goodish relax to put console with spirit, for pacify hot-tempered enter or moody temper have
Goodish effect, can improve work efficiency.
The present invention with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine and repeatedly verifies, gives full play to respectively
Group weight portion synergism, the most each Chinese medicinal components brief introduction is as follows.
Fructus Quisqualis: for the most famous anthelmintic, at least have more than 1600 year history in treatment children's's sufferer, can
Anti-dermatophyte, Gan Wen, returns taste warp.Expelling intestinal worms and removing food stagnancy.
Rhizoma Acori Graminei: its flower, stem aromatic flavor, has the effect had one's ideas straightened out, eliminate the phlegm, dissipate wind, and epidemic disease of can dispelling Fructus Alpiniae Oxyphyllae, building body can
Make spice or mosquito dispersing.
Aloe: " Bencao Jingshu ": Aloe, cold can heat extraction, hardship can expel the heat-evil dampness, bitter can parasite killing, to bitter to cold, therefore be heat extraction
The key medicine of parasite killing.Its main hot blast is unhappy, steam between the breast side of body, improving eyesight, relieving palpitation, and children epilepsy cool breeze is treated five kinds of child malnutrition, killed three worm persons, heat
Then giving birth to wind, heat energy makes people unhappy, and between evanescence of heat then wind heat unhappiness and chest and diaphragm, steam is explained by oneself.
Lavandula angustifolia can remove ant, except roach, acaricide, the when of being placed under wardrobe, medicated pillow, not only can replace camphor ball, moreover it is possible to stay
The fragrance of one people that oozes lower, research finds, lavandula angustifolia has obvious antibacterial action, and the linalool contained in lavandula angustifolia is lavandula angustifolia
Antibacterial main component, it can suppress 17 kinds of antibacterials (including gram-negative bacteria and gram-positive bacteria), the life of 10 kinds of funguses
Long.
Herba Anemones Hupehensis: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature,
Slightly poisonous." removing toxic substances, evacuation of pus granulation promoting, dissipating blood stasis of subsiding a swelling, have and kill maggot, wriggler, change long-pending, detumescence, dissipating blood stasis, control stubborn dermatitis, tinea alba, malaria
Disease, infantile malnutrition, dysentery, carbuncle furuncle swells, scrofula, traumatic injury.
Fructus Schisandrae Chinensis: for Magnoliacea plant, have antibacterial action, to anthrax bacillus, staphylococcus aureus, white grapes ball
Bacterium, Bacillus typhi, vibrio cholera etc. all have inhibitory action.
Origanum majorana: can improve that mood is depressed and addictive disease, especially effective to liberal-mindedness and vigorous endurance stress symptom, can expand blood vessel,
Blood pressure lowering, alleviate and burden, help to eliminate cardiopalmus, have the nerve of excellence to pacify and calm function.
Cortex ulmi pumilae: for dry bark or the root bark of Ulmaceae, sweet, flat, nontoxic；Diuretic, treating stranguria, detumescence, for urine
Obstructed, stranguria with turbid discharge, edema, carbuncle carbuncle on the back, erysipelas, scabies.
Lignum Aquilariae Resinatum: " Compendium of Materia Medica " record wood have strong antibacterial efficacy, fragrance enters spleen, clear god regulates the flow of vital energy, tonifying five ZANG-organs, cough-relieving
Reduce phlegm, warming the stomach warming the spleen, ventilation analgesic therapy, can be used as medicine, be first-class medical material superfine product.
Lignum cinnamomi camphorae: aiphyllium, bark yellowish-brown, there is irregular longitudinal crack, on the south main product the Changjiang river and various places, southwest.Winter
Cut down trees and split broken or be sawn into bulk, dry or air-dry.Timber bulk is not of uniform size, surface red brown to burgundy, and transverse section is visible
Annual ring.Matter is heavily hard.Having strong Camphora fragrance, taste is refrigerant, has pungent sense, warm in nature, acrid in the mouth；Only sensible can ward off dirty, warming middle-JIAO
Bitterly, dampness removing parasite killing.
Rhizoma Acori Graminei: its flower, stem aromatic flavor, has the effect had one's ideas straightened out, eliminate the phlegm, dissipate wind, and epidemic disease of can dispelling Fructus Alpiniae Oxyphyllae, building body can
Make spice or mosquito dispersing.
Herba Menthae: for the dry aerial parts of labiate Herba Menthae, dispelling wind and heat pathogens, the clear profit head, sore-throat relieving rash, soothing the liver row
Gas.
XIAONIE: evergreen shrubs, high 1-2 rice.Old branch is cylindrical, lead, and sprout is faint yellow, tool rib groove and wart point；Stem thorn
Three bifurcateds, slotless, long 1.5-2 centimetre, homochromy with branch.Cure mainly: remove steam in trusted subordinate, kill parasites, control metrorrhagia.Release name tiller, mountain
Punica granatum L..Abnormal smells from the patient: hardship, Great Cold, nontoxic.
Radix Paeoniae Alba quintessence oil: have the effect such as blood-supplementing blood-nourishing, astringing YIN to stop sweating, wherein paeoniflorin has antibacterial, antipyretic, antiinflammatory, changes
Kind myocardial nutritional flow, expansion blood vessel, antagonism acute myocardial ischemia, suppression platelet aggregation, calmness, analgesia, spasmolytic, anti-burst
Infections, the effect of regulation blood glucose.Decoct can suppress dysentery bacterium, streptococcus pneumoniae, escherichia coli, Bacillus typhi, hemolytic hammer
Bacterium, bacillus pyocyaneus etc..
Juniperus rigida Sieb.et Zucc. quintessence oil: there is purification air, mosquito-proof insect bite, antibacterial, rheumatism, antitetanic effect, it may have calm
Refresh oneself, encourage emotion, purify the state of mind and the function of release soul, it is possible to make people's body and mind relaxed and comfortable, it may have the effect promoted the sexual maturity；Separately
Outward, the function of its toxin expelling is the most famous, and it can discharge the toxin of accumulation, purifies intestinal mucosa.
Propolis quintessence oil: the antibacterial antiviral efficacy of energy, recent studies proves, enriching and the biological work of uniqueness contained by propolis
Property material so that it is there is the several functions such as antibacterial, antiinflammatory, antipruritic, antioxidation, enhancing immunity.
Peppermint essential oil: not only fragrance, moreover it is possible to driving away mosquito, has contraction blood capillary simultaneously, gets rid of vivotoxin, improve wet
Rash, tinea, releive itch, inflammation and burning, soft skin, eliminate blackhead, be of value to oiliness hair quality and skin quality, purify air
And the effect refreshed oneself.
Cypress quintessence oil: have a succinum taste charming as wooden and face cream, rheumatism, antibacterial, spasmolytic, suppression diaphoresis, convergence,
Promote to scab, except bromhidrosis, diuresis, bring down a fever, stop blooding, sharp liver, parasite killing, rehabilitation, calmness, astringing to arrest bleeding, benefit body, vasoconstrictive.Disappear
Except fatigue, indignation of releiving emotion, alleviate heart anxiety and pressure, purification of the mind.
Herba Origani oil: the herb of Labiatae origanum Adeps Bovis seu Bubali ORIGZNUM VUL-GAREL., has another name called dysentery relieving chaste tree careless, wild
The ground such as mustard symbol name, have heat clearing away, removing dampness, drive away summer heat, induce sweat, the sterilization of regulating the flow of vital energy extremely strong, bacteriostasis, the volatilization extracted from Adeps Bovis seu Bubali
Oil, to 31 kinds of common cause enteritis antibacterials and shigella flexneri, is the pure Chinese medicine additive most with broad-spectrum antiseptic.
Herba et Flos Pyrethri Cinerariifolii: Tanacetum vulgare L belongs to the general designation of (Tanacetum) several plants, removing dampness and killing parasites, kills pubic louse, head louse, body
Louse, flea, effect except mosquito parasite killing.
Borneolum Syntheticum: pungent, bitter, cool.Having refreshment of having one's ideas straightened out, heat clearing away dissipates poison, improving acuity of vision and removing nebula.Cure mainly calentura unconsciousness due to high fever, middle wind-phlegm
Fainting infantile convulsion, heat-damp in summer blinds clear key, and sore throat is deaf, and aphtha tooth swells, carbuncle sore infantile malnutrition hemorrhoid, conjunctival congestion and swelling pain, pterygium.
Folium Nelumbinis: for the leaf of nymphaeaceae plant lotus, have the effect of heat-clearing and toxic substances removing, removing heat from blood, hemostasis.There is clearing away summer-heat and eliminating dampness, rise and send out clearly
The effects such as sun, cooling blood for hemostasis.
Eucalyptus oil: one of most common and widest quintessence oil of purposes, has good health-care effect, helps focused attention
Power.Can effectively alleviate sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory system diseases.There is good resisting
Bacterium and sterilization idiocratic, in some certain food, Eucalyptus oil is also as fragrance component.This quintessence oil is carried at whilst on tour, permissible
Effectively resist mosquito bite and insect bite, treat skin measles.It it is good anophelifuge.Mixing with water can become a kind of and simple and effective disappear
Toxic agent.
Beneficial effects of the present invention:
The present invention provides a kind of abnormal smells from the patient pure and fresh for user, has stimulating effect and the ink of negative ion health effect, and it is not only
Negative aeroion can be discharged for a long time, purify air, beneficially health；Also thin to staphylococcus, escherichia coli, Grain-positive
The multiple pathogenic bacteria such as bacterium and fungus have certain suppression, killing action；Fragrant odour simultaneously, pure and fresh soothes the spirit, and pressure of releiving also can drive
Catch up with mosquito, human body will not be produced harmful effect, it is adaptable to each age groups, its appropriate add other function ingredients after still
Original effect and quality can be kept.
1, tourmaline is a kind of silicate mineral, and its chemical formula is Na (Mg, Fe, Mn, Li, Al) 3Al6 (Si6O18)
(Bo3) 3 (OH, F) 4, it contacts with hydrone under electrostatic field, and hydrone just can be ionized into hydrion (H+) and hydrogen-oxygen
Radical ion (OH-), hydroxide ion and water molecules form basic hydroxide group anion (H2O OH-), be " air bear from
Son ", current scientific research proves: anion can not only facilitate human body synthesis and vitamin storage, strengthening and the life of human activin
Reason activity, has highly important impact to the vital movement of human body and other biological, is referred to as " air vitamin ".Anion
Active adsorption indoor harmful substance, such as the construction and decoration harmful substance such as formaldehyde, toluene, not only self does not increase pollution, Er Qieqing
Purifying room air, is inherently eliminated construction and decoration syndrome, ensures that health is unaffected.
2, the Chinese medicine ingredients contained in the present invention, not only thin to staphylococcus, tubercule bacillus, bacillus pyocyaneus, Grain-negative
The multiple pathogenic bacteria such as bacterium and gram-positive bacteria and fungus have certain suppression, killing action；Fragrant odour simultaneously, character is gentle,
Pure and fresh soothe the spirit, help hormone secretion, the effect of anxiety of releiving, also there is certain mosquito-repelling effect simultaneously, more it is essential that
The life-time service present invention will not produce harmful effect to human body, it is adaptable to each age groups, before having application widely
Scape.
Detailed description of the invention
Embodiment.
A kind of modified form printing-ink, it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight
Amount part, bisphenol-A 19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine
3.3 weight portions, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surface
Activating agent compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, institute
The pigment stating mill base is high-carbon black pigment, and the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanium
Stone, fluorite, tourmaline, gahnite are by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and lithium electricity
Gas stone is by weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, and wherein said essential oil of traditional Chinese medicine is by such as
Lower step is prepared from,
S1, take Fructus Quisqualis 35 weight portion and clean, naturally dry, be subsequently placed in 90 DEG C of frying pans stir-fry extremely savory effusion, then spray
Drench deionized water 17 weight portion, be placed in less than 60 DEG C drying, water content≤6.5% in constant temperature oven；
S2, Pericarpium Citri Reticulatae 18 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality 3.7
Times, to put into and pot steams thoroughly, take out, dry, the concentration of saline is 27%；
S3, by Aloe 15.5 weight portion, lavandula angustifolia 12 weight portion, Herba Anemones Hupehensis 4.5 weight portion, Fructus Schisandrae Chinensis 1 weight portion, sweet horse
Yu Lan 0.75 weight portion decontamination, puts into together with crude drug made with step S1 and S2 and is crushed to 60 mesh in super micron mill, system
Obtain crude drug powder, standby；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, directly separating
Still outlet triangular flask collects volatile oil A, standby；
S5, by Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 15.5 weight portion, Rhizoma Acori Graminei 4.5 weight portion, Herba Menthae 1 weight
Amount part, XIAONIE 1 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 70 mesh, and then adding deionized water, to soak 6 little
Time, amount of water by 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S6, Traditional Chinese drug mixture step S5 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate and be dried, i.e. prepares volatile oil B, standby；
S7, made to step S4 and S6 volatile oil A and volatile oil B are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Radix Paeoniae Alba quintessence oil, Juniperus rigida Sieb.et Zucc. quintessence oil, propolis quintessence oil, Peppermint essential oil and cypress quintessence oil, be sufficiently stirred for 35 minutes, stands 30 minutes, fills
Stirring is divided to mix well, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Radix Paeoniae Alba quintessence oil, Juniperus rigida Sieb.et Zucc. quintessence oil, propolis essence
The mass ratio of oil, Peppermint essential oil and cypress quintessence oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the crude drug powder of step S3, also include Herba Origani oil 1.3 weight portion and spend in vain
Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step S5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4
Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step S7 also includes Eucalyptus oil 0.3 weight portion.
Using air ion static method of testing to test the ink in this above-described embodiment, anion burst size is at 430-650
Individual/m3, and sustained release negative aeroion, it is more beneficial for purifying for a long time air, reaches the basic demand of health of people.
Reference examples.
Colour carbon black 20g, phenol 11g, glycerol 4g, BTA 3g, triethanolamine 1g, triethylamine 3g, sodium bicarbonate
5g, polyoxyethylene groups ethers nonionic fluorocarbon surfactant 1.5g, slow releasing agent 0.4g, Origanum majorana quintessence oil 0.6g, Semen Tritici aestivi
Bud quintessence oil 0.5g, Herba Lysimachiae foenum-graeci quintessence oil 0.5g, Radix Paeoniae Alba quintessence oil 0.4g, cypress quintessence oil 0. 4g, eucalyptus quintessence oil 0.4g, Folium Artemisiae Argyi essence
Oil 0. 4g, Peppermint essential oil 0.4g, deionized water 75g.
Using air ion static method of testing to test the ink in this above-mentioned reference examples, anion burst size is at 0/m3,
Not there is the function of release negative aeroion.
(1) obtained essential oil of traditional Chinese medicine being carried out acute toxicity test, result is as follows:
1. Mouse oral acute toxicity test: the LD50 of Mouse oral essential oil of traditional Chinese medicine is 383.55g/kg, 95% credible be limited to
294.68g/kg～499.31g/kg.And the toxicity criterion of air freshener is: Mouse oral anxious poison LD50 >=5g/
Kg, it is determined that for nontoxic.The LD50 of this essential oil of traditional Chinese medicine is higher than 76 times of nontoxic standard, therefore, it is determined that be nontoxic.
2. chmice acute toxicity on inhalation test: it is 24863.99g/m3 that chmice acute sucks the LC50 of essential oil of traditional Chinese medicine, 95%
Credible be limited to 16837.34g/m3～33387.46g/m3.And the toxicity criterion of air freshener is: chmice acute
Suck (2h) LC50 ＞ 10000mg/m3, the nontoxic level in true border.The LC50 of this essential oil of traditional Chinese medicine is higher than the 2486 of nontoxic standard
Times, therefore, it is determined that be nontoxic.
Obtained essential oil of traditional Chinese medicine is through inspection, and its fragrance, color and luster, refraction index, relative density, arsenic content, heavy metal contain
Amount, pH value all meet the requirement of national standard.
(2) above-mentioned ink anion burst size result such as table 1 is checked.
(3) repelling effect test.
Contrast test is carried out with the repelling effect of ink in above-described embodiment, test according to common ink of the prior art
Data are shown in Table 2.
Conclusion: the ink in the embodiment of the present invention has certain repelling effect.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, common for art
For technical staff, can also make other changes in different forms on the basis of the above description, here without also
Cannot all of embodiment be given exhaustive, all within the spirit and principles in the present invention, any amendment of being made, equivalent are replaced
Change, improvement etc., within being still included in protection scope of the present invention.
Claims (1)
1. a modified form printing-ink, it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight
Part, bisphenol-A 19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine
3.3 weight portions, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surface
Activating agent compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, institute
The pigment stating mill base is high-carbon black pigment, and the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanium
Stone, fluorite, tourmaline, gahnite are by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and lithium electricity
Gas stone is by weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, and wherein said essential oil of traditional Chinese medicine is by such as
Lower step is prepared from,
S1, take Fructus Quisqualis 35 weight portion and clean, naturally dry, be subsequently placed in 90 DEG C of frying pans stir-fry extremely savory effusion, then spray
Drench deionized water 17 weight portion, be placed in less than 60 DEG C drying, water content≤6.5% in constant temperature oven；
S2, Pericarpium Citri Reticulatae 18 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality 3.7
Times, to put into and pot steams thoroughly, take out, dry, the concentration of saline is 27%；
S3, by Aloe 15.5 weight portion, lavandula angustifolia 12 weight portion, Herba Anemones Hupehensis 4.5 weight portion, Fructus Schisandrae Chinensis 1 weight portion, sweet horse
Yu Lan 0.75 weight portion decontamination, puts into together with crude drug made with step S1 and S2 and is crushed to 60 mesh in super micron mill, system
Obtain crude drug powder, standby；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction
Pressure power 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, directly separating
Still outlet triangular flask collects volatile oil A, standby；
S5, by Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 15.5 weight portion, Rhizoma Acori Graminei 4.5 weight portion, Herba Menthae 1 weight
Amount part, XIAONIE 1 weight portion is cleaned and is dried, and puts in super micron mill together and is crushed to 70 mesh, and then adding deionized water, to soak 6 little
Time, amount of water by 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S6, Traditional Chinese drug mixture step S5 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation
Liquid is 2:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate and be dried, i.e. prepares volatile oil B, standby；
S7, made to step S4 and S6 volatile oil A and volatile oil B are mixed and mixes well prepared miscella, then be sequentially added into while stirring
Radix Paeoniae Alba quintessence oil, Juniperus rigida Sieb.et Zucc. quintessence oil, propolis quintessence oil, Peppermint essential oil and cypress quintessence oil, be sufficiently stirred for 35 minutes, stands 30 minutes, fills
Stirring is divided to mix well, filtering and impurity removing, obtain essential oil of traditional Chinese medicine, wherein, described miscella and Radix Paeoniae Alba quintessence oil, Juniperus rigida Sieb.et Zucc. quintessence oil, propolis essence
The mass ratio of oil, Peppermint essential oil and cypress quintessence oil is 1.3:0.4:0.75:0.6:0.5:0.3.
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Application publication date: 20161116 |