CN105504992A - Covering type textile ink jet printing pigment ink - Google Patents

Covering type textile ink jet printing pigment ink Download PDF

Info

Publication number
CN105504992A
CN105504992A CN201610093678.8A CN201610093678A CN105504992A CN 105504992 A CN105504992 A CN 105504992A CN 201610093678 A CN201610093678 A CN 201610093678A CN 105504992 A CN105504992 A CN 105504992A
Authority
CN
China
Prior art keywords
weight part
oil
essential oil
traditional chinese
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610093678.8A
Other languages
Chinese (zh)
Inventor
魏本武
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201610093678.8A priority Critical patent/CN105504992A/en
Publication of CN105504992A publication Critical patent/CN105504992A/en
Priority to CN201610723008.XA priority patent/CN106336735A/en
Priority to CN201610735659.0A priority patent/CN106189513A/en
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/30—Inkjet printing inks
    • C09D11/38—Inkjet printing inks characterised by non-macromolecular additives other than solvents, pigments or dyes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/30—Inkjet printing inks
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/30—Inkjet printing inks
    • C09D11/32—Inkjet printing inks characterised by colouring agents
    • C09D11/322—Pigment inks
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/645—Aliphatic, araliphatic or cycloaliphatic compounds containing amino groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/651—Compounds without nitrogen
    • D06P1/65106—Oxygen-containing compounds
    • D06P1/65118—Compounds containing hydroxyl groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D06P1/67333—Salts or hydroxides
    • D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/30—Ink jet printing
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Abstract

The invention discloses covering type textile ink jet printing pigment ink. The covering type textile ink jet printing pigment ink can release negative air ions for a long time, purify air and be beneficial to human health, can further have certain inhibition and killing functions on various bacteria and fungi such as staphylococcus, escherichia coli and gram-positive bacteria, is fragrant in smell, refreshing and capable of calming the mind, relieving pressure and leaving lasting aroma after being used, has the health care effects of refreshing and restoring consciousness and eliminating fatigue, is suitable for people of all ages and has quite wide application prospect.

Description

A kind of covering type textile inkjet printing paint ink
Technical field
The present invention relates to a kind of ink, particularly one covering type textile inkjet printing paint ink.
Background technology
Ink can be used for routine office work or textile printing field, but traditional general ink does not have refreshes oneself and produces the health-care effects such as negative ion, user's use when long produces taediumvitae, due to the function singleness of conventional inks, can not meet the multi-demands of people.
Summary of the invention
For the deficiency that prior art exists, the user that the present invention is ink provides a kind of smell pure and fresh, has the ink of stimulating effect and negative ion health effect, and it not only can release air negative ion for a long time, purifies air, is beneficial to HUMAN HEALTH; Also there are certain suppression, killing action to the multiple germs such as staphylococcus, intestinal bacteria, gram-positive bacteria and fungi; Simultaneously fragrant odour, pure and freshly soothes the spirit, pressure of releiving, also can expelling mosquito, can not produce detrimentally affect, have application prospect widely to human body.
The object of the invention is to be achieved through the following technical solutions:
A kind of covering type textile inkjet printing paint ink, it is characterized in that: be made up of according to parts by weight following component: dispersible pigment color paste 23 weight part, dihydroxyphenyl propane 19 weight part, glycerine 4.5 weight part, anhydrous sodium sulphate 2.3 weight part, trolamine 2.7 weight part, triethylamine 3.3 weight part, acetone 3.6 weight part, two thiocarbamate 0.25 weight part, active mineral matter powder 1.7 weight part, surfactant blend 1.2 weight part, sustained release dosage 0.55 weight part, essential oil of traditional Chinese medicine 3.85 weight part, deionized water 62 weight part, the median size of described dispersible pigment color paste is 75nm, described active mineral matter powder is germanite, fluorite, tourmalinite, zinc spinel is by weight the mixture of 2.5:3:3.7:2, wherein tourmalinite is dravite and the elbaite mixture by weight 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is prepared from as follows,
S1, get rhamnus crenata sieb.et zucc. 35 weight part and clean, naturally dry, be then placed in 90 DEG C of frying pans and fry extremely savory effusion, then Air washer 17 weight part, be placed in constant temperature oven less than 60 DEG C oven dry, water content≤6.5%;
S2, Spica Prunellae 12.5 weight part to be cleaned, puts into salt solution and soak 3.5 hours, the salt water yield by 3.7 times of immersions spice quality, put into pot and steam thoroughly, taking-up, dry, the concentration of salt solution is 27%;
S3, by honeycomb 12 weight part, lavandula angustifolia 15.5 weight part, Hupeh Anemone Herb 4.5 weight part, Moschus 4.5 weight part, peppermint 1 weight part, Rosmarinus officinalis 1 weight part, sweet marjoram 0.75 weight part, grane ambra 0.65 weight part decon, drops in supper micron mill and is crushed to 60 orders together with the made bulk drug of step S1 and S2, obtained bulk drug powder, for subsequent use;
S4, dropped into by bulk drug powder obtained in step S3 in the extraction kettle of supercritical carbon dioxide extraction apparatus, regulate extracting pressure 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m 3/ h, dynamic extraction 2.5h, directly collect volatile oil A at separating still outlet triangular flask, for subsequent use;
S5, by Cortex ulmi pumilae 8.5 weight part, agalloch eaglewood 2.5 weight part, camphorwood 35-40 weight part, the Radix Astragali 1 weight part is cleaned and is dried, and drops in supper micron mill together and is crushed to 70 orders, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersion bulk drug quality, dispersed with stirring is mixed well, obtained Traditional Chinese drug mixture, for subsequent use;
S6, the Traditional Chinese drug mixture obtained by step S5 decoct 2 hours in 80 DEG C, and collect distillate, and add extracted with diethyl ether, the volume ratio of distillate and ether is 2:1, gets upper oil phase, then adds anhydrous sodium sulfate drying, and namely obtained volatile oil B, for subsequent use;
S7, by made for step S4 and S6 volatile oil A and volatile oil B mixing mix well obtained mixing oil, add needle juniper essential oil, Moschus essential oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene while stirring successively again, abundant stirring 35 minutes, leave standstill 30 minutes, abundant stirring is mixed well, and filtering and impurity removing obtains essential oil of traditional Chinese medicine, wherein, the mass ratio of described mixing oil and needle juniper essential oil, Moschus essential oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the bulk drug powder of step S3, wild marjoram oil 1.3 weight part and pyrethre 1.5 weight part is also included.
In a preferred embodiment, in the Traditional Chinese drug mixture of step S5, also include borneol 0.6 weight part and lotus leaf 0.4 weight part.
In a preferred embodiment, in the essential oil of traditional Chinese medicine of step S7, Oil of Eucalyptus 0.3 weight part is also included.
Equipment involved in the present invention, raw material and method, be equipment, raw material and method that the industry usually uses, do not repeat them here.
Wherein each essential oil component must and tensio-active agent, sustained release dosage fully mixes, to reach slow release effect, the addition of each essential oil and negative ion natural mineral matter powder must be appropriate, not only antibiotic and sterilizing, mood can also be stabilized, so there is the effect in front to not normal psychological condition, can purify, pacify soul, indignation and beaten sensation can be alleviated, make people can even-tempered and good-humouredly in the face of life, because its energy centre of equilibrium is neural, so helpful to alarmed and dejected state, also significantly tranquil and function of releiving is had, goodish easypro putting is had to console with spirit to insomniac, for pacify hot-tempered enter or moody temper have goodish effect, can increase work efficiency.
The present invention is with reference to modern Chinese herbal medicine pharmacological research, and from the drug screening of existing Chinese medicine with repeatedly verify, give full play to each group of weight part and act synergistically, wherein each traditional Chinese medicinal components brief introduction is as follows.
Rhamnus crenata sieb.et zucc.:: machaka or dungarunga, Gen Pi or complete stool are used as medicine, and property is flat, bitter, dry, sterilization, desinsection.
Spica Prunellae: there is effect that is clearing heat and detoxicating, cooling blood for hemostasis, all have certain restraining effect to streptococcus aureus, beta hemolytic streptococcus, intestinal bacteria, Corynebacterium diphtheriae, dysentery bacterium, diphtheria corynebacterium, anthrax bacillus, Pseudomonas aeruginosa, dysentery bacterium, Corynebacterium diphtheriae, vibrio cholerae, intestinal bacteria, Pseudomonas aeruginosa and staphylococcus, suis and Bacillus tuberculosis.
Honeycomb: the lair picking up from honeybee, effect: dispel the wind, attacks poison, desinsection, pain relieving, antianaphylaxis, there is deactivation to hepatitis B surface antigen(HBsAg), also have very strong restraint to streptococcus aureus, Pseudomonas aeruginosa, intestinal bacteria, dysentery bacterium, Corynebacterium diphtheriae and proteus vulgaris etc.; Also restraining effect is had to fungies such as Aspergillus fumigatus, flavus, eggplant sickle bacterium, leukonids.
Lavandula angustifolia can remove ant, except roach, except mite, when being placed under wardrobe, pillow, not only mothball can be replaced, the fragrance of one people that oozes can also be left, research finds, lavandula angustifolia has obvious anti-microbial effect, and the phantol contained in lavandula angustifolia is the antibacterial main component of lavandula angustifolia, and it can suppress the growth of 17 kinds of bacteriums (comprising gram-negative bacteria and gram-positive bacteria), 10 kinds of fungies.
Hupeh Anemone Herb: 1. " Shaanxi herbal medicine ": " bitter, cool, slightly poisonous." 2. " herbal medicine is commonly used in Sichuan ": " and toil, temperature, slightly poisonous." removing toxic substances, apocenosis myogenic, the Sweeling-eliminating medicine powder stasis of blood, has and kills maggot, wriggler, eliminate indigestion, detumescence, and the loose stasis of blood, controls stubborn dermatitis, the favus of the scalp, malaria, infantile malnutrition, dysentery, and carbuncle furuncle sore swells, scrofula, wound.
Moschus: have and have one's ideas straightened out, wards off dirty, dredging collateral, effect of the loose stasis of blood; Control apoplexy, coma due to blocking of the respiratory system, frightened epilepsy, middle evil is unhappy, the trusted subordinate sudden and violent Tong ， Disorder lump in the abdomen hypochondriac lump, wound, swollen ulcer drug." herbal classic ": master wards off bad odor, a kind of malaria, epilepsy convulsion, goes three worms.
Peppermint: be the dry aerial parts of labiate peppermint, dispelling wind and heat pathogens, the clear sharp head, relieve sore throat promoting eruption, soothing the liver promoting the circulation of qi.
Rosmarinus officinalis: have tranquilizing and allaying excitement, restoring consciouness effect, all have certain curative effect to maldigestion and stomachache, have calmness, diuretic properties, also can be used for the various diseases such as Cure for insomnia, palpitaition, headache, maldigestion, external application can treat wound and sacroiliitis.Also there is strong heart, promote metabolism, promote the effects such as the blood circulation of peripheral vessel.
Sweet marjoram: the depressed and addictive disease of mood can be improved, especially effective to liberal-mindedness and vigorous endurance stress symptom, can vasodilation, hypotensive, alleviate and burden, help to eliminate palpitaition, have excellent nerve to pacify and calm function.
Grane ambra: be the most lasting spices of lasting, any one spices all can not compare favourably with it in the world, have the saying of " perfume and the life of imperial saliva coexist ".Compendium of Material Medica is carried: can invigorate blood circulation, beneficial marrow, supporing yang road, promoting blood circulation, resolving phlegm and relieving asthma; A lump in the abdomen causing distension and pain; Trusted subordinate's pain; Coma; Liao Yongyan: relieving stranguria by diuresis, loose Disorder knot, knot of cooling down, by labor worm.
Cortex ulmi pumilae: be dry bark or the root skin of Ulmaceae is sweet, flat, nontoxic; Li Shui, treating stranguria, detumescence, for urinary obstruction, stranguria with turbid discharge, oedema, ulcer carbuncle on the back, erysipelas, mange.
Agalloch eaglewood: " Compendium of Materia Medica " records that wood has strong antibacterial efficacy, fragrance enters spleen, clear god regulates the flow of vital energy, tonifying the five internal organs, relieving cough and reducing sputum, warm stomach temperature spleen, analgesic therapy of ventilating, can be used as medicine is first-class medicinal material superfine product.
Camphorwood: aiphyllium, bark tawny, has irregular longitudinal crack, on the south main product the Changjiang river and southwestern various places.Cut down trees winter and split broken or be sawn into bulk, to dry or air-dry.Timber bulk is not of uniform size, and surface red is brown to burgundy, the visible annual ring in transverse section.Matter is heavily hard.Have strong camphor fragrance, taste is refrigerant, has pungent sense, and warm in nature, taste is pungent; Sensiblely can ward off dirty, warming middle-JIAO to relieve pain, dampness removing desinsection.
The Radix Astragali: have another name called continuous stilbene.Perennial herb, the history of medicinal existing more than 2000 year so far of the Radix Astragali, it has enhancing body immunologic function, protects the liver, diuresis, anti-ageing, anti-stress, step-down and anti-microbial effect more widely.
Needle juniper essential oil: have purify air, anti-mosquito worm Cheng stings, antibacterial, rheumatism, antitetanic effect, also there is the calm function refreshing oneself, encourage mood, the purification state of mind and discharge soul, people's body and mind can be allowed relaxed and comfortable, also there is the effect of promoting the sexual maturity; In addition, the function of its toxin expelling is very famous, and it can discharge the toxin of accumulation, purification intestinal mucosa.
Moschus essential oil: have light fragrance, has and releives, calms, removes melancholy and anti-dejected effect, increase romantic mood, naturally fragrance and bring warm impression by body and mind.
Geranium Essential: there is hemostasis, vasoconstriction, asthma, liver and expelling toxin, gallbladdergallstonecholetithiasis, kidney toxin expelling, urinary stone disease, diuresis, sore muscle, oily skin, aging skin activates, bleb, ochrodermia, fat-reducing, promotes to scab, eczema, to burn sunburn, tinea, menstruation has some setbacks, engorgement of breasts inflammation, alleviate melancholy uneasy, there is deodorizing, antibacterial, the effect of sterilization.
Eucalyptus quintessence oil has effect of anti-infective, antiviral, sterilization, desinsection, deodorizing, antiviral effect, the most effective to respiratory tract disease, can relax inflammation phenomenon, make nasal mucosa comfortable; There is calm effect to mood simultaneously, can sanity be made, focus one's attention on.
P-Cymene: all have anti-microbial effect to 10 kinds of Gram-positive aerophils such as anthrax bacillus, Alpha-hemolytic streptococcus, B-Streptococcus hemolyticus, diphtheria corynebacterium, bacillus pseudodiphthericus, lung diplococcoid, streptococcus aureus, Staphylococcus citreus, white Portugal Portugal coccus, Bacillus subtilus, also have bacteriostatic action for multiple pathomycete.
Wild marjoram oil: the herb of Labiatae origanum wild marjoram ORIGZNUMVUL-GAREL., have another name called the symbol name such as the ground that stops dysentery grass, wild catmint, there is heat-clearing, dampness elimination, drive away summer heat, induce sweat, regulate the flow of vital energy extremely strong sterilization, bacteriostatic action, the volatile oil extracted from wild marjoram, commonly causing enteritis bacterium and shigella flexneri to 31 kinds, is the pure Chinese medicine additive most with broad-spectrum antimicrobial.
Pyrethre: the general designation of chrysanthemum artemisia (Tanacetum) several plants, removing dampness and killing parasites, kills crab louse, head louse, body louse, flea, effect except mosquito desinsection.
Borneol: pungent is bitter, cool.There is inducing resuscitation of having one's ideas straightened out, the loose poison of heat-clearing, improving acuity of vision and removing nebula.Cure mainly pyreticosis unconsciousness due to high fever, apoplexy coma due to blocking of the respiratory system shies epilepsy, and summer-heat and damp hoodwinks key clearly, and larynx numbness is deaf, and aphtha tooth swells, sore carbuncle infantile malnutrition due to digestive disturbances or intestinalparasites hemorrhoid, conjunctival congestion with pain and swelling of the eye, pterygium.
Lotus leaf: be the leaf of nymphaeaceae plant lotus, has the effect of clearing heat and detoxicating, cool blood, hemostasis.There are the effects such as clearing summer-heat and damp, sending up the lucid YANG, cooling blood for hemostasis.
Oil of Eucalyptus: the most common and purposes one of essential oil the most widely, has good health-care effect, help to focus one's attention on.Effectively can alleviate sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory system diseases.Have good antibacterial and sterilization idiocratic, in some certain food, Oil of Eucalyptus is also as fragrance component.Carry this essential oil at whilst on tour, effectively can resist mosquito bite and insect bite, treatment skin measles.It is good anophelifuge.Mix with water and can become a kind of simple and effective sterilizing agent.
Beneficial effect of the present invention:
The present invention provides a kind of smell pure and fresh for user, has the ink of stimulating effect and negative ion health effect, and it not only can release air negative ion for a long time, purifies air, is beneficial to HUMAN HEALTH; Also there are certain suppression, killing action to the multiple germs such as staphylococcus, intestinal bacteria, gram-positive bacteria and fungi; Simultaneously fragrant odour, pure and freshly soothes the spirit, pressure of releiving, also can expelling mosquito, can not produce detrimentally affect, be applicable to each age groups to human body, its appropriate add other function ingredients after still can keep original effect and quality.
1, tourmalinite is a kind of silicate minerals, its chemical formula is Na (Mg, Fe, Mn, Li, Al) 3Al6 (Si6O18) (Bo3) 3 (OH, F) 4, it contacts with water molecules under electrostatic field, just water molecules can be ionized into hydrogen ion (H+) and hydroxide ion (OH-), hydroxide ion and water molecules form basic hydroxide group negative ion (H2OOH-), be " negative aeroion ", current scientific research proves: negative ion can not only facilitate human body to synthesize and vitamin storage, the physiological activity of strengthening and human activin, very important impact is had on the vital movement of human body and other biological, be called as " air VITAMIN ".The indoor objectionable impurities of negative ion active adsorption, as the construction and decoration such as formaldehyde, toluene objectionable impurities, not only self does not increase pollution, and Cress room air, fundamentally eliminates construction and decoration syndromes, ensures that HUMAN HEALTH is unaffected.
2, the traditional Chinese medicine ingredients contained in the present invention, not only has certain suppression, killing action to the multiple germs such as staphylococcus, tubercule bacillus, Pseudomonas aeruginosa, gram-negative bacteria and gram-positive bacteria and fungi; Simultaneously fragrant odour, character is gentle, pure and freshly soothes the spirit, and helps hormone secretion, the effect of anxiety of releiving, also has certain mosquito-repelling effect, more crucially simultaneously, life-time service the present invention can not produce detrimentally affect to human body, is applicable to each age groups, has application prospect widely.
Embodiment
Embodiment.
A kind of covering type textile inkjet printing paint ink, it is characterized in that: be made up of according to parts by weight following component: dispersible pigment color paste 23 weight part, dihydroxyphenyl propane 19 weight part, glycerine 4.5 weight part, anhydrous sodium sulphate 2.3 weight part, trolamine 2.7 weight part, triethylamine 3.3 weight part, acetone 3.6 weight part, two thiocarbamate 0.25 weight part, active mineral matter powder 1.7 weight part, surfactant blend 1.2 weight part, sustained release dosage 0.55 weight part, essential oil of traditional Chinese medicine 3.85 weight part, deionized water 62 weight part, the median size of described dispersible pigment color paste is 75nm, described active mineral matter powder is germanite, fluorite, tourmalinite, zinc spinel is by weight the mixture of 2.5:3:3.7:2, wherein tourmalinite is dravite and the elbaite mixture by weight 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is prepared from as follows,
S1, get rhamnus crenata sieb.et zucc. 35 weight part and clean, naturally dry, be then placed in 90 DEG C of frying pans and fry extremely savory effusion, then Air washer 17 weight part, be placed in constant temperature oven less than 60 DEG C oven dry, water content≤6.5%;
S2, Spica Prunellae 12.5 weight part to be cleaned, puts into salt solution and soak 3.5 hours, the salt water yield by 3.7 times of immersions spice quality, put into pot and steam thoroughly, taking-up, dry, the concentration of salt solution is 27%;
S3, by honeycomb 12 weight part, lavandula angustifolia 15.5 weight part, Hupeh Anemone Herb 4.5 weight part, Moschus 4.5 weight part, peppermint 1 weight part, Rosmarinus officinalis 1 weight part, sweet marjoram 0.75 weight part, grane ambra 0.65 weight part decon, drops in supper micron mill and is crushed to 60 orders together with the made bulk drug of step S1 and S2, obtained bulk drug powder, for subsequent use;
S4, dropped into by bulk drug powder obtained in step S3 in the extraction kettle of supercritical carbon dioxide extraction apparatus, regulate extracting pressure 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m 3/ h, dynamic extraction 2.5h, directly collect volatile oil A at separating still outlet triangular flask, for subsequent use;
S5, by Cortex ulmi pumilae 8.5 weight part, agalloch eaglewood 2.5 weight part, camphorwood 35-40 weight part, the Radix Astragali 1 weight part is cleaned and is dried, and drops in supper micron mill together and is crushed to 70 orders, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersion bulk drug quality, dispersed with stirring is mixed well, obtained Traditional Chinese drug mixture, for subsequent use;
S6, the Traditional Chinese drug mixture obtained by step S5 decoct 2 hours in 80 DEG C, and collect distillate, and add extracted with diethyl ether, the volume ratio of distillate and ether is 2:1, gets upper oil phase, then adds anhydrous sodium sulfate drying, and namely obtained volatile oil B, for subsequent use;
S7, by made for step S4 and S6 volatile oil A and volatile oil B mixing mix well obtained mixing oil, add needle juniper essential oil, Moschus essential oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene while stirring successively again, abundant stirring 35 minutes, leave standstill 30 minutes, abundant stirring is mixed well, and filtering and impurity removing obtains essential oil of traditional Chinese medicine, wherein, the mass ratio of described mixing oil and needle juniper essential oil, Moschus essential oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the bulk drug powder of step S3, wild marjoram oil 1.3 weight part and pyrethre 1.5 weight part is also included.
In a preferred embodiment, in the Traditional Chinese drug mixture of step S5, also include borneol 0.6 weight part and lotus leaf 0.4 weight part.
In a preferred embodiment, in the essential oil of traditional Chinese medicine of step S7, Oil of Eucalyptus 0.3 weight part is also included.
Use air ion static method of testing tests the ink in this above-described embodiment, and negative ion burst size is at 430-650/m 3, and sustained release negative aeroion, be more conducive to purifying air for a long time, reach the basic demand of health of people.
Reference examples.
Colour carbon black 20g, phenol 11g, glycerine 4g, benzotriazole 3g, trolamine 1g, triethylamine 3g, sodium bicarbonate 5g, polyoxyethylene groups ethers non-ionic type fluorocarbon surfactant 1.5g, sustained release dosage 0.4g, sweet marjoram essential oil 0.6g, wheat malt essential oil 0.5g, Herba Lysimachiae foenumgraeci quintessence oil 0.5g, RADIX PAEONIAE ALBA essential oil 0.4g, cypress essential oil 0.4g, eucalyptus quintessence oil 0.4g, P-Cymene 0.4g, Peppermint essential oil 0.4g, deionized water 75g.
Use air ion static method of testing tests the ink in this above-mentioned reference examples, and negative ion burst size is at 0/m 3, not there is the function of release air negative ion.
(1) carry out acute toxicity test to obtained essential oil of traditional Chinese medicine, result is as follows:
1. Mouse oral acute toxicity test: the LD50 of Mouse oral essential oil of traditional Chinese medicine is 383.55g/kg, 95% be crediblely limited to 294.68g/kg ~ 499.31g/kg.And the toxicity criterion of air freshener is: the anxious malicious LD50 >=5g/kg of Mouse oral, is judged to be nontoxic.The LD50 of this essential oil of traditional Chinese medicine, higher than 76 times of nontoxic standard, is therefore judged to be nontoxic.
2. chmice acute toxicity on inhalation test: it is 24863.99g/m3 that chmice acute sucks the LC50 of essential oil of traditional Chinese medicine, 95% be crediblely limited to 16837.34g/m3 ~ 33387.46g/m3.And the toxicity criterion of air freshener is: chmice acute sucks (2h) LC50 > 10000mg/m3, the nontoxic level in true border.The LC50 of this essential oil of traditional Chinese medicine, higher than 2486 times of nontoxic standard, is therefore judged to be nontoxic.
Obtained essential oil of traditional Chinese medicine is through inspection, and its fragrance, color and luster, refractive index, relative density, arsenic content, heavy metal content, pH value all meet the requirement of national standard.
(2) check above-mentioned ink performance test result as table 1:
(3) to the test improving the mental status.
Main method is that ink uses volunteer's experiment, recruit 60 people, use the ink in above-mentioned 2 kinds of embodiments respectively, by SCL-90 questionnaire (i.e. " Self-reporting inventory-SCL90 ", one of foremost Mental health test scale in the world), followed the tracks of by the use of continuous 1 week, judge the actual efficacy effect of the present invention in refreshing oneself, wherein 3 people are noninductive is subject to; 7 people experience general; 1 people thinks that this product is invalid for stimulating effect; Have 49 people to feed back this product and have effect of refreshing oneself preferably, the power that can warn is concentrated, and efficient is 81.67%.
(4) repelling effect test.
Repelling effect according to common ink of the prior art and above-described embodiment ink inside carries out contrast test, and test data is in table 2.
Conclusion: the ink in the embodiment of the present invention has good repelling effect.
The foregoing is only preferred embodiment of the present invention; not in order to limit the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; here exhaustive without the need to also giving all embodiments; within the spirit and principles in the present invention all, any amendment made, equivalent replacement, improvement etc., be still included within protection scope of the present invention.

Claims (1)

1. a covering type textile inkjet printing paint ink, it is characterized in that: be made up of according to parts by weight following component: dispersible pigment color paste 23 weight part, dihydroxyphenyl propane 19 weight part, glycerine 4.5 weight part, anhydrous sodium sulphate 2.3 weight part, trolamine 2.7 weight part, triethylamine 3.3 weight part, acetone 3.6 weight part, two thiocarbamate 0.25 weight part, active mineral matter powder 1.7 weight part, surfactant blend 1.2 weight part, sustained release dosage 0.55 weight part, essential oil of traditional Chinese medicine 3.85 weight part, deionized water 62 weight part, the median size of described dispersible pigment color paste is 75nm, described active mineral matter powder is germanite, fluorite, tourmalinite, zinc spinel is by weight the mixture of 2.5:3:3.7:2, wherein tourmalinite is dravite and the elbaite mixture by weight 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is prepared from as follows,
S1, get rhamnus crenata sieb.et zucc. 35 weight part and clean, naturally dry, be then placed in 90 DEG C of frying pans and fry extremely savory effusion, then Air washer 17 weight part, be placed in constant temperature oven less than 60 DEG C oven dry, water content≤6.5%;
S2, Spica Prunellae 12.5 weight part to be cleaned, puts into salt solution and soak 3.5 hours, the salt water yield by 3.7 times of immersions spice quality, put into pot and steam thoroughly, taking-up, dry, the concentration of salt solution is 27%;
S3, by honeycomb 12 weight part, lavandula angustifolia 15.5 weight part, Hupeh Anemone Herb 4.5 weight part, Moschus 4.5 weight part, peppermint 1 weight part, Rosmarinus officinalis 1 weight part, sweet marjoram 0.75 weight part, grane ambra 0.65 weight part decon, drops in supper micron mill and is crushed to 60 orders together with the made bulk drug of step S1 and S2, obtained bulk drug powder, for subsequent use;
S4, dropped into by bulk drug powder obtained in step S3 in the extraction kettle of supercritical carbon dioxide extraction apparatus, regulate extracting pressure 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m 3/ h, dynamic extraction 2.5h, directly collect volatile oil A at separating still outlet triangular flask, for subsequent use;
S5, by Cortex ulmi pumilae 8.5 weight part, agalloch eaglewood 2.5 weight part, camphorwood 35-40 weight part, the Radix Astragali 1 weight part is cleaned and is dried, and drops in supper micron mill together and is crushed to 70 orders, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersion bulk drug quality, dispersed with stirring is mixed well, obtained Traditional Chinese drug mixture, for subsequent use;
S6, the Traditional Chinese drug mixture obtained by step S5 decoct 2 hours in 80 DEG C, and collect distillate, and add extracted with diethyl ether, the volume ratio of distillate and ether is 2:1, gets upper oil phase, then adds anhydrous sodium sulfate drying, and namely obtained volatile oil B, for subsequent use;
S7, by made for step S4 and S6 volatile oil A and volatile oil B mixing mix well obtained mixing oil, add needle juniper essential oil, Moschus essential oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene while stirring successively again, abundant stirring 35 minutes, leave standstill 30 minutes, abundant stirring is mixed well, and filtering and impurity removing obtains essential oil of traditional Chinese medicine, wherein, the mass ratio of described mixing oil and needle juniper essential oil, Moschus essential oil, Geranium Essential, eucalyptus quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
CN201610093678.8A 2016-02-19 2016-02-19 Covering type textile ink jet printing pigment ink Pending CN105504992A (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN201610093678.8A CN105504992A (en) 2016-02-19 2016-02-19 Covering type textile ink jet printing pigment ink
CN201610723008.XA CN106336735A (en) 2016-02-19 2016-08-25 Covering type textile inkjet printing pigment ink
CN201610735659.0A CN106189513A (en) 2016-02-19 2016-08-25 Covering type textile inkjet printing pigment ink

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610093678.8A CN105504992A (en) 2016-02-19 2016-02-19 Covering type textile ink jet printing pigment ink

Publications (1)

Publication Number Publication Date
CN105504992A true CN105504992A (en) 2016-04-20

Family

ID=55713311

Family Applications (2)

Application Number Title Priority Date Filing Date
CN201610093678.8A Pending CN105504992A (en) 2016-02-19 2016-02-19 Covering type textile ink jet printing pigment ink
CN201610723008.XA Withdrawn CN106336735A (en) 2016-02-19 2016-08-25 Covering type textile inkjet printing pigment ink

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN201610723008.XA Withdrawn CN106336735A (en) 2016-02-19 2016-08-25 Covering type textile inkjet printing pigment ink

Country Status (1)

Country Link
CN (2) CN105504992A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109881504A (en) * 2019-03-13 2019-06-14 深圳凯奇化工有限公司 A kind of coating ink and preparation method thereof

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104212236B (en) * 2014-08-20 2016-01-27 中山艺展装饰工程有限公司 A kind of fragrant ink with stimulating effect

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109881504A (en) * 2019-03-13 2019-06-14 深圳凯奇化工有限公司 A kind of coating ink and preparation method thereof

Also Published As

Publication number Publication date
CN106336735A (en) 2017-01-18

Similar Documents

Publication Publication Date Title
CN105504966B (en) A kind of offset litho printing ink
CN105542557A (en) Waterborne UV ink for ink jet printing
CN104186565A (en) Electric-heating liquid mosquito-repellent incense with natural plant fragrance of agilawood and preparation method of electric-heating liquid mosquito-repellent incense
CN105504987A (en) Compound activated mineral environment-friendly ink
CN105504967A (en) Environment-friendly water-based black ink
CN104186577A (en) Slow-release electrothermal mosquito incense liquor containing ambergris extract and preparation method
CN105504992A (en) Covering type textile ink jet printing pigment ink
CN104957952B (en) There is the rhamnus crenata sieb.et zucc. carpet of health care function of driving mosquitoes
CN104206444B (en) A kind of electric liquid device fragrant containing lavender natural and preparation method
CN105504964A (en) Improved printing ink
CN106189513A (en) Covering type textile inkjet printing pigment ink
CN105504986A (en) Natural water-based oil paint ink
CN104186571A (en) Electric heating liquid mosquito-repellent incense with sweet marjoram fragrance and preparation method thereof
CN105504989A (en) Color ink for light-color teaching board
CN105504993A (en) Novel color ink-jet printing ink
CN105504965A (en) Colored ink composition
CN106243832A (en) A kind of calligraphy prepared Chinese ink
CN105963970A (en) Improved multifunctional child toy
CN106189516A (en) Novel color ink-jet printing ink
CN108102461A (en) A kind of calligraphy prepared Chinese ink
CN104186575A (en) Refreshing electrothermal liquid mosquito-repellent incense containing vanilla extract and a preparation method
CN104972811A (en) Multifunctional crocus sativus odor type stationery containing box capable of purifying air
CN104951109A (en) Health-type antibacterial musk mouse wrist pad
CN104958026A (en) Home furnishing type sweet marjoram fragrant tissue box with mosquito expelling effect
CN106280704A (en) Water-base writing ink composition

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20160420