CN105542557A - Waterborne UV ink for ink jet printing - Google Patents
Waterborne UV ink for ink jet printing Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/101—Inks specially adapted for printing processes involving curing by wave energy or particle radiation, e.g. with UV-curing following the printing
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/324—Inkjet printing inks characterised by colouring agents containing carbon black
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- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/38—Inkjet printing inks characterised by non-macromolecular additives other than solvents, pigments or dyes
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
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Abstract
The invention discloses waterborne UV ink for ink jet printing. The waterborne UV ink has certain inhibiting and killing effects on multiple bacteria and fungi such as staphylococcus, escherichia coli and gram-positive bacteria, can release negative air ions for a long term to purify the air, is fragrant in smell, fresh and capable of soothing mentality and relieving pressure, has the healthcare effects of refreshing mentality and the brain and eliminating fatigue, and is suitable for people at all ages.
Description
Technical field
The present invention relates to a kind of ink, particularly a kind of ink jet printing water-based UV ink.
Background technology
Ink can be used for routine office work or textile printing field, but traditional general ink does not have refreshes oneself and produces the health-care effects such as negative ion, user's use when long produces taediumvitae, due to the function singleness of conventional inks, can not meet the multi-demands of people.
Summary of the invention
For the deficiency that prior art exists, the user that the present invention is ink provides a kind of smell pure and fresh, has the ink of stimulating effect and negative ion health effect, and it not only can release air negative ion for a long time, purifies air, is beneficial to HUMAN HEALTH; Also there are certain suppression, killing action to the multiple germs such as staphylococcus, intestinal bacteria, gram-positive bacteria and fungi; Simultaneously fragrant odour, pure and freshly soothes the spirit, pressure of releiving, also can expelling mosquito, can not produce detrimentally affect, have application prospect widely to human body.
The object of the invention is to be achieved through the following technical solutions:
A kind of ink jet printing water-based UV ink, it is characterized in that: be made up of according to parts by weight following component: dispersible pigment color paste 23 weight part, dihydroxyphenyl propane 19 weight part, glycerine 4.5 weight part, anhydrous sodium sulphate 2.3 weight part, trolamine 2.7 weight part, triethylamine 3.3 weight part, acetone 3.6 weight part, two thiocarbamate 0.25 weight part, active mineral matter powder 1.7 weight part, surfactant blend 1.2 weight part, sustained release dosage 0.55 weight part, essential oil of traditional Chinese medicine 3.85 weight part, deionized water 62 weight part, the pigment of described mill base is high-carbon black pigment, the median size of described dispersible pigment color paste is 75nm, described active mineral matter powder is germanite, fluorite, tourmalinite, zinc spinel is by weight the mixture of 2.5:3:3.7:2, wherein tourmalinite is dravite and the elbaite mixture by weight 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is prepared from as follows,
S1, get Herba Artemisiae annuae 35 weight part and clean, naturally dry, be then placed in 90 DEG C of frying pans and fry extremely savory effusion, then Air washer 17 weight part, be placed in constant temperature oven less than 60 DEG C oven dry, water content≤6.5%;
S2, the root of three-nerved spicebush 11.5 weight part to be cleaned, puts into salt solution and soak 3.5 hours, the salt water yield by 3.7 times of immersions spice quality, put into pot and steam thoroughly, taking-up, dry, the concentration of salt solution is 27%;
S3, by lavandula angustifolia 15.5 weight part, Hupeh Anemone Herb 4.5 weight part, Moschus 4.5 weight part, Wild Chrysanthemum 1 weight part, sweet marjoram 0.75 weight part decon, drops in supper micron mill and is crushed to 60 orders together with the made bulk drug of step S1 and S2, obtained bulk drug powder, for subsequent use;
S4, dropped into by bulk drug powder obtained in step S3 in the extraction kettle of supercritical carbon dioxide extraction apparatus, regulate extracting pressure 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m
3/ h, dynamic extraction 2.5h, directly collect volatile oil A at separating still outlet triangular flask, for subsequent use;
S5, by rhizome of cyrtomium 12 weight part, Cortex ulmi pumilae 8.5 weight part, agalloch eaglewood 2.5 weight part, camphorwood 15.5 weight part, peppermint 1 weight part, taraxacum 1 weight part is cleaned and is dried, and drops in supper micron mill together and is crushed to 70 orders, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersion bulk drug quality, dispersed with stirring is mixed well, obtained Traditional Chinese drug mixture, for subsequent use;
S6, the Traditional Chinese drug mixture obtained by step S5 decoct 2 hours in 80 DEG C, and collect distillate, and add extracted with diethyl ether, the volume ratio of distillate and ether is 2:1, gets upper oil phase, then adds anhydrous sodium sulfate drying, and namely obtained volatile oil B, for subsequent use;
S7, by made for step S4 and S6 volatile oil A and volatile oil B mixing mix well obtained mixing oil, add Flos Rosae Rugosae quintessence oil, P-Cymene, Geranium Essential, tea tree ethereal oil and cypress essential oil while stirring successively again, abundant stirring 35 minutes, leave standstill 30 minutes, abundant stirring is mixed well, and filtering and impurity removing obtains essential oil of traditional Chinese medicine, wherein, the mass ratio of described mixing oil and Flos Rosae Rugosae quintessence oil, P-Cymene, Geranium Essential, tea tree ethereal oil and cypress essential oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the bulk drug powder of step S3, wild marjoram oil 1.3 weight part and pyrethre 1.5 weight part is also included.
In a preferred embodiment, in the Traditional Chinese drug mixture of step S5, also include borneol 0.6 weight part and lotus leaf 0.4 weight part.
In a preferred embodiment, in the essential oil of traditional Chinese medicine of step S7, Oil of Eucalyptus 0.3 weight part is also included.
Equipment involved in the present invention, raw material and method, be equipment, raw material and method that the industry usually uses, do not repeat them here.
Wherein each essential oil component must and tensio-active agent, sustained release dosage fully mixes, to reach slow release effect, the addition of each essential oil and negative ion natural mineral matter powder must be appropriate, not only antibiotic and sterilizing, mood can also be stabilized, so there is the effect in front to not normal psychological condition, can purify, pacify soul, indignation and beaten sensation can be alleviated, make people can even-tempered and good-humouredly in the face of life, because its energy centre of equilibrium is neural, so helpful to alarmed and dejected state, also significantly tranquil and function of releiving is had, goodish easypro putting is had to console with spirit to insomniac, for pacify hot-tempered enter or moody temper have goodish effect, can increase work efficiency.
The present invention is with reference to modern Chinese herbal medicine pharmacological research, and from the drug screening of existing Chinese medicine with repeatedly verify, give full play to each group of weight part and act synergistically, wherein each traditional Chinese medicinal components brief introduction is as follows.
Herba Artemisiae annuae: pungent, bitter, cool.Clearing heat and cooling blood, preventing malaria, reducing the asthenic fever, relieving summer-heat.For tuberculosis hectic fever, malaria, hinders heat low-heat, lossless, and infantile convulsion, has loose bowels, and dislikes sore mange, kill mosquito.Root: for labor heat, hectic fever due to yin, joint ache, the lower blood of stool.Fruit: sweet is cool.Removing heat to brighten vision, desinsection.
The root of three-nerved spicebush: savory, micro-hardship, irritant refrigerant sense.There are promoting the circulation of QI to relieve pain, warming kidney for dispelling cold, pharmaceutical use.External application makes local vessel expansion, and circulation of blood is accelerated, and relaxes muscle spasm pain; To streptococcus aureus, alpha hemolytic streptococcus, Corynebacterium diphtheriae, Bacillus proteus, Pseudomonas aeruginosa, intestinal bacteria all have restraining effect.
Lavandula angustifolia can remove ant, except roach, except mite, when being placed under wardrobe, pillow, not only mothball can be replaced, the fragrance of one people that oozes can also be left, research finds, lavandula angustifolia has obvious anti-microbial effect, and the phantol contained in lavandula angustifolia is the antibacterial main component of lavandula angustifolia, and it can suppress the growth of 17 kinds of bacteriums (comprising gram-negative bacteria and gram-positive bacteria), 10 kinds of fungies.
Hupeh Anemone Herb: 1. " Shaanxi herbal medicine ": " bitter, cool, slightly poisonous." 2. " herbal medicine is commonly used in Sichuan ": " and toil, temperature, slightly poisonous." removing toxic substances, apocenosis myogenic, the Sweeling-eliminating medicine powder stasis of blood, has and kills maggot, wriggler, eliminate indigestion, detumescence, and the loose stasis of blood, controls stubborn dermatitis, the favus of the scalp, malaria, infantile malnutrition, dysentery, and carbuncle furuncle sore swells, scrofula, wound.
Moschus: have and have one's ideas straightened out, wards off dirty, dredging collateral, effect of the loose stasis of blood; Control apoplexy, coma due to blocking of the respiratory system, frightened epilepsy, middle evil is unhappy, the trusted subordinate sudden and violent Tong ， Disorder lump in the abdomen hypochondriac lump, wound, swollen ulcer drug." herbal classic ": master wards off bad odor, a kind of malaria, epilepsy convulsion, goes three worms.
Wild Chrysanthemum: tool dispelling wind and heat pathogens, subduing swelling and detoxicating.The various active compositions such as its alantol contained, yejuhua lactone, amino acid, trace element.Kill or inhibit activities various pathogens, virus, the inhibit activities of water extract to streptococcus aureus, dysentery bacterium, escherichia coli, Corynebacterium diphtheriae etc. is better than volatile oil; And have anti-inflammatory, anti-oxidant, analgesic activities.
Sweet marjoram: the depressed and addictive disease of mood can be improved, especially effective to liberal-mindedness and vigorous endurance stress symptom, can vasodilation, hypotensive, alleviate and burden, help to eliminate palpitaition, have excellent nerve to pacify and calm function.
Rhizome of cyrtomium: hardship is slightly cold, returns liver the spleen channel, slightly poisonous.Desinsection, clearing heat and detoxicating, hemostasis.
Cortex ulmi pumilae: be dry bark or the root skin of Ulmaceae is sweet, flat, nontoxic; Li Shui, treating stranguria, detumescence, for urinary obstruction, stranguria with turbid discharge, oedema, ulcer carbuncle on the back, erysipelas, mange.
Agalloch eaglewood: " Compendium of Materia Medica " records that wood has strong antibacterial efficacy, fragrance enters spleen, clear god regulates the flow of vital energy, tonifying the five internal organs, relieving cough and reducing sputum, warm stomach temperature spleen, analgesic therapy of ventilating, can be used as medicine is first-class medicinal material superfine product.
Camphorwood: aiphyllium, bark tawny, has irregular longitudinal crack, on the south main product the Changjiang river and southwestern various places.Cut down trees winter and split broken or be sawn into bulk, to dry or air-dry.Timber bulk is not of uniform size, and surface red is brown to burgundy, the visible annual ring in transverse section.Matter is heavily hard.Have strong camphor fragrance, taste is refrigerant, has pungent sense, and warm in nature, taste is pungent; Sensiblely can ward off dirty, warming middle-JIAO to relieve pain, dampness removing desinsection.
Peppermint: be the dry aerial parts of labiate peppermint, dispelling wind and heat pathogens, the clear sharp head, relieve sore throat promoting eruption, soothing the liver promoting the circulation of qi.
Taraxacum: composite family, Dandelion per nnial herb, has and clearing heat and detoxicatingly can be used for heat toxin syndrome, especially kind removing heat from the liver, the hot conjunctival congestion with pain and swelling of the eye for the treatment of liver, and multi-infection, purulent disease; Restraining effect is had to streptococcus aureus, Corynebacterium diphtheriae; Permitted blue achorion to microsporon audouini, trichophyton etc. have restraining effect simultaneously.
Stigma Croci essential oil: Compendium of Material Medica is just recorded Stigma Croci and there is the effects such as calmness, analgesia, blood circulation and promoting silt, there is powerful physiologically active, its column cap Asia and Europe as medicinal, have calmness, eliminate the phlegm, spasmolysis, external as calm, carminative, promoting blood circulation and removing blood stasis, removing pattogenic heat from the blood and toxic material from the body, resolving stagnation for tranquilization.Maculae caused by violent heat pathogen, melancholy ruffian are vexed, palpitation with fear is gone mad.
Propolis essential oil: can anti-bacteria and anti-virus effect, recent studies proves, abundant contained by propolis and the biologically active substance of uniqueness, make it have antibacterial, anti-inflammatory, antipruritic, anti-oxidant, strengthen the several functions such as immunity.
Geranium Essential: there is hemostasis, vasoconstriction, asthma, liver and expelling toxin, gallbladdergallstonecholetithiasis, kidney toxin expelling, urinary stone disease, diuresis, sore muscle, oily skin, aging skin activates, bleb, ochrodermia, fat-reducing, promotes to scab, eczema, to burn sunburn, tinea, menstruation has some setbacks, engorgement of breasts inflammation, alleviate melancholy uneasy, there is deodorizing, antibacterial, the effect of sterilization.
Grane ambra essential oil: grane ambra is the most lasting spices of lasting, and any one spices all can not compare favourably with it in the world, have the saying of " perfume and the life of imperial saliva coexist ".Compendium of Material Medica is carried: can invigorate blood circulation, beneficial marrow, supporing yang road, promoting blood circulation, resolving phlegm and relieving asthma; A lump in the abdomen causing distension and pain; Trusted subordinate's pain; Coma; Liao Yongyan: relieving stranguria by diuresis, loose Disorder knot, knot of cooling down, by labor worm.
Bodhi flower essential oil: spasmolytic, convergence, cough-relieving, sharp brain, eliminate nasal obstruction, diuresis, make skin emolliency, reduce blood pressure, profit is neural, calm, promotion sweating.
Wild marjoram oil: the herb of Labiatae origanum wild marjoram ORIGZNUMVUL-GAREL., have another name called the symbol name such as the ground that stops dysentery grass, wild catmint, there is heat-clearing, dampness elimination, drive away summer heat, induce sweat, regulate the flow of vital energy extremely strong sterilization, bacteriostatic action, the volatile oil extracted from wild marjoram, commonly causing enteritis bacterium and shigella flexneri to 31 kinds, is the pure Chinese medicine additive most with broad-spectrum antimicrobial.
Pyrethre: the general designation of chrysanthemum artemisia (Tanacetum) several plants, removing dampness and killing parasites, kills crab louse, head louse, body louse, flea, effect except mosquito desinsection.
Borneol: pungent is bitter, cool.There is inducing resuscitation of having one's ideas straightened out, the loose poison of heat-clearing, improving acuity of vision and removing nebula.Cure mainly pyreticosis unconsciousness due to high fever, apoplexy coma due to blocking of the respiratory system shies epilepsy, and summer-heat and damp hoodwinks key clearly, and larynx numbness is deaf, and aphtha tooth swells, sore carbuncle infantile malnutrition due to digestive disturbances or intestinalparasites hemorrhoid, conjunctival congestion with pain and swelling of the eye, pterygium.
Lotus leaf: be the leaf of nymphaeaceae plant lotus, has the effect of clearing heat and detoxicating, cool blood, hemostasis.There are the effects such as clearing summer-heat and damp, sending up the lucid YANG, cooling blood for hemostasis.
Oil of Eucalyptus: the most common and purposes one of essential oil the most widely, has good health-care effect, help to focus one's attention on.Effectively can alleviate sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory system diseases.Have good antibacterial and sterilization idiocratic, in some certain food, Oil of Eucalyptus is also as fragrance component.Carry this essential oil at whilst on tour, effectively can resist mosquito bite and insect bite, treatment skin measles.It is good anophelifuge.Mix with water and can become a kind of simple and effective sterilizing agent.
Beneficial effect of the present invention:
The present invention provides a kind of smell pure and fresh for user, has the ink of stimulating effect and negative ion health effect, and it not only can release air negative ion for a long time, purifies air, is beneficial to HUMAN HEALTH; Also there are certain suppression, killing action to the multiple germs such as staphylococcus, intestinal bacteria, gram-positive bacteria and fungi; Simultaneously fragrant odour, pure and freshly soothes the spirit, pressure of releiving, also can expelling mosquito, can not produce detrimentally affect, be applicable to each age groups to human body, its appropriate add other function ingredients after still can keep original effect and quality.
1, tourmalinite is a kind of silicate minerals, its chemical formula is Na (Mg, Fe, Mn, Li, Al) 3Al6 (Si6O18) (Bo3) 3 (OH, F) 4, it contacts with water molecules under electrostatic field, just water molecules can be ionized into hydrogen ion (H+) and hydroxide ion (OH-), hydroxide ion and water molecules form basic hydroxide group negative ion (H2OOH-), be " negative aeroion ", current scientific research proves: negative ion can not only facilitate human body to synthesize and vitamin storage, the physiological activity of strengthening and human activin, very important impact is had on the vital movement of human body and other biological, be called as " air VITAMIN ".The indoor objectionable impurities of negative ion active adsorption, as the construction and decoration such as formaldehyde, toluene objectionable impurities, not only self does not increase pollution, and Cress room air, fundamentally eliminates construction and decoration syndromes, ensures that HUMAN HEALTH is unaffected.
2, the traditional Chinese medicine ingredients contained in the present invention, not only has certain suppression, killing action to the multiple germs such as staphylococcus, tubercule bacillus, Pseudomonas aeruginosa, gram-negative bacteria and gram-positive bacteria and fungi; Simultaneously fragrant odour, character is gentle, pure and freshly soothes the spirit, and helps hormone secretion, the effect of anxiety of releiving, also has certain mosquito-repelling effect, more crucially simultaneously, life-time service the present invention can not produce detrimentally affect to human body, is applicable to each age groups, has application prospect widely.
Embodiment
Embodiment.
A kind of ink jet printing water-based UV ink, it is characterized in that: be made up of according to parts by weight following component: dispersible pigment color paste 23 weight part, dihydroxyphenyl propane 19 weight part, glycerine 4.5 weight part, anhydrous sodium sulphate 2.3 weight part, trolamine 2.7 weight part, triethylamine 3.3 weight part, acetone 3.6 weight part, two thiocarbamate 0.25 weight part, active mineral matter powder 1.7 weight part, surfactant blend 1.2 weight part, sustained release dosage 0.55 weight part, essential oil of traditional Chinese medicine 3.85 weight part, deionized water 62 weight part, the pigment of described mill base is high-carbon black pigment, the median size of described dispersible pigment color paste is 75nm, described active mineral matter powder is germanite, fluorite, tourmalinite, zinc spinel is by weight the mixture of 2.5:3:3.7:2, wherein tourmalinite is dravite and the elbaite mixture by weight 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is prepared from as follows,
S1, get Herba Artemisiae annuae 35 weight part and clean, naturally dry, be then placed in 90 DEG C of frying pans and fry extremely savory effusion, then Air washer 17 weight part, be placed in constant temperature oven less than 60 DEG C oven dry, water content≤6.5%;
S2, the root of three-nerved spicebush 11.5 weight part to be cleaned, puts into salt solution and soak 3.5 hours, the salt water yield by 3.7 times of immersions spice quality, put into pot and steam thoroughly, taking-up, dry, the concentration of salt solution is 27%;
S3, by lavandula angustifolia 15.5 weight part, Hupeh Anemone Herb 4.5 weight part, Moschus 4.5 weight part, Wild Chrysanthemum 1 weight part, sweet marjoram 0.75 weight part decon, drops in supper micron mill and is crushed to 60 orders together with the made bulk drug of step S1 and S2, obtained bulk drug powder, for subsequent use;
S4, dropped into by bulk drug powder obtained in step S3 in the extraction kettle of supercritical carbon dioxide extraction apparatus, regulate extracting pressure 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m
3/ h, dynamic extraction 2.5h, directly collect volatile oil A at separating still outlet triangular flask, for subsequent use;
S5, by rhizome of cyrtomium 12 weight part, Cortex ulmi pumilae 8.5 weight part, agalloch eaglewood 2.5 weight part, camphorwood 15.5 weight part, peppermint 1 weight part, taraxacum 1 weight part is cleaned and is dried, and drops in supper micron mill together and is crushed to 70 orders, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersion bulk drug quality, dispersed with stirring is mixed well, obtained Traditional Chinese drug mixture, for subsequent use;
S6, the Traditional Chinese drug mixture obtained by step S5 decoct 2 hours in 80 DEG C, and collect distillate, and add extracted with diethyl ether, the volume ratio of distillate and ether is 2:1, gets upper oil phase, then adds anhydrous sodium sulfate drying, and namely obtained volatile oil B, for subsequent use;
S7, by made for step S4 and S6 volatile oil A and volatile oil B mixing mix well obtained mixing oil, add Flos Rosae Rugosae quintessence oil, P-Cymene, Geranium Essential, tea tree ethereal oil and cypress essential oil while stirring successively again, abundant stirring 35 minutes, leave standstill 30 minutes, abundant stirring is mixed well, and filtering and impurity removing obtains essential oil of traditional Chinese medicine, wherein, the mass ratio of described mixing oil and Flos Rosae Rugosae quintessence oil, P-Cymene, Geranium Essential, tea tree ethereal oil and cypress essential oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the bulk drug powder of step S3, wild marjoram oil 1.3 weight part and pyrethre 1.5 weight part is also included.
In a preferred embodiment, in the Traditional Chinese drug mixture of step S5, also include borneol 0.6 weight part and lotus leaf 0.4 weight part.
In a preferred embodiment, in the essential oil of traditional Chinese medicine of step S7, Oil of Eucalyptus 0.3 weight part is also included.
Use air ion static method of testing tests the ink in this above-described embodiment, and negative ion burst size is at 430-650/m
3, and sustained release negative aeroion, be more conducive to purifying air for a long time, reach the basic demand of health of people.
Reference examples.
Colour carbon black 20g, phenol 11g, glycerine 4g, benzotriazole 3g, trolamine 1g, triethylamine 3g, sodium bicarbonate 5g, polyoxyethylene groups ethers non-ionic type fluorocarbon surfactant 1.5g, sustained release dosage 0.4g, sweet marjoram essential oil 0.6g, wheat malt essential oil 0.5g, Herba Lysimachiae foenumgraeci quintessence oil 0.5g, RADIX PAEONIAE ALBA essential oil 0.4g, cypress essential oil 0.4g, eucalyptus quintessence oil 0.4g, P-Cymene 0.4g, Peppermint essential oil 0.4g, deionized water 75g.
Use air ion static method of testing tests the ink in this above-mentioned reference examples, and negative ion burst size is at 0/m
3, not there is the function of release air negative ion.
(1) carry out acute toxicity test to obtained essential oil of traditional Chinese medicine, result is as follows:
1. Mouse oral acute toxicity test: the LD50 of Mouse oral essential oil of traditional Chinese medicine is 383.55g/kg, 95% be crediblely limited to 294.68g/kg ~ 499.31g/kg.And the toxicity criterion of air freshener is: the anxious malicious LD50 >=5g/kg of Mouse oral, is judged to be nontoxic.The LD50 of this essential oil of traditional Chinese medicine, higher than 76 times of nontoxic standard, is therefore judged to be nontoxic.
2. chmice acute toxicity on inhalation test: it is 24863.99g/m3 that chmice acute sucks the LC50 of essential oil of traditional Chinese medicine, 95% be crediblely limited to 16837.34g/m3 ~ 33387.46g/m3.And the toxicity criterion of air freshener is: chmice acute sucks (2h) LC50 > 10000mg/m3, the nontoxic level in true border.The LC50 of this essential oil of traditional Chinese medicine, higher than 2486 times of nontoxic standard, is therefore judged to be nontoxic.
Obtained essential oil of traditional Chinese medicine is through inspection, and its fragrance, color and luster, refractive index, relative density, arsenic content, heavy metal content, pH value all meet the requirement of national standard.
(2) check above-mentioned ink performance test result as table 1:
(3) to the test improving the mental status.
Main method is that ink uses volunteer's experiment, recruit 60 people, use the ink in above-mentioned 2 kinds of embodiments respectively, by SCL-90 questionnaire (i.e. " Self-reporting inventory-SCL90 ", one of foremost Mental health test scale in the world), followed the tracks of by the use of continuous 1 week, judge the actual efficacy effect of the present invention in refreshing oneself, wherein 3 people are noninductive is subject to; 7 people experience general; 1 people thinks that this product is invalid for stimulating effect; Have 49 people to feed back this product and have effect of refreshing oneself preferably, the power that can warn is concentrated, and efficient is 81.67%.
(4) repelling effect test.
Repelling effect according to common ink of the prior art and above-described embodiment ink inside carries out contrast test, and test data is in table 2.
Conclusion: the ink in the embodiment of the present invention has good repelling effect.
The foregoing is only preferred embodiment of the present invention; not in order to limit the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; here exhaustive without the need to also giving all embodiments; within the spirit and principles in the present invention all, any amendment made, equivalent replacement, improvement etc., be still included within protection scope of the present invention.
Claims (1)
1. an ink jet printing water-based UV ink, it is characterized in that: be made up of according to parts by weight following component: dispersible pigment color paste 23 weight part, dihydroxyphenyl propane 19 weight part, glycerine 4.5 weight part, anhydrous sodium sulphate 2.3 weight part, trolamine 2.7 weight part, triethylamine 3.3 weight part, acetone 3.6 weight part, two thiocarbamate 0.25 weight part, active mineral matter powder 1.7 weight part, surfactant blend 1.2 weight part, sustained release dosage 0.55 weight part, essential oil of traditional Chinese medicine 3.85 weight part, deionized water 62 weight part, the pigment of described mill base is high-carbon black pigment, the median size of described dispersible pigment color paste is 75nm, described active mineral matter powder is germanite, fluorite, tourmalinite, zinc spinel is by weight the mixture of 2.5:3:3.7:2, wherein tourmalinite is dravite and the elbaite mixture by weight 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is prepared from as follows,
S1, get Herba Artemisiae annuae 35 weight part and clean, naturally dry, be then placed in 90 DEG C of frying pans and fry extremely savory effusion, then Air washer 17 weight part, be placed in constant temperature oven less than 60 DEG C oven dry, water content≤6.5%;
S2, the root of three-nerved spicebush 11.5 weight part to be cleaned, puts into salt solution and soak 3.5 hours, the salt water yield by 3.7 times of immersions spice quality, put into pot and steam thoroughly, taking-up, dry, the concentration of salt solution is 27%;
S3, by lavandula angustifolia 15.5 weight part, Hupeh Anemone Herb 4.5 weight part, Moschus 4.5 weight part, Wild Chrysanthemum 1 weight part, sweet marjoram 0.75 weight part decon, drops in supper micron mill and is crushed to 60 orders together with the made bulk drug of step S1 and S2, obtained bulk drug powder, for subsequent use;
S4, dropped into by bulk drug powder obtained in step S3 in the extraction kettle of supercritical carbon dioxide extraction apparatus, regulate extracting pressure 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m
3/ h, dynamic extraction 2.5h, directly collect volatile oil A at separating still outlet triangular flask, for subsequent use;
S5, by rhizome of cyrtomium 12 weight part, Cortex ulmi pumilae 8.5 weight part, agalloch eaglewood 2.5 weight part, camphorwood 15.5 weight part, peppermint 1 weight part, taraxacum 1 weight part is cleaned and is dried, and drops in supper micron mill together and is crushed to 70 orders, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersion bulk drug quality, dispersed with stirring is mixed well, obtained Traditional Chinese drug mixture, for subsequent use;
S6, the Traditional Chinese drug mixture obtained by step S5 decoct 2 hours in 80 DEG C, and collect distillate, and add extracted with diethyl ether, the volume ratio of distillate and ether is 2:1, gets upper oil phase, then adds anhydrous sodium sulfate drying, and namely obtained volatile oil B, for subsequent use;
S7, by made for step S4 and S6 volatile oil A and volatile oil B mixing mix well obtained mixing oil, add Flos Rosae Rugosae quintessence oil, P-Cymene, Geranium Essential, tea tree ethereal oil and cypress essential oil while stirring successively again, abundant stirring 35 minutes, leave standstill 30 minutes, abundant stirring is mixed well, and filtering and impurity removing obtains essential oil of traditional Chinese medicine, wherein, the mass ratio of described mixing oil and Flos Rosae Rugosae quintessence oil, P-Cymene, Geranium Essential, tea tree ethereal oil and cypress essential oil is 1.3:0.4:0.75:0.6:0.5:0.3.
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| CN201610093680.5A CN105542557A (en) | 2016-02-19 | 2016-02-19 | Waterborne UV ink for ink jet printing |
| CN201610735663.7A CN106318038A (en) | 2016-02-19 | 2016-08-25 | Water-based UV (ultraviolet) ink |
| CN201610723042.7A CN106280707A (en) | 2016-02-19 | 2016-08-25 | A kind of ink jet printing aqueous UV ink |
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| CN201610723042.7A Pending CN106280707A (en) | 2016-02-19 | 2016-08-25 | A kind of ink jet printing aqueous UV ink |
| CN201610735663.7A Pending CN106318038A (en) | 2016-02-19 | 2016-08-25 | Water-based UV (ultraviolet) ink |
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| CN106280707A (en) | 2017-01-04 |
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Application publication date: 20160504 |