CN105504986A - Natural water-based oil paint ink - Google Patents

Natural water-based oil paint ink Download PDF

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Publication number
CN105504986A
CN105504986A CN201610093675.4A CN201610093675A CN105504986A CN 105504986 A CN105504986 A CN 105504986A CN 201610093675 A CN201610093675 A CN 201610093675A CN 105504986 A CN105504986 A CN 105504986A
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weight part
oil
essential oil
traditional chinese
weight
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魏本武
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Priority to CN201610093675.4A priority Critical patent/CN105504986A/en
Publication of CN105504986A publication Critical patent/CN105504986A/en
Priority to CN201610722971.6A priority patent/CN106318037A/en
Priority to CN201610735660.3A priority patent/CN106349812A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/16—Writing inks
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Abstract

The invention discloses natural water-based oil paint ink. Negative air ions can be released for a long time, air can be purified, and human health is facilitated. Multiple germs and fungi such as staphylococcus, escherichia coli and gram-positive bacteria are restrained and killed to a certain degree, the smell is fragrant, refreshing and soothing, pressure is relieved, lasting fragrance can be left after the ink is used, the ink has the healthcare effects of refreshing, consciousness restoring and fatigue relieving, and the natural water-based oil paint ink is suitable for people of all ages and has very wide application prospects.

Description

A kind of natural water-based greasepaint ink
Technical field
The present invention relates to a kind of ink, particularly one natural water-based greasepaint ink.
Background technology
Ink can be used for routine office work or textile printing field, but traditional general ink does not have refreshes oneself and produces the health-care effects such as negative ion, user's use when long produces taediumvitae, due to the function singleness of conventional inks, can not meet the multi-demands of people.
Summary of the invention
For the deficiency that prior art exists, the user that the present invention is ink provides a kind of smell pure and fresh, has the ink of stimulating effect and negative ion health effect, and it not only can release air negative ion for a long time, purifies air, is beneficial to HUMAN HEALTH; Also there are certain suppression, killing action to the multiple germs such as staphylococcus, intestinal bacteria, gram-positive bacteria and fungi; Simultaneously fragrant odour, pure and freshly soothes the spirit, pressure of releiving, also can expelling mosquito, can not produce detrimentally affect, have application prospect widely to human body.
The object of the invention is to be achieved through the following technical solutions:
A kind of natural water-based greasepaint ink, it is characterized in that: be made up of according to parts by weight following component: dispersible pigment color paste 23 weight part, dihydroxyphenyl propane 19 weight part, glycerine 4.5 weight part, anhydrous sodium sulphate 2.3 weight part, trolamine 2.7 weight part, triethylamine 3.3 weight part, acetone 3.6 weight part, two thiocarbamate 0.25 weight part, active mineral matter powder 1.7 weight part, surfactant blend 1.2 weight part, sustained release dosage 0.55 weight part, essential oil of traditional Chinese medicine 3.85 weight part, deionized water 62 weight part, the median size of described dispersible pigment color paste is 75nm, described active mineral matter powder is germanite, fluorite, tourmalinite, zinc spinel is by weight the mixture of 2.5:3:3.7:2, wherein tourmalinite is dravite and the elbaite mixture by weight 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is prepared from as follows,
S1, get Hupeh Anemone Herb 35 weight part and clean, naturally dry, be then placed in 90 DEG C of frying pans and fry extremely savory effusion, then Air washer 17 weight part, be placed in constant temperature oven less than 60 DEG C oven dry, water content≤6.5%;
S2, rhizome of cyrtomium 13 weight to be cleaned, puts into salt solution and soak 3.5 hours, the salt water yield by 3.7 times of immersions spice quality, put into pot and steam thoroughly, taking-up, dry, the concentration of salt solution is 27%;
S3, by clore basil 0.75 weight part, the tuber of stemona 13 weight part, aloe 1 weight part, RADIX PAEONIAE ALBA 1 weight part, Moschus 0.6-18 weight part decon, drops in supper micron mill and is crushed to 60 orders together with the made bulk drug of step S1 and S2, obtained bulk drug powder, for subsequent use;
S4, dropped into by bulk drug powder obtained in step S3 in the extraction kettle of supercritical carbon dioxide extraction apparatus, regulate extracting pressure 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m 3/ h, dynamic extraction 2.5h, directly collect volatile oil A at separating still outlet triangular flask, for subsequent use;
S5, by Leaf of Indigowoad 12 weight part, radix bupleuri 1 weight part, golden cypress 1 weight part, the capsule of weeping forsythia 1 weight part is cleaned and is dried, and drops in supper micron mill together and is crushed to 70 orders, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersion bulk drug quality, dispersed with stirring is mixed well, obtained Traditional Chinese drug mixture, for subsequent use;
S6, the Traditional Chinese drug mixture obtained by step S5 decoct 2 hours in 80 DEG C, and collect distillate, and add extracted with diethyl ether, the volume ratio of distillate and ether is 2:1, gets upper oil phase, then adds anhydrous sodium sulfate drying, and namely obtained volatile oil B, for subsequent use;
S7, by made for step S4 and S6 volatile oil A and volatile oil B mixing mix well obtained mixing oil, add vanilla essential oil, propolis essential oil, needle juniper essential oil, jasmin quintessence oil and Flos Rosae Rugosae quintessence oil while stirring successively again, abundant stirring 35 minutes, leave standstill 30 minutes, abundant stirring is mixed well, and filtering and impurity removing obtains essential oil of traditional Chinese medicine, wherein, the mass ratio of described mixing oil and vanilla essential oil, propolis essential oil, needle juniper essential oil, jasmin quintessence oil and Flos Rosae Rugosae quintessence oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the bulk drug powder of step S3, wild marjoram oil 1.3 weight part and pyrethre 1.5 weight part is also included.
In a preferred embodiment, in the Traditional Chinese drug mixture of step S5, also include borneol 0.6 weight part and lotus leaf 0.4 weight part.
In a preferred embodiment, in the essential oil of traditional Chinese medicine of step S7, Oil of Eucalyptus 0.3 weight part is also included.
Equipment involved in the present invention, raw material and method, be equipment, raw material and method that the industry usually uses, do not repeat them here.
Wherein each essential oil component must and tensio-active agent, sustained release dosage fully mixes, to reach slow release effect, the addition of each essential oil and negative ion natural mineral matter powder must be appropriate, not only antibiotic and sterilizing, mood can also be stabilized, so there is the effect in front to not normal psychological condition, can purify, pacify soul, indignation and beaten sensation can be alleviated, make people can even-tempered and good-humouredly in the face of life, because its energy centre of equilibrium is neural, so helpful to alarmed and dejected state, also significantly tranquil and function of releiving is had, goodish easypro putting is had to console with spirit to insomniac, for pacify hot-tempered enter or moody temper have goodish effect, can increase work efficiency.
The present invention is with reference to modern Chinese herbal medicine pharmacological research, and from the drug screening of existing Chinese medicine with repeatedly verify, give full play to each group of weight part and act synergistically, wherein each traditional Chinese medicinal components brief introduction is as follows.
Hupeh Anemone Herb: 1. " Shaanxi herbal medicine ": " bitter, cool, slightly poisonous." 2. " herbal medicine is commonly used in Sichuan ": " and toil, temperature, slightly poisonous." removing toxic substances, apocenosis myogenic, the Sweeling-eliminating medicine powder stasis of blood, has and kills maggot, wriggler, eliminate indigestion, detumescence, and the loose stasis of blood, controls stubborn dermatitis, the favus of the scalp, malaria, infantile malnutrition, dysentery, and carbuncle furuncle sore swells, scrofula, wound.
Rhizome of cyrtomium: hardship is slightly cold, returns liver the spleen channel, slightly poisonous.Desinsection, clearing heat and detoxicating, hemostasis.
Clore basil: pungent, temperature, has mosquito repellent, relieving the exterior syndrome by diaphoresis, expelling wind and removing dampness, effect of blood stasis removing analgesic.
The tuber of stemona: can driving away mosquito, resisting pathogenic microbes effect, have certain restraining effect to multiple pathomycetes such as beta hemolytic streptococcus, meningococcus, streptococcus aureus, Staphylococcus albus, Corynebacterium diphtheriae, pneumobacillus, plague bacillus, anthrax bacilluss, its infusion all has killing action to mosquitos and flies larva, head louse, clothing lice and bedbug etc.
Aloe: " Bencao Jingshu ": aloe, cold can heat extraction, hardship can expel the heat-evil eliminating dampness, bitter can desinsection, to bitter to cold, therefore be the key medicine of heat extraction desinsection.Its main hot blast is unhappy, hot gas between the chest side of body, improving eyesight, relieving palpitation, and children epilepsy cool breeze, treats five infantile malnutrition due to digestive disturbances or intestinalparasites, kills three worm persons, and heat is raw wind then, and heat energy makes people unhappy, and heat is except then wind-heat is unhappy and between chest diaphragm, hot gas is explained by oneself.
RADIX PAEONIAE ALBA: wherein paeoniflorin has antibacterial, antipyretic, anti-inflammatory, increase coronary flow, improves the effect of myocardial nutritional flow, vasodilation, antagonism acute myocardial ischemia, anticoagulant, calmness, analgesia, spasmolysis, antiulcer agent, adjustment blood sugar.Root of herbaceous peony decoction can suppress dysentery bacterium, streptococcus pneumoniae, intestinal bacteria, Corynebacterium diphtheriae, Hemolytic streptococcus, Pseudomonas aeruginosa etc.
Moschus: have and have one's ideas straightened out, wards off dirty, dredging collateral, effect of the loose stasis of blood; Control apoplexy, coma due to blocking of the respiratory system, frightened epilepsy, middle evil is unhappy, the trusted subordinate sudden and violent Tong ， Disorder lump in the abdomen hypochondriac lump, wound, swollen ulcer drug." herbal classic ": master wards off bad odor, a kind of malaria, epilepsy convulsion, goes three worms.
Leaf of Indigowoad: have certain restraining effect to streptococcus aureus, alpha streptococcus, meningococcus, streptococcus pneumoniae, micrococcus catarrhalis, Corynebacterium diphtheriae, intestinal bacteria, hemophilus influenza, diphtheria corynebacterium and dysentery bacterium; Leaf of Indigowoad also has restraining effect to encephalitis b virus, mumps virus, influenza virus etc. and Leaf of Indigowoad kills leptospiral effect in addition.
Radix bupleuri: treating SHAO YANG disease by mediation, relax liver and stomach, yang invigorating.Control alternate attacks of chills and fever, fullness in the chest and hypochondriac pain, bitter taste is deaf, headache and dizziness, malaria, lower sharp prolapse of the anus, menoxenia, uterine prolapse, invasion of the blood-chamber by heat.
Golden cypress: to streptococcus aureus, streptococcus pneumoniae, diphtheria corynebacterium, Streptococcus viridans, dysentery bacterium (except Song Nei Shi), Hemolytic streptococcus, meningococcus, vibrio cholerae, anthrax bacillus all effectively or have stronger restraining effect; Also restraining effect is had to Bacillus subtilus, bordetella pertussis, tetanus bacillus.
The capsule of weeping forsythia: clearing heat and detoxicating, dispersing swelling and dissipating binds, dispelling wind and heat pathogens, have the title of " persons particularly liable to develop skin infection's panacea ", can suppress Corynebacterium diphtheriae, paratyphosum Bacterium, intestinal bacteria, dysentery bacterium, diphtheria corynebacterium and vibrio cholerae, staphylococcus, suis etc.
Vanilla essential oil: vanilla has special fragrance, has antifatigue and mood is gloomy, help hormone secretion, anxiety of releiving and improve the effects such as insomnia.There is cardiac stimulant, mend effect of brain, stomach invigorating, removing toxic substances, wind dispelling, strengthen muscle strength, make fragrant nervous system stimulant and kidney-reinforcing drug, be used for treating hysteria, melancholia, impotence, abnormal heat and rheumatosis.
Propolis essential oil: can anti-bacteria and anti-virus effect, recent studies proves, abundant contained by propolis and the biologically active substance of uniqueness, make it have antibacterial, anti-inflammatory, antipruritic, anti-oxidant, strengthen the several functions such as immunity.
Needle juniper essential oil: have purify air, anti-mosquito worm Cheng stings, antibacterial, rheumatism, antitetanic effect, also there is the calm function refreshing oneself, encourage mood, the purification state of mind and discharge soul, people's body and mind can be allowed relaxed and comfortable, also there is the effect of promoting the sexual maturity; In addition, the function of its toxin expelling is very famous, and it can discharge the toxin of accumulation, purification intestinal mucosa.
Jasmin quintessence oil: have obvious relaxation effect, can inspire enthusiasm, and promotes self-confidence, and powerful anti-melancholy ability can make people in high spirits, forgets worry.Pacify nerve simultaneously, produce the impression in front, set up a kind of self-confident, have sensation that is optimistic and euphoria, contribute to regaining one's vigor, it has function that is lax and warm mood simultaneously.
Flos Rosae Rugosae quintessence oil: there is antibacterial, sterilization, promote the sexual maturity, calm, mend the effects such as body, have and smooth mood, improve mood, calm nerves anxiety and pressure, woman can be made to produce impression actively and positively to oneself, and its natural fragrance enters after human body through olfactory nerve, people's spiritual happiness, satisfied can be made, alleviate anxiety, depression, pressure, help for sleep, enhance metabolism, sanguimotor effect.
Wild marjoram oil: the herb of Labiatae origanum wild marjoram ORIGZNUMVUL-GAREL., have another name called the symbol name such as the ground that stops dysentery grass, wild catmint, there is heat-clearing, dampness elimination, drive away summer heat, induce sweat, regulate the flow of vital energy extremely strong sterilization, bacteriostatic action, the volatile oil extracted from wild marjoram, commonly causing enteritis bacterium and shigella flexneri to 31 kinds, is the pure Chinese medicine additive most with broad-spectrum antimicrobial.
Pyrethre: the general designation of chrysanthemum artemisia (Tanacetum) several plants, removing dampness and killing parasites, kills crab louse, head louse, body louse, flea, effect except mosquito desinsection.
Borneol: pungent is bitter, cool.There is inducing resuscitation of having one's ideas straightened out, the loose poison of heat-clearing, improving acuity of vision and removing nebula.Cure mainly pyreticosis unconsciousness due to high fever, apoplexy coma due to blocking of the respiratory system shies epilepsy, and summer-heat and damp hoodwinks key clearly, and larynx numbness is deaf, and aphtha tooth swells, sore carbuncle infantile malnutrition due to digestive disturbances or intestinalparasites hemorrhoid, conjunctival congestion with pain and swelling of the eye, pterygium.
Lotus leaf: be the leaf of nymphaeaceae plant lotus, has the effect of clearing heat and detoxicating, cool blood, hemostasis.There are the effects such as clearing summer-heat and damp, sending up the lucid YANG, cooling blood for hemostasis.
Oil of Eucalyptus: the most common and purposes one of essential oil the most widely, has good health-care effect, help to focus one's attention on.Effectively can alleviate sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory system diseases.Have good antibacterial and sterilization idiocratic, in some certain food, Oil of Eucalyptus is also as fragrance component.Carry this essential oil at whilst on tour, effectively can resist mosquito bite and insect bite, treatment skin measles.It is good anophelifuge.Mix with water and can become a kind of simple and effective sterilizing agent.
Beneficial effect of the present invention:
The present invention provides a kind of smell pure and fresh for user, has the ink of stimulating effect and negative ion health effect, and it not only can release air negative ion for a long time, purifies air, is beneficial to HUMAN HEALTH; Also there are certain suppression, killing action to the multiple germs such as staphylococcus, intestinal bacteria, gram-positive bacteria and fungi; Simultaneously fragrant odour, pure and freshly soothes the spirit, pressure of releiving, also can expelling mosquito, can not produce detrimentally affect, be applicable to each age groups to human body, its appropriate add other function ingredients after still can keep original effect and quality.
1, tourmalinite is a kind of silicate minerals, its chemical formula is Na (Mg, Fe, Mn, Li, Al) 3Al6 (Si6O18) (Bo3) 3 (OH, F) 4, it contacts with water molecules under electrostatic field, just water molecules can be ionized into hydrogen ion (H+) and hydroxide ion (OH-), hydroxide ion and water molecules form basic hydroxide group negative ion (H2OOH-), be " negative aeroion ", current scientific research proves: negative ion can not only facilitate human body to synthesize and vitamin storage, the physiological activity of strengthening and human activin, very important impact is had on the vital movement of human body and other biological, be called as " air VITAMIN ".The indoor objectionable impurities of negative ion active adsorption, as the construction and decoration such as formaldehyde, toluene objectionable impurities, not only self does not increase pollution, and Cress room air, fundamentally eliminates construction and decoration syndromes, ensures that HUMAN HEALTH is unaffected.
2, the traditional Chinese medicine ingredients contained in the present invention, not only has certain suppression, killing action to the multiple germs such as staphylococcus, tubercule bacillus, Pseudomonas aeruginosa, gram-negative bacteria and gram-positive bacteria and fungi; Simultaneously fragrant odour, character is gentle, pure and freshly soothes the spirit, and helps hormone secretion, the effect of anxiety of releiving, also has certain mosquito-repelling effect, more crucially simultaneously, life-time service the present invention can not produce detrimentally affect to human body, is applicable to each age groups, has application prospect widely.
Embodiment
Embodiment.
A kind of natural water-based greasepaint ink, it is characterized in that: be made up of according to parts by weight following component: dispersible pigment color paste 23 weight part, dihydroxyphenyl propane 19 weight part, glycerine 4.5 weight part, anhydrous sodium sulphate 2.3 weight part, trolamine 2.7 weight part, triethylamine 3.3 weight part, acetone 3.6 weight part, two thiocarbamate 0.25 weight part, active mineral matter powder 1.7 weight part, surfactant blend 1.2 weight part, sustained release dosage 0.55 weight part, essential oil of traditional Chinese medicine 3.85 weight part, deionized water 62 weight part, the median size of described dispersible pigment color paste is 75nm, described active mineral matter powder is germanite, fluorite, tourmalinite, zinc spinel is by weight the mixture of 2.5:3:3.7:2, wherein tourmalinite is dravite and the elbaite mixture by weight 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is prepared from as follows,
S1, get Hupeh Anemone Herb 35 weight part and clean, naturally dry, be then placed in 90 DEG C of frying pans and fry extremely savory effusion, then Air washer 17 weight part, be placed in constant temperature oven less than 60 DEG C oven dry, water content≤6.5%;
S2, rhizome of cyrtomium 13 weight to be cleaned, puts into salt solution and soak 3.5 hours, the salt water yield by 3.7 times of immersions spice quality, put into pot and steam thoroughly, taking-up, dry, the concentration of salt solution is 27%;
S3, by clore basil 0.75 weight part, the tuber of stemona 13 weight part, aloe 1 weight part, RADIX PAEONIAE ALBA 1 weight part, Moschus 0.6-18 weight part decon, drops in supper micron mill and is crushed to 60 orders together with the made bulk drug of step S1 and S2, obtained bulk drug powder, for subsequent use;
S4, dropped into by bulk drug powder obtained in step S3 in the extraction kettle of supercritical carbon dioxide extraction apparatus, regulate extracting pressure 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m 3/ h, dynamic extraction 2.5h, directly collect volatile oil A at separating still outlet triangular flask, for subsequent use;
S5, by Leaf of Indigowoad 12 weight part, radix bupleuri 1 weight part, golden cypress 1 weight part, the capsule of weeping forsythia 1 weight part is cleaned and is dried, and drops in supper micron mill together and is crushed to 70 orders, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersion bulk drug quality, dispersed with stirring is mixed well, obtained Traditional Chinese drug mixture, for subsequent use;
S6, the Traditional Chinese drug mixture obtained by step S5 decoct 2 hours in 80 DEG C, and collect distillate, and add extracted with diethyl ether, the volume ratio of distillate and ether is 2:1, gets upper oil phase, then adds anhydrous sodium sulfate drying, and namely obtained volatile oil B, for subsequent use;
S7, by made for step S4 and S6 volatile oil A and volatile oil B mixing mix well obtained mixing oil, add vanilla essential oil, propolis essential oil, needle juniper essential oil, jasmin quintessence oil and Flos Rosae Rugosae quintessence oil while stirring successively again, abundant stirring 35 minutes, leave standstill 30 minutes, abundant stirring is mixed well, and filtering and impurity removing obtains essential oil of traditional Chinese medicine, wherein, the mass ratio of described mixing oil and vanilla essential oil, propolis essential oil, needle juniper essential oil, jasmin quintessence oil and Flos Rosae Rugosae quintessence oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the bulk drug powder of step S3, wild marjoram oil 1.3 weight part and pyrethre 1.5 weight part is also included.
In a preferred embodiment, in the Traditional Chinese drug mixture of step S5, also include borneol 0.6 weight part and lotus leaf 0.4 weight part.
In a preferred embodiment, in the essential oil of traditional Chinese medicine of step S7, Oil of Eucalyptus 0.3 weight part is also included.
Use air ion static method of testing tests the ink in this above-described embodiment, and negative ion burst size is at 430-650/m 3, and sustained release negative aeroion, be more conducive to purifying air for a long time, reach the basic demand of health of people.
Reference examples.
Colour carbon black 20g, phenol 11g, glycerine 4g, benzotriazole 3g, trolamine 1g, triethylamine 3g, sodium bicarbonate 5g, polyoxyethylene groups ethers non-ionic type fluorocarbon surfactant 1.5g, sustained release dosage 0.4g, sweet marjoram essential oil 0.6g, wheat malt essential oil 0.5g, Herba Lysimachiae foenumgraeci quintessence oil 0.5g, RADIX PAEONIAE ALBA essential oil 0.4g, cypress essential oil 0.4g, eucalyptus quintessence oil 0.4g, P-Cymene 0.4g, Peppermint essential oil 0.4g, deionized water 75g.
Use air ion static method of testing tests the ink in this above-mentioned reference examples, and negative ion burst size is at 0/m 3, not there is the function of release air negative ion.
(1) carry out acute toxicity test to obtained essential oil of traditional Chinese medicine, result is as follows:
1. Mouse oral acute toxicity test: the LD50 of Mouse oral essential oil of traditional Chinese medicine is 383.55g/kg, 95% be crediblely limited to 294.68g/kg ~ 499.31g/kg.And the toxicity criterion of air freshener is: the anxious malicious LD50 >=5g/kg of Mouse oral, is judged to be nontoxic.The LD50 of this essential oil of traditional Chinese medicine, higher than 76 times of nontoxic standard, is therefore judged to be nontoxic.
2. chmice acute toxicity on inhalation test: it is 24863.99g/m3 that chmice acute sucks the LC50 of essential oil of traditional Chinese medicine, 95% be crediblely limited to 16837.34g/m3 ~ 33387.46g/m3.And the toxicity criterion of air freshener is: chmice acute sucks (2h) LC50 > 10000mg/m3, the nontoxic level in true border.The LC50 of this essential oil of traditional Chinese medicine, higher than 2486 times of nontoxic standard, is therefore judged to be nontoxic.
Obtained essential oil of traditional Chinese medicine is through inspection, and its fragrance, color and luster, refractive index, relative density, arsenic content, heavy metal content, pH value all meet the requirement of national standard.
(2) check above-mentioned ink performance test result as table 1:
(3) to the test improving the mental status.
Main method is that ink uses volunteer's experiment, recruit 60 people, use the ink in above-mentioned 2 kinds of embodiments respectively, by SCL-90 questionnaire (i.e. " Self-reporting inventory-SCL90 ", one of foremost Mental health test scale in the world), followed the tracks of by the use of continuous 1 week, judge the actual efficacy effect of the present invention in refreshing oneself, wherein 3 people are noninductive is subject to; 7 people experience general; 1 people thinks that this product is invalid for stimulating effect; Have 49 people to feed back this product and have effect of refreshing oneself preferably, the power that can warn is concentrated, and efficient is 81.67%.
(4) repelling effect test.
Repelling effect according to common ink of the prior art and above-described embodiment ink inside carries out contrast test, and test data is in table 2.
Conclusion: the ink in the embodiment of the present invention has good repelling effect.
The foregoing is only preferred embodiment of the present invention; not in order to limit the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; here exhaustive without the need to also giving all embodiments; within the spirit and principles in the present invention all, any amendment made, equivalent replacement, improvement etc., be still included within protection scope of the present invention.

Claims (1)

1. a natural water-based greasepaint ink, it is characterized in that: be made up of according to parts by weight following component: dispersible pigment color paste 23 weight part, dihydroxyphenyl propane 19 weight part, glycerine 4.5 weight part, anhydrous sodium sulphate 2.3 weight part, trolamine 2.7 weight part, triethylamine 3.3 weight part, acetone 3.6 weight part, two thiocarbamate 0.25 weight part, active mineral matter powder 1.7 weight part, surfactant blend 1.2 weight part, sustained release dosage 0.55 weight part, essential oil of traditional Chinese medicine 3.85 weight part, deionized water 62 weight part, the median size of described dispersible pigment color paste is 75nm, described active mineral matter powder is germanite, fluorite, tourmalinite, zinc spinel is by weight the mixture of 2.5:3:3.7:2, wherein tourmalinite is dravite and the elbaite mixture by weight 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine is prepared from as follows,
S1, get Hupeh Anemone Herb 35 weight part and clean, naturally dry, be then placed in 90 DEG C of frying pans and fry extremely savory effusion, then Air washer 17 weight part, be placed in constant temperature oven less than 60 DEG C oven dry, water content≤6.5%;
S2, rhizome of cyrtomium 13 weight to be cleaned, puts into salt solution and soak 3.5 hours, the salt water yield by 3.7 times of immersions spice quality, put into pot and steam thoroughly, taking-up, dry, the concentration of salt solution is 27%;
S3, by clore basil 0.75 weight part, the tuber of stemona 13 weight part, aloe 1 weight part, RADIX PAEONIAE ALBA 1 weight part, Moschus 0.6-18 weight part decon, drops in supper micron mill and is crushed to 60 orders together with the made bulk drug of step S1 and S2, obtained bulk drug powder, for subsequent use;
S4, dropped into by bulk drug powder obtained in step S3 in the extraction kettle of supercritical carbon dioxide extraction apparatus, regulate extracting pressure 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m 3/ h, dynamic extraction 2.5h, directly collect volatile oil A at separating still outlet triangular flask, for subsequent use;
S5, by Leaf of Indigowoad 12 weight part, radix bupleuri 1 weight part, golden cypress 1 weight part, the capsule of weeping forsythia 1 weight part is cleaned and is dried, and drops in supper micron mill together and is crushed to 70 orders, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersion bulk drug quality, dispersed with stirring is mixed well, obtained Traditional Chinese drug mixture, for subsequent use;
S6, the Traditional Chinese drug mixture obtained by step S5 decoct 2 hours in 80 DEG C, and collect distillate, and add extracted with diethyl ether, the volume ratio of distillate and ether is 2:1, gets upper oil phase, then adds anhydrous sodium sulfate drying, and namely obtained volatile oil B, for subsequent use;
S7, by made for step S4 and S6 volatile oil A and volatile oil B mixing mix well obtained mixing oil, add vanilla essential oil, propolis essential oil, needle juniper essential oil, jasmin quintessence oil and Flos Rosae Rugosae quintessence oil while stirring successively again, abundant stirring 35 minutes, leave standstill 30 minutes, abundant stirring is mixed well, and filtering and impurity removing obtains essential oil of traditional Chinese medicine, wherein, the mass ratio of described mixing oil and vanilla essential oil, propolis essential oil, needle juniper essential oil, jasmin quintessence oil and Flos Rosae Rugosae quintessence oil is 1.3:0.4:0.75:0.6:0.5:0.3.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106280692A (en) * 2016-08-15 2017-01-04 安徽明诚塑业有限公司 A kind of Environmental-protection water-based ink and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106280692A (en) * 2016-08-15 2017-01-04 安徽明诚塑业有限公司 A kind of Environmental-protection water-based ink and preparation method thereof

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