CN106366760A - Aqueous writing ink composition - Google Patents
Aqueous writing ink composition Download PDFInfo
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- CN106366760A CN106366760A CN201610735662.2A CN201610735662A CN106366760A CN 106366760 A CN106366760 A CN 106366760A CN 201610735662 A CN201610735662 A CN 201610735662A CN 106366760 A CN106366760 A CN 106366760A
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- weight portion
- oil
- weight
- essential oil
- traditional chinese
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- 208000024794 sputum Diseases 0.000 description 1
- 210000003802 sputum Anatomy 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 229940031000 streptococcus pneumoniae Drugs 0.000 description 1
- 238000013268 sustained release Methods 0.000 description 1
- 239000012730 sustained-release form Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 208000011580 syndromic disease Diseases 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- CEIZFXOZIQNICU-UHFFFAOYSA-N tenuazonic acid Chemical compound CCC(C)C1NC(=O)C(C(C)=O)=C1O CEIZFXOZIQNICU-UHFFFAOYSA-N 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 230000008736 traumatic injury Effects 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
- 230000003639 vasoconstrictive effect Effects 0.000 description 1
- 239000002435 venom Substances 0.000 description 1
- 210000001048 venom Anatomy 0.000 description 1
- 231100000611 venom Toxicity 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The water-based writing ink composition comprises 1.7 parts by weight of active mineral powder, 1.2 parts by weight of surfactant compound and 0.55 part by weight of slow release agent, and can release negative air ions for a long time, purify air and benefit human health; also has certain inhibiting and killing effects on staphylococcus, escherichia coli, gram-positive bacteria and other various germs and fungi; meanwhile, the tea has aromatic smell, is fresh and refreshing, and is suitable for people of all ages.
Description
The application is the Application No. 2016107229595 that 2016 applyings date August is submitted on the 25th, invention entitled " water
The divisional application of the Chinese invention patent application of property base writing ink composition ".
Technical field
The present invention relates to a kind of ink, particularly to water-base writing ink composition.
Background technology
Ink can be used for routine office work or textile printing field, but traditional general ink do not have refresh oneself and generation bear from
The health-care effects such as son, user using with producing taediumvitae, due to the single function of conventional inks, can not meet people when long
Multi-demandses.
Content of the invention
In view of the shortcomings of the prior art, the present invention provides a kind of abnormal smells from the patient pure and fresh for the user of ink, has and refreshes oneself
Effect and the ink of negative ion health effect, it not only can discharge negative aeroion, purify air for a long time, is good for beneficial to human body
Health；Also to staphylococcuses, escherichia coli, gram-positive bacteria etc., multiple pathogenic bacterias and funguses have certain suppression, killing action；With
When fragrant odour, pure and fresh soothe the spirit, pressure of releiving, also can expelling mosquito, will not to human body produce harmful effect, have widely
Application prospect.
The purpose of the present invention is achieved by the following technical solution:
Water-base writing ink composition it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight
Part, bis-phenol a19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine
3.3 weight portions, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surface
Activating agent compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, institute
The pigment stating mill base is high-carbon black pigment, and the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanium
Stone, fluorite, tourmaline, gahnite are dravite and lithium electricity by weight the mixture of 2.5:3:3.7:2, wherein tourmaline
By weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine passes through such as gas stone
Lower step is prepared from,
S1, take Fructus Carpesii 35 weight portion clean, naturally dry, be subsequently placed in 90 DEG C of frying pans and fry to savory effusion, then spray
Deionized water 17 weight portion, is placed in constant temperature oven less than 60 DEG C and dries, water content≤6.5%；
S2, Cortex Moutan 16 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality 3.7
Times, put into and steam in pot thoroughly, take out, dry, the concentration of saline is 27%；
S3, by lavandula angustifolia 12 weight portion, Herba Anemones Hupehensiss 4.5 weight portion, rhododendron molle (bl.) g.don 1 weight portion, the Rhizoma Atractylodis Macrocephalae 1 weight portion, sweet Ma Yu
Blue 0.75 weight portion decontamination, is put into together with step s1 and the made crude drug of s2 and is crushed to 60 mesh in super micron mill, is obtained
Crude drug powder, standby；
S4, by step s3 be obtained crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, adjust extraction
Pressure power 27.65mpa, 45.10 DEG C of extraction temperature, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, are directly separating
Kettle outlet triangular flask collects volatile oil a, standby；
S5, by Herba Artemisiae Scopariae 15.5 weight portion, Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 15.5 weight portion, Rhizoma Acori Graminei 4.5
Weight portion clean dry, together put into super micron mill in be crushed to 70 mesh, then plus deionized water soak 6 hours, amount of water
By 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, prepared Traditional Chinese drug mixture, standby；
S6, the Traditional Chinese drug mixture that step s5 is obtained decoct 2 hours in 80 DEG C, collect distillate, and add ether to extract, distillation
Then plus anhydrous sodium sulfate drying the volume ratio of liquid and ether is 2:1, takes upper oil phase, that is, volatile oil b is obtained, standby；
S7, step s4 and s6 made volatile oil a and volatile oil b mixing are mixed well prepared miscella, then sequentially add while stirring
Peppermint essential oil, sarranine flower essential oil, Geranium Essential, Herba Duchesneae Indicae quintessence oil and P-Cymene, are sufficiently stirred for 35 minutes, stand 30 minutes,
It is sufficiently stirred for mixing well, filtering and impurity removing, obtains final product essential oil of traditional Chinese medicine, wherein, described miscella and Peppermint essential oil, sarranine flower essential oil, India
The mass ratio of certain herbaceous plants with big flowers quintessence oil, Herba Duchesneae Indicae quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, also include Herba Origani oil 1.3 weight portion in the crude drug powder of step s3 and spend in vain
Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step s5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4
Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step s7 also includes Eucalyptus oil 0.3 weight portion.
Equipment involved in the present invention, raw material and method, are the usual equipment using of the industry, raw material and method,
This repeats no more.
Wherein each essential oil component must be sufficiently mixed with surfactant, slow releasing agent, to reach slow release effect, each quintessence oil and
The addition of anion natural mineral powder must be appropriate, and not only antibiotic and sterilizing is moreover it is possible to stable emotion, so to the not normal heart
Reason state has the effect in front, can purify, pacify soul, can mitigate angry and beaten sensation, and making one can be with the flat gas of the heart
With ground to life, because its energy centre of equilibrium nerve, helpful to alarmed and dejected state, also have significantly flat
Quiet with releive function, insomniac is had goodish relax to put console with spirit, for pacify hot-tempered enter or moody temper have
Goodish effect, can improve work efficiency.
The present invention with reference to modern Chinese medicine pharmacological research, verifies from the drug screening of existing Chinese medicine and repeatedly, gives full play to respectively
Group weight portion synergism, wherein each Chinese medicinal components are described as follows.
Fructus Carpesii: [mongolian medicine] capsule gives a chapter ancient: fruit is used for ascariasis, enterobiasiss, skin infection, and joint is hindered, and scrofula " is covered and planted medicine
Will " fruit: bitter, pungent, put down.Eliminating stagnated food and killing intestinal worms
Cortex Moutan: to bacillus subtilis, escherichia coli, Bacillus typhi, Salmonella paratyphi, Bacillus proteuss, bacillus pyocyaneus, staphylococcuses,
Hemolytic streptococcuss, streptococcus pneumoniae, vibrio cholera etc. all have stronger antibacterial action.
Lavandula angustifolia not only can replace camphor ball moreover it is possible to stay except ant, except roach, acaricide when being placed under wardrobe, medicated pillow
The fragrance of one people that oozes lower, research finds, lavandula angustifolia has obvious antibacterial action, and the linalool containing in lavandula angustifolia is lavandula angustifolia
The main component of antibacterial, it can suppress 17 kinds of antibacterials (including gram-negative bacteria and gram-positive bacteria), the life of 10 kinds of funguses
Long.
Herba Anemones Hupehensiss: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature,
Slightly poisonous." removing toxic substances, evacuation of pus granulation promoting, scattered stasis detumescence, have and kill maggot, wriggler, change long-pending, detumescence, dissipating blood stasis, control stubborn dermatitis, tinea alba, malaria
Disease, infantile malnutrition, dysentery, carbuncle furuncle swells, scrofula, traumatic injury.
Rhododendron molle (bl.) g.don: also known as Flos Rhododendri Mollis, Azalea pontica, yellow Rhododendron simsii Planch., there is expelling wind and removing dampness；Analgesic therapy；Effect of parasite killing.
The Rhizoma Atractylodis Macrocephalae: belong to Compositae, [WTBX herbaceos perennial has suppression to make acrothesium floccosum, star nocardia
With.Decoct also has inhibitory action to meningococcuss.Nearly report Rhizoma Atractylodis Macrocephalae decoct and decoction of four noble drugs are to Bacillus typhi, paratyphoid A
Bacillus, shigella flexneri, escherichia coli, bacillus pyocyaneus etc. all have different degrees of bacteriostasis.
Origanum majorana: can improve that mood is depressed and addictive disease, especially to liberal-mindedness and vigorous endurance stress symptom effectively, can expansion of blood vessels,
Blood pressure lowering, mitigation and burden, help eliminate cardiopalmus, have excellent nerve to pacify and calm function.
Herba Artemisiae Scopariae: there is significant hepatic cholagogic effect, improve microcirculation, and have blood pressure lowering, blood fat reducing, anticoagulation, diuresis solution
Heat is relievingd asthma, the effect driven away ascarid and suppress multiple pathogenic dermatophytess and antibacterial.
Cortex ulmi pumilae: the dry bark for Ulmaceae or root bark, sweet, flat, nontoxic；Diuretic, treating stranguria, detumescence, for urine
Obstructed, stranguria with turbid discharge, edema, carbuncle carbuncle on the back, erysipelas, scabies.
Lignum Aquilariae Resinatum: " Compendium of Materia Medica " record wood has strong antibacterial efficacy, fragrance enters spleen, god's qi-regulating, tonifying five ZANG-organses, cough-relieving clearly
Resolving sputum, warming the stomach warming the spleen, ventilation analgesic therapy, can be used as medicine, be first-class medical material superfine product.
Lignum cinnamomi camphorae: aiphyllium, bark yellowish-brown, there is irregular longitudinal crack, on the south main product the Changjiang river and southwestern various places.Winter
Cut down trees and split broken or be sawn into bulk, dry or air-dry.Timber bulk is not of uniform size, surface rufous to burgundy, and transverse section is visible
Annual ring.Matter is again hard.There is strong Camphora fragrance, taste is refrigerant, have pungent sense, warm in nature, acrid in the mouth；Sensible can ward off dirty, warming middle-JIAO to stop
Bitterly, dampness removing parasite killing.
Rhizoma Acori Graminei: its flower, stem aromatic flavor, have functions that to have one's ideas straightened out, eliminating the phlegm, dissipate wind, epidemic disease of can dispelling Fructus Alpiniae Oxyphyllae, building body, can
Make spice or mosquito dispersing.
Peppermint essential oil: not only fragrance, moreover it is possible to driving away mosquito, has contraction blood capillary simultaneously, excludes vivotoxin, improves wet
Rash, tinea, releive itch, inflammation and burning, soft skin, eliminate blackhead, be beneficial to oily hair and skin quality, purify air
And the effect refreshed oneself.
Sarranine flower essential oil: Stigma Croci is just recorded on Compendium of Material Medica there is the effects such as calmness, analgesia, blood circulation and promoting silt, have
Powerful physiologically active, its stigma has calmness, eliminating the phlegm, spasmolysises in Asia and Europe as medicinal, external be used as calm,
Carminative, blood circulation promoting and blood stasis dispelling, removing pathogenic heat from blood and toxic substance from the body, resolving stagnation for tranquilization.Maculae caused by violent heat pathogen, melancholy painful abdominal mass are vexed, palpitation with fear is gone mad.
Geranium Essential: there is hemostasis, vasoconstrictive, asthma, liver and expelling toxin, cholelithiasis, kidney toxin expelling, renal calculuss, diuresis, flesh
Carnic acid pain, oily skin, aging skin activates, herpess, palor, fat-reducing, promotes to scab, eczema, sunburn of burning, tinea, the moon
Through having some setbacks, engorgement of breasts inflammation, mitigate melancholy uneasy, there is deodorization, antibacterial, the effect of sterilization.
Herba Duchesneae Indicae quintessence oil: have heat-clearing and toxic substances removing, promoting blood circulation to remove blood stasis, astringing to arrest bleeding effect, venom can be controlled again, apply and control furuncle etc.；
And be used for killing fly larvae.
P-Cymene: to anthrax bacillus, Alpha-hemolytic streptococcus, b- Streptococcus hemolyticuss, diphtheria corynebacterium, bacillus pseudodiphthericus, lung
10 kinds of Gram-positives such as diplococcoid, staphylococcus aureuses, Staphylococcus citreus, white Portugal Portugal coccus, bacillus subtilis
Aerophil all has antibacterial action, also has bacteriostasis for multiple pathomycetes.
Herba Origani oil: the herb of Labiatae origanum Adeps Bovis seu Bubali origznum vul-garel., also known as careless, the wild chaste tree of dysentery relieving
The ground such as mustard accord with name, have heat clearing away, removing dampness, driving away summer heat, induce sweat, sterilization that qi-regulating is extremely strong, bacteriostasis, the volatilization extracted from Adeps Bovis seu Bubali
Oil, cause enteritis antibacterial common to 31 kinds and shigella flexneri, are the pure Chinese medicine additives of most broad-spectrum antiseptic.
Herba et Flos Pyrethri Cinerariifolii: Tanacetum vulgare L belongs to the general designation of (tanacetum) several plants, removing dampness and killing parasites, kills pubic louse, head louse, body
Louse, flea, the effect except mosquito parasite killing.
Borneolum Syntheticum: pungent, bitter, cool.There is inducing resuscitation of having one's ideas straightened out, heat-clearing dissipates poison, improving acuity of vision and removing nebula.Cure mainly high fever apoplexy coma due to blocking of the respiratory system shies epilepsy, middle wind-phlegm
Faint infantile convulsion, summer-heat and damp blinds clear key, larynx numbness is deaf, aphtha tooth swells, sore carbuncle infantile malnutrition due to digestive disturbances or intestinalparasites hemorrhoid, conjunctival congestion and swelling pain, pterygium.
Folium Nelumbinis: for the leaf of nymphaeaceae plant lotus, play the role of heat-clearing and toxic substances removing, removing heat from blood, hemostasis.There is clearing away summer-heat and eliminating dampness, rise and send out clearly
The effects such as sun, cooling blood for hemostasis.
Eucalyptus oil: one of most common and widest quintessence oil of purposes, there is good health-care effect, help focused attention
Power.Sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory system diseases can effectively be alleviated.There is good resisting
Bacterium and sterilization idiocratic, in some certain food, Eucalyptus oil is also as fragrance component.Carry this quintessence oil in travelling, permissible
Effectively resist mosquito bite and insect bite, treat skin measles.It is good anophelifuge.Mixing with water can become a kind of and simple and effective disappear
Toxic agent.
Beneficial effects of the present invention:
The present invention provides a kind of abnormal smells from the patient pure and fresh for user, has stimulating effect and the ink of negative ion health effect, it is not only
Negative aeroion can be discharged for a long time, purify air, beneficial to health；Also thin to staphylococcuses, escherichia coli, Grain-positive
Multiple pathogenic bacteria such as bacterium and funguses have certain suppression, killing action；Fragrant odour simultaneously, pure and fresh soothe the spirit, pressure of releiving, also can drive
Catch up with mosquito, harmful effect will not be produced it is adaptable to each age groups to human body, its appropriate add other function ingredients after still
Original effect and quality can be kept.
1st, tourmaline is a kind of silicate mineral, and its chemical formula is na (mg, fe, mn, li, al) 3al6 (si6o18)
(bo3) 3 (oh, f) 4, it contacts under electrostatic field with hydrone, just hydrone can be ionized into hydrion (h+) and hydrogen-oxygen
Radical ion (oh-), hydroxide ion and water molecules form basic hydroxide group anion (h2o oh-), as " air bear from
Son ", current scientific research proves: anion can not only facilitate human body synthesis and vitamin storage, the life of strengthening and human activin
Reason activity, has highly important impact to the vital movement of human body and other biological, is referred to as " air vitamin ".Anion
Active adsorption interior harmful substance, the such as construction and decoration harmful substance such as formaldehyde, toluene, not only itself do not increase pollution, Er Qieqing
Purifying room air, is inherently eliminated construction and decoration syndrome, ensures that health is unaffected.
2nd, the Chinese medicine ingredients containing in the present invention, not only thin to staphylococcuses, tubercule bacillus, bacillus pyocyaneus, Grain-negative
Multiple pathogenic bacteria such as bacterium and gram-positive bacteria and funguses have certain suppression, killing action；Fragrant odour simultaneously, property is gentle,
Pure and fresh soothe the spirit, help hormone secretion, the effect of anxiety of releiving, also there is certain mosquito-repelling effect simultaneously, more it is essential that
The life-time service present invention will not produce harmful effect it is adaptable to each age groups to human body, before having application widely
Scape.
Specific embodiment
Embodiment.
Water-base writing ink composition it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight
Amount part, bis-phenol a19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine
3.3 weight portions, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surface
Activating agent compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, institute
The pigment stating mill base is high-carbon black pigment, and the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanium
Stone, fluorite, tourmaline, gahnite are dravite and lithium electricity by weight the mixture of 2.5:3:3.7:2, wherein tourmaline
By weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine passes through such as gas stone
Lower step is prepared from,
S1, take Fructus Carpesii 35 weight portion clean, naturally dry, be subsequently placed in 90 DEG C of frying pans and fry to savory effusion, then spray
Deionized water 17 weight portion, is placed in constant temperature oven less than 60 DEG C and dries, water content≤6.5%；
S2, Cortex Moutan 16 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality 3.7
Times, put into and steam in pot thoroughly, take out, dry, the concentration of saline is 27%；
S3, by lavandula angustifolia 12 weight portion, Herba Anemones Hupehensiss 4.5 weight portion, rhododendron molle (bl.) g.don 1 weight portion, the Rhizoma Atractylodis Macrocephalae 1 weight portion, sweet Ma Yu
Blue 0.75 weight portion decontamination, is put into together with step s1 and the made crude drug of s2 and is crushed to 60 mesh in super micron mill, is obtained
Crude drug powder, standby；
S4, by step s3 be obtained crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, adjust extraction
Pressure power 27.65mpa, 45.10 DEG C of extraction temperature, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, are directly separating
Kettle outlet triangular flask collects volatile oil a, standby；
S5, by Herba Artemisiae Scopariae 15.5 weight portion, Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 15.5 weight portion, Rhizoma Acori Graminei 4.5
Weight portion clean dry, together put into super micron mill in be crushed to 70 mesh, then plus deionized water soak 6 hours, amount of water
By 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, prepared Traditional Chinese drug mixture, standby；
S6, the Traditional Chinese drug mixture that step s5 is obtained decoct 2 hours in 80 DEG C, collect distillate, and add ether to extract, distillation
Then plus anhydrous sodium sulfate drying the volume ratio of liquid and ether is 2:1, takes upper oil phase, that is, volatile oil b is obtained, standby；
S7, step s4 and s6 made volatile oil a and volatile oil b mixing are mixed well prepared miscella, then sequentially add while stirring
Peppermint essential oil, sarranine flower essential oil, Geranium Essential, Herba Duchesneae Indicae quintessence oil and P-Cymene, are sufficiently stirred for 35 minutes, stand 30 minutes,
It is sufficiently stirred for mixing well, filtering and impurity removing, obtains final product essential oil of traditional Chinese medicine, wherein, described miscella and Peppermint essential oil, sarranine flower essential oil, India
The mass ratio of certain herbaceous plants with big flowers quintessence oil, Herba Duchesneae Indicae quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, also include Herba Origani oil 1.3 weight portion in the crude drug powder of step s3 and spend in vain
Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step s5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4
Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step s7 also includes Eucalyptus oil 0.3 weight portion.
Test the ink in this above-described embodiment using air ion static method of testing, anion burst size is in 430-650
Individual/m3, and sustained release negative aeroion, it is more beneficial for long-term purify air, reach the basic demand of health of people.
Reference examples.
Colour carbon black 20g, phenol 11g, glycerol 4g, BTA 3g, triethanolamine 1g, triethylamine 3g, sodium bicarbonate
5g, polyoxyethylene groups ethers nonionic fluorocarbon surfactant 1.5g, slow releasing agent 0.4g, Origanum majorana quintessence oil 0.6g, Semen Tritici aestivi
Bud quintessence oil 0.5g, Herba Lysimachiae foenum-graeci quintessence oil 0.5g, Radix Paeoniae Alba quintessence oil 0.4g, cypress quintessence oil 0. 4g, eucalyptus quintessence oil 0.4g, Folium Artemisiae Argyi essence
Oily 0. 4g, Peppermint essential oil 0.4g, deionized water 75g.
Test the ink in this above-mentioned reference examples using air ion static method of testing, anion burst size is in 0/m3,
There is no the function of release negative aeroion.
(1) acute toxicity test is carried out to obtained essential oil of traditional Chinese medicine, result is as follows:
1. Mouse oral acute toxicity test: the ld50 of Mouse oral essential oil of traditional Chinese medicine is 383.55g/kg, 95% credible is limited to
294.68g/kg～499.31g/kg.And the toxicity criterion of air freshener is: Mouse oral anxious poison ld50 >=5g/
Kg, is judged to nontoxic.The ld50 of this essential oil of traditional Chinese medicine is higher than 76 times of nontoxic standard, therefore, it is determined that being nontoxic.
2. chmice acute toxicity on inhalation test: the lc50 that chmice acute sucks essential oil of traditional Chinese medicine is 24863.99g/m3,95%
Credible be limited to 16837.34g/m3～33387.46g/m3.And the toxicity criterion of air freshener is: chmice acute
Suck (2h) lc50 ＞ 10000mg/m3, the nontoxic level in true border.The lc50 of this essential oil of traditional Chinese medicine is higher than the 2486 of nontoxic standard
Times, therefore, it is determined that being nontoxic.
Through inspection, its fragrance, color and luster, refraction index, relative density, arsenic content, heavy metal contain obtained essential oil of traditional Chinese medicine
Amount, ph value all meet the requirement of national standard.
(2) check above-mentioned ink anion burst size result such as table 1:
(3) repelling effect test.
Carry out contrast test according to the repelling effect of common ink of the prior art and above-described embodiment ink inside, test
Data is shown in Table 2.
Conclusion: the ink in the embodiment of the present invention has certain repelling effect.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, common for art
For technical staff, can also make other changes in different forms on the basis of the above description, here need not
All of embodiment cannot be exhaustive, all any modifications within the spirit and principles in the present invention, made, equivalent replace
Change, improve, be still included within protection scope of the present invention.
Claims (1)
1. water-base writing ink composition it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight
Part, bis-phenol a19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine
3.3 weight portions, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surface
Activating agent compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, institute
The pigment stating mill base is high-carbon black pigment, and the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanium
Stone, fluorite, tourmaline, gahnite are dravite and lithium electricity by weight the mixture of 2.5:3:3.7:2, wherein tourmaline
By weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine passes through such as gas stone
Lower step is prepared from,
S1, take Fructus Carpesii 35 weight portion clean, naturally dry, be subsequently placed in 90 DEG C of frying pans and fry to savory effusion, then spray
Deionized water 17 weight portion, is placed in constant temperature oven less than 60 DEG C and dries, water content≤6.5%；
S2, Cortex Moutan 16 weight portion is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality 3.7
Times, put into and steam in pot thoroughly, take out, dry, the concentration of saline is 27%；
S3, by lavandula angustifolia 12 weight portion, Herba Anemones Hupehensiss 4.5 weight portion, rhododendron molle (bl.) g.don 1 weight portion, the Rhizoma Atractylodis Macrocephalae 1 weight portion, sweet Ma Yu
Blue 0.75 weight portion, Herba Origani oil 1.3 weight portion and Herba et Flos Pyrethri Cinerariifolii 1.5 weight portion decontamination, with step s1 and the made raw material of s2
Medicine puts into together in super micron mill and is crushed to 60 mesh, and prepared crude drug powder is standby；
S4, by step s3 be obtained crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, adjust extraction
Pressure power 27.65mpa, 45.10 DEG C of extraction temperature, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, are directly separating
Kettle outlet triangular flask collects volatile oil a, standby；
S5, by Herba Artemisiae Scopariae 15.5 weight portion, Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 15.5 weight portion, Rhizoma Acori Graminei 4.5
Weight portion, Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4 weight portion are cleaned and are dried, and put in super micron mill together and are crushed to 70 mesh, so
Afterwards plus deionized water soaks 6 hours, amount of water by 6.5 times of immersions crude drug quality, dispersed with stirring is mixed well, and prepared Chinese medicine is mixed
Compound, standby；
S6, the Traditional Chinese drug mixture that step s5 is obtained decoct 2 hours in 80 DEG C, collect distillate, and add ether to extract, distillation
Then plus anhydrous sodium sulfate drying the volume ratio of liquid and ether is 2:1, takes upper oil phase, that is, volatile oil b is obtained, standby；
S7, step s4 and s6 made volatile oil a and volatile oil b mixing are mixed well prepared miscella, then sequentially add while stirring
Peppermint essential oil, sarranine flower essential oil, Geranium Essential, Herba Duchesneae Indicae quintessence oil and P-Cymene, are sufficiently stirred for 35 minutes, stand 30 minutes,
It is sufficiently stirred for mixing well, filtering and impurity removing, obtains final product essential oil of traditional Chinese medicine, wherein, described miscella and Peppermint essential oil, sarranine flower essential oil, India
The mass ratio of certain herbaceous plants with big flowers quintessence oil, Herba Duchesneae Indicae quintessence oil and P-Cymene is 1.3:0.4:0.75:0.6:0.5:0.3, in described essential oil of traditional Chinese medicine also
Include Eucalyptus oil 0.3 weight portion.
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