CN106147393A - Colored ink for teaching board - Google Patents

Colored ink for teaching board Download PDF

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Publication number
CN106147393A
CN106147393A CN201610735646.3A CN201610735646A CN106147393A CN 106147393 A CN106147393 A CN 106147393A CN 201610735646 A CN201610735646 A CN 201610735646A CN 106147393 A CN106147393 A CN 106147393A
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weight portion
oil
weight
traditional chinese
extraction
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魏本武
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/16—Writing inks
    • C09D11/17—Writing inks characterised by colouring agents
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/16—Writing inks
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The color ink for the teaching board can release air anions for a long time, purify air and benefit human health; also has certain inhibiting and killing effects on staphylococcus, escherichia coli, gram-positive bacteria and other various germs and fungi; meanwhile, the refreshing tea has fragrant smell, is fresh and refreshing, relieves pressure, can leave lasting fragrance after being used, has the health-care effects of refreshing and restoring consciousness and eliminating fatigue, is suitable for all ages, and has very wide application prospect.

Description

A kind of board of education colour prepared Chinese ink
The application is the Application No. 2016107230060 submitted to August 25 2016 applying date, invention entitled " one The colored prepared Chinese ink that kind of light-color teaching board uses " the divisional application of Chinese invention patent application.
Technical field
The present invention relates to a kind of prepared Chinese ink, particularly to a kind of board of education colour prepared Chinese ink.
Background technology
Prepared Chinese ink can be used for routine office work or textile printing field, but traditional general prepared Chinese ink do not have refresh oneself and generation bear from The health-care effects such as son, user use when long produces taediumvitae, due to the function singleness of tradition prepared Chinese ink, can not meet people Multi-demands.
Summary of the invention
The deficiency existed for prior art, the user that the present invention is prepared Chinese ink provides a kind of abnormal smells from the patient pure and fresh, has and refresh oneself Effect and the prepared Chinese ink of negative ion health effect, it is possible not only to discharge for a long time negative aeroion, purifies air, beneficially human body strong Health；Also the multiple pathogenic bacterias such as staphylococcus, escherichia coli, gram-positive bacteria and fungus are had certain suppression, killing action；With Time fragrant odour, pure and fresh soothe the spirit, pressure of releiving, also can expelling mosquito, human body will not be produced harmful effect, have widely Application prospect.
It is an object of the invention to be achieved through the following technical solutions:
A kind of board of education colour prepared Chinese ink, it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight Part, bisphenol-A 19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine 3.3 weight portions, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surface Activating agent compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, institute The pigment stating mill base is high-carbon black pigment, and the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanium Stone, fluorite, tourmaline, gahnite are by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and lithium electricity Gas stone is by weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, and wherein said essential oil of traditional Chinese medicine is by such as Lower step is prepared from,
S1, take Omphalia 35 weight portion and clean, naturally dry, be subsequently placed in 90 DEG C of frying pans stir-fry extremely savory effusion, then spray Deionized water 17 weight portion, is placed in less than 60 DEG C drying, water content≤6.5% in constant temperature oven；
S2, Radix Isatidis 18.5 weight is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality 3.7 Times, to put into and pot steams thoroughly, take out, dry, the concentration of saline is 27%；
S3, by lavandula angustifolia 12 weight portion, Herba anemones vitifoliae 4.5 weight portion, Herba Anemones Hupehensis 4.5 weight portion, Rhizoma Cimicifugae 1 weight portion, sweet horse Yu Lan 0.75 weight portion decontamination, puts into together with crude drug made with step S1 and S2 and is crushed to 60 mesh in super micron mill, system Obtain crude drug powder, standby；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, directly separating Still outlet triangular flask collects volatile oil A, standby；
S5, by Semen Torreyae 15.5 weight portion, Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 15.5 weight portion, Rhizoma Acori Graminei 4.5 Weight portion, Herba Menthae 1 weight is cleaned and is dried, and puts in super micron mill together and is crushed to 70 mesh, and then adding deionized water, to soak 6 little Time, amount of water by 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S6, Traditional Chinese drug mixture step S5 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate and be dried, i.e. prepares volatile oil B, standby；
S7, made to step S4 and S6 volatile oil A and volatile oil B are mixed and mixes well prepared miscella, then be sequentially added into while stirring P-Cymene, Geranium Essential, Essential Oil From Pine Needles, vanilla quintessence oil and rosemary ethereal oil, be sufficiently stirred for 35 minutes, stands 30 points Clock, is sufficiently stirred for mixing well, filtering and impurity removing, obtains essential oil of traditional Chinese medicine, wherein, and described miscella and P-Cymene, Geranium Essential, pine The mass ratio of pin quintessence oil, vanilla quintessence oil and rosemary ethereal oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the crude drug powder of step S3, also include Herba Origani oil 1.3 weight portion and spend in vain Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step S5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4 Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step S7 also includes Eucalyptus oil 0.3 weight portion.
Equipment, raw material and method involved in the present invention, is equipment, raw material and method that the industry usually uses, This repeats no more.
The most each essential oil component must be sufficiently mixed with surfactant, slow releasing agent, to reach slow release effect, each quintessence oil and The addition of anion natural mineral matter powder must be appropriate, not only antibiotic and sterilizing, moreover it is possible to stable emotion, so to the not normal heart Reason state has the effect in front, can purify, pacify soul, can alleviate angry and beaten sensation, makes the people can be with the flat gas of the heart With ground in the face of life, because its energy centre of equilibrium is neural, thus helpful to alarmed and dejected state, also have the most flat Quiet with releive function, insomniac is had goodish relax to put console with spirit, for pacify hot-tempered enter or moody temper have Goodish effect, can improve work efficiency.
The present invention with reference to modern Chinese medicine pharmacological research, from the drug screening of existing Chinese medicine and repeatedly verifies, gives full play to respectively Group weight portion synergism, the most each Chinese medicinal components brief introduction is as follows.
Omphalia: bitter cold, returns stomach large intestine channel, slightly poisonous.Parasite killing.
Radix Isatidis: various bacteria is had inhibitory action, infusion to bacillus subtilis, staphylococcus aureus, sarcine, Escherichia coli, Bacillus typhi, Salmonella paratyphi, dysentery (will he, Freund) bacillus, bacillus enteritidis etc. have suppression in various degree Effect；Acetone leachate also has similar effect, and effective to Hemolytic streptococcus.
Lavandula angustifolia can remove ant, except roach, acaricide, the when of being placed under wardrobe, medicated pillow, not only can replace camphor ball, moreover it is possible to stay The fragrance of one people that oozes lower, research finds, lavandula angustifolia has obvious antibacterial action, and the linalool contained in lavandula angustifolia is lavandula angustifolia Antibacterial main component, it can suppress 17 kinds of antibacterials (including gram-negative bacteria and gram-positive bacteria), the life of 10 kinds of funguses Long.
Herba anemones vitifoliae: have another name called Herba anemones vitifoliae, blow Paeonia suffruticosa, soil Paeonia suffruticosa, Qiu Mingju, your ship chrysanthemum, parasite killing；Heat-clearing and toxic substances removing, parasite killing；Clearly Pyrolysis poison.
Herba Anemones Hupehensis: 1. " Shaanxi Chinese herbal medicine ": " bitter, cool, slightly poisonous." 2. " Chinese herbal medicine is commonly used in Sichuan ": " and toil, temperature, Slightly poisonous." removing toxic substances, evacuation of pus granulation promoting, dissipating blood stasis of subsiding a swelling, have and kill maggot, wriggler, change long-pending, detumescence, dissipating blood stasis, control stubborn dermatitis, tinea alba, malaria Disease, infantile malnutrition, dysentery, carbuncle furuncle swells, scrofula, traumatic injury.
Rhizoma Cimicifugae: have antibacterial action, to being permitted blue achorion, Du big belly microspore tinea bacterium, rust microspore tinea bacterium, redness difficult to understand Epidermophyton, staphylococcus aureus, anthrax bacillus have stronger inhibitory action；To group B streptococcus, diphtheria corynebacterium, typhoid fever bar Bacterium, bacillus pyocyaneus, escherichia coli, dysentery bacterium also have inhibitory action in various degree, also have calmness, convulsion work simultaneously With.
Origanum majorana: can improve that mood is depressed and addictive disease, especially effective to liberal-mindedness and vigorous endurance stress symptom, can expand blood vessel, Blood pressure lowering, alleviate and burden, help to eliminate cardiopalmus, have the nerve of excellence to pacify and calm function.
Semen Torreyae " herbal classic ": pathogen in main abdomen, goes three worms, and Serpentis stings.
Cortex ulmi pumilae: for dry bark or the root bark of Ulmaceae, sweet, flat, nontoxic；Diuretic, treating stranguria, detumescence, for urine Obstructed, stranguria with turbid discharge, edema, carbuncle carbuncle on the back, erysipelas, scabies.
Lignum Aquilariae Resinatum: " Compendium of Materia Medica " record wood have strong antibacterial efficacy, fragrance enters spleen, clear god regulates the flow of vital energy, tonifying five ZANG-organs, cough-relieving Reduce phlegm, warming the stomach warming the spleen, ventilation analgesic therapy, can be used as medicine, be first-class medical material superfine product.
Lignum cinnamomi camphorae: aiphyllium, bark yellowish-brown, there is irregular longitudinal crack, on the south main product the Changjiang river and various places, southwest.Winter Cut down trees and split broken or be sawn into bulk, dry or air-dry.Timber bulk is not of uniform size, surface red brown to burgundy, and transverse section is visible Annual ring.Matter is heavily hard.Having strong Camphora fragrance, taste is refrigerant, has pungent sense, warm in nature, acrid in the mouth；Only sensible can ward off dirty, warming middle-JIAO Bitterly, dampness removing parasite killing.
Rhizoma Acori Graminei: its flower, stem aromatic flavor, has the effect had one's ideas straightened out, eliminate the phlegm, dissipate wind, and epidemic disease of can dispelling Fructus Alpiniae Oxyphyllae, building body can Make spice or mosquito dispersing.
Herba Menthae: for the dry aerial parts of labiate Herba Menthae, dispelling wind and heat pathogens, the clear profit head, sore-throat relieving rash, soothing the liver row Gas.
P-Cymene: to anthrax bacillus, Alpha-hemolytic streptococcus, B-Streptococcus hemolyticus, diphtheria corynebacterium, bacillus pseudodiphthericus, lung 10 kinds of Gram-positives such as diplococcoid, staphylococcus aureus, Staphylococcus citreus, white Portugal Portugal coccus, bacillus subtilis Aerophil all has antibacterial action, also has bacteriostasis for multiple pathomycete.
Geranium Essential: there is hemostasis, vasoconstrictive, asthma, liver and expelling toxin, cholelithiasis, kidney toxin expelling, renal calculus, diuresis, flesh Carnic acid pain, oily skin, aging skin activates, herpes, palor, and fat-reducing promotes to scab, eczema, sunburn of burning, tinea, the moon Through having some setbacks, engorgement of breasts inflammation, alleviate melancholy uneasy, there is deodorization, antibacterial, the effect of sterilization.
Essential Oil From Pine Needles: the quintessence oil i.e. extracted from Folium Pini.This oils, rich in unsaturated fatty acid, is that " dissolving " gallbladder is solid In alcohol, removing blood vessel, the important composition of impurity, can effectively remove endovascular excess cholesterol, plays very reducing blood viscosity Big effect.It can also promote blood vessel elasticity simultaneously, makes blood flow smooth and easy, and it can regulate blood pressure, and hyperpietic is had antihypertensive effect, Essential Oil From Pine Needles is also the secret factor that blood pressure rises dual regulation.
Vanilla quintessence oil: have special fragrance, have resisting fatigue and mood is gloomy, help hormone secretion, anxiety of releiving and Improve the effects such as insomnia.There is heart tonifying, supplementing the brain, stomach invigorating, removing toxic substances, wind dispelling, effect of enhancing muscle strength, make aroma type nerveous system System analeptic and kidney-reinforcing drug, be used for treating hysteria, melancholia, sexual impotence, deficiency-heat and rheumatism.
Rosemary ethereal oil: have tranquillizing and allaying excitement, refreshment effect, all has certain curative effect to dyspepsia and stomachache, has town Quiet, diuresis, it is possible to being used for treating the multiple diseases such as insomnia, cardiopalmus, headache, dyspepsia, external can treat wound and pass Joint inflammation.Also there is strong heart, promote that metabolism, the blood circulation etc. of promotion peripheral vessel act on.
Herba Origani oil: the herb of Labiatae origanum Adeps Bovis seu Bubali ORIGZNUM VUL-GAREL., has another name called dysentery relieving chaste tree careless, wild The ground such as mustard symbol name, have heat clearing away, removing dampness, drive away summer heat, induce sweat, the sterilization of regulating the flow of vital energy extremely strong, bacteriostasis, the volatilization extracted from Adeps Bovis seu Bubali Oil, to 31 kinds of common cause enteritis antibacterials and shigella flexneri, is the pure Chinese medicine additive most with broad-spectrum antiseptic.
Herba et Flos Pyrethri Cinerariifolii: Tanacetum vulgare L belongs to the general designation of (Tanacetum) several plants, removing dampness and killing parasites, kills pubic louse, head louse, body Louse, flea, effect except mosquito parasite killing.
Borneolum Syntheticum: pungent, bitter, cool.Having refreshment of having one's ideas straightened out, heat clearing away dissipates poison, improving acuity of vision and removing nebula.Cure mainly calentura unconsciousness due to high fever, middle wind-phlegm Fainting infantile convulsion, heat-damp in summer blinds clear key, and sore throat is deaf, and aphtha tooth swells, carbuncle sore infantile malnutrition hemorrhoid, conjunctival congestion and swelling pain, pterygium.
Folium Nelumbinis: for the leaf of nymphaeaceae plant lotus, have the effect of heat-clearing and toxic substances removing, removing heat from blood, hemostasis.There is clearing away summer-heat and eliminating dampness, rise and send out clearly The effects such as sun, cooling blood for hemostasis.
Eucalyptus oil: one of most common and widest quintessence oil of purposes, has good health-care effect, helps focused attention Power.Can effectively alleviate sinus infection, influenza, bronchitis, cold nasal obstruction and other respiratory system diseases.There is good resisting Bacterium and sterilization idiocratic, in some certain food, Eucalyptus oil is also as fragrance component.This quintessence oil is carried at whilst on tour, permissible Effectively resist mosquito bite and insect bite, treat skin measles.It it is good anophelifuge.Mixing with water can become a kind of and simple and effective disappear Toxic agent.
Beneficial effects of the present invention:
The present invention provides a kind of abnormal smells from the patient pure and fresh for user, has stimulating effect and the prepared Chinese ink of negative ion health effect, and it is not only Negative aeroion can be discharged for a long time, purify air, beneficially health；Also thin to staphylococcus, escherichia coli, Grain-positive The multiple pathogenic bacteria such as bacterium and fungus have certain suppression, killing action；Fragrant odour simultaneously, pure and fresh soothes the spirit, and pressure of releiving also can drive Catch up with mosquito, human body will not be produced harmful effect, it is adaptable to each age groups, its appropriate add other function ingredients after still Original effect and quality can be kept.
1, tourmaline is a kind of silicate mineral, and it contacts with hydrone under electrostatic field, just can be by hydrone electricity From becoming hydrion and hydroxide ion, hydroxide ion forms basic hydroxide group anion with water molecules, be " air bear from Son ", current scientific research proves: anion can not only facilitate human body synthesis and vitamin storage, strengthening and the life of human activin Reason activity, has highly important impact to the vital movement of human body and other biological, is referred to as " air vitamin ".Anion Active adsorption indoor harmful substance, such as the construction and decoration harmful substance such as formaldehyde, toluene, not only self does not increase pollution, Er Qieqing Purifying room air, is inherently eliminated construction and decoration syndrome, ensures that health is unaffected.
2, the Chinese medicine ingredients contained in the present invention, not only thin to staphylococcus, tubercule bacillus, bacillus pyocyaneus, Grain-negative The multiple pathogenic bacteria such as bacterium and gram-positive bacteria and fungus have certain suppression, killing action；Fragrant odour simultaneously, character is gentle, Pure and fresh soothe the spirit, help hormone secretion, the effect of anxiety of releiving, also there is certain mosquito-repelling effect simultaneously, more it is essential that The life-time service present invention will not produce harmful effect to human body, it is adaptable to each age groups, before having application widely Scape.
Detailed description of the invention
Embodiment.
A kind of board of education colour prepared Chinese ink, it is characterised in that: by following component by weight: dispersible pigment color paste 23 Weight portion, bisphenol-A 19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, three second Amine 3.3 weight portion, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, table Face activating agent compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, The pigment of described mill base is high-carbon black pigment, and the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is Germanite, fluorite, tourmaline, gahnite are by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and lithium Tourmaline is by weight the mixture of 5:3, and particle diameter≤13 μm of described active mineral matter powder, wherein said essential oil of traditional Chinese medicine passes through Following steps are prepared from,
S1, take Omphalia 35 weight portion and clean, naturally dry, be subsequently placed in 90 DEG C of frying pans stir-fry extremely savory effusion, then spray Deionized water 17 weight portion, is placed in less than 60 DEG C drying, water content≤6.5% in constant temperature oven；
S2, Radix Isatidis 18.5 weight is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality 3.7 Times, to put into and pot steams thoroughly, take out, dry, the concentration of saline is 27%；
S3, by lavandula angustifolia 12 weight portion, Herba anemones vitifoliae 4.5 weight portion, Herba Anemones Hupehensis 4.5 weight portion, Rhizoma Cimicifugae 1 weight portion, sweet horse Yu Lan 0.75 weight portion decontamination, puts into together with crude drug made with step S1 and S2 and is crushed to 60 mesh in super micron mill, system Obtain crude drug powder, standby；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, directly separating Still outlet triangular flask collects volatile oil A, standby；
S5, by Semen Torreyae 15.5 weight portion, Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 15.5 weight portion, Rhizoma Acori Graminei 4.5 Weight portion, Herba Menthae 1 weight is cleaned and is dried, and puts in super micron mill together and is crushed to 70 mesh, and then adding deionized water, to soak 6 little Time, amount of water by 6.5 times of immersion crude drug quality, dispersed with stirring is mixed well, and prepares Traditional Chinese drug mixture, standby；
S6, Traditional Chinese drug mixture step S5 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate and be dried, i.e. prepares volatile oil B, standby；
S7, made to step S4 and S6 volatile oil A and volatile oil B are mixed and mixes well prepared miscella, then be sequentially added into while stirring P-Cymene, Geranium Essential, Essential Oil From Pine Needles, vanilla quintessence oil and rosemary ethereal oil, be sufficiently stirred for 35 minutes, stands 30 points Clock, is sufficiently stirred for mixing well, filtering and impurity removing, obtains essential oil of traditional Chinese medicine, wherein, and described miscella and P-Cymene, Geranium Essential, pine The mass ratio of pin quintessence oil, vanilla quintessence oil and rosemary ethereal oil is 1.3:0.4:0.75:0.6:0.5:0.3.
In a preferred embodiment, in the crude drug powder of step S3, also include Herba Origani oil 1.3 weight portion and spend in vain Pyrethrum 1.5 weight portion.
In a preferred embodiment, the Traditional Chinese drug mixture of step S5 also includes Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4 Weight portion.
In a preferred embodiment, the essential oil of traditional Chinese medicine of step S7 also includes Eucalyptus oil 0.3 weight portion.
Using air ion static method of testing to test the prepared Chinese ink in this above-described embodiment, anion burst size is at 430-650 Individual/m3, and sustained release negative aeroion, it is more beneficial for purifying for a long time air, reaches the basic demand of health of people.
Reference examples.
Colour carbon black 20g, phenol 11g, glycerol 4g, BTA 3g, triethanolamine 1g, triethylamine 3g, sodium bicarbonate 5g, polyoxyethylene groups ethers nonionic fluorocarbon surfactant 1.5g, slow releasing agent 0.4g, Origanum majorana quintessence oil 0.6g, Semen Tritici aestivi Bud quintessence oil 0.5g, Herba Lysimachiae foenum-graeci quintessence oil 0.5g, Radix Paeoniae Alba quintessence oil 0.4g, cypress quintessence oil 0. 4g, eucalyptus quintessence oil 0.4g, Folium Artemisiae Argyi essence Oil 0. 4g, Peppermint essential oil 0.4g, deionized water 75g.
Using air ion static method of testing to test the prepared Chinese ink in this above-mentioned reference examples, anion burst size is at 0/m3, Not there is the function of release negative aeroion.
(1) obtained essential oil of traditional Chinese medicine being carried out acute toxicity test, result is as follows:
1. Mouse oral acute toxicity test: the LD50 of Mouse oral essential oil of traditional Chinese medicine is 383.55g/kg, 95% credible be limited to 294.68g/kg～499.31g/kg.And the toxicity criterion of air freshener is: Mouse oral anxious poison LD50 >=5g/ Kg, it is determined that for nontoxic.The LD50 of this essential oil of traditional Chinese medicine is higher than 76 times of nontoxic standard, therefore, it is determined that be nontoxic.
2. chmice acute toxicity on inhalation test: it is 24863.99g/m3 that chmice acute sucks the LC50 of essential oil of traditional Chinese medicine, 95% Credible be limited to 16837.34g/m3～33387.46g/m3.And the toxicity criterion of air freshener is: chmice acute Suck (2h) LC50 ＞ 10000mg/m3, the nontoxic level in true border.The LC50 of this essential oil of traditional Chinese medicine is higher than the 2486 of nontoxic standard Times, therefore, it is determined that be nontoxic.
Obtained essential oil of traditional Chinese medicine is through inspection, and its fragrance, color and luster, refraction index, relative density, arsenic content, heavy metal contain Amount, pH value all meet the requirement of national standard.
(2) above-mentioned ink anion burst size result such as table 1 is checked:
(3) repelling effect test.
Contrast test is carried out with the repelling effect of prepared Chinese ink in above-described embodiment, test according to common prepared Chinese ink of the prior art Data are shown in Table 2.
Conclusion: the prepared Chinese ink in the embodiment of the present invention has certain repelling effect.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, common for art For technical staff, can also make other changes in different forms on the basis of the above description, here without also Cannot all of embodiment be given exhaustive, all within the spirit and principles in the present invention, any amendment of being made, equivalent are replaced Change, improvement etc., within being still included in protection scope of the present invention.

Claims (1)

1. a board of education colour prepared Chinese ink, it is characterised in that: by following component by weight: dispersible pigment color paste 23 weight Amount part, bisphenol-A 19 weight portion, glycerol 4.5 weight portion, anhydrous sodium sulfate 2.3 weight portion, triethanolamine 2.7 weight portion, triethylamine 3.3 weight portions, acetone 3.6 weight portion, double thiocarbamate 0.25 weight portions, active mineral matter powder 1.7 weight portion, surface Activating agent compound 1.2 weight portion, slow releasing agent 0.55 weight portion, essential oil of traditional Chinese medicine 3.85 weight portion, deionized water 62 weight portion, institute The pigment stating mill base is high-carbon black pigment, and the mean diameter of described dispersible pigment color paste is 75nm, and described active mineral matter powder is germanium Stone, fluorite, tourmaline, gahnite are by weight the mixture of 2.5:3:3.7:2, and wherein tourmaline is dravite and lithium electricity Gas stone is by weight the mixture of 5:3, particle diameter≤13 μm of described active mineral matter powder, and wherein said essential oil of traditional Chinese medicine is by such as Lower step is prepared from,
S1, take Omphalia 35 weight portion and clean, naturally dry, be subsequently placed in 90 DEG C of frying pans stir-fry extremely savory effusion, then spray Deionized water 17 weight portion, is placed in less than 60 DEG C drying, water content≤6.5% in constant temperature oven；
S2, Radix Isatidis 18.5 weight is cleaned, puts in saline and soak 3.5 hours, the salt water yield by immersion spice quality 3.7 Times, to put into and pot steams thoroughly, take out, dry, the concentration of saline is 27%；
S3, by lavandula angustifolia 12 weight portion, Herba anemones vitifoliae 4.5 weight portion, Herba Anemones Hupehensis 4.5 weight portion, Rhizoma Cimicifugae 1 weight portion, sweet horse Yu Lan 0.75 weight portion, Herba Origani oil 1.3 weight portion and Herba et Flos Pyrethri Cinerariifolii 1.5 weight portion decontamination, made with step S1 and S2 former Material medicine puts into together in super micron mill and is crushed to 60 mesh, prepares crude drug powder, standby；
S4, by step S3 prepare crude drug powder put into supercritical carbon dioxide extraction apparatus extraction kettle in, regulation extraction Pressure power 27.65MPa, extraction temperature 45.10 DEG C, carbon dioxide flow is 0.6m3/ h, dynamic extraction 2.5h, directly separating Still outlet triangular flask collects volatile oil A, standby；
S5, by Semen Torreyae 15.5 weight portion, Cortex ulmi pumilae 8.5 weight portion, Lignum Aquilariae Resinatum 2.5 weight portion, Lignum cinnamomi camphorae 15.5 weight portion, Rhizoma Acori Graminei 4.5 Weight portion, Herba Menthae 1 weight, Borneolum Syntheticum 0.6 weight portion and Folium Nelumbinis 0.4 weight portion are cleaned and are dried, and put into powder in super micron mill together Be broken to 70 mesh, then add deionized water and soak 6 hours, amount of water by 6.5 times of immersions crude drug quality, dispersed with stirring tune Even, prepare Traditional Chinese drug mixture, standby；
S6, Traditional Chinese drug mixture step S5 prepared decoct 2 hours in 80 DEG C, collect distillate, and add ether extraction, distillation Liquid is 2:1 with the volume ratio of ether, takes upper oil phase, then adds anhydrous sodium sulfate and be dried, i.e. prepares volatile oil B, standby；
S7, made to step S4 and S6 volatile oil A and volatile oil B are mixed and mixes well prepared miscella, then be sequentially added into while stirring P-Cymene, Geranium Essential, Essential Oil From Pine Needles, vanilla quintessence oil and rosemary ethereal oil, be sufficiently stirred for 35 minutes, stands 30 points Clock, is sufficiently stirred for mixing well, filtering and impurity removing, obtains essential oil of traditional Chinese medicine, wherein, and described miscella and P-Cymene, Geranium Essential, pine The mass ratio of pin quintessence oil, vanilla quintessence oil and rosemary ethereal oil is 1.3:0.4:0.75:0.6:0.5:0.3, described essential oil of traditional Chinese medicine In also include Eucalyptus oil 0.3 weight portion.
CN201610735646.3A 2016-02-19 2016-08-25 Colored ink for teaching board Pending CN106147393A (en)

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CN2016100936769 2016-02-19
CN201610093676.9A CN105504989A (en) 2016-02-19 2016-02-19 Color ink for light-color teaching board
CN201610723006.0A CN106118241A (en) 2016-02-19 2016-08-25 The colored prepared Chinese ink that a kind of light-color teaching board uses

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CN201610735646.3A Pending CN106147393A (en) 2016-02-19 2016-08-25 Colored ink for teaching board
CN201610723006.0A Pending CN106118241A (en) 2016-02-19 2016-08-25 The colored prepared Chinese ink that a kind of light-color teaching board uses

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Application publication date: 20161123