CN106318691A - Ultrafine calcium powder-containing bacteriostasis liquid detergent and preparation method thereof - Google Patents
Ultrafine calcium powder-containing bacteriostasis liquid detergent and preparation method thereof Download PDFInfo
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- CN106318691A CN106318691A CN201610640708.2A CN201610640708A CN106318691A CN 106318691 A CN106318691 A CN 106318691A CN 201610640708 A CN201610640708 A CN 201610640708A CN 106318691 A CN106318691 A CN 106318691A
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- China
- Prior art keywords
- calcium powder
- ultra micro
- liquid detergent
- detergent containing
- antibacterial liquid
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/1233—Carbonates, e.g. calcite or dolomite
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
Abstract
The invention discloses an ultrafine calcium powder-containing bacteriostasis liquid detergent and a preparation method thereof. The ultrafine calcium powder-containing bacteriostasis liquid detergent comprises, by weight, 70-85% of deionized water, 10-25% of a surfactant, 2-10% of a washing auxiliary agent and 0.01-1% of ultrafine calcium powder. The ultrafine calcium powder-containing bacteriostasis liquid detergent has good permeability, good cleaning effects and good sterilization effects, can effectively inhibit bacteria, can remove pesticide residues, contains eco-friendly and nontoxic ingredients, has no side effect on the human body health and can be used for a long time.
Description
Technical field
The present invention relates to cleaning agent technical field, particularly to a kind of antibacterial liquid detergent containing ultra micro calcium powder and preparation thereof
Method.
Background technology
Liquid detergent is current consumption articles for use, can clean kitchen tools, tableware and fruit and vegerable.In order to remove kitchen tools, tableware and fruit
The antibacterial on vegetables surface, people often add antibacterial substance, such as bleaching powder, sodium hypochlorite etc., these chemical classes in liquid detergent
Although antibacterial substance can be good with bacteriostasis property, but is corrosive human body or vessel, also penetrating odor is readily volatilized
To environment.How to improve the composition of existing liquid detergent so that it is while there is preferable clean effect, possess stable
, eco-friendly bacteriostasis property, be to be presently required to solve the technical problem that.
Summary of the invention
For above-mentioned the deficiencies in the prior art, the present invention provides a kind of antibacterial liquid detergent containing ultra micro calcium powder and preparation thereof
Method.
The technical scheme is that such realization:
A kind of antibacterial liquid detergent containing ultra micro calcium powder, including the component of following percentage by weight: deionized water 70-
85%, surfactant 10-25%, washing assisant 2-10% and ultra micro calcium powder 0.01-1%.
The antibacterial liquid detergent permeability that above formula is joined is good, strong detergency, and bactericidal effect is good, be have fungistatic effect and
Deoil under the conditions of same recipe, detergent that clean effect is optimal, can effectively suppress antibacterial, remove pesticide residue,
And each component environment-protecting asepsis, health is had no side effect, can be with life-time service.
Preferably, surfactant is alkyl polyglucoside, sodium alkyl benzene sulfonate, glycine betaine, amine oxide, ethyl oxidation of alkyl sulfur
One or more in acid sodium.
Preferably, during washing assisant is sodium metasilicate, sodium carbonate, sodium citrate, salicylic acid, citric acid any one or
The combination that person is several.
Preferably, the raw material of ultra micro calcium powder is one or more in Margarita, shell or calcium mineral matter, described ultra micro
The particle diameter of calcium powder is 1-100 μm.
Preferably, shell is one or more in Concha Tridacna squamosa shellfish, Concha Ostreae shellfish and Concha rapanae thomasianae, calcium mineral matter be limestone and
One or both in Stalactitum.
Natural seashell powder, as primary raw material, can quickly be scattered in clear water, has good absorption pesticide and kills
Kitchen tools, tableware and fruit and vegerable are had good washability, and product are natural harmless by bacterium fresh keeping property, and degradable meets ring
Guaranteed request.
Preferably, the component of following percentage by weight is also included: Kazon 0.1-0.6% and sodium chloride 2.5-5%.
The effective chemical analysis of Kazon is isothiazolone, and its antibacterial efficiency is high, and degradability is good, does not produce residual, operation peace
Entirely, compatibility good, stability is strong, use cost is low.Sodium chloride is viscosity modifier, can increase the viscosity of liquid, to liquid detergent
Use and outward appearance the most critically important.
The invention allows for the preparation method of a kind of antibacterial liquid detergent containing ultra micro calcium powder, first prepare ultra micro calcium powder,
Again by various raw material mix homogeneously, finally it is stirred continuously in the agitator of 50-60 DEG C until forming stable and uniform liquid.
Preferably, the preparation process of ultra micro calcium powder includes: cleans, pulverize, calcine, grind, hydrolyze, dry, superfine grinding；
Pulverizing is to particle diameter 10-20mm the raw material pulverizing after cleaning；
The temperature of calcining is 600-1200 DEG C, the time is 3-8h；
Grinding be calcining after raw mill to 10-30 μm；
Dry temperature be 280 DEG C, the time be 2-6h.
Compared with prior art, the antibacterial liquid detergent permeability containing ultra micro calcium powder that the present invention prepares is good, strong detergency,
Bactericidal effect is good, can effectively suppress antibacterial, remove pesticide residue, and each component environment-protecting asepsis, to health without pair
Effect, can be with life-time service.
Detailed description of the invention
Below the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment
It is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
All other embodiments that art personnel are obtained under not making creative work premise, broadly fall into the model of present invention protection
Enclose.
Embodiment 1
A kind of antibacterial liquid detergent containing ultra micro calcium powder, including the component of following percentage by weight: deionized water 83.2%,
Alkyl polyglucoside 8%, ethyl oxidation of alkyl sodium sulfate 4%, amine oxide 2%, citric acid 0.5%, the Margarita ultrafine ultramicropowder of particle diameter 10 μm
With agstone 0.2%, Kazon 0.1% and sodium chloride 2%.
The preparation method of the above-mentioned antibacterial liquid detergent containing ultra micro calcium powder, first prepares Margarita ultrafine ultramicropowder and agstone, then
By various raw material mix homogeneously, finally it is stirred continuously in the agitator of 60 DEG C until forming stable and uniform liquid；
Margarita ultrafine ultramicropowder includes with the preparation process of agstone: cleans, pulverize, calcine, grind, hydrolyze, dry, ultra micro
Grind；Pulverizing is to particle diameter 20mm the raw material pulverizing after cleaning；The temperature of calcining is 1200 DEG C, the time is 5h；Grinding is handle
Raw mill after calcining is to 10 μm；Dry temperature be 280 DEG C, the time be 3h.
Embodiment 2
A kind of antibacterial liquid detergent containing ultra micro calcium powder, including the component of following percentage by weight: deionized water 76%, alkane
Base benzene sulfonic acid sodium salt 15%, sodium metasilicate 4.5%, the Margarita ultrafine ultramicropowder 0.4% of particle diameter 1 μm, Kazon 0.2% and sodium chloride 3.9%.
The preparation method of the above-mentioned antibacterial liquid detergent containing ultra micro calcium powder, first prepares Margarita ultrafine ultramicropowder, then by various raw materials
Mix homogeneously, is finally stirred continuously until forming stable and uniform liquid in the agitator of 52 DEG C；
The preparation process of Margarita ultrafine ultramicropowder includes: cleans, pulverize, calcine, grind, hydrolyze, dry, superfine grinding；Pulverize
It is to particle diameter 10mm the raw material pulverizing after cleaning；The temperature of calcining is 1000 DEG C, the time is 6h；Grinding be calcining after former
Abrasive lapping is to 10 μm；Dry temperature be 280 DEG C, the time be 4h.
Embodiment 3
A kind of antibacterial liquid detergent containing ultra micro calcium powder is including the component of following percentage by weight: deionized water 80%, sweet
Dish alkali 10%, sodium carbonate 4.4%, the ultra micro Concha Tridacna squamosa shellfish powder 0.2% of particle diameter 100 μm, Kazon 0.6% and sodium chloride 3%.
The preparation method of the above-mentioned antibacterial liquid detergent containing ultra micro calcium powder, first prepares ultra micro calcium powder, then is mixed by various raw materials
Closing uniformly, being finally stirred continuously in the agitator of 50 DEG C until forming stable and uniform liquid；
The preparation process of ultra micro Concha Tridacna squamosa shellfish powder includes: cleans, pulverize, calcine, grind, hydrolyze, dry, superfine grinding；Powder
Broken is to particle diameter 15mm the raw material pulverizing after cleaning；The temperature of calcining is 900 DEG C, the time is 5h；Grinding is after calcining
Raw mill is to 20 μm；Dry temperature be 280 DEG C, the time be 3h.
Embodiment 4
A kind of antibacterial liquid detergent containing ultra micro calcium powder, including the component of following percentage by weight: deionized water 76%, oxygen
Change amine 10%, sodium citrate 10%, the ultra micro Concha Ostreae shellfish powder 0.1% of particle diameter 50 μm, Kazon 0.5% and sodium chloride 3.4%.
The preparation method of the above-mentioned antibacterial liquid detergent containing ultra micro calcium powder, first prepares ultra micro calcium powder, then is mixed by various raw materials
Closing uniformly, being finally stirred continuously in the agitator of 58 DEG C until forming stable and uniform liquid；
The preparation process of ultra micro Concha Tridacna squamosa shellfish powder includes: cleans, pulverize, calcine, grind, hydrolyze, dry, superfine grinding；Powder
Broken is to particle diameter 20mm the raw material pulverizing after cleaning；The temperature of calcining is 900 DEG C, the time is 5h；Grinding is after calcining
Raw mill is to 30 μm；Dry temperature be 280 DEG C, the time be 3h.
Embodiment 5
A kind of antibacterial liquid detergent containing ultra micro calcium powder, including the component of following percentage by weight: deionized water 70%, second
Base oxidation of alkyl sodium sulfate 25%, salicylic acid 2%, the ultra micro Concha rapanae thomasianae powder 0.4% of particle diameter 60 μm, Kazon 0.1% and sodium chloride
2.5%.
The preparation method of the above-mentioned antibacterial liquid detergent containing ultra micro calcium powder, first prepares ultra micro calcium powder, then is mixed by various raw materials
Closing uniformly, being finally stirred continuously in the agitator of 55 DEG C until forming stable and uniform liquid；
The preparation process of ultra micro Concha rapanae thomasianae powder includes: cleans, pulverize, calcine, grind, hydrolyze, dry, superfine grinding；Powder
Broken is to particle diameter 20mm the raw material pulverizing after cleaning；The temperature of calcining is 600 DEG C, the time is 8h；Grinding is after calcining
Raw mill is to 10 μm；Dry temperature be 280 DEG C, the time be 5h.
Embodiment 6
A kind of antibacterial liquid detergent containing ultra micro calcium powder, including the component of following percentage by weight: deionized water 78%, alkane
Base glucosides 6%, glycine betaine 6%, citric acid 4.5%, the ultra micro agstone of particle diameter 50 μm and Stalactitum powder 1%, Kazon 0.5%
With sodium chloride 4%.
The preparation method of the above-mentioned antibacterial liquid detergent containing ultra micro calcium powder, first prepares ultra micro calcium powder, then is mixed by various raw materials
Closing uniformly, being finally stirred continuously in the agitator of 60 DEG C until forming stable and uniform liquid；
The preparation process of ultra micro Concha rapanae thomasianae powder includes: cleans, pulverize, calcine, grind, hydrolyze, dry, superfine grinding；Powder
Broken is to particle diameter 15mm the raw material pulverizing after cleaning；The temperature of calcining is 980 DEG C, the time is 8h；Grinding is after calcining
Raw mill is to 10 μm；Dry temperature be 280 DEG C, the time be 6h.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention
Within god and principle, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.
Claims (8)
1. the antibacterial liquid detergent containing ultra micro calcium powder, it is characterised in that: include the component of following percentage by weight: deionization
Water 70-85%, surfactant 10-25%, washing assisant 2-10% and ultra micro calcium powder 0.01-1%.
Antibacterial liquid detergent containing ultra micro calcium powder the most according to claim 1, it is characterised in that described surfactant is
One or more in alkyl polyglucoside, sodium alkyl benzene sulfonate, glycine betaine, amine oxide, ethyl oxidation of alkyl sodium sulfate.
Antibacterial liquid detergent containing ultra micro calcium powder the most according to claim 1, it is characterised in that described washing assisant is inclined
Any one or several combination in sodium silicate, sodium carbonate, sodium citrate, salicylic acid, citric acid.
Antibacterial liquid detergent containing ultra micro calcium powder the most according to claim 1, it is characterised in that described ultra micro calcium powder former
Material is one or more in Margarita, shell or calcium mineral matter, and the particle diameter of described ultra micro calcium powder is 1-100 μm.
Antibacterial liquid detergent containing ultra micro calcium powder the most according to claim 4, it is characterised in that described shell is Concha Tridacna squamosa
One or more in shellfish, Concha Ostreae shellfish and Concha rapanae thomasianae, described calcium mineral matter is one or both in limestone and Stalactitum.
6. according to the antibacterial liquid detergent containing ultra micro calcium powder described in any one of claim 1-5, it is characterised in that also include as
The component of lower percentage by weight: Kazon 0.1-0.6% and sodium chloride 2.5-5%.
7. the preparation method of the antibacterial liquid detergent containing ultra micro calcium powder as claimed in claim 1, it is characterised in that first make
Standby ultra micro calcium powder, then by various raw material mix homogeneously, be finally stirred continuously in the agitator of 50-60 DEG C until being formed stable equal
Even liquid.
The preparation method of the antibacterial liquid detergent containing ultra micro calcium powder the most according to claim 7, it is characterised in that micro-calcium
The preparation process of powder includes: cleans, pulverize, calcine, grind, hydrolyze, dry, superfine grinding；
Described pulverizing is to particle diameter 10-20mm the raw material pulverizing after cleaning；
The temperature of described calcining is 600-1200 DEG C, the time is 3-8h；
Described grinding be calcining after raw mill to 10-30 μm；
Described drying temperature is 280 DEG C, the time is 2-6h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610640708.2A CN106318691A (en) | 2016-08-08 | 2016-08-08 | Ultrafine calcium powder-containing bacteriostasis liquid detergent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610640708.2A CN106318691A (en) | 2016-08-08 | 2016-08-08 | Ultrafine calcium powder-containing bacteriostasis liquid detergent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
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| CN106318691A true CN106318691A (en) | 2017-01-11 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610640708.2A Pending CN106318691A (en) | 2016-08-08 | 2016-08-08 | Ultrafine calcium powder-containing bacteriostasis liquid detergent and preparation method thereof |
Country Status (1)
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109609289A (en) * | 2019-01-25 | 2019-04-12 | 李东 | A kind of calcined shell calcium powder fruits and vegetables cleaning powder and preparation method thereof |
| CN114456883A (en) * | 2022-02-16 | 2022-05-10 | 西北师范大学 | Clay-based fruit and vegetable cleaning powder |
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| CN103892285A (en) * | 2014-04-10 | 2014-07-02 | 青岛食安生物工程有限公司 | Process for preparing pure natural ultrafine calcium powder |
| CN104388208A (en) * | 2014-11-07 | 2015-03-04 | 舟山赛莱特海洋科技有限公司 | Method for preparing pesticide-removing fruit and vegetable cleaning agent based on shell powder |
| CN104877808A (en) * | 2015-06-26 | 2015-09-02 | 浙江海洋学院 | Method for preparing aquatic product cleaning agent based on shell powder |
| CN105779171A (en) * | 2016-04-07 | 2016-07-20 | 中海得金科技有限公司 | Micro-nano shell powder fruit-vegetable cleaning agent and preparation method thereof |
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2016
- 2016-08-08 CN CN201610640708.2A patent/CN106318691A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007302840A (en) * | 2006-05-15 | 2007-11-22 | Takenet:Kk | Detergent composition for laundry |
| CN101955864A (en) * | 2010-09-28 | 2011-01-26 | 广东海洋大学 | Environmentally-friendly shell cleaning powder and preparation method thereof |
| CN103892285A (en) * | 2014-04-10 | 2014-07-02 | 青岛食安生物工程有限公司 | Process for preparing pure natural ultrafine calcium powder |
| CN104388208A (en) * | 2014-11-07 | 2015-03-04 | 舟山赛莱特海洋科技有限公司 | Method for preparing pesticide-removing fruit and vegetable cleaning agent based on shell powder |
| CN104877808A (en) * | 2015-06-26 | 2015-09-02 | 浙江海洋学院 | Method for preparing aquatic product cleaning agent based on shell powder |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109609289A (en) * | 2019-01-25 | 2019-04-12 | 李东 | A kind of calcined shell calcium powder fruits and vegetables cleaning powder and preparation method thereof |
| CN114456883A (en) * | 2022-02-16 | 2022-05-10 | 西北师范大学 | Clay-based fruit and vegetable cleaning powder |
| CN114456883B (en) * | 2022-02-16 | 2023-09-19 | 西北师范大学 | Clay-based fruit and vegetable cleaning powder |
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Application publication date: 20170111 |