CN107384629A - A kind of powdery dish washing detergent and its production technology - Google Patents

A kind of powdery dish washing detergent and its production technology Download PDF

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Publication number
CN107384629A
CN107384629A CN201710661186.9A CN201710661186A CN107384629A CN 107384629 A CN107384629 A CN 107384629A CN 201710661186 A CN201710661186 A CN 201710661186A CN 107384629 A CN107384629 A CN 107384629A
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CN
China
Prior art keywords
raw material
carried out
powdery
inactivation
detergent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710661186.9A
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Chinese (zh)
Inventor
张先军
张宇
张先兵
张琳
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Anji Jiangsu Ya Daily Chemical Co Ltd
Original Assignee
Anji Jiangsu Ya Daily Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anji Jiangsu Ya Daily Chemical Co Ltd filed Critical Anji Jiangsu Ya Daily Chemical Co Ltd
Priority to CN201710661186.9A priority Critical patent/CN107384629A/en
Publication of CN107384629A publication Critical patent/CN107384629A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/044—Hydroxides or bases
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/1213—Oxides or hydroxides, e.g. Al2O3, TiO2, CaO or Ca(OH)2
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/1233—Carbonates, e.g. calcite or dolomite
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/384—Animal products

Abstract

The invention discloses a kind of powdery dish washing detergent and its production technology, the detergent is made up of the raw material of following mass percent：Soapberry 10%, anise 0.5% -6%, gleditsia sinensis 0.5% -2%, shell 3% -10%, calcium carbonate 15% -50%, magnesia 3% -5%, silica 2% -10%, concavo-convex ore deposit 5% -15%, amphoteric surfactant 1% -8%, dietary alkali 0.5% -2%, the production technology of the detergent, comprises the following steps：The purchasing of raw materials and material screening, sterilization inactivation, X miberal powders prepare, extract and cold reserve system, Y miberal powders prepare, dry-mixed preparation, final package.Present invention employs twice to sterilize inactivation process, and one of solid saponifiable extraction and the process of absorption and separating twice, its raw material are derived from nature green mineral and animals and plants, and not phosphorous, benzene, the molecule thing of chloride, are green products；When this product breaks a seal in use, under base catalysis effect, former absorptiveminerals discharge rapidly effective decontamination composition, to wash clean effect up to rapid.

Description

A kind of powdery dish washing detergent and its production technology
Technical field
The present invention relates to detergent technical field, and in particular to a kind of powdery dish washing detergent and its production technology, is applicable In the cleanings such as kitchen tools, toilet, floor and decontamination.
Background technology
At present, in the market detergent a great variety, Various Functions, but many products are meeting people's washing purpose simultaneously, Also unfriendly, even damage, destruction is generated to human body and environment.Especially a small number of pure chemical industry synthesis with human body frequency The product of numerous contact, such as hand washing meal（Kitchen, defend）Have detergent, in addition to more or less endangering human organ and system, Substantial amounts of water resource is also consumed, its washings is discharged into after water body, to consume a large amount of oxygen, and promotes water body unwanted growth, Degraded is slower, also there is long-term negative effect to soil.Meeting people's demand simultaneously to solve detergent, overcoming generation, these are secondary Effect, daily use chemicals industry have carried out many explorations and effort, have sought that people's daily life demand can be met always, and can is to ring The friendly beneficial product in border.
The content of the invention
It is an object of the invention to：For above-mentioned technical problem present in prior art, there is provided a kind of powdery tableware is washed Agent and its production technology are washed, to overcome above-mentioned caused side effect.
The present invention is achieved by the following technical solutions：
A kind of powdery dish washing detergent, is made up of the raw material of following mass percent：Soapberry 10% -40%, anise 0.5% - 6%th, gleditsia sinensis 0.5% -2%, shell 3% -10%, calcium carbonate 15% -50%, magnesia 3% -5%, silica 2% -10%, recessed Convex rod ore deposit 5% -15%, amphoteric surfactant 1% -8%, alkali 0.5% -2%.
A kind of production technology of powdery dish washing detergent as described above, comprises the following steps：
Step S1, the purchasing of raw materials, buying soapberry, anise, gleditsia sinensis, shell, calcium carbonate, magnesia, silica, concave convex rod Ore deposit, amphoteric surfactant, dietary alkali；
Step S2, by plant composition sieving and grading, sterilization inactivates and material screening, by plant raw material roasting, and from 150 DEG C Once sterilization inactivation is carried out to 60 DEG C of cooling-down types, then again crushes raw material more than 120 mesh；
Step S3, after the raw material that step S2 is obtained adds alkali, dry and wet mix is carried out under certain moisture content and temperature conditionss, is gone forward side by side 1 month or so saponification of row, carries out drying and other treatment, separating twice is standby afterwards；
Step S4, X miberal powder prepares, by the concave convex rod ore deposit in step S1, shell, calcium carbonate carry out crush 100 mesh more than, according to Than carrying out preparation mixing, re-pasteurization inactivation is then carried out；
Step S5, extraction and cold reserve system, the raw material that step S3 is obtained, in humidity 50-90,30 DEG C-50 DEG C of temperature, pressure Active ingredient absorption and extraction are carried out under 1-2 air pressure, in sealing container, and carries out cold reserve system；
Step S6, Y miberal powder is prepared, and silica, magnesia are carried out purity and hygrometry, and prepared according to dosage, Then inactivation treatment is baked and banked up with earth and sterilized to Y miberal powders；
Step S7, by the step S4 materials obtained and amphoteric surfactant under the conditions of air humidity 50-70, in desinfection chamber It is interior to carry out dry-mixed preparation, then with step S5 it is dry-mixed after, add Y miberal powders made from step S6；
Step S8, active ingredient is carried out to product and mark is detected, encapsulation is transferred to after qualified；
Step S9, final package, packing producing line of the finished product at 20 DEG C -30 DEG C encapsulates in desinfection chamber with dedicated custom Line is packaged.
In summary, by adopting the above-described technical solution, the beneficial effects of the invention are as follows：
1st, present invention employs twice to sterilize inactivation process, and one of solid phase extraction and absorption process, is used when this product breaks a seal When, under the effect of acid or base catalysis, former adsorbent meets water and discharges active surface active matter rapidly, strengthens clean result.
2nd, the present invention is meeting national standard simultaneously, also complies with world's green product standard, raw material is derived from nature green mineral And animals and plants, it is based on natural plants matter non-amphoteric surfactant, is aided with surfactant, silica, concave convex rod ore deposit Deng miberal powder agent, content of beary metal is all within national standard among them, while the also disputable compound such as not phosphorous, benzene, chlorine.
3rd, the present invention is powdery, is easy to use, transport and storage, at the same at normal temperatures will not spontaneous combustion, the mineral in formula Itself has anti-flaming function.
4th, during present invention washing, in the presence of surfactant and alkali, effectively washings meeting in the case of water is exceeded naturally It is secondary from adsorbent to discharge, promote clean result.
5th, the present invention is discharged into overall situation body after cleaning, due to its raw material physicochemical property, can to overall situation water body and There is lasting cleaning and improving effect in soil, be green product.
Embodiment
All features disclosed in this specification, or disclosed all methods or during the step of, except mutually exclusive Feature and/or step beyond, can combine in any way.
This specification（Including any accessory claim, summary）Disclosed in any feature, unless specifically stated otherwise, Replaced by other equivalent or with similar purpose alternative features.I.e., unless specifically stated otherwise, each feature is a series of An example in equivalent or similar characteristics.
Embodiment 1
A kind of powdery dish washing detergent, is made up of the raw material of following mass percent：Soapberry 15%, anise 6%, gleditsia sinensis 2%, Shell 3%, calcium carbonate 50%, magnesia 3%, silica 3%, concave convex rod ore deposit 15%, amphoteric surfactant 2%, dietary alkali 2%。
Embodiment 2
A kind of powdery dish washing detergent, is made up of the raw material of following mass percent：Soapberry 40%, anise 2%, gleditsia sinensis 1%, Shell 10%, calcium carbonate 15%, magnesia 3.5%, silica 1 3%, concave convex rod 10%, amphoteric surfactant 5%, dietary alkali 2%。
Embodiment 3
A kind of powdery dish washing detergent, is made up of the raw material of following mass percent：Soapberry 25%, anise 1%, gleditsia sinensis 3%, Shell 6%, calcium carbonate 30%, magnesia 10%, silica 1 5%, concave convex rod 8.5%, amphoteric surfactant 1%, dietary alkali 0.5%。
A kind of production technology of powdery dish washing detergent as described above, comprises the following steps：
Step S1, the purchasing of raw materials, buying soapberry, anise, gleditsia sinensis, shell, calcium carbonate, magnesia, silica, concave convex rod Ore deposit, amphoteric surfactant, dietary alkali；
Step S2, by plant composition sieving and grading, sterilization inactivates and material screening, by plant raw material roasting, and from 150 DEG C Once sterilization inactivation is carried out to 60 DEG C of cooling-down types, then again crushes raw material more than 120 mesh；
Step S3, after the raw material that step S2 is obtained adds alkali, dry and wet mix is carried out under certain moisture content and temperature conditionss, is gone forward side by side 1 month or so saponification of row, carries out drying and other treatment, separating twice is standby afterwards；
Step S4, X miberal powder prepares, by the concave convex rod ore deposit in step S1, shell, calcium carbonate carry out crush 100 mesh more than, according to Than carrying out preparation mixing, re-pasteurization inactivation is then carried out；
Step S5, extraction and cold reserve system, the raw material that step S3 is obtained, in humidity 50-90,30 DEG C-50 DEG C of temperature, pressure Active ingredient absorption and extraction are carried out under 1-2 air pressure, in sealing container, and carries out cold reserve system；
Step S6, Y miberal powder is prepared, and silica, magnesia are carried out purity and hygrometry, and prepared according to dosage, Then inactivation treatment is baked and banked up with earth and sterilized to Y miberal powders；
Step S7, by the step S4 materials obtained and amphoteric surfactant under the conditions of air humidity 50-70, in desinfection chamber It is interior to carry out dry-mixed preparation, then with step S5 it is dry-mixed after, add Y miberal powders made from step S6；
Step S8, active ingredient is carried out to product and mark is detected, encapsulation is transferred to after qualified；
Step S9, final package, packing producing line of the finished product at 20 DEG C -30 DEG C encapsulates in desinfection chamber with dedicated custom Line is packaged.
The usage of the present invention：
1. the method for scouring：After needing cleaning materials first to be moistened with water, with brush or rag（Or other soft materials）, it is stained with this product repeatedly Substrate is wiped, is then rinsed well with clear water.
2. infusion method：Substrate is immersed in illustrate to prepare in solution by this product and taken out within two to three minutes or so, with clear Water and rag or brush are dried.Practice display, such as warm water in using（30℃-65℃）Clean and immersion effect is more preferable.
Although the present invention is produced using dry pigmentation, gone out without a large amount of dust（It is only few micro, to human body and environment Also it is harmless）, in addition, reflecting according to experiment user, the present invention more economizes on water, and can be used simultaneously than original water saving 1/3rd or so Way is wider, and on tableware, kitchen tools, toilet, floor etc., object plane cleaning performance is all fine.
Particular embodiments described above, the purpose of the present invention, technical scheme and beneficial effect are carried out further in detail Describe in detail it is bright, should be understood that the foregoing is only the present invention specific embodiment, be not intended to limit the invention.This Invention expands to any new feature disclosed in this manual or any new combination, and any new method for disclosing or The step of process or any new combination.

Claims (2)

1. a kind of powdery dish washing detergent, it is characterised in that be made up of the raw material of following mass percent：Soapberry 10%- 40%th, anise 0.5% -6%, gleditsia sinensis 0.5% -2%, shell 3% -10%, calcium carbonate 15% -50%, magnesia 3% -5%, two Silica 2% -10%, concave convex rod ore deposit 5% -15%, amphoteric surfactant 1% -8%, alkali 0.5% -2%.
2. a kind of production technology of powdery dish washing detergent as claimed in claim 1, it is characterised in that comprise the following steps：
Step S1, the purchasing of raw materials, buying soapberry, anise, gleditsia sinensis, shell, calcium carbonate, magnesia, silica, concave convex rod Ore deposit, amphoteric surfactant, dietary alkali；
Step S2, by plant composition sieving and grading, sterilization inactivates and material screening, by plant raw material roasting, and from 150 DEG C Once sterilization inactivation is carried out to 60 DEG C of cooling-down types, then again crushes raw material more than 120 mesh；
Step S3, after the raw material that step S2 is obtained adds alkali, dry and wet mix is carried out under certain moisture content and temperature conditionss, is gone forward side by side 1 month or so saponification of row, carries out drying and other treatment, separating twice is standby afterwards；
Step S4, X miberal powder prepares, by the concave convex rod ore deposit in step S1, shell, calcium carbonate carry out crush 100 mesh more than, according to Than carrying out preparation mixing, re-pasteurization inactivation is then carried out；
Step S5, extraction and cold reserve system, the raw material that step S3 is obtained, in humidity 50-90,30 DEG C-50 DEG C of temperature, pressure Active ingredient absorption and extraction are carried out under 1-2 air pressure, in sealing container, and carries out cold reserve system；
Step S6, Y miberal powder is prepared, and silica, magnesia are carried out purity and hygrometry, and prepared according to dosage, Then inactivation treatment is baked and banked up with earth and sterilized to Y miberal powders；
Step S7, by the step S4 materials obtained and amphoteric surfactant under the conditions of air humidity 50-70, in desinfection chamber It is interior to carry out dry-mixed preparation, then with step S5 it is dry-mixed after, add Y miberal powders made from step S6；
Step S8, active ingredient is carried out to product and mark is detected, encapsulation is transferred to after qualified；
Step S9, final package, packing producing line of the finished product at 20 DEG C -30 DEG C encapsulates in desinfection chamber with dedicated custom Line is packaged.
CN201710661186.9A 2017-08-04 2017-08-04 A kind of powdery dish washing detergent and its production technology Pending CN107384629A (en)

Priority Applications (1)

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CN201710661186.9A CN107384629A (en) 2017-08-04 2017-08-04 A kind of powdery dish washing detergent and its production technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710661186.9A CN107384629A (en) 2017-08-04 2017-08-04 A kind of powdery dish washing detergent and its production technology

Publications (1)

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CN107384629A true CN107384629A (en) 2017-11-24

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108728269A (en) * 2018-08-03 2018-11-02 冠道（广州）科技有限公司 A kind of super Strong cleaning strengths nanometer coral calcium powder cleaning agent and preparation method thereof
CN110964608A (en) * 2019-12-13 2020-04-07 陕西速源节能科技有限公司 Preparation method of powerful decontamination cleaning agent capable of cleaning inner surface

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1388236A (en) * 2001-05-25 2003-01-01 美蓓亚株式会社 Powder detergent
CN102533472A (en) * 2011-12-01 2012-07-04 天台县满园春农林开发有限公司 Process for producing pure-plant-original-powder detergent suitable for machine washing
CN102911797A (en) * 2012-11-14 2013-02-06 沈阳信达信息科技有限公司 Plant cleaner
CN103194329A (en) * 2013-03-30 2013-07-10 杭州师范大学 Environment-friendly type powder high-efficiency hand cleaner
CN105238600A (en) * 2014-07-11 2016-01-13 上海家化联合股份有限公司 Powdery natural cleaning composition for vegetables and fruits and preparation method thereof
CN106726865A (en) * 2016-11-11 2017-05-31 宁波亿拍客网络科技有限公司 It is a kind of to the addition of the daily chemical product that natural medicinal ingredient is not destroyed Chinese herbal medicine

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1388236A (en) * 2001-05-25 2003-01-01 美蓓亚株式会社 Powder detergent
CN102533472A (en) * 2011-12-01 2012-07-04 天台县满园春农林开发有限公司 Process for producing pure-plant-original-powder detergent suitable for machine washing
CN102911797A (en) * 2012-11-14 2013-02-06 沈阳信达信息科技有限公司 Plant cleaner
CN103194329A (en) * 2013-03-30 2013-07-10 杭州师范大学 Environment-friendly type powder high-efficiency hand cleaner
CN105238600A (en) * 2014-07-11 2016-01-13 上海家化联合股份有限公司 Powdery natural cleaning composition for vegetables and fruits and preparation method thereof
CN106726865A (en) * 2016-11-11 2017-05-31 宁波亿拍客网络科技有限公司 It is a kind of to the addition of the daily chemical product that natural medicinal ingredient is not destroyed Chinese herbal medicine

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108728269A (en) * 2018-08-03 2018-11-02 冠道（广州）科技有限公司 A kind of super Strong cleaning strengths nanometer coral calcium powder cleaning agent and preparation method thereof
CN108728269B (en) * 2018-08-03 2020-12-18 冠道（广州）科技有限公司 Ultra-strong cleaning nano coral calcium powder cleaning agent and preparation method thereof
CN110964608A (en) * 2019-12-13 2020-04-07 陕西速源节能科技有限公司 Preparation method of powerful decontamination cleaning agent capable of cleaning inner surface

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Application publication date: 20171124

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