CN103343056B - A kind of multi-functional washing oxygen particle and preparation method thereof - Google Patents

A kind of multi-functional washing oxygen particle and preparation method thereof Download PDF

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CN103343056B
CN103343056B CN201310321707.8A CN201310321707A CN103343056B CN 103343056 B CN103343056 B CN 103343056B CN 201310321707 A CN201310321707 A CN 201310321707A CN 103343056 B CN103343056 B CN 103343056B
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sodium carbonate
mucine
xylo
sulfonic acid
sodium sulfate
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CN103343056A (en
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龚志农
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SICHUAN LVJIE TECHNOLOGY Co Ltd
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SICHUAN LVJIE TECHNOLOGY Co Ltd
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Abstract

The present invention discloses a kind of multi-functional washing oxygen particle and preparation method thereof, solves existing cleaning product washing effect poor and human body is had to the problem of harm.This oxygen particle is made up of sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide and Xylo-Mucine.The preparation method of this oxygen particle, comprise: (1) raw material: sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide and Xylo-Mucine, various material mass ratio is respectively: sulfonic acid 5% ~ 10%, sodium carbonate 25% ~ 35%, sodium sulfate 10% ~ 25%, sodium carbonate peroxide 25% ~ 59%, Xylo-Mucine 1% ~ 5%; (2) under anhydrous and low constant temperature, mix sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide and Xylo-Mucine successively, obtain mixture; (3) under low temperature, granulation is carried out to mixture; (4) under constant temperature, the particle obtained is dried.Present invention process is simple, its obtained oxygen particle, and washing effect is good, has very strong to remove stain, sterilization, bleaching and odor removing ability.

Description

A kind of multi-functional washing oxygen particle and preparation method thereof
Technical field
The present invention relates to a kind of cleaning product, specifically, relate to a kind of multi-functional washing oxygen particle and preparation method thereof.
Background technology
At present, what the washing of the aspects such as clothing, family product, kitchenware mainly adopted is cleaning product, and as washing powder, washing liquid, cleaning liquid, washings etc., it has the function of stain, sterilization, bleaching and taste removal.
But, existing cleaning product on the market, all there is the problem of washing effect difference in it, the dirt on product and spot can not be removed well, its sterilizing ability also await improve, and due to cleaning product in use, it can with residual spot generation chemical reaction, then produce harmful gas (such as carbon monoxide, chlorine etc.), therefore, this returns user and brings certain harm.
In sum, the practicality of existing cleaning product is not high, therefore, develops the good and cleaning product of safety non-toxic of a kind of washing effect, just becomes one of content of those skilled in the art's primary study.
Summary of the invention
The object of the present invention is to provide a kind of multi-functional washing oxygen particle and preparation method thereof, mainly solve existing cleaning product washing effect poor and human body is had to the problem of harm.
To achieve these goals, the technical solution used in the present invention is as follows:
A kind of multi-functional washing oxygen particle, the material being following numerical value by mass ratio forms:
Sulfonic acid: 5% ~ 10%;
Sodium carbonate: 25% ~ 35%;
Sodium sulfate: 10% ~ 25%;
Sodium carbonate peroxide: 25% ~ 59%;
Xylo-Mucine: 1% ~ 5%.
Present invention also offers the preparation method of above-mentioned washing oxygen particle, comprise the following steps:
(1) raw material is prepared: sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine and water, the mass ratio of various material is respectively: sulfonic acid 5% ~ 10%, sodium carbonate 25% ~ 35%, sodium sulfate 10% ~ 25%, sodium carbonate peroxide 25% ~ 59%, Xylo-Mucine 1% ~ 5%;
(2) in anhydrous and temperature lower than under the constant temperature of 40 DEG C, mix sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide and Xylo-Mucine successively, obtain mixture;
(3) Squeezinggranulator is adopted under the constant temperature of temperature lower than 40 DEG C, the mixture in step (2) to be carried out granulation and extrudes;
(4) under constant temperature, the particle obtained is dried, and be packaged into bag.
Specifically, in described step (4), constant temperature fluidized-bed is adopted to dry the particle obtained.
Further, the washing oxygen particle effect that in the present invention, following proportioning is formed is especially good:
1, in described step (1), the mass ratio of sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine is respectively: sulfonic acid 5%, sodium carbonate 25%, sodium sulfate 10%, sodium carbonate peroxide 59%, Xylo-Mucine 1%.
2, in described step (1), the mass ratio of sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine is respectively: sulfonic acid 7.5%, sodium carbonate 30%, sodium sulfate 17.5%, sodium carbonate peroxide 42%, Xylo-Mucine 3%.
3, in described step (1), the mass ratio of sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine is respectively: sulfonic acid 10%, sodium carbonate 35%, sodium sulfate 25%, sodium carbonate peroxide 25%, Xylo-Mucine 5%.
Compared with prior art, the present invention has following beneficial effect:
(1) the present invention makes washing oxygen particle by rational preparation of raw material ratio, it takes full advantage of the oxygen performance alive of sodium carbonate peroxide, the content that sodium carbonate peroxide can be made to decompose oxygen at normal temperatures reduces, thus improve the content of its tensio-active agent, and fully demonstrated sodium carbonate peroxide and go stain, the function of bleaching and taste removal, and the Xylo-Mucine added has thickening as washing auxiliary detergent, dispersion, emulsification, the effect of suspension and stable foam, dirt is stably suspended in washings, thus can soil redeposition be prevented, therefore, the present invention can realize good washing effect, it compared with prior art, there is outstanding substantive distinguishing features and significant progress.
(2) the oxygen particle that the present invention obtains has very strong soil removability, and washing time is short, instant effect, and therefore, it can directly replace the cleaning product commonly used on the market to use.
(3) the oxygen particle that the present invention obtains has very strong sterilizing ability, the Sauerstoffatom that its water soluble produces, and can penetrate and kill various common germ and virus, and therefore, this kind of washing oxygen particle can be used as permanent stores for the daily sterilization of household and sterilization.
(4) the present invention adopts Squeezinggranulator to be extruded with the form of granulation by mixture, this kind of Squeezinggranulator have granulating rate high, without returning charge, granule strength is high, rounding is even, granulating moisture is low advantage, and the energy consumption of subsequent baking process can be reduced.
(5) the present invention adopts fluidized-bed to dry granulation, and fluidized-bed can make granulation to the same continuous feeding and discharging of fluid, and therefore, it is suitable for making final oxygen particle very much.
(6) cost performance of the present invention is high, and function is various, with strong points, technical process is simple, is with a wide range of applications, and its obtained oxygen particle can discharge the oxygen useful to human body in washing process, safe, nontoxic, therefore, the present invention has very high practical value and promotional value.
Embodiment
Below in conjunction with embodiment, the invention will be further described, and embodiments of the present invention include but not limited to the following example.
Embodiment 1
The present invention is mainly used in the washing of the article such as clothing, towel, quilt cover be made up of various materials such as cotton, fiber crops, silk, hair synthon, also can be applied to the washing of household, kitchenware aspect, the present invention has very strong decontamination and removes stain, sterilization, bleaching and odor removing ability.Specifically, the oxygen particle in the present invention is formed by the preparation of raw material of following mass ratio:
Sulfonic acid: 5% ~ 10%;
Sodium carbonate: 25% ~ 35%;
Sodium sulfate: 10% ~ 25%;
Sodium carbonate peroxide: 25% ~ 59%;
Xylo-Mucine: 1% ~ 5%.
Utilize above-mentioned raw materials, the present embodiment prepares raw material according to certain mass ratio, and make washing oxygen particle by preparation technology, this preparation technology comprises the following steps:
(1) raw material is prepared: sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine and water, the mass ratio of various material is respectively: sulfonic acid 5% ~ 10%, sodium carbonate 25% ~ 35%, sodium sulfate 10% ~ 25%, sodium carbonate peroxide 20% ~ 60%, Xylo-Mucine 1% ~ 5%;
In this step, the mass ratio of sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine is respectively: sulfonic acid 5%, sodium carbonate 25%, sodium sulfate 10%, sodium carbonate peroxide 59%, Xylo-Mucine 1%;
(2) order of the raw material in step (1) according to sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide and Xylo-Mucine mixed successively under constant temperature, anhydrous condition, its mixing temperature, lower than 40 DEG C, generally selects 30 DEG C;
(3) mixture that step (2) obtains is made granulation, for improving granulating rate, in the present embodiment, adopt Squeezinggranulator to be extruded with the form of granulation by mixture under the constant temperature of temperature lower than 40 DEG C, under being typically chosen in the constant temperature of 30 DEG C, carry out granulation;
(4) granulation being dried, for improving the production efficiency of oxygen particle, in the present embodiment, as preferably, adopting fluidized-bed granulation to be dried, dry the granulation obtained and be washing oxygen particle, be finally packaged into bag.
In above-mentioned preparation process, because sodium carbonate peroxide all can decomposite Sauerstoffatom when meeting water, heat, therefore, all need carry out under constant temperature when raw material mixing, extruder grain, the present embodiment preferably carries out raw material mixing and extruder grain under lower than the constant temperature of 40 DEG C, and adopt fluidized-bed granulation to be dried, so just can guarantee the oxygen performance alive of sodium carbonate peroxide to the full extent, enable last obtained oxygen particle be applied to the washing of product better.In the present invention, except the reaction of sulfonic acid and sodium carbonate is that except chemical reaction, all the other are physical change.
Because sodium carbonate peroxide component is very large in the present embodiment, therefore its clean effect is extremely strong, very be applicable to strong dirt-removing, such as the environment of the pollution of the emphasis such as kitchen, lavatory, easily breed bacteria, lower list 1 is the service check report that the present invention makes after professional inspection mechanism of Sichuan Province is detected as cleaning product:
Table 1
As can be seen from the above Table 1, gross activity thing and active o content all reach more than 6.5, and pH value is about 10, there is weakly alkaline, can well to product carry out moistening, foaming and decontamination, simultaneously, the content of all the other various materials all remains in suitable scope, therefore, the present invention has extraordinary washing effect, can be advantageously applied to the washing of product.
The present embodiment, to remove tea stain, sets forth use procedure of the present invention.
Prepare to be soaked with the glass teacup of tea stain, stainless steel teacup or plastic tea cup, in cup, first pour the warm water of 80 ~ 90% into, then add appropriate oxygen particle (being about about 10g).Wait for for some time quietly, can see that the warm water in teacup is dark brown shape, in water, have bubble to emerge, and the surfactant suspension of water there is the tea stain particle after dissolving, Here it is oxygen clean.Water is outwelled, then with rag, teacup is dried, just can obtain clean teacup, because oxygen particle can discharge oxygen in the process of washing, both useful to human body, again can not to environment, therefore, compared with existing cleaning product, its benefit is self-evident.
Embodiment 2
Be with the difference of embodiment 1, in the present embodiment, the mass ratio of described sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide and Xylo-Mucine is respectively: sulfonic acid 7.5%, sodium carbonate 30%, sodium sulfate 17.5%, sodium carbonate peroxide 42%, Xylo-Mucine 3%.The preparation process of the present embodiment is identical with embodiment 1.Under this proportioning, because sodium carbonate peroxide composition is more less slightly than embodiment 1, therefore its moderate performance, is relatively applicable to washing clothes, is usually used in the regular wash environment such as laundry, hospital, hotel.
Embodiment 3
Be with the difference of embodiment 1, in the present embodiment, the mass ratio of described sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide and Xylo-Mucine is respectively: sulfonic acid 10%, sodium carbonate 35%, sodium sulfate 25%, sodium carbonate peroxide 25%, Xylo-Mucine 5%.The preparation process of the present embodiment is identical with embodiment 1.Under this proportioning, sodium carbonate peroxide composition is minimum, and therefore its washing effect is relatively poor, but its taste removal, bleaching effect are then very outstanding, are relatively applicable to being not easy dirty article, if dining table, furniture etc. are to the less demanding article of decontamination.
According to above-described embodiment, just the present invention can be realized well.What deserves to be explained is; the foregoing is only several preferred embodiment of the present invention; not in order to limit the present invention, all do within body design thought of the present invention and principle any amendment, equivalent to replace and improvement etc., all should be included within protection scope of the present invention.

Claims (6)

1. a multi-functional washing oxygen particle, is characterized in that, the material being following numerical value by mass ratio forms:
Sulfonic acid: 5% ~ 10%;
Sodium carbonate: 25% ~ 35%;
Sodium sulfate: 10% ~ 25%;
Sodium carbonate peroxide: 25% ~ 59%;
Xylo-Mucine: 1% ~ 5%.
2. a preparation method for multi-functional washing oxygen particle, is characterized in that, comprise the following steps:
(1) raw material is prepared: sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine and water, the mass ratio of various material is respectively: sulfonic acid 5% ~ 10%, sodium carbonate 25% ~ 35%, sodium sulfate 10% ~ 25%, sodium carbonate peroxide 25% ~ 59%, Xylo-Mucine 1% ~ 5%;
(2) in anhydrous and temperature lower than under the constant temperature of 40 DEG C, mix sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide and Xylo-Mucine successively, obtain mixture;
(3) Squeezinggranulator is adopted under the constant temperature of temperature lower than 40 DEG C, the mixture in step (2) to be carried out granulation and extrudes;
(4) under constant temperature, the particle obtained is dried, and be packaged into bag.
3. the preparation method of a kind of multi-functional washing oxygen particle according to claim 2, is characterized in that, in described step (4), adopts constant temperature fluidized-bed to dry the particle obtained.
4. the preparation method of a kind of multi-functional washing oxygen particle according to Claims 2 or 3, it is characterized in that, in described step (1), the mass ratio of sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine is respectively: sulfonic acid 5%, sodium carbonate 25%, sodium sulfate 10%, sodium carbonate peroxide 59%, Xylo-Mucine 1%.
5. the preparation method of a kind of multi-functional washing oxygen particle according to Claims 2 or 3, it is characterized in that, in described step (1), the mass ratio of sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine is respectively: sulfonic acid 7.5%, sodium carbonate 30%, sodium sulfate 17.5%, sodium carbonate peroxide 42%, Xylo-Mucine 3%.
6. the preparation method of a kind of multi-functional washing oxygen particle according to Claims 2 or 3, it is characterized in that, in described step (1), the mass ratio of sulfonic acid, sodium carbonate, sodium sulfate, sodium carbonate peroxide, Xylo-Mucine is respectively: sulfonic acid 10%, sodium carbonate 35%, sodium sulfate 25%, sodium carbonate peroxide 25%, Xylo-Mucine 5%.
CN201310321707.8A 2013-07-29 2013-07-29 A kind of multi-functional washing oxygen particle and preparation method thereof Active CN103343056B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109181904A (en) * 2018-08-16 2019-01-11 上海菱量纳米科技有限公司 A kind of high efficiency environment protection clean powder and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1131185A (en) * 1995-12-20 1996-09-18 北京洛娃新型化工材料技术开发有限公司 Making bleaching compound soap power containing oxygen
CN1389554A (en) * 2002-06-18 2003-01-08 陶华西 Oxygen-containing detergent and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1131185A (en) * 1995-12-20 1996-09-18 北京洛娃新型化工材料技术开发有限公司 Making bleaching compound soap power containing oxygen
CN1389554A (en) * 2002-06-18 2003-01-08 陶华西 Oxygen-containing detergent and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109181904A (en) * 2018-08-16 2019-01-11 上海菱量纳米科技有限公司 A kind of high efficiency environment protection clean powder and preparation method thereof

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