CN106305863A - Antifungal insecticide for blueberries and preparation method and application thereof - Google Patents
Antifungal insecticide for blueberries and preparation method and application thereof Download PDFInfo
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- CN106305863A CN106305863A CN201610606939.1A CN201610606939A CN106305863A CN 106305863 A CN106305863 A CN 106305863A CN 201610606939 A CN201610606939 A CN 201610606939A CN 106305863 A CN106305863 A CN 106305863A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom not containing sulfur-to-oxygen bonds, e.g. polysulfides
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses an antifungal insecticide for blueberries and a preparation method and application thereof. The preparation method includes the steps that firstly, Chinese herbal medicines are decocted in water and filtered to obtain filtrate, and a Chinese herbal medicine extract is prepared; secondly, nano carbon, amino acid, pyridalyl and water are subjected to hydrothermal reaction, and a modified nano carbon solution is prepared; thirdly, water, fosetyl-aluminum, trypsin, humic acid, dimethyl disulfide, ergosterol, norethindrone, the Chinese herbal medicine extract and the modified nano carbon solution are mixed to prepare the antifungal insecticide for blueberries, wherein Chinese herbal medicines include menthol, mulberry twigs, stemona tuber, dried ginger, spatholobus suberctu, euphorbia pekinensis rupr and caulis trachelospermi. The insecticide prepared through the method can make blueberries effectively resist fungi, the preparation method is simple in process, and raw materials are easy to obtain.
Description
Technical field
The present invention relates to antifungal medicine, in particular it relates to a kind of antifungal medicine for blue berry and preparation method thereof
And application.
Background technology
Blue berry (Blueberry) can be divided into two kinds: a kind of is low shrub, and short-foot is wild, and fruit granule is little, but anthocyanidin
Content the highest；Another kind is artificial culture's blue berry, can grow to the height of 240cm, and fruit is relatively big, and moisture is more, anthocyanidin
Content is the most on the low side.The Vaccinium plant of whole world distribution is planted up to more than 400, originates in and main product is blue in U.S. that is otherwise known as of the U.S.
The certain kind of berries；China's blue berry mainly produces at Daxing'an Mountainrange and Xiao Xing'an Ling forest region especially Central Greater Khingan Mountains, and is all pure wild.
The most just domestication cultivates successfully.Containing abundant nutritional labeling in Blueberry, it not only has good nutrition
Health-care effect, also has and prevents that cranial nerve is aging, heart tonifying, anticancer vessel softening, strengthens the functions such as human organism's immunity.
Existing blue berry, in cultivating process, is often encroached on by factors such as disease, worm, grass, the wherein pest and disease damage of blue berry
Mainly there are mummy, stem canker disease, branch droop, leaf spot, virosis and aphid demodicid mite, weevil class, really maggot, leafhopper and shell
Worm etc..These infringements greatly have impact on the quality of the growth of blue berry, fruiting rate and fruit, the especially impact of disease.
Summary of the invention
It is an object of the invention to provide a kind of antifungal medicine for blue berry and its preparation method and application, pass through the party
The medicament that method prepares enables to blue berry effective against fungus, and this preparation method operation is simple simultaneously, raw material is easy to get.
To achieve these goals, the invention provides the preparation method of a kind of antifungal medicine for blue berry, including:
1) carry out Chinese herbal medicine in water decocting, crossing leaching filtrate with prepared extracts of Chinese herbal medicine；
2) nano-sized carbon, aminoacid, pyridalyl and water are carried out hydro-thermal reaction with prepared modified Nano carbon solution；
3) water, phosethyl-Al, trypsin, humic acid, Methyl disulfide, ergosterol, norethindrone, Chinese herbal medicine are carried
Take liquid to mix to prepare the antifungal medicine for blue berry with modified Nano carbon solution；
Wherein, Chinese herbal medicine is Mentholum, Ramulus Mori, the Radix Stemonae, Rhizoma Zingiberis, Caulis Spatholobi, Radix Euphorbiae Pekinensis and Caulis Trachelospermi.
Present invention also offers a kind of antifungal medicine for blue berry, this is used for the antifungal medicine of blue berry by above-mentioned
Method be prepared.
Invention further provides the application in blue berry antifungal of a kind of above-mentioned antifungal medicine for blue berry.
By technique scheme, the present invention passes through above steps and the synergism of each raw material so that prepared system
Medicament enable to blue berry effective against fungus, this preparation method operation is simple simultaneously, raw material is easy to get.
Other features and advantages of the present invention will be described in detail in detailed description of the invention part subsequently.
Detailed description of the invention
Hereinafter the detailed description of the invention of the present invention is described in detail.It should be appreciated that described herein specifically
Embodiment is merely to illustrate and explains the present invention, is not limited to the present invention.
The invention provides the preparation method of a kind of antifungal medicine for blue berry, including:
1) carry out Chinese herbal medicine in water decocting, crossing leaching filtrate with prepared extracts of Chinese herbal medicine；
2) nano-sized carbon, aminoacid, pyridalyl and water are carried out hydro-thermal reaction with prepared modified Nano carbon solution；
3) water, phosethyl-Al, trypsin, humic acid, Methyl disulfide, ergosterol, norethindrone, Chinese herbal medicine are carried
Take liquid to mix to prepare the antifungal medicine for blue berry with modified Nano carbon solution；
Wherein, Chinese herbal medicine is Mentholum, Ramulus Mori, the Radix Stemonae, Rhizoma Zingiberis, Caulis Spatholobi, Radix Euphorbiae Pekinensis and Caulis Trachelospermi.
Step 1 in the present invention) in, the consumption of each material can select in wide scope, but in order to carry further
The antifungal effect of this medicament high, it is preferable that in step 1) in, relative to the water of 300 weight portions, the consumption of Mentholum is
20-28 weight portion, the consumption of Ramulus Mori is 10-16 weight portion, and the consumption of the Radix Stemonae is 30-38 weight portion, and the consumption of Rhizoma Zingiberis is 4-9 weight
Amount part, the consumption of Caulis Spatholobi is 25-40 weight portion, and the consumption of Radix Euphorbiae Pekinensis is 40-62 weight portion, and the consumption of Caulis Trachelospermi is 22-34
Weight portion.
Step 1 in the present invention) in, decocting condition can select in wide scope, but in order to improve this further
The antifungal effect of medicament, it is preferable that in step 1) in, decoct and at least meet following condition: decoction temperature is 120-140
DEG C, decocting time is 5-7h.
Step 2 in the present invention) in, the consumption of each material can select in wide scope, but in order to carry further
The antifungal effect of this medicament high, it is preferable that in step 2) in, relative to the nano-sized carbon relative to 50 weight portions, aminoacid
Consumption be 12-19 weight portion, the consumption of pyridalyl is 31-42 weight portion, and the consumption of water is 150-300 weight portion.
Step 2 in the present invention) in, the actual conditions of hydro-thermal reaction can select in wide scope, but in order to enter
One step improves the antifungal effect of this medicament, it is preferable that in step 2) in, hydro-thermal reaction at least meets following condition: reaction
Temperature is 180-220 DEG C, and the response time is 4-8h.
Step 2 in the present invention) in, amino acid whose concrete kind can select in wide scope, but in order to enter one
Step improves the antifungal effect of this medicament, it is preferable that in step 2) in, aminoacid is selected from albumen propylhomoserin, valine, different bright ammonia
One or more in acid, lysine, threonine, tryptophan and phenylalanine.
Step 2 in the present invention) in, the particle diameter of nano-sized carbon can select in wide scope, but in order to carry further
The antifungal effect of this medicament high, it is preferable that in step 2) in, the particle diameter of nano-sized carbon is 10-30nm.
Step 3 in the present invention) in, the consumption of each material can select in wide scope, but in order to carry further
The antifungal effect of this medicament high, it is preferable that in step 3) in, relative to the water of 100 weight portions, the consumption of phosethyl-Al
For 2-8 weight portion, tryptic consumption is 5-11 weight portion, and the consumption of humic acid is 1-5 weight portion, the use of Methyl disulfide
Amount is 0.1-0.8 weight portion, and the consumption of ergosterol is 1.1-1.8 weight portion, and the consumption of norethindrone is 0.5-1.2 weight portion,
The consumption of extracts of Chinese herbal medicine is 30-39 weight portion, and the consumption of modified Nano carbon solution is 10-17 weight portion.
Step 3 in the present invention) in, the actual conditions of mixing can select in wide scope, but in order to further
Improve the antifungal effect of this medicament, it is preferable that mixing at least meets following condition: mixing temperature is 15-35 DEG C, during mixing
Between be 15-25min.
Present invention also offers a kind of antifungal medicine for blue berry, this is used for the antifungal medicine of blue berry by above-mentioned
Method be prepared.
Invention further provides the application in blue berry antifungal of a kind of above-mentioned antifungal medicine for blue berry.
Hereinafter will be described the present invention by embodiment.
Embodiment 1
1) by Mentholum, Ramulus Mori, the Radix Stemonae, Rhizoma Zingiberis, Caulis Spatholobi, Radix Euphorbiae Pekinensis, Caulis Trachelospermi, water according to 25:14:34:7:30:
The weight ratio of 52:29:300 is mixed and is incorporated at 130 DEG C decoction 6h, crosses leaching filtrate with prepared extracts of Chinese herbal medicine；
2) by nano-sized carbon (particle diameter is 20nm), aminoacid (albumen propylhomoserin), pyridalyl and water according to 50:17:38:200
Mixed hydro-thermal reaction 6h that is incorporated at 200 DEG C of weight ratio with prepared modified Nano carbon solution；
3) water, phosethyl-Al, trypsin, humic acid, Methyl disulfide, ergosterol, norethindrone, Chinese herbal medicine are carried
Take liquid and at 25 DEG C, mix 20min according to the weight ratio of 100:6:8:3:0.6:1.6:0.9:35:14 with modified Nano carbon solution
To prepare the antifungal medicine A1 for blue berry.
Embodiment 2
1) by Mentholum, Ramulus Mori, the Radix Stemonae, Rhizoma Zingiberis, Caulis Spatholobi, Radix Euphorbiae Pekinensis, Caulis Trachelospermi, water according to 20:10:30:4:25:
The weight ratio of 40:22:300 is mixed and is incorporated at 120 DEG C decoction 5h, crosses leaching filtrate with prepared extracts of Chinese herbal medicine；
2) by nano-sized carbon (particle diameter is 10nm), aminoacid (isoleucine), pyridalyl and water according to 50:12:31:150
Mixed hydro-thermal reaction 4h that is incorporated at 180 DEG C of weight ratio with prepared modified Nano carbon solution；
3) water, phosethyl-Al, trypsin, humic acid, Methyl disulfide, ergosterol, norethindrone, Chinese herbal medicine are carried
Take liquid and at 15 DEG C, mix 15min according to the weight ratio of 100:2:5:1:0.1:1.1:0.5:30:10 with modified Nano carbon solution
To prepare the antifungal medicine A2 for blue berry.
Embodiment 3
1) by Mentholum, Ramulus Mori, the Radix Stemonae, Rhizoma Zingiberis, Caulis Spatholobi, Radix Euphorbiae Pekinensis, Caulis Trachelospermi, water according to 28:16:38:9:40:
The weight ratio of 62:34:300 is mixed and is incorporated at 140 DEG C decoction 7h, crosses leaching filtrate with prepared extracts of Chinese herbal medicine；
2) by nano-sized carbon (particle diameter is 30nm), aminoacid (phenylalanine), pyridalyl and water according to 50:19:42:300
Mixed hydro-thermal reaction 8h that is incorporated at 220 DEG C of weight ratio with prepared modified Nano carbon solution；
3) water, phosethyl-Al, trypsin, humic acid, Methyl disulfide, ergosterol, norethindrone, Chinese herbal medicine are carried
Take liquid and at 35 DEG C, mix 25min according to the weight ratio of 100:8:11:5:0.8:1.8:1.2:39:17 with modified Nano carbon solution
To prepare the antifungal medicine A3 for blue berry.
Comparative example 1
Carry out preparing medicament B1, except for the difference that, step 1 according to the method for embodiment 1) in do not use Mentholum, Ramulus Mori, hundred
Portion and Rhizoma Zingiberis.
Comparative example 2
Carry out preparing medicament B2, except for the difference that, step 1 according to the method for embodiment 1) in do not use Caulis Spatholobi, Radix Euphorbiae Pekinensis,
Caulis Trachelospermi.
Comparative example 3
Carry out preparing medicament B3, except for the difference that, step 2 according to the method for embodiment 1) in do not use nano-sized carbon.
Comparative example 4
Carry out preparing medicament B4, except for the difference that, step 2 according to the method for embodiment 1) in do not use aminoacid.
Comparative example 5
Carry out preparing medicament B5, except for the difference that, step 2 according to the method for embodiment 1) in do not use pyridalyl.
Comparative example 6
Carry out preparing medicament B6, except for the difference that, step 3 according to the method for embodiment 1) in do not use extracts of Chinese herbal medicine.
Comparative example 7
Carry out preparing medicament B7, except for the difference that, step 3 according to the method for embodiment 1) in do not use modified Nano carbon molten
Liquid.
Detection example 1
Take a collection of bud stage blue berry as detection object, then to detection object spray Monilina Vaccinii-
Corybosi fungus (can induce mummy) and Phomopsis Vaccinii fungus (can induced ulcer sick), then by upper
Stating blue berry and be divided into 11 groups, wherein 10 groups are sprayed with above-mentioned medicament A1-A3 and B1-B7 respectively, and every 12h sprays once, the
11 groups of spray water, spray one week continuously, by observing the cure rate of statistics blue berry after January, wherein,At the diseased fruit rate of statistics blue berry after fruit maturation,Concrete outcome is shown in Table 1.
Table 1
| Group number | The material sprayed | Diseased fruit rate/% | Cure rate/% |
| 1 | A1 | 0.8 | 98 |
| 2 | A2 | 0.6 | 98 |
| 3 | A3 | 0.5 | 99 |
| 4 | B1 | 4.8 | 67 |
| 5 | B2 | 5.1 | 74 |
| 6 | B3 | 5.5 | 73 |
| 7 | B4 | 6.2 | 68 |
| 8 | B5 | 7.3 | 75 |
| 9 | B6 | 9.5 | 41 |
| 10 | B7 | 11.4 | 32 |
| 11 | Water | 42 | 0 |
By above-described embodiment, comparative example and detection example, the medicament that the present invention provides has excellence for blue berry
Anti-mycotic efficiency.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited in above-mentioned embodiment
Detail, in the technology concept of the present invention, technical scheme can be carried out multiple simple variant, this
A little simple variant belong to protection scope of the present invention.
It is further to note that each the concrete technical characteristic described in above-mentioned detailed description of the invention, at not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to various can
The compound mode of energy illustrates the most separately.
Additionally, combination in any can also be carried out between the various different embodiment of the present invention, as long as it is without prejudice to this
The thought of invention, it should be considered as content disclosed in this invention equally.
Claims (10)
1. the preparation method for the antifungal medicine of blue berry, it is characterised in that including:
1) carry out Chinese herbal medicine in water decocting, crossing leaching filtrate with prepared extracts of Chinese herbal medicine；
2) nano-sized carbon, aminoacid, pyridalyl and water are carried out hydro-thermal reaction with prepared modified Nano carbon solution；
3) water, phosethyl-Al, trypsin, humic acid, Methyl disulfide, ergosterol, norethindrone, described Chinese herbal medicine are carried
Take liquid to mix with modified Nano carbon solution to prepare the described antifungal medicine for blue berry；
Wherein, described Chinese herbal medicine is Mentholum, Ramulus Mori, the Radix Stemonae, Rhizoma Zingiberis, Caulis Spatholobi, Radix Euphorbiae Pekinensis and Caulis Trachelospermi.
Preparation method the most according to claim 1, wherein, in step 1) in, relative to the water of 300 weight portions, described thin
The consumption of lotus brain is 20-28 weight portion, and the consumption of described Ramulus Mori is 10-16 weight portion, and the consumption of the described Radix Stemonae is 30-38 weight
Part, the consumption of described Rhizoma Zingiberis is 4-9 weight portion, and the consumption of described Caulis Spatholobi is 25-40 weight portion, and the consumption of described Radix Euphorbiae Pekinensis is
40-62 weight portion, the consumption of described Caulis Trachelospermi is 22-34 weight portion.
Preparation method the most according to claim 1, wherein, in step 1) in, described decoction at least meets following condition: decoct
Boiling temperature and be 120-140 DEG C, decocting time is 5-7h.
4. according to the preparation method described in any one in claim 1-3, wherein, in step 2) in, relative to relative to 50
The nano-sized carbon of weight portion, described amino acid whose consumption is 12-19 weight portion, and the consumption of described pyridalyl is 31-42 weight portion,
The consumption of described water is 150-300 weight portion.
Preparation method the most according to claim 4, wherein, in step 2) in, described hydro-thermal reaction at least meets following bar
Part: reaction temperature is 180-220 DEG C, the response time is 4-8h.
Preparation method the most according to claim 4, wherein, in step 2) in, described aminoacid is selected from albumen propylhomoserin, figured silk fabrics ammonia
One or more in acid, isoleucine, lysine, threonine, tryptophan and phenylalanine.
Preparation method the most according to claim 4, wherein, in step 2) in, the particle diameter of described nano-sized carbon is 10-30nm.
8. according to the preparation method described in any one in claim 5-7, wherein, in step 3) in, relative to 100 weight portions
Water, the consumption of described phosethyl-Al is 2-8 weight portion, and described tryptic consumption is 5-11 weight portion, described humic
The consumption of acid is 1-5 weight portion, and the consumption of described Methyl disulfide is 0.1-0.8 weight portion, and the consumption of described ergosterol is
1.1-1.8 weight portion, the consumption of described norethindrone is 0.5-1.2 weight portion, and the consumption of described extracts of Chinese herbal medicine is 30-39 weight
Amount part, the consumption of described modified Nano carbon solution is 10-17 weight portion；
Preferably, described mixing at least meets following condition: mixing temperature is 15-35 DEG C, and incorporation time is 15-25min.
9. the antifungal medicine for blue berry, it is characterised in that the described antifungal medicine for blue berry is wanted by right
The method described in any one is asked in 1-8 to be prepared.
10. one kind is used for the application in blue berry antifungal of the antifungal medicine of blue berry as claimed in claim 9.
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