CN106172558A - Anti-crop smothering medicament for blue berry and its preparation method and application - Google Patents
Anti-crop smothering medicament for blue berry and its preparation method and application Download PDFInfo
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- CN106172558A CN106172558A CN201610607152.7A CN201610607152A CN106172558A CN 106172558 A CN106172558 A CN 106172558A CN 201610607152 A CN201610607152 A CN 201610607152A CN 106172558 A CN106172558 A CN 106172558A
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
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- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
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- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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Abstract
The invention discloses a kind of anti-crop smothering medicament for blue berry and its preparation method and application, this preparation method includes: 1) carry out Chinese herbal medicine in water decocting, crossing leaching filtrate with prepared extracts of Chinese herbal medicine；2) nano-sized carbon, aminoacid, pyridalyl and water are carried out hydro-thermal reaction with prepared modified Nano carbon solution；3) mix water, 2,4,6 trimethylanilines, yellow uride, diphenyl ether, sec-o-glucosylhamaudol, ergosterol, norethindrone, extracts of Chinese herbal medicine with modified Nano carbon solution to prepare the anti-crop smothering medicament being used for blue berry；Wherein, Chinese herbal medicine is Concretio Silicea Bambusae, Rhizoma Smilacis Glabrae, Fructus Hippophae, Rhizoma Zingiberis, Pericarpium Granati, Radix Gentianae Macrophyllae and Flos Campsis.The medicament prepared by the method enables to blue berry effective against crop smothering, and this preparation method operation is simple simultaneously, raw material is easy to get.
Description
Technical field
The present invention relates to anti-crop smothering medicament, in particular it relates to a kind of anti-crop smothering medicament for blue berry and preparation method thereof
And application.
Background technology
Blue berry (Blueberry) can be divided into two kinds: a kind of is low shrub, and short-foot is wild, and fruit granule is little, but anthocyanidin
Content the highest；Another kind is artificial culture's blue berry, can grow to the height of 240cm, and fruit is relatively big, and moisture is more, anthocyanidin
Content is the most on the low side.The Vaccinium plant of whole world distribution is planted up to more than 400, originates in and main product is blue in U.S. that is otherwise known as of the U.S.
The certain kind of berries；China's blue berry mainly produces at Daxing'an Mountainrange and Xiao Xing'an Ling forest region especially Central Greater Khingan Mountains, and is all pure wild.
The most just domestication cultivates successfully.Containing abundant nutritional labeling in Blueberry, it not only has good nutrition
Health-care effect, also has and prevents that cranial nerve is aging, heart tonifying, anticancer vessel softening, strengthens the functions such as human organism's immunity.
Existing blue berry, in cultivating process, is often encroached on by factors such as disease, worm, grass, the wherein pest and disease damage of blue berry
Mainly there are mummy, stem canker disease, branch droop, leaf spot, virosis and aphid demodicid mite, weevil class, really maggot, leafhopper and shell
Worm etc..These infringements greatly have impact on the quality of the growth of blue berry, fruiting rate and fruit, the especially impact of crop smothering.
Summary of the invention
It is an object of the invention to provide a kind of anti-crop smothering medicament for blue berry and its preparation method and application, pass through the party
The medicament that method prepares enables to blue berry effective against crop smothering, and this preparation method operation is simple simultaneously, raw material is easy to get.
To achieve these goals, the invention provides the preparation method of a kind of anti-crop smothering medicament for blue berry, including:
1) carry out Chinese herbal medicine in water decocting, crossing leaching filtrate with prepared extracts of Chinese herbal medicine；
2) nano-sized carbon, aminoacid, pyridalyl and water are carried out hydro-thermal reaction with prepared modified Nano carbon solution；
3) by water, 2,4,6-trimethylaniline, yellow uride, diphenyl ether, sec-o-glucosylhamaudol, ergosterol, norethindrone, Chinese herbal medicine
Extracting solution mixes with modified Nano carbon solution to prepare the anti-crop smothering medicament for blue berry；
Wherein, Chinese herbal medicine is Concretio Silicea Bambusae, Rhizoma Smilacis Glabrae, Fructus Hippophae, Rhizoma Zingiberis, Pericarpium Granati, Radix Gentianae Macrophyllae and Flos Campsis.
Present invention also offers a kind of anti-crop smothering medicament for blue berry, this is used for the anti-crop smothering medicament of blue berry by above-mentioned
Method be prepared.
Invention further provides the application in the anti-crop smothering of blue berry of a kind of above-mentioned anti-crop smothering medicament for blue berry.
By technique scheme, the present invention passes through above steps and the synergism of each raw material so that prepared system
Medicament enable to blue berry effective against crop smothering, this preparation method operation is simple simultaneously, raw material is easy to get.
Other features and advantages of the present invention will be described in detail in detailed description of the invention part subsequently.
Detailed description of the invention
Hereinafter the detailed description of the invention of the present invention is described in detail.It should be appreciated that described herein specifically
Embodiment is merely to illustrate and explains the present invention, is not limited to the present invention.
The invention provides the preparation method of a kind of anti-crop smothering medicament for blue berry, including:
1) carry out Chinese herbal medicine in water decocting, crossing leaching filtrate with prepared extracts of Chinese herbal medicine；
2) nano-sized carbon, aminoacid, pyridalyl and water are carried out hydro-thermal reaction with prepared modified Nano carbon solution；
3) by water, 2,4,6-trimethylaniline, yellow uride, diphenyl ether, sec-o-glucosylhamaudol, ergosterol, norethindrone, Chinese herbal medicine
Extracting solution mixes with modified Nano carbon solution to prepare the anti-crop smothering medicament for blue berry；
Wherein, Chinese herbal medicine is Concretio Silicea Bambusae, Rhizoma Smilacis Glabrae, Fructus Hippophae, Rhizoma Zingiberis, Pericarpium Granati, Radix Gentianae Macrophyllae and Flos Campsis.
Step 1 in the present invention) in, the consumption of each material can select in wide scope, but in order to carry further
The effect of the anti-crop smothering of this medicament high, it is preferable that in step 1) in, relative to the water of 300 weight portions, the consumption of Concretio Silicea Bambusae is
21-28 weight portion, the consumption of Rhizoma Smilacis Glabrae is 8-19 weight portion, and the consumption of Fructus Hippophae is 40-55 weight portion, and the consumption of Rhizoma Zingiberis is 4-9
Weight portion, the consumption of Pericarpium Granati is 14-32 weight portion, and the consumption of Radix Gentianae Macrophyllae is 30-37 weight portion, and the consumption of Flos Campsis is 24-29
Weight portion.
Step 1 in the present invention) in, decocting condition can select in wide scope, but in order to improve this further
The effect of the anti-crop smothering of medicament, it is preferable that in step 1) in, decoct and at least meet following condition: decoction temperature is 120-140
DEG C, decocting time is 5-7h.
Step 2 in the present invention) in, the consumption of each material can select in wide scope, but in order to carry further
The effect of the anti-crop smothering of this medicament high, it is preferable that in step 2) in, relative to the nano-sized carbon relative to 50 weight portions, aminoacid
Consumption be 12-19 weight portion, the consumption of pyridalyl is 31-42 weight portion, and the consumption of water is 150-300 weight portion.
Step 2 in the present invention) in, the actual conditions of hydro-thermal reaction can select in wide scope, but in order to enter
One step improves the effect of the anti-crop smothering of this medicament, it is preferable that in step 2) in, hydro-thermal reaction at least meets following condition: reaction
Temperature is 180-220 DEG C, and the response time is 4-8h.
Step 2 in the present invention) in, amino acid whose concrete kind can select in wide scope, but in order to enter one
Step improves the effect of the anti-crop smothering of this medicament, it is preferable that in step 2) in, aminoacid is selected from albumen propylhomoserin, valine, different bright ammonia
One or more in acid, lysine, threonine, tryptophan and phenylalanine.
Step 2 in the present invention) in, the particle diameter of nano-sized carbon can select in wide scope, but in order to carry further
The effect of the anti-crop smothering of this medicament high, it is preferable that in step 2) in, the particle diameter of nano-sized carbon is 10-30nm.
Step 3 in the present invention) in, the consumption of each material can select in wide scope, but in order to carry further
The effect of the anti-crop smothering of this medicament high, it is preferable that in step 3) in, relative to the water of 100 weight portions, 2，4，6-trimethyl aniline
Consumption be 3-6 weight portion, the consumption of yellow uride is 8-11 weight portion, and the consumption of diphenyl ether is 22-34 weight portion, sec-o-glucosylhamaudol
Consumption be 2.2-3.4 weight portion, the consumption of ergosterol is 2.2-2.8 weight portion, and the consumption of norethindrone is 0.5-1.2 weight
Part, the consumption of extracts of Chinese herbal medicine is 40-51 weight portion, and the consumption of modified Nano carbon solution is 9-18 weight portion.
Step 3 in the present invention) in, the actual conditions of mixing can select in wide scope, but in order to further
Improve the effect of the anti-crop smothering of this medicament, it is preferable that mixing at least meets following condition: mixing temperature is 15-35 DEG C, during mixing
Between be 15-25min.
Present invention also offers a kind of anti-crop smothering medicament for blue berry, this is used for the anti-crop smothering medicament of blue berry by above-mentioned
Method be prepared.
Invention further provides the application in the anti-crop smothering of blue berry of a kind of above-mentioned anti-crop smothering medicament for blue berry.
Hereinafter will be described the present invention by embodiment.
Embodiment 1
1) by Concretio Silicea Bambusae, Rhizoma Smilacis Glabrae, Fructus Hippophae, Rhizoma Zingiberis, Pericarpium Granati, Radix Gentianae Macrophyllae, Flos Campsis, water according to 24:15:48:7:22:
The weight ratio of 34:26:300 is mixed and is incorporated at 130 DEG C decoction 6h, crosses leaching filtrate with prepared extracts of Chinese herbal medicine；
2) by nano-sized carbon (particle diameter is 20nm), aminoacid (albumen propylhomoserin), pyridalyl and water according to 50:14:37:200
Mixed hydro-thermal reaction 6h that is incorporated at 200 DEG C of weight ratio with prepared modified Nano carbon solution；
3) by water, 2,4,6-trimethylaniline, yellow uride, diphenyl ether, sec-o-glucosylhamaudol, ergosterol, norethindrone, Chinese herbal medicine
Extracting solution mixes according to the weight ratio of 100:4:10:27:2.9:2.5:0.9:45:10 with modified Nano carbon solution at 25 DEG C
20min is to prepare the anti-crop smothering medicament A1 for blue berry.
Embodiment 2
1) by Concretio Silicea Bambusae, Rhizoma Smilacis Glabrae, Fructus Hippophae, Rhizoma Zingiberis, Pericarpium Granati, Radix Gentianae Macrophyllae, Flos Campsis, water according to 21:8:40:4:14:30:
The weight ratio of 24:300 is mixed and is incorporated at 120 DEG C decoction 5h, crosses leaching filtrate with prepared extracts of Chinese herbal medicine；
2) by nano-sized carbon (particle diameter is 10nm), aminoacid (isoleucine), pyridalyl and water according to 50:12:31:150
Mixed hydro-thermal reaction 4h that is incorporated at 180 DEG C of weight ratio with prepared modified Nano carbon solution；
3) by water, 2,4,6-trimethylaniline, yellow uride, diphenyl ether, sec-o-glucosylhamaudol, ergosterol, norethindrone, Chinese herbal medicine
Extracting solution mixes according to the weight ratio of 100:3:8:22:2.2:2.2:0.5:40:9 with modified Nano carbon solution at 15 DEG C
15min is to prepare the anti-crop smothering medicament A2 for blue berry.
Embodiment 3
1) by Concretio Silicea Bambusae, Rhizoma Smilacis Glabrae, Fructus Hippophae, Rhizoma Zingiberis, Pericarpium Granati, Radix Gentianae Macrophyllae, Flos Campsis, water according to 28:19:55:9:32:
The weight ratio of 37:29:300 is mixed and is incorporated at 140 DEG C decoction 7h, crosses leaching filtrate with prepared extracts of Chinese herbal medicine；
2) by nano-sized carbon (particle diameter is 30nm), aminoacid (phenylalanine), pyridalyl and water according to 50:19:42:300
Mixed hydro-thermal reaction 8h that is incorporated at 220 DEG C of weight ratio with prepared modified Nano carbon solution；
3) by water, 2,4,6-trimethylaniline, yellow uride, diphenyl ether, sec-o-glucosylhamaudol, ergosterol, norethindrone, Chinese herbal medicine
Extracting solution mixes according to the weight ratio of 100:6:11:34:3.4:2.8:1.2:51:18 with modified Nano carbon solution at 35 DEG C
25min is to prepare the anti-crop smothering medicament A3 for blue berry.
Comparative example 1
Carry out preparing medicament B1, except for the difference that, step 1 according to the method for embodiment 1) in do not use Concretio Silicea Bambusae, Rhizoma Smilacis Glabrae,
Fructus Hippophae and Rhizoma Zingiberis.
Comparative example 2
Carry out preparing medicament B2, except for the difference that, step 1 according to the method for embodiment 1) in do not use Pericarpium Granati, Radix Gentianae Macrophyllae, icepro
Clouds flower.
Comparative example 3
Carry out preparing medicament B3, except for the difference that, step 2 according to the method for embodiment 1) in do not use nano-sized carbon.
Comparative example 4
Carry out preparing medicament B4, except for the difference that, step 2 according to the method for embodiment 1) in do not use aminoacid.
Comparative example 5
Carry out preparing medicament B5, except for the difference that, step 2 according to the method for embodiment 1) in do not use pyridalyl.
Comparative example 6
Carry out preparing medicament B6, except for the difference that, step 3 according to the method for embodiment 1) in do not use extracts of Chinese herbal medicine.
Comparative example 7
Carry out preparing medicament B7, except for the difference that, step 3 according to the method for embodiment 1) in do not use modified Nano carbon molten
Liquid.
Detection example 1
Take a collection of bud stage blue berry as detection object, then above-mentioned blue berry is divided into 11 groups, wherein uses above-mentioned medicine respectively for 10 groups
Agent A1-A3 and B1-B7 carries out being sprayed on the soil of blue berry, and every day sprays once, the 11st group of spray water, sprays one week continuously；Connect
On soil, sow grass seed, by observing the germination percentage of statistics grass seed after January,
Concrete outcome is shown in Table 1.
Table 1
| Group number | The material sprayed | Germination percentage/% |
| 1 | A1 | 0.2 |
| 2 | A2 | 0.5 |
| 3 | A3 | 0.7 |
| 4 | B1 | 11.1 |
| 5 | B2 | 9.8 |
| 6 | B3 | 7.5 |
| 7 | B4 | 8.1 |
| 8 | B5 | 7.4 |
| 9 | B6 | 15.7 |
| 10 | B7 | 17.1 |
| 11 | Water | 89 |
By above-described embodiment, comparative example and detection example, the medicament that the present invention provides has excellence for blue berry
Anti-crop smothering effect.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited in above-mentioned embodiment
Detail, in the technology concept of the present invention, technical scheme can be carried out multiple simple variant, this
A little simple variant belong to protection scope of the present invention.
It is further to note that each the concrete technical characteristic described in above-mentioned detailed description of the invention, at not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to various can
The compound mode of energy illustrates the most separately.
Additionally, combination in any can also be carried out between the various different embodiment of the present invention, as long as it is without prejudice to this
The thought of invention, it should be considered as content disclosed in this invention equally.
Claims (10)
1. the preparation method for the anti-crop smothering medicament of blue berry, it is characterised in that including:
1) carry out Chinese herbal medicine in water decocting, crossing leaching filtrate with prepared extracts of Chinese herbal medicine；
2) nano-sized carbon, aminoacid, pyridalyl and water are carried out hydro-thermal reaction with prepared modified Nano carbon solution；
3) by water, 2,4,6-trimethylaniline, yellow uride, diphenyl ether, sec-o-glucosylhamaudol, ergosterol, norethindrone, described Chinese herbal medicine
Extracting solution mixes with modified Nano carbon solution to prepare the described anti-crop smothering medicament for blue berry；
Wherein, described Chinese herbal medicine is Concretio Silicea Bambusae, Rhizoma Smilacis Glabrae, Fructus Hippophae, Rhizoma Zingiberis, Pericarpium Granati, Radix Gentianae Macrophyllae and Flos Campsis.
Preparation method the most according to claim 1, wherein, in step 1) in, relative to the water of 300 weight portions, described sky
The consumption of Zhu's Huang is 21-28 weight portion, and the consumption of described Rhizoma Smilacis Glabrae is 8-19 weight portion, and the consumption of described Fructus Hippophae is 40-55 weight
Amount part, the consumption of described Rhizoma Zingiberis is 4-9 weight portion, and the consumption of described Pericarpium Granati is 14-32 weight portion, and the consumption of described Radix Gentianae Macrophyllae is
30-37 weight portion, the consumption of described Flos Campsis is 24-29 weight portion.
Preparation method the most according to claim 1, wherein, in step 1) in, described decoction at least meets following condition: decoct
Boiling temperature and be 120-140 DEG C, decocting time is 5-7h.
4. according to the preparation method described in any one in claim 1-3, wherein, in step 2) in, relative to relative to 50
The nano-sized carbon of weight portion, described amino acid whose consumption is 12-19 weight portion, and the consumption of described pyridalyl is 31-42 weight portion,
The consumption of described water is 150-300 weight portion.
Preparation method the most according to claim 4, wherein, in step 2) in, described hydro-thermal reaction at least meets following bar
Part: reaction temperature is 180-220 DEG C, the response time is 4-8h.
Preparation method the most according to claim 4, wherein, in step 2) in, described aminoacid is selected from albumen propylhomoserin, figured silk fabrics ammonia
One or more in acid, isoleucine, lysine, threonine, tryptophan and phenylalanine.
Preparation method the most according to claim 4, wherein, in step 2) in, the particle diameter of described nano-sized carbon is 10-30nm.
8. according to the preparation method described in any one in claim 5-7, wherein, in step 3) in, relative to 100 weight portions
Water, the consumption of described 2，4，6-trimethyl aniline is 3-6 weight portion, and the consumption of described yellow uride is 8-11 weight portion, described
The consumption of diphenyl ether is 22-34 weight portion, and the consumption of described sec-o-glucosylhamaudol is 2.2-3.4 weight portion, the use of described ergosterol
Amount is 2.2-2.8 weight portion, and the consumption of described norethindrone is 0.5-1.2 weight portion, and the consumption of described extracts of Chinese herbal medicine is 40-
51 weight portions, the consumption of described modified Nano carbon solution is 9-18 weight portion；
Preferably, described mixing at least meets following condition: mixing temperature is 15-35 DEG C, and incorporation time is 15-25min.
9. the anti-crop smothering medicament for blue berry, it is characterised in that the described anti-crop smothering medicament for blue berry is wanted by right
The method described in any one is asked in 1-8 to be prepared.
10. one kind is used for the application in the anti-crop smothering of blue berry of the anti-crop smothering medicament of blue berry as claimed in claim 9.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
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Application publication date: 20161207 |