CN106281704A - A kind of extracting method of Fructus Citri Limoniae quintessence oil - Google Patents
A kind of extracting method of Fructus Citri Limoniae quintessence oil Download PDFInfo
- Publication number
- CN106281704A CN106281704A CN201610731698.3A CN201610731698A CN106281704A CN 106281704 A CN106281704 A CN 106281704A CN 201610731698 A CN201610731698 A CN 201610731698A CN 106281704 A CN106281704 A CN 106281704A
- Authority
- CN
- China
- Prior art keywords
- fructus citri
- citri limoniae
- quintessence oil
- extracting method
- limoniae quintessence
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention discloses the extracting method of a kind of Fructus Citri Limoniae quintessence oil, comprises the steps: the Fructus Citri Limoniae peel lyophilization that (1) will clean up, pulverized 150 mesh sieves；(2) powder of step (1) is added water, by ultrasonic Treatment 50～70min；(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Fructus Citri Limoniae quintessence oil.Compared with the conventional steam way of distillation, the extracting method of the present invention is remarkably improved the oil yield of Fructus Citri Limoniae quintessence oil.
Description
Technical field
The invention belongs to field of plant extraction, be specifically related to the extracting method of a kind of Fructus Citri Limoniae quintessence oil.
Background technology
Fructus Citri Limoniae quintessence oil abnormal smells from the patient is strong, pure and fresh, chlorine, water quality viscosity.It can improve circulatory function, including promoting
Blood circulation, to reduce blood pressure, only nose bleeding.It can strengthen immune system, purifies health, improves digestive system function, decomposes
Liparitosis, treatment dyspepsia and constipation.There is consoling and alleviate the effect of headache and migraine, by the acid in general physical
Property material, the most helpful to treatment of arthritis and rheumatism.Additionally aid cleaning acne, clean Greasy Skin and hair, and
Remove dead skin cells.The common extracting method of Fructus Citri Limoniae quintessence oil has steam distillation and organic solvent extraction, due to water vapour
Way of distillation equipment cost is low, simple to operate and is widely used.
Summary of the invention
It is an object of the invention to the steam distillation of existing Fructus Citri Limoniae quintessence oil is improved, it is provided that a kind of Fructus Citri Limoniae quintessence oil
The higher extracting method of oil yield.
In order to solve above-mentioned technical problem, the invention provides following technical scheme:
The extracting method of a kind of Fructus Citri Limoniae quintessence oil, comprises the steps:
(1) the Fructus Citri Limoniae peel lyophilization that will clean up, pulverized 150 mesh sieves；
(2) powder of step (1) is added water, by ultrasonic Treatment 50～70min；
(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Fructus Citri Limoniae quintessence oil.
Detailed description of the invention
Hereinafter the preferred embodiments of the present invention are illustrated, it will be appreciated that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Embodiment 1
The extracting method of a kind of Fructus Citri Limoniae quintessence oil, comprises the steps:
(1) first fresh Fructus Citri Limoniae peel is cleaned up, then lyophilization, pulverized 150 mesh sieves, the powder obtained is standby；
(2) powder of step (1) is added in ultrasonic cell-break machine, add appropriate water (solid-liquid ratio be generally 1:3～
5 g/g), ultrasound wave (power 500～1500w, ultrasonic frequency 19～23KHz) processes 50～70min, and during process, temperature should be controlled
System is less than 30 DEG C；
(3) powder after step (2) processes being put in steam distillation apparatus and distilled, after steam condensation, liquid liquid divides
From obtaining Fructus Citri Limoniae quintessence oil.
With tradition without compared with the steam distillation of ultrasonic Treatment, in distillation condition and conventional steam distillation technique
In the case of identical, the oil yield of extracting method of the present invention can improve 1.5～2 times, and distillation time can shorten 1/6.
Finally it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention,
Although being described in detail the present invention with reference to previous embodiment, for a person skilled in the art, it still may be used
So that the technical scheme described in foregoing embodiments to be modified, or wherein portion of techniques feature is carried out equivalent.
All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in the present invention's
Within protection domain.
Claims (1)
1. an extracting method for Fructus Citri Limoniae quintessence oil, comprises the steps:
(1) the Fructus Citri Limoniae peel lyophilization that will clean up, pulverized 150 mesh sieves；
(2) powder of step (1) is added water, by ultrasonic Treatment 50～70min；
(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Fructus Citri Limoniae quintessence oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731698.3A CN106281704A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Fructus Citri Limoniae quintessence oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731698.3A CN106281704A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Fructus Citri Limoniae quintessence oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106281704A true CN106281704A (en) | 2017-01-04 |
Family
ID=57676254
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610731698.3A Pending CN106281704A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Fructus Citri Limoniae quintessence oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106281704A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103897805A (en) * | 2014-04-03 | 2014-07-02 | 广东添乐化妆品有限公司 | Solvent-free extraction method of lemon essential oil |
| CN103897806A (en) * | 2014-04-03 | 2014-07-02 | 广东添乐化妆品有限公司 | Microwave assisted extraction method of lemon essential oil |
| CN104531360A (en) * | 2014-12-17 | 2015-04-22 | 谢振文 | Low-temperature refining method of lemon oil |
-
2016
- 2016-08-26 CN CN201610731698.3A patent/CN106281704A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103897805A (en) * | 2014-04-03 | 2014-07-02 | 广东添乐化妆品有限公司 | Solvent-free extraction method of lemon essential oil |
| CN103897806A (en) * | 2014-04-03 | 2014-07-02 | 广东添乐化妆品有限公司 | Microwave assisted extraction method of lemon essential oil |
| CN104531360A (en) * | 2014-12-17 | 2015-04-22 | 谢振文 | Low-temperature refining method of lemon oil |
Non-Patent Citations (3)
| Title |
|---|
| 侯滨滨，等: "微波辅助水蒸汽蒸馏提取柠檬精油", 《食品研究与开发》 * |
| 林洪斌，等: "微波辅助水蒸气法提取柠檬精油工艺研究", 《中国酿造》 * |
| 王伟，等: "超声波辅助法提取柠檬皮中香精油的工艺研究", 《广州化工》 * |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170104 |
|
| RJ01 | Rejection of invention patent application after publication |