CN106244328A - A kind of extracting method of Herba Pogostemonis essential oil - Google Patents
A kind of extracting method of Herba Pogostemonis essential oil Download PDFInfo
- Publication number
- CN106244328A CN106244328A CN201610732118.2A CN201610732118A CN106244328A CN 106244328 A CN106244328 A CN 106244328A CN 201610732118 A CN201610732118 A CN 201610732118A CN 106244328 A CN106244328 A CN 106244328A
- Authority
- CN
- China
- Prior art keywords
- herba pogostemonis
- essential oil
- extracting method
- pogostemonis essential
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention discloses the extracting method of a kind of Herba Pogostemonis essential oil, comprises the steps: the Herba Pogostemonis blade lyophilization that (1) will clean up, pulverized 120 mesh sieves；(2) powder of step (1) adds water, by ultrasonic Treatment 45～75min；(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Herba Pogostemonis essential oil.Compared with the conventional steam way of distillation, the extracting method of the present invention is remarkably improved the oil yield of Herba Pogostemonis essential oil.
Description
Technical field
The invention belongs to field of plant extraction, be specifically related to the extracting method of a kind of Herba Pogostemonis essential oil.
Background technology
Herba Pogostemonis quintessence oil is good fixastive, is raw material indispensable in perfumes industry, in champignon therapy, and compound recipe
Quintessence oil drips Herba Pogostemonis quintessence oil, fragrance can be allowed more longlasting.Herba Pogostemonis essence main body of oil is Herba Pogostemonis alcohol, Herba Pogostemonis
Alkene, eugenol, cadinene etc..Wherein the structure of patchoulene is similar with the azulene in blue Flos Chrysanthemi, thus also has same
Antibacterial, anti-inflammatory effect of sample.Several Herba Pogostemonis essential oil are instilled in the hot water of foot bath, the purpose of the meridians that can reach to invigorate blood circulation,
Can also reach to remove the effect of tinea pedis foot odor.The common extracting method of Herba Pogostemonis essential oil has steam distillation and organic solvent leaching
Lifting manipulation, is widely used owing to steam distillation equipment cost is low, simple to operate.
Summary of the invention
It is an object of the invention to the steam distillation of existing Herba Pogostemonis essential oil is improved, it is provided that a kind of Herba Pogostemonis
The higher extracting method of quintessence oil oil yield.
In order to solve above-mentioned technical problem, the invention provides following technical scheme:
The extracting method of a kind of Herba Pogostemonis essential oil, comprises the steps:
(1) the Herba Pogostemonis blade lyophilization that will clean up, pulverized 120 mesh sieves；
(2) powder of step (1) adds water, by ultrasonic Treatment 45～75min；
(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Herba Pogostemonis essential oil.
Detailed description of the invention
Hereinafter the preferred embodiments of the present invention are illustrated, it will be appreciated that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Embodiment 1
The extracting method of a kind of Herba Pogostemonis essential oil, comprises the steps:
(1) first that fresh Herba Pogostemonis leaf cleaning is clean, then lyophilization, pulverized 120 mesh sieves, the powder obtained is standby；
(2) powder of step (1) is added in ultrasonic cell-break machine, add appropriate water (solid-liquid ratio be generally 1:7～
8 g/g), ultrasound wave (power 1000～2000w, ultrasonic frequency 20～25KHz) processes 45～75min, and during process, temperature should
Control less than 30 DEG C；
(3) powder after step (2) processes being put in steam distillation apparatus and distilled, after steam condensation, liquid liquid divides
From obtaining Herba Pogostemonis essential oil.
With tradition without compared with the steam distillation of ultrasonic Treatment, in distillation condition and conventional steam distillation technique
In the case of identical, the oil yield of extracting method of the present invention can improve 25～35% relatively, and distillation time can shorten 1/3.
Finally it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention,
Although being described in detail the present invention with reference to previous embodiment, for a person skilled in the art, it still may be used
So that the technical scheme described in foregoing embodiments to be modified, or wherein portion of techniques feature is carried out equivalent.
All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in the present invention's
Within protection domain.
Claims (1)
1. an extracting method for Herba Pogostemonis essential oil, comprises the steps:
(1) the Herba Pogostemonis blade lyophilization that will clean up, pulverized 120 mesh sieves；
(2) powder of step (1) adds water, by ultrasonic Treatment 45～75min；
(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Herba Pogostemonis essential oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610732118.2A CN106244328A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Herba Pogostemonis essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610732118.2A CN106244328A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Herba Pogostemonis essential oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106244328A true CN106244328A (en) | 2016-12-21 |
Family
ID=57596351
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610732118.2A Pending CN106244328A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Herba Pogostemonis essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106244328A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114432358A (en) * | 2021-12-31 | 2022-05-06 | 海南黎草纪新生物科技有限公司 | Method for extracting patchouli hydrosol |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101935591A (en) * | 2010-09-10 | 2011-01-05 | 吉水县金海天然香料油科技有限公司 | Refinement and extraction method of patchouli oil |
-
2016
- 2016-08-26 CN CN201610732118.2A patent/CN106244328A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101935591A (en) * | 2010-09-10 | 2011-01-05 | 吉水县金海天然香料油科技有限公司 | Refinement and extraction method of patchouli oil |
Non-Patent Citations (3)
| Title |
|---|
| 唐春红 等: "《天然防腐剂与抗氧化剂》", 31 May 2010, 中国轻工业出版社 * |
| 毛海舫 等: "《天然香料加工工艺学》", 31 January 2006, 中国轻工业出版社 * |
| 谭银丰 等: "海南广藿香油水蒸气蒸馏最佳工艺筛选研究", 《海南医学院学报》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114432358A (en) * | 2021-12-31 | 2022-05-06 | 海南黎草纪新生物科技有限公司 | Method for extracting patchouli hydrosol |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161221 |
|
| RJ01 | Rejection of invention patent application after publication |