CN106221927A - A kind of extracting method of Fructus Fortunellae Margaritae quintessence oil - Google Patents
A kind of extracting method of Fructus Fortunellae Margaritae quintessence oil Download PDFInfo
- Publication number
- CN106221927A CN106221927A CN201610731747.3A CN201610731747A CN106221927A CN 106221927 A CN106221927 A CN 106221927A CN 201610731747 A CN201610731747 A CN 201610731747A CN 106221927 A CN106221927 A CN 106221927A
- Authority
- CN
- China
- Prior art keywords
- fortunellae margaritae
- fructus fortunellae
- quintessence oil
- extracting method
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Seasonings (AREA)
Abstract
The present invention discloses the extracting method of a kind of Fructus Fortunellae Margaritae quintessence oil, comprises the steps: the Fructus Fortunellae Margaritae peel lyophilization that (1) will clean up, pulverized 120 mesh sieves；(2) powder of step (1) adds water, by ultrasonic Treatment 60～90min；(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Fructus Fortunellae Margaritae quintessence oil.Compared with the conventional steam way of distillation, the extracting method of the present invention is remarkably improved the oil yield of Fructus Fortunellae Margaritae quintessence oil.
Description
Technical field
The invention belongs to field of plant extraction, be specifically related to the extracting method of a kind of Fructus Fortunellae Margaritae quintessence oil.
Background technology
In Fructus Fortunellae Margaritae fruit, oil content is about at 1-2%, and Fructus Fortunellae Margaritae quintessence oil oil is gentle, quality be citrus quintessence oil, be
Important industrial chemicals and edible essence are it can also be used to the modulation of some senior daily chemical essence.The extraction side that Fructus Fortunellae Margaritae quintessence oil is common
Method has steam distillation and organic solvent extraction, owing to steam distillation equipment cost is low, simple to operate by extensively
Application.
Summary of the invention
It is an object of the invention to the steam distillation of existing Fructus Fortunellae Margaritae quintessence oil is improved, it is provided that a kind of Fructus Fortunellae Margaritae quintessence oil
The higher extracting method of oil yield.
In order to solve above-mentioned technical problem, the invention provides following technical scheme:
The extracting method of a kind of Fructus Fortunellae Margaritae quintessence oil, comprises the steps:
(1) the Fructus Fortunellae Margaritae peel lyophilization that will clean up, pulverized 120 mesh sieves；
(2) powder of step (1) adds water, by ultrasonic Treatment 60～90min；
(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Fructus Fortunellae Margaritae quintessence oil.
Detailed description of the invention
Hereinafter the preferred embodiments of the present invention are illustrated, it will be appreciated that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Embodiment 1
The extracting method of a kind of Fructus Fortunellae Margaritae quintessence oil, comprises the steps:
(1) first Fructus Fortunellae Margaritae peel is cleaned up, more freeze-dried after, pulverized 120 mesh sieves, the powder obtained is standby；
(2) powder of step (1) is added in ultrasonic cell-break machine, add appropriate water (solid-liquid ratio be generally 1:2～
3 g/g), ultrasound wave (power 1500～1800w, ultrasonic frequency 20～25KHz) processes 60～90min, and during process, temperature should
Control less than 30 DEG C；
(3) powder after step (2) processes being put in steam distillation apparatus and distilled, after steam condensation, liquid liquid divides
From obtaining Fructus Fortunellae Margaritae quintessence oil.
With tradition without compared with the steam distillation of ultrasonic Treatment, in distillation condition and conventional steam distillation technique
In the case of identical, the oil yield of extracting method of the present invention can improve 20～30% relatively, and distillation time can shorten 1/4.
Finally it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention,
Although being described in detail the present invention with reference to previous embodiment, for a person skilled in the art, it still may be used
So that the technical scheme described in foregoing embodiments to be modified, or wherein portion of techniques feature is carried out equivalent.
All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in the present invention's
Within protection domain.
Claims (1)
1. an extracting method for Fructus Fortunellae Margaritae quintessence oil, comprises the steps:
(1) the Fructus Fortunellae Margaritae peel lyophilization that will clean up, pulverized 120 mesh sieves；
(2) powder of step (1) adds water, by ultrasonic Treatment 60～90min；
(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Fructus Fortunellae Margaritae quintessence oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731747.3A CN106221927A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Fructus Fortunellae Margaritae quintessence oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731747.3A CN106221927A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Fructus Fortunellae Margaritae quintessence oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106221927A true CN106221927A (en) | 2016-12-14 |
Family
ID=57554895
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610731747.3A Pending CN106221927A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Fructus Fortunellae Margaritae quintessence oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106221927A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107691958A (en) * | 2017-10-26 | 2018-02-16 | 黄武强 | A kind of processing method of cumquat solid-state cream |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101457178A (en) * | 2008-12-10 | 2009-06-17 | 广西中烟工业有限责任公司 | Method for extracting water-soluble volatilization component from lysimachia foenum-graecum |
| CN103122277A (en) * | 2013-01-23 | 2013-05-29 | 兰州大学 | Method for extracting natural flavor with dimethyl ether |
-
2016
- 2016-08-26 CN CN201610731747.3A patent/CN106221927A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101457178A (en) * | 2008-12-10 | 2009-06-17 | 广西中烟工业有限责任公司 | Method for extracting water-soluble volatilization component from lysimachia foenum-graecum |
| CN103122277A (en) * | 2013-01-23 | 2013-05-29 | 兰州大学 | Method for extracting natural flavor with dimethyl ether |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107691958A (en) * | 2017-10-26 | 2018-02-16 | 黄武强 | A kind of processing method of cumquat solid-state cream |
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| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161214 |