CN106667857A - Preparation method of white Chinese floweringquince extract for facial mask through microwave-assisted extraction - Google Patents
Preparation method of white Chinese floweringquince extract for facial mask through microwave-assisted extraction Download PDFInfo
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- CN106667857A CN106667857A CN201710136427.8A CN201710136427A CN106667857A CN 106667857 A CN106667857 A CN 106667857A CN 201710136427 A CN201710136427 A CN 201710136427A CN 106667857 A CN106667857 A CN 106667857A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention discloses a preparation method of white Chinese floweringquince extract for a facial mask through microwave-assisted extraction. The preparation method is characterized by comprising the following steps: cleanly washing white Chinese floweringquince, putting and drying the white Chinese floweringquince in a baking oven under 105 to 115 DEG C after naturally airing, and pulverizing the white Chinese floweringquince into raw material powder of which the average grain diameter is 30 to 45 meshes by using a tissue pulverizer; taking 80 to 95 percent of ethanol as a leaching solution, mixing the raw material powder with the leaching solution according to a mass ratio of 1 to (5 to 10), carrying out microwave extraction for 30 to 40 minutes under a condition of 35 to 45 DEG C, and putting the extract in a leaching tank, wherein the leaching temperature is 45 to 55 DEG C, the leaching time is 0.5 to 1 hour, and the leaching frequency is 2 to 3 times, and each time lasts for one hour; then merging extracting solutions, recycling the leaching solution through filtration, decompression and evaporation, wherein the pressure is -1 to -0.8 MPa, and the evaporation temperature is 30 to 40 DEG C; evaporating and separating an original solvent, thus obtaining a solution, i.e., the white Chinese floweringquince extract for the facial mask. The preparation method disclosed by the invention has the advantages that a production technology process is simple, a technological route is short, the whole production process is based on an ethanol solution, no toxic or harmful matters exist, and follow-up treatment is convenient; production equipment is simple, the scale can be easily expanded for industrial production, and the production cost is lower.
Description
Technical field
The present invention relates to a kind of method of whitewood's melon extracts active ingredients, particularly a kind of microwave radiation exaraction facial mask is with vain
The preparation method of pawpaw extract solution.It is applicable and makes an addition to the cosmetics such as cream class, white class, newborn class, it is main to be applied in facial mask.
Background technology
Whitewood's melon is rosaceae chaenomeles plant, is one of conventional traditional Chinese medicinal materials assortment, be also important medicine food resource it
One.Whitewood's melon rich in various organic acids, triterpene compound, flavone compound etc., with " liver protecting, stimulating the circulation of the blood and cause the muscles and joints to relax, resist
Decline beauty treatment " three zones.Due to its clinical practice extensively, cosmetics and field of health care products are applied to again in recent years, as research
One of focus.Organic acid in whitewood's melon, such as malic acid, citric acid are considered as being produced with human skin cell's respiratory metabolism
Organic acid have much in common, so be easy to be absorbed by the skin, skin capillary vascular expansion can be made, promote epiderm skin
Metabolism, make skin smooth fine and smooth, reach nourishes rough skin, the purpose of delay skin aging.Simultaneously tests prove that pawpaw
Extract in the Extraction solvent of 50% alcohol to the inhibiting rate of melanocyte up to 56%, therefore spend papaya extractives in vain and can be used for
Skin-lightening cosmetic.
At present, the extraction to pawpaw active ingredient mainly has traditional extraction, ultrasound assisted extraction method, microwave radiation exaraction
Method etc..But simple extraction has disadvantages that such as time-consuming, extraction efficiency is low, extract component is imperfect；Ultrasound assisted extraction
Method and microwave―assisted extraction are a kind of Novel extraction methods, can more effectively improve active component recovery rate, time-consuming short,
Extraction efficiency is fast, but the method poor reproducibility is difficult to all extract active ingredient.
Based on this, on the basis of microwave leaching technology, we are successful and are effectively applied to microwave auxiliary extraction technology white
In the extraction of pawpaw, and there are significant results.
The content of the invention
The present invention is primarily to solve that traditional microwave leaching technology is low to extracts active ingredients efficiency in pawpaw, short time consumption is long
And the problems such as extract imperfect, there is provided the microwave radiation exaraction facial mask preparation method of whitewood's melon extract solution.
The technical solution adopted in the present invention is a kind of preparation method of microwave radiation exaraction facial mask whitewood's melon extract solution,
It is characterized in that comprising the following steps：
（1）Whitewood's melon is cleaned, after drying naturally, is placed in baking oven, control oven temperature after 80 ~ 130 DEG C, whitewood's melon to be dried
It is dry, the material powder of 10~80 mesh is ground into after drying with tissue pulverizer；
（2）It is leaching liquor with 60% ~ 95% alcohol-water, by material powder and leaching liquor by by 1:In 35- after 2 ~ 15 mass ratio
Under the conditions of 65 DEG C, Microwave Extraction 15-40min；
（3）After mixed liquor after Microwave Extraction is loaded into batch extractor, extraction temperature is controlled for 35 ~ 60 DEG C with vapor, during extraction
Between be 0.25 ~ 4 h；
（4）Mixed system is filtered by decompression after extraction obtains leaching liquor, remaining solid is extracted 1 ~ 4 time again, extracted
Time is 0.25 ~ 4 h, and decompression is filtered and obtains leaching liquor；
（5）By recovery leaching liquor is evaporated under reduced pressure after leaching liquor is merged, and leaching liquor is concentrated, used by evaporation recovery
Pressure is -1.5 ~ -0.5MPa, and evaporating temperature is 25 ~ 55 DEG C；
（6）By vacuum distillation, the solution by gained after organic solvent evaporating completely is exactly the whitewood's melon extract solution used by facial mask.
In above-mentioned technical proposal, the step（1）In, the control of whitewood's melon drying temperature is optimal at 105 ~ 115 DEG C, crushes flat
Equal particle diameter is that 30 ~ 45 mesh are optimal.
In above-mentioned technical proposal, the step（2）In, solid-liquid ratio is 1：5 ~ 10 is optimal.
In above-mentioned technical proposal, the step（2）In, the control of alcohol extract concentration is optimal 80% ~ 95%.
In above-mentioned technical proposal, the step（2）In, the Microwave Extraction time is 30 ~ 40min optimal, Microwave Extraction temperature
For 35-45 DEG C most preferably.
In above-mentioned technical proposal, the step（3）In, extraction temperature control is optimal at 45 ~ 55 DEG C, and extraction time is 0.5 ~
1 h is optimal.
In above-mentioned technical proposal, the step（4）Described in extracting times be 1 ~ 2 suboptimum, carry the time be 0.5
~ 1h is optimal.
In above-mentioned technical proposal, the step（5）In, return pressure is evaporated under reduced pressure and controls, steaming optimal in -1 ~ -0.8 MPa
Hair temperature is 35 ~ 40 DEG C optimal.
In above-mentioned technical proposal, the step（6）Described in whitewood's melon extract solution organic solvent content should be less than
0.05%。
The present invention is proposed by repeatedly screening, experiment and after summarizing, and the raw material sources of this research enrich, price is low
Honest and clean, production process is simple, and process route is short, and whole production process does not have poisonous and harmful substances based on ethanol solution,
Subsequent treatment is convenient, and production equipment is simple, and easy expansion scale carries out industrialized production, and production cost is relatively low.And with tradition
Extraction is compared with ultrasound assisted extraction method, and extraction time is not only substantially reduced using microwave auxiliary extraction technology, is also improved
Whitewood's melon extract solution purity and yield.Use it in facial mask, using effect significantly, has the anti-oxidant grade work(of skin whitening, moisturizing concurrently
Effect, does not have any side effect or ill effect to application on human skin, is the excellent product of beauty and skin care.
Specific embodiment
Embodiment one
A kind of microwave radiation exaraction facial mask preparation method of whitewood's melon extract solution, it is characterized in that：Whitewood's melon is placed in baking oven
After being dried at 110 DEG C, the material powder that average grain diameter is 40 mesh is ground into tissue pulverizer, is extraction with 95% ethanol
Liquid, 1 is pressed by material powder and leaching liquor:Microwave treatment is carried out after 8 mass ratio dress mixing, microwave treatment time is 30min, micro-
Ripple controls temperature for 40 DEG C, is extracted under the conditions of 40 DEG C after mixed liquor then is loaded into batch extractor, and extracting times are 3 times, every time
1h, merges extract solution after extraction, carry out filtering and recovery leaching liquor is evaporated under reduced pressure, and pressure is -0.9 MPa, and evaporating temperature is 35 DEG C.
The solution that evaporation is separated after extract solution is exactly the whitewood's melon extract solution used by facial mask, and yield is 64.24%.
Embodiment two
A kind of microwave radiation exaraction facial mask preparation method of whitewood's melon extract solution, it is characterized in that：Whitewood's melon is placed in baking oven
In being dried at 100 DEG C, the material powder that average grain diameter is 50 mesh is ground into tissue pulverizer.It is leaching liquor with 70% ethanol,
Material powder and leaching liquor are pressed 1:Microwave treatment is carried out after 10 mass ratio mixing, microwave treatment time is 35min, microwave control
Temperature processed is 38 DEG C, is then loaded and then by extraction is 3 times under the conditions of 35 DEG C after mixed liquor loading batch extractor mixed liquor, often
Secondary 1h.Extract solution is then combined with, filtering is carried out and recovery leaching liquor is evaporated under reduced pressure, pressure is -0.85 MPa, and evaporating temperature is 38
℃.The solution that evaporation is separated after extract solution is exactly the whitewood's melon extract solution used by facial mask, and yield is 66.81%.
Carried with whitewood's melon the following is this microwave radiation exaraction facial mask is observed by the contrast test carried out with prior art
Take the technique effect of liquid.
Prior embodiment one
Reflux extraction：Whitewood's melon is placed in and is baked and banked up with earth in being dried at 110 DEG C in case, being ground into average grain diameter with tissue pulverizer is
The material powder of 40 mesh.It is leaching liquor with 95% ethanol, material powder and leaching liquor is pressed 1:8 mass ratio loads batch extractor,
Extraction temperature is 40 DEG C, and extraction time is 6 h, and extracting times are 3 times, each 1h.Extract solution is then combined with, filtering decompression is carried out
Leaching liquor is reclaimed in evaporation, and pressure is -0.9 MPa, and evaporating temperature is 35 DEG C.The solution that evaporation is separated after extract solution is exactly facial mask
Whitewood's melon extract solution used.
Prior embodiment two
Ultrasonic assistant extraction method：Whitewood's melon is placed in and is baked and banked up with earth in case in being dried at 110 DEG C, be ground into averagely with tissue pulverizer
Particle diameter is the material powder of 40 mesh.It is leaching liquor with 95% ethanol, material powder and leaching liquor is pressed 1:8 mass ratio loads
Batch extractor, to enter carry out before tank ultrasonically treated, and sonication treatment time is 35min, and extraction temperature is 35 DEG C, and extraction time is 1h, leaching
It is 3 times, each 1h to carry number of times.Extract solution is then combined with, filtering is carried out and recovery leaching liquor is evaporated under reduced pressure, pressure is -0.85 MPa,
Evaporating temperature is 35 DEG C.The solution that evaporation is separated after extract solution is exactly the whitewood's melon extract solution used by facial mask.
Comparative example of the invention
Above-mentioned microwave―assisted extraction and prior art are contrasted, result such as table 1 is obtained.
Contrast between the different extraction methods of table 1
| Extraction method | Total extraction time | Average yield % |
| Embodiment 1 | 3.5h | 62.24 |
| Embodiment 2 | 3.6h | 66.81 |
| Prior embodiment 1 | 6h | 12.31 |
| Prior embodiment 2 | 3.6min | 16.06 |
Result shows not only to shorten extraction time using the method for microwave radiation exaraction, the extraction efficiency for also improving.
Performance evaluation
The whitewood's melon extract solution that will be obtained is applied in facial mask detect its whitening, moisturizing and antioxygenic property.
1. whitening performance test
It is main to suppress tyrosinase activity ability, measure whitewood's melon extract solution and 14.29% is reached to the clearance rate of TYR enzyme, can
See that whitewood's melon extract solution is still very strong for the activity suppression ability of TYR enzyme, there is whitening effect.
2. antioxygenic property test
The main activity for suppressing DPPH free radicals, measures and spends pawpaw in vain and reach 91.77% to the clearance rate of DPPH, it is seen that whitewood's melon
Extract solution is very strong for the rejection ability of DPPH free radicals, with stronger antioxygenic property, can be used in oxidation resistant product.
3. moisture-retaining capacity（Weight method）
The h moisturizing rates of 2 whitewood's melon of table 24
| Time（h） | 4 | 8 | 24 |
| Moisturizing rate (%) | 16.2 | 14.9 | 14.1 |
Show whitewood's melon extract solution for facial mask, water loss is less within 24h, illustrates that it has preferable performance of keeping humidity, can
For in the moisturizing of cosmetics.
Claims (9)
1. a kind of microwave radiation exaraction facial mask preparation method of whitewood's melon extract solution, it is characterised in that comprise the following steps：
（1）Whitewood's melon is cleaned, after drying naturally, is placed in baking oven, control oven temperature after 80 ~ 130 DEG C, whitewood's melon to be dried
It is dry, the material powder of 10~80 mesh is ground into after drying with tissue pulverizer；
（2）It is leaching liquor with 60% ~ 95% alcohol-water, material powder and leaching liquor is pressed 1:In 35-65 after 2 ~ 15 mass ratio
Under the conditions of DEG C, Microwave Extraction 15-40min；
（3）After mixed liquor after Microwave Extraction is loaded into batch extractor, extraction temperature is controlled for 35 ~ 60 DEG C with vapor, during extraction
Between be 0.25 ~ 4 h；
（4）Mixed system is filtered by decompression after extraction obtains leaching liquor, remaining solid is extracted 1 ~ 4 time again, extracted
Time is 0.25 ~ 4 h, and decompression is filtered and obtains leaching liquor；
（5）By recovery leaching liquor is evaporated under reduced pressure after leaching liquor is merged, and leaching liquor is concentrated, used by evaporation recovery
Pressure is -1.5 ~ -0.5MPa, and evaporating temperature is 25 ~ 55 DEG C；
（6）By vacuum distillation, the solution by gained after organic solvent evaporating completely is exactly the whitewood's melon extract solution used by facial mask.
2. the microwave radiation exaraction facial mask according to claim 1 preparation method of whitewood's melon extract solution, it is characterised in that
The step（1）In, the control of whitewood's melon drying temperature is optimal at 105 ~ 115 DEG C, and it is that 30 ~ 45 mesh are optimal to crush average grain diameter.
3. the microwave radiation exaraction facial mask according to claim 1 preparation method of whitewood's melon extract solution, it is characterised in that
The step（2）In, solid-liquid ratio is 1：5 ~ 10 is optimal.
4. the microwave radiation exaraction facial mask according to claim 1 preparation method of whitewood's melon extract solution, it is characterised in that
The step（2）In, the control of alcohol extract concentration is optimal 80% ~ 95%.
5. the microwave radiation exaraction facial mask according to claim 1 preparation method of whitewood's melon extract solution, it is characterised in that
The step（2）In, the Microwave Extraction time is 30 ~ 40min optimal, and Microwave Extraction temperature is 35-45 DEG C optimal.
6. the microwave radiation exaraction facial mask according to claim 1 preparation method of whitewood's melon extract solution, it is characterised in that
The step（3）In, extraction temperature control is optimal at 45 ~ 55 DEG C, and extraction time is that 0.5 ~ 1 h is optimal.
7. ultrasonic assistant according to claim 1 extracts the preparation method of facial mask whitewood's melon extract solution, and its feature exists
In the step（4）Described in extracting times be 1-2 suboptimums, carry the time be 0.5 ~ 1h it is optimal.
8. the microwave radiation exaraction facial mask according to claim 1 preparation method of whitewood's melon extract solution, it is characterised in that
The step（5）In, return pressure being evaporated under reduced pressure and controls in -1 ~ -0.8 MPa most preferably, evaporating temperature is 35 ~ 40 DEG C optimal.
9. ultrasonic assistant according to claim 1 extracts the preparation method of facial mask whitewood's melon extract solution, and its feature exists
In the step（6）Described in whitewood's melon extract solution organic solvent content should be less than 0.05%.
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| CN201710136427.8A CN106667857A (en) | 2017-03-08 | 2017-03-08 | Preparation method of white Chinese floweringquince extract for facial mask through microwave-assisted extraction |
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| CN201710136427.8A CN106667857A (en) | 2017-03-08 | 2017-03-08 | Preparation method of white Chinese floweringquince extract for facial mask through microwave-assisted extraction |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108969438A (en) * | 2018-08-23 | 2018-12-11 | 广东幸美化妆品股份有限公司 | Contain bletilla striata extract, white flower papaya extractives and anti-wrinkle cream of Herba Agrimoniae extract and preparation method thereof |
| CN109091449A (en) * | 2018-10-31 | 2018-12-28 | 广东巴松那生物科技有限公司 | A kind of set face cream and the sleep mask of gel and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108969438A (en) * | 2018-08-23 | 2018-12-11 | 广东幸美化妆品股份有限公司 | Contain bletilla striata extract, white flower papaya extractives and anti-wrinkle cream of Herba Agrimoniae extract and preparation method thereof |
| CN108969438B (en) * | 2018-08-23 | 2021-09-21 | 广东幸美化妆品股份有限公司 | Anti-wrinkle cream containing bletilla striata extract, chaenomeles speciosa extract and hairyvein agrimony extract and preparation method thereof |
| CN109091449A (en) * | 2018-10-31 | 2018-12-28 | 广东巴松那生物科技有限公司 | A kind of set face cream and the sleep mask of gel and preparation method thereof |
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Application publication date: 20170517 |