CN106176282A - Protein facial mask liquid and production method - Google Patents
Protein facial mask liquid and production method Download PDFInfo
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- CN106176282A CN106176282A CN201610693592.9A CN201610693592A CN106176282A CN 106176282 A CN106176282 A CN 106176282A CN 201610693592 A CN201610693592 A CN 201610693592A CN 106176282 A CN106176282 A CN 106176282A
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Abstract
Heavy source protein facial mask liquid disclosed by the invention, including basic recipe, described basic recipe be hyaluronate sodium 0.4 ~ 1.0%, PE9010 0.3 ~ 0.5%, surplus be water；Adding oligopeptide 1 in this basic recipe, the addition of described oligopeptide 1 is 1 ~ 20ug/mL.Adding pentapeptide 3 in described basic recipe, the addition of described pentapeptide 3 is 10 ~ 20ug/mL.Adding recombination human source collagen protein in described basic recipe, the addition of described recombination human source collagen protein is 0.05 ~ 0.1%.Adding hexapeptide 3 in described basic recipe, the addition of described hexapeptide 3 is 10ug/mL.The facial mask liquid of the present invention has quickly repairs damaged skin, increases moisture content of skin, skin care, improve dim complexion, tarnish, strengthen skin elasticity, firm skin, whitening and speckle dispelling, and have crease-resistant wrinkle resistant, anti-acne, goes cicatrix, the sun-proof and effectiveness of after-sun.
Description
Technical field
The invention belongs to cosmetic technical field, specially protein facial mask liquid and production method thereof.
Background technology
Facial film is the most common a kind of skin care item.Cover in the of short duration time of face mainly by it, outside being temporarily isolating
Boundary's environment, makes skin temperature raise, and skin pore is expanded, and accelerates sweat gland secretion and blood circulation, makes in skin oxygen content
Rise, accelerate to get rid of oil substances in the metabolic product of skin epidermis and skin.Meanwhile, the moisture in facial film, nutrition become
Divide, active component penetrates into epidermis cell, makes skin become soft, and it is flexible that skin is rich in gloss.
Facial film mainly has mud cream type, tear-pull, gel-type, four kinds of l Water Paper type at present.
Summary of the invention
It is an object of the invention to provide protein facial mask formula for a product and production technology thereof.These products are with recombination human source glue
Former albumen and oligopeptide-1, pentapeptide-3 or hexapeptide-3 albumen are main active substances, with hyaluronate sodium for major auxiliary burden composition.
The present invention adopts the following technical scheme that realization:
The basic recipe of recombiant protein facial mask liquid, comprises following component, is all weight percentage:
Hyaluronate sodium 0.4 ~ 1.0%,
Sensiva SC50 phenoxyethanol (PE 9010) 0.3 ~ 0.5%
Water surplus.
On the basis of above-mentioned basic recipe, add, according to each activated protein feature and ratio, the activity that different proportion is different
Albumen composition has the silk mask of different qualities.Specific as follows:
1, adding oligopeptide-1 in basic recipe, the addition of described oligopeptide-1 is 1 ~ 20 μ g/mL.
2, adding oligopeptide-1 and pentapeptide-3 in basic recipe, the addition of described oligopeptide-1 is 1 ~ 20 μ g/mL, described five
The addition of peptide-3 is 10 ~ 50 μ g/mL.
3, in basic recipe, oligopeptide-1, pentapeptide-3 and recombination human source collagen protein, the addition of described oligopeptide-1 are added
Being 1 ~ 20 μ g/mL, the addition of described pentapeptide-3 is 10 ~ 50 μ g/mL, and the addition of described recombination human source collagen protein is 0.01
~1%。
4, in basic recipe, oligopeptide-1, pentapeptide-3, recombination human source collagen protein and hexapeptide-3 are added, described oligopeptide-1
Addition is 1 ~ 20 μ g/mL, and the addition of described pentapeptide-3 is 10-50 μ g/mL, the addition of described recombination human source collagen protein
Being 0.01 ~ 1%, the addition of described hexapeptide-3 is 10 ~ 50 μ g/mL.
5, adding oligopeptide-1 and recombination human source collagen protein in basic recipe, the addition of described oligopeptide-1 is 1 ~ 20 μ
G/mL, the addition of described recombination human source collagen protein is 0.01 ~ 1%.
6, in basic recipe, oligopeptide-1, recombination human source collagen protein and hexapeptide-3, the addition of described oligopeptide-1 are added
Being 1 ~ 20 μ g/mL, the addition of described recombination human source collagen protein is 0.01 ~ 1%, and the addition of described hexapeptide-3 is 10 ~ 50 μ
g/mL。
Above-mentioned each money facial mask liquid production craft step is as follows:
1, during hyaluronate sodium is dissolved into pure water, homogenizing is stirred so that it is fully dissolve；
2, when 115 DEG C of sterilizings are down to 40 DEG C in 30 minutes；
3, add PE 9010 and each corresponding activated protein with the membrane filtration of 0.22 μm, then proceed to stir；
4, finally regulation pH value, between 5.5 to 6.0, gets product；Fill, sealing, packaging.
Hyaluronate sodium (Sodium Hyaluronate): for the material extracted from cockscomb, it is possible to pass through Lactococcus
Fermentation prepares, and for white or off-white color granule or powder, odorless, has the strongest hygroscopicity, is dissolved in water, insoluble in alcohol, ketone, second
The organic solvents such as ether.Its aqueous solution is electronegative, has the highest viscoelasticity, rheological characteristic and osmotic pressure during high concentration.At cosmetics
Field uses more, have moisture-keeping function.In the products such as the cream of cosmetics, frost, honey, milk, facial film, shampoo, have solely
Special keeps skin, the moisture of hair, makes skin moisturizing smooth, and fine and smooth tender, high resilience, hair is rich in gloss；Have simultaneously
Have and prevent chapped skin, wrinkle resistant crease-resistant, aesthetic health care and the effect of recovery skin physiology function.
PE 9010 is the liquid preservative used for cosmetic that phenoxyethanol and Sensiva SC50 are compounding, Sensiva SC50
Have impact on the surface tension on microbial cell film, thus improve the antiseptic power of phenoxyethanol.To antibacterial, yeast and mycete
There is the inhibitory action of wide spectrum equilibrium, be a kind of typical antibacterial aseptic production, also there is certain sterilizing ability simultaneously.PE
9010 is highly stable, not facile hydrolysis.Temperature and pH value had good toleration.Its favorable solubility, even if at low temperatures
Also can be well dispersed in each system.
The recombination human source collagen protein (hereinafter referred to as " collagen ") of the active component in each facial film of the present invention, for type III
Human collagen sequence is the sequence of long-term screening and optimizing, uses escherichia expression system, and the sequence in gene is for large intestine
Bacillus expression system has carried out codon optimized expression and has formed, and its preparation method is shown in 201210482543.2(recombination human source
Collagen protein and production method thereof) described in.There is extraordinary hydrophilic and stability, its aminoacid composition and natural collagen
Protein amino acid sequence appropriate section 100% is identical, is applied to human body and will not produce immunologic rejection and anaphylaxis, can be extensive
It is applied to biological medicine and cosmetic industry, the function of native protein can be exercised in human body.
Oligopeptide-1 of the active component in each facial film of the present invention, i.e. EGF(recombinant human epidermal growth factor).EGF can
Promote the proliferation and differentiation of cell, thus replace senile cell and the process of dead cell with regenerative cell.Traditional makeup rises
It is outside modification, it is impossible to fundamentally solve skin problem, and EGF applies and is based on human body skin in cosmetics
Physiological structure, on a molecular scale cell repaired and adjust, having and quickly repair damaged skin, improving repairing of skin
Multiple, nursing；Skin care, strengthens skin elasticity, calms down eye wrinkle-removing, firm skin；Whitening and speckle dispelling, sun-proof and after-sun；
And there is anti-acne, go cicatrix, shortening wound healing time and reduce the effect of cicatrization, be described as " beautiful by beauty treatment circle
The factor ".This oligopeptide-1 preparation method is shown in that 200810211603.0(prepares the side of dissolvable high activity recombinant human epidermal growth factor
Method) described in, repeat no more.
The pentapeptide-3 of active component in each facial film of the present invention, hexapeptide-3, although be all to act on anti-wrinkle, but
The approach passed through is different.Little molecule pentapeptide-3, beneficially skin absorption, there is stimulation collagen, elastic fibers and hyalomitome
Acid hypertrophy, increases skin elasticity, makes skin fine and smooth, tender, glossy；The preparation method of pentapeptide-3 is shown in 201410755706.9
Described in (defying age small peptide and preparation method thereof).Hexapeptide-3 can suppress the contraction of muscle thus reach to resist the effect of microgroove
Really, eye microgroove, cheilogramma can be desalinated, improve cutis laxa, sagging, increase skin elasticity, make skin moistening, smooth, recover thin
Greasy beautiful, the preparation method of hexapeptide-3 as 201510252409.7(smoothing wrinkle small peptide and preparation method thereof) described in.Often transport
Wrinkle produced by dynamic position, uses the meeting of Argireline effect more preferably, and usual no motion of position, use Wushengtai to have
More preferably effect.
The facial mask liquid of the present invention has quickly repairs damaged skin, increases moisture content of skin, skin care, improves complexion dark
Secretly, matt, strengthen skin elasticity, firm skin, whitening and speckle dispelling, and have crease-resistant wrinkle resistant, anti-acne, remove cicatrix, sun-proof
And the effectiveness of after-sun.
A kind of facial film, including face paper, described face paper infiltrates above-mentioned facial mask liquid.Described face paper is silkworm silk face
Film.
L Water Paper type is exactly the face paper infiltrating facial mask liquid of mmic package, and the face paper of this product is a kind of by silkworm silk system
Become, therefore belong to l Water Paper profile film.Silk mask, is mainly made up of silk fiber and activity fibroin.Due to fibroin
In containing 18 kinds of aminoacid of nutritive value great to human body, and be the splendid porous material of good permeability, water absorption,
And non-stimulated to skin, there is " artificial skin " laudatory title.Silk mask has the strongest adsorptivity, can carry attached more facial film elite
Liquid, applies face more comfortable, more firmly, does not haves and fall down and facial mask liquid drip phenomenon.Silk mask uses the softst exquisiteness
Silkworm silk, can be close to skin texture, therefore the highest at the docile degree of deposited face, and matter is thin, transparent, ventilative, and the wing of nose corners of the mouth can take
Note, lock water moisturizing is persistently deeply.And silk mask can accelerate the reparation of skin self, can be closed by the fine and smooth note of silk fiber
Impaired skin is allowed to rapidly be reparation.Heavier can promote the secretion of collagen protein, potent brighten, uvioresistant, antiinflammatory and pock
Ability.
The facial film of the present invention is reasonable in design, after only needing face cleaning, takes out facial film and spreads on face, make silk mask be close to face each
Place's skin, waits for percutaneous absorption facial mask liquid quietly, after 15-20min, removes facial film, No clean, be massaged into gently and absorb.
Detailed description of the invention
Below the specific embodiment of the present invention is described in detail.
Embodiment one
The basic recipe of facial film, comprises following component, is all weight percentage:
Hyaluronate sodium 1%,
Sensiva SC50 phenoxyethanol (PE9010) 0.35%
Water surplus.
On the basis of above-mentioned basic recipe, add, according to each activated protein feature and ratio, the activity that different proportion is different
Albumen composition have different qualities silk mask (amount of active component according to cosmetics usual amounts, produce facial film characteristic and
Depending on cost).
1, Re Origin Wushengtai biology skin rejuvenating facial mask
Add in basic recipe: pentapeptide-3 20 μ g/mL
Oligopeptide-1 1 μ g/mL
2, Re Origin Argireline biology compacts facial film
Add in basic recipe: hexapeptide-3 20 μ g/mL
Collagen 0.05%
Oligopeptide-1 1 μ g/mL
3, the bionical facial film of Re Origin collagen protein
Add in basic recipe: collagen 0.1%
Oligopeptide-1 1 μ g/mL
4, Re Origin hyaluronic acid moisturizing skin rejuvenating facial mask
Add in basic recipe: oligopeptide-1 15 μ g/mL
5, Re Origin polypeptide Face-protecting mask
Add in basic recipe: pentapeptide-3 10 μ g/mL
Hexapeptide-3 10 μ g/mL
Collagen 0.05%
Oligopeptide-1 1 μ g/mL
6, Wushengtai stock solution facial film
Add in basic recipe: pentapeptide-3 20 μ g/mL
Oligopeptide-1 1 μ g/mL
7, Argireline stock solution facial film
Add in basic recipe: hexapeptide-3 20 μ g/mL
Collagen 0.05%
Oligopeptide-1 1 μ g/mL
8, customized bioprotein facial film (preservative free)
Add in basic recipe: hexapeptide-3 20 μ g/mL
Collagen 0.1%
Oligopeptide-1 1 μ g/mL
9, customized bionic facial film (preservative free)
Add in basic recipe: pentapeptide-3 20 μ g/mL
Collagen 0.1%
Oligopeptide-1 1 μ g/mL
Embodiment two
The basic recipe of facial film, comprises following component, is all weight percentage:
Hyaluronate sodium 0.8%,
Sensiva SC50 phenoxyethanol (PE9010) 0.3%
Water surplus.
On the basis of above-mentioned basic recipe, add, according to each activated protein feature and ratio, the activity that different proportion is different
Albumen composition have different qualities silk mask (amount of active component according to cosmetics usual amounts, produce facial film characteristic and
Depending on cost).
Embodiment three
The basic recipe of facial film, comprises following component, is all weight percentage:
Hyaluronate sodium 0.4%,
Sensiva SC50 phenoxyethanol (PE9010) 0.5%
Water surplus.
On the basis of above-mentioned basic recipe, add, according to each activated protein feature and ratio, the activity that different proportion is different
Albumen composition have different qualities silk mask (amount of active component according to cosmetics usual amounts, produce facial film characteristic and
Depending on cost).
Embodiment four
The basic recipe of facial film, comprises following component, is all weight percentage:
Hyaluronate sodium 0.6%,
Sensiva SC50 phenoxyethanol (PE9010) 0.4%
Water surplus.
On the basis of above-mentioned basic recipe, add, according to each activated protein feature and ratio, the activity that different proportion is different
Albumen composition have different qualities silk mask (amount of active component according to cosmetics usual amounts, produce facial film characteristic and
Depending on cost).
Each money facial mask liquid production technology, step is as follows:
(1), hyaluronate sodium be dissolved in pure water, stir homogenizing so that it is fully dissolve；
(2) when, 115 DEG C of sterilizings are down to 40 DEG C in 30 minutes；
(3), add PE9010 and each corresponding activated protein with the membrane filtration of 0.22 μm, then proceed to stir；
(4), finally regulation pH value, between 5.5 to 6.0, gets product；
(5), fill, sealing, packaging.
A kind of facial film, including face paper, described face paper infiltrates above-mentioned facial mask liquid.Face paper selects silk mask.
It should be noted last that, above example is only in order to illustrate technical scheme and unrestricted, although ginseng
It is described in detail according to the embodiment of the present invention, it will be understood by those within the art that, to technical scheme
Modifying or equivalent, without departure from the spirit and scope of technical scheme, it all should contain the present invention's
In claims.
Claims (9)
1. a protein facial mask liquid, it is characterised in that: include basic recipe, described basic recipe be hyaluronate sodium 0.4 ~
1.0%, PE9010 0.3 ~ 0.5%, surplus are water；
Adding oligopeptide-1 in this basic recipe, the addition of described oligopeptide-1 is 1 ~ 20 μ g/mL.
Protein facial mask liquid the most according to claim 1, it is characterised in that: described basic recipe adds pentapeptide-3, described
The addition of pentapeptide-3 is 10 ~ 50 μ g/mL.
Protein facial mask liquid the most according to claim 2, it is characterised in that: described basic recipe adds recombination human source collagen
Albumen, the addition of described recombination human source collagen protein is 0.01 ~ 1%.
Protein facial mask liquid the most according to claim 3, it is characterised in that: described basic recipe adds hexapeptide-3, described
The addition of hexapeptide-3 is 10 ~ 50 μ g/mL.
Protein facial mask liquid the most according to claim 1, it is characterised in that: described basic recipe adds recombination human source collagen
Albumen, the addition of described recombination human source collagen protein is 0.01 ~ 1%.
Protein facial mask liquid the most according to claim 5, it is characterised in that: described basic recipe adds hexapeptide-3, described
The addition of hexapeptide-3 is 10 ~ 50 μ g/mL.
7. the arbitrary described protein facial mask liquid and preparation method thereof of claim 1-6, it is characterised in that: comprise the steps:
(1), hyaluronate sodium be dissolved in pure water, stir homogenizing so that it is fully dissolve；
When 115 DEG C of sterilizings are down to 40 DEG C in 30 minutes；
(2), add PE9010 and each corresponding activated protein with the membrane filtration of 0.22 μm, then proceed to stir；
(3), finally regulation pH value, between 5.5 to 6.0, gets product.
8. a facial film, including face paper, it is characterised in that: infiltration facial mask liquid described in claim 1-6 on described face paper.
Facial film the most according to claim 8, it is characterised in that: described face paper is silk mask.
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| CN201610693592.9A CN106176282B (en) | 2016-08-19 | 2016-08-19 | Protein powder film liquid and production method |
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| CN201610693592.9A CN106176282B (en) | 2016-08-19 | 2016-08-19 | Protein powder film liquid and production method |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108085973A (en) * | 2018-01-13 | 2018-05-29 | 成光耀 | A kind of nti-freckle silk mask of high-moisture-retention |
| CN110960443A (en) * | 2019-12-26 | 2020-04-07 | 广州领衔生物科技有限公司 | Composition containing recombinant human collagen, freeze-dried material, preparation method of freeze-dried material and cosmetic |
| CN111374933A (en) * | 2020-04-06 | 2020-07-07 | 陕西斯戴木生物科技有限公司 | Improved silk mask with high water retention and high freckle removing activity |
| CN111658573A (en) * | 2020-06-17 | 2020-09-15 | 广州艾尔亿医药有限公司 | Human-like serum protein preparation for regenerative medicine cosmetology |
| CN113456522A (en) * | 2021-05-19 | 2021-10-01 | 太原理工大学 | Hand cream with recombinant human collagen as nutrient component and preparation method thereof |
| CN113509545A (en) * | 2021-06-23 | 2021-10-19 | 哈尔滨运美达生物科技有限公司 | Medical recombinant collagen repair patch and essence of medical recombinant collagen repair patch and preparation methods of medical recombinant collagen repair patch and essence |
| CN113520899A (en) * | 2021-03-25 | 2021-10-22 | 甘肃天际生物科技有限公司 | Recombinant collagen product for skin photodamage repair |
| CN114632037A (en) * | 2021-12-29 | 2022-06-17 | 佛山市南海朗肽生物制药工程研究院有限公司 | Repairing and relieving mask composition, freeze-dried mask and preparation method of freeze-dried mask |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108085973A (en) * | 2018-01-13 | 2018-05-29 | 成光耀 | A kind of nti-freckle silk mask of high-moisture-retention |
| CN110960443A (en) * | 2019-12-26 | 2020-04-07 | 广州领衔生物科技有限公司 | Composition containing recombinant human collagen, freeze-dried material, preparation method of freeze-dried material and cosmetic |
| CN111374933A (en) * | 2020-04-06 | 2020-07-07 | 陕西斯戴木生物科技有限公司 | Improved silk mask with high water retention and high freckle removing activity |
| CN111658573A (en) * | 2020-06-17 | 2020-09-15 | 广州艾尔亿医药有限公司 | Human-like serum protein preparation for regenerative medicine cosmetology |
| CN113520899A (en) * | 2021-03-25 | 2021-10-22 | 甘肃天际生物科技有限公司 | Recombinant collagen product for skin photodamage repair |
| CN113456522A (en) * | 2021-05-19 | 2021-10-01 | 太原理工大学 | Hand cream with recombinant human collagen as nutrient component and preparation method thereof |
| CN113509545A (en) * | 2021-06-23 | 2021-10-19 | 哈尔滨运美达生物科技有限公司 | Medical recombinant collagen repair patch and essence of medical recombinant collagen repair patch and preparation methods of medical recombinant collagen repair patch and essence |
| CN114632037A (en) * | 2021-12-29 | 2022-06-17 | 佛山市南海朗肽生物制药工程研究院有限公司 | Repairing and relieving mask composition, freeze-dried mask and preparation method of freeze-dried mask |
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Address after: 030032 No.18, Jinbo street, Tanghuai Park, Taiyuan comprehensive reform demonstration zone, Taiyuan City, Shanxi Province Patentee after: SHANXI JINBO BIOMEDICAL Co.,Ltd. Address before: 030032 Shanxi city of Taiyuan province by the economic and Technological Development Zone No. 18 North Street Patentee before: SHANXI JINBO BIOMEDICAL Co.,Ltd. |