CN106165965A - A kind of nano-negative ion bristle formula and preparation technology - Google Patents

A kind of nano-negative ion bristle formula and preparation technology Download PDF

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Publication number
CN106165965A
CN106165965A CN201610766111.2A CN201610766111A CN106165965A CN 106165965 A CN106165965 A CN 106165965A CN 201610766111 A CN201610766111 A CN 201610766111A CN 106165965 A CN106165965 A CN 106165965A
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China
Prior art keywords
grams
nano
powder
weight
gram
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CN201610766111.2A
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Chinese (zh)
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CN106165965B (en
Inventor
梁超军
梁超杰
丁胡红
肖问问
肖春晓
闫金丹
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Dongguan City Is Daily Use Products Co Ltd
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Dongguan City Is Daily Use Products Co Ltd
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    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/006Antimicrobial, disinfectant bristles, handle, bristle-carrier or packaging
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/02Bristles details
    • A46D1/0207Bristles characterised by the choice of material, e.g. metal
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/04Preparing bristles
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/04Preparing bristles
    • A46D1/045Cleaning, e.g. washing, drying
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/04Preparing bristles
    • A46D1/06Machines or apparatus for cutting bristles

Landscapes

  • Cosmetics (AREA)

Abstract

The invention discloses a kind of nano-negative ion bristle formula, calculate by weight, including following component thermoplastic polyester granulate, 25 grams to 60 grams;Nanometer anion powder solution, 19 grams to 30 grams;Couplant, 1.5 grams to 10 grams;Nano-magnetic powder, 1.5 grams to 5 grams;Corallium Japonicum Kishinouye nano powder, 1.5 grams to 2 grams;Nanometer Margarita powder, 1.5 grams to 3 grams.The preparation technology of the present invention is simple, cheap, prove through statistics, the antibacterial effect of the present invention has the probability of more than 99% to be higher than the antibacterial effect of normal bristles, having the skin of human body blood circulation promoting, stimulate the function such as cell regeneration, slow down aging, economic worth is high.

Description

A kind of nano-negative ion bristle formula and preparation technology
Technical field
The present invention relates to bristle preparation technology, prescription, antimicrobial technology field, particularly relate to a kind of nano-negative ion bristle and join Side and preparation technology.
Background technology
Nanometer anion powder is by nanotechnology elaborate by natural material.Scientific investigations showed that, nano-negative ion Human body is kept energetic and to human residential environment improvement to have great help by powder.
Nano-negative ion gram has good effect, also has good effect especially for health care, beauty treatment fields.? Hairbrush used in field of cleaning chemical products, the beauty treatment fields such as beauty treatment, face cleaning, due to direct and the contact skin of human body, its matter Amount and skin effect, health preserving effect, health-care effect, most important for user, during life-time service hairbrush, even can be to trouble Person causes subtle impact, and existing hairbrush, its antibacterial ability is more weak, and this problems demand solves.
Summary of the invention
It is an object of the invention to overcome the deficiency of above-mentioned prior art to provide a kind of nano-negative ion bristle formula, this Invention uses nanometer silver technology to carry out strengthening the anti-microbial property of the cilium of hairbrush, and antibacterial effect is outstanding, has spectrum antibacterial effect Really, population density and kind, cleaning health again, the very useful convenience of microorganism on hairbrush are reduced.
For achieving the above object, the present invention provides a kind of nano-negative ion bristle formula, calculates by weight, including following group Point:
Thermoplastic polyester granule, 25 grams to 60 grams;
Nanometer anion powder solution, 19 grams to 30 grams;
Couplant, 1.5 grams to 10 grams;
Nano-magnetic powder, 1.5 grams to 5 grams;
Corallium Japonicum Kishinouye nano powder, 1.5 grams to 2 grams;
Nanometer Margarita powder, 1.5 grams to 3 grams.
Preferably, calculate by weight, also comprise the following components: hyaluronic acid, 1 gram to 3 gram.
Preferably, calculate by weight, also comprise the following components: there is the Chinese herbal medicine extract dry powder of fungistatic effect, 0.2 gram To 0.5 gram.
Preferably, calculate by weight, also comprise the following components: natural perfume material, 0.1 gram to 0.2 gram.
Preferably, calculate by weight, also comprise the following components: polynucleotide extract dry powder, 0.01 gram to 0.03 gram.
Preferably, calculate by weight, also comprise the following components: soft agent, 1 gram to 10 gram.
Preferably, calculating by weight, described thermoplastic polyester granule is PBT granule.
The present invention provides the preparation technology of a kind of nano-antibacterial bristle, comprises the steps:
S801, by weight, adds mixer by PBT granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder;Add The nanometer anion powder solution of 30%;Drying, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing;
S802, cuts into chunks according to customization size, utilizes sodium hydroxide to burn a mao peak, then utilize organic acid to clean;
S803, put into dye vat equipment dyeing, add after fixation 30% nanometer anion powder solution and 30% couplant pass through High temperature dye vat is warmed up to 80 to 110 degree insulation 30 minutes;
S804, again cleans, is dehydrated, enters baking box 110 degree baking drying in 100 minutes.
Preferably, comprise the steps:
S801, by weight, by PBT granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder, hyaluronic acid, Chinese herbal medicine Extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent add mixer;The nanometer anion powder of addition 30% is molten Liquid, mixes 40 minutes;Drying 1.5 hours, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing;
S802, cuts into chunks according to customization size, utilizes sodium hydroxide to burn a mao peak, then utilize organic acid to clean, then with swashing Light subtracts material process equipment and repairs a mao peak further;
S803, put into dye vat equipment dyeing, add after fixation 30% nanometer anion powder solution and 30% couplant pass through High temperature dye vat is warmed up to 80 to 110 degree insulation 30 minutes;
S804, again cleans, is dehydrated, enters baking box 110 degree baking drying in 100 minutes.
The invention has the beneficial effects as follows:
Its antibacterial abilities of product such as 1, the preparation technology of the present invention is simple, cheap, this technique the hairbrush prepared are outstanding, Contribute to the clean hygiene of user, and avoid skin infection.
2, by arranging nano-magnetic powder, the hairbrush of the present invention also skin to human body has the effect of magnetic therapy physical therapy.Pass through Arranging Corallium Japonicum Kishinouye nano powder can be using hairbrush when, and penetrate to the skin surface by the element of Corallium Japonicum Kishinouye;By arranging Margarita powder, Nanometer Margarita powder can be stretched in Skin Cell.Play good whitening effect.By arranging Chinese herbal medicine extract dry powder, when When hairbrush contacts with the trace perspiration of body surface, can medicinal herb components be penetrated in skin, as having the Chinese herbal medicine of whitening composition Component.By adding natural perfume material, the bristle of the present invention has good fragrant breath.By mixing polynucleotide extract, can With in use, supplement a certain amount of polynucleotide material for skin, play good health-care effect.
3, proving through statistics, the antibacterial effect of the present invention has the probability of more than 99% to be higher than the antibacterial of normal bristles Effect, anti-microbial property is superior.
4, the used bristle of cosmetic brush is all made by filling material, traditional handicraft in the market, along with the development of society, Mankind's pursuit to quality of the life, the attention to safety, we, through the research and development of 2 years, have devised nano-negative ion bristle, The fields such as cosmetic brush, wig makeups instrument, accessory will be applicable to.
Nano-negative ion bristle active component in anion of the present invention, is widely used in medical treatment, and proves safe and efficient, right No skin irritation, nontoxic, without anaphylaxis, in use, the skin of human body is had blood circulation promoting, stimulate thin The functions such as born of the same parents' regeneration, slow down aging, economic worth is high.The present invention demonstrates its antibacterial effect by statistics.
Accompanying drawing explanation
Fig. 1 is the experiment effect figure of one embodiment of the invention, and abscissa represents group, and 1 to 4 group represents hairbrush D respectively Group, hairbrush A group, hairbrush B group, hairbrush C group;Vertical coordinate represents microorganism concn rank, and 10 grades of representatives are the highest.
Detailed description of the invention
Embodiment one: formula and preparation technology
  Prescription A(gram) Prescription B(gram) Prescription C(gram)
PBT granule 25 50 60
Nanometer silver antimicrobial liquid 19 25 30
Nano-magnetic powder 1.5 3 5
Corallium Japonicum Kishinouye nano powder 1.5 1.5 2
Nanometer Margarita powder 1.5 2 3
Hyaluronic acid 1.5 1.5 2
There is the Chinese herbal medicine extract dry powder of fungistatic effect 0.2 0.3 0.5
Natural perfume material 0.1 0.15 0.2
Polynucleotide extract dry powder 0.01 0.02 0.03
Soft agent 2 5 10
Couplant 1.5 5 20
Preparation technology is as follows: S801, by weight, by PBT granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder, thoroughly The acid of bright matter, Chinese herbal medicine extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent add mixer;Add 30% Nanometer anion powder solution, mixes 40 minutes;Drying 1.5 hours, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing;S802, according to fixed Size processed is cut into chunks, and utilizes sodium hydroxide to burn a mao peak, then utilizes organic acid to clean, then subtracts material process equipment with laser and enter One step finishing hair peak;S803, puts into the dyeing of dye vat equipment, adds 30% nanometer anion powder solution and the coupling of 30% after fixation Mixture is warmed up to 80 to 110 degree insulation 30 minutes by high temperature dye vat;S804, again cleans, is dehydrated, enters baking box 110 degree baking Within roasting 100 minutes, dry.Wherein, organic acid is citric acid.Nanometer anion powder solution is that mass concentration represents.
Embodiment two: antibacterial effect experimental design
Take microorganism nature culture (containing human body surface, such as the multiple-microorganism of facial surface);Prepare various culture Suspension;Prepare hairbrush A, hairbrush B, hairbrush C respectively by component A, component B, component C, and select commercially available common hair Brush D, it is ensured that the specification of four kinds of hairbrush is identical.Soak certain time in suspension with hairbrush, such as 30 minutes, 60 minutes, 180 points Clock.Take out hairbrush, clean with tap water slowly.Dry, then, hairbrush is carried out in the container determine volume ultrasonic waves for cleaning (cleanout fluid constant volume), after cleaning, the liquid in extracting container, count with cell counting count board under the microscope, will The number of cell carries out classification, is divided into 1 to 10 grade, and 1 grade of density is minimum, and 10 grades of density are the highest.Often group hairbrush selects 20 hairbrush, altogether Four groups, totally 80 hairbrush.10 grades of concentration are defined as the cell concentration after suspension directly dilutes.With dividing otherwise, intuitively Express microorganism residual quantity.Certainly the anti-microbial property for the microorganism such as escherichia coli, staphylococcus aureus can also be verified.
Embodiment three: experimental result
  Hairbrush D group Hairbrush A group Hairbrush B group Hairbrush C group
1 9.75 6.79 4.05 1.29
2 9.44 6.53 4.65 1.17
3 9.43 5.80 5.40 2.39
4 9.65 6.37 4.36 1.73
5 9.50 5.38 4.49 2.41
6 9.55 6.30 4.16 2.96
7 9.42 5.10 5.45 2.34
8 9.29 6.45 5.00 1.59
9 9.45 6.39 4.70 1.42
10 9.49 5.19 5.26 1.51
11 9.17 6.77 5.50 1.44
12 9.80 5.29 4.43 1.21
13 9.20 6.52 4.91 1.68
14 9.26 6.20 4.69 1.90
15 9.69 5.74 4.18 2.65
16 9.70 6.04 5.27 1.29
17 9.23 5.10 4.36 1.39
18 9.57 5.23 4.66 2.36
19 9.34 5.38 5.44 2.96
20 9.23 5.27 4.19 2.30
Maximum 9.80 6.79 5.50 2.96
Minima 9.17 5.10 4.05 1.17
Meansigma methods 9.46 5.89 4.76 1.90
Standard deviation 0.1877574 0.589412346 0.47656 0.57773
Above-mentioned experimental result is the experimental data drawn on the experimental design of embodiment two, and soak time uses 30 minutes.
Embodiment four: statistics conclusion
Referring to Fig. 1, Fig. 1 is data process figures, from Fig. 1, it is also possible to find 1 to 4 groups (i.e. D group, A group, B group, C group), its Meansigma methods reduces (bacteria containing amount level) successively.
Additionally, carry out statistical test (T inspection), P=1.9811E-18 < 0.01 between A group and D group, illustrate at A group and D Group has significant difference, say, that in statistics, and its antibacterial ability of the hairbrush of A group has 99% with the antibacterial ability of D group Probability there is significant difference, wherein D group is matched group, and the antibacterial ability of A group is significantly better than the antibacterial ability of D group.
Carry out T inspection between B group and D group, between P=2.552E-24 < 0.01, C group and D, carry out T inspection, P= 4.73419E-26 < 0.01, illustrates that B group, the antibacterial ability of C group and the antibacterial ability of D group have the probability of 99% to have significantly The difference of property, B group, the antibacterial ability of C group are significantly better than the antibacterial ability of D group.
Although above it has been shown and described that embodiments of the invention, it is to be understood that above-described embodiment is example Property, it is impossible to be interpreted as limitation of the present invention, those of ordinary skill in the art is without departing from the principle of the present invention and objective In the case of above-described embodiment can be changed within the scope of the invention, revise, replace and modification.

Claims (9)

1. a nano-negative ion bristle formula, it is characterised in that calculate by weight, including following component:
Thermoplastic polyester granule, 25 grams to 60 grams;
Nanometer anion powder solution, 19 grams to 30 grams;
Couplant, 1.5 grams to 10 grams;
Nano-magnetic powder, 1.5 grams to 5 grams;
Corallium Japonicum Kishinouye nano powder, 1.5 grams to 2 grams;
Nanometer Margarita powder, 1.5 grams to 3 grams.
Nano-negative ion bristle formula the most according to claim 1, it is characterised in that calculate by weight, also include as follows Component: hyaluronic acid, 1 gram to 3 gram.
Nano-negative ion bristle formula the most according to claim 2, it is characterised in that calculate by weight, also include as follows Component: there is the Chinese herbal medicine extract dry powder of fungistatic effect, 0.2 gram to 0.5 gram.
Nano-negative ion bristle formula the most according to claim 3, it is characterised in that calculate by weight, also include as follows Component: natural perfume material, 0.1 gram to 0.2 gram.
Nano-negative ion bristle formula the most according to claim 3, it is characterised in that calculate by weight, also include as follows Component: polynucleotide extract dry powder, 0.01 gram to 0.03 gram.
Nano-negative ion bristle formula the most according to claim 3, it is characterised in that calculate by weight, also include as follows Component: soft agent, 2 grams to 10 grams.
7. according to the nano-negative ion bristle formula described in any one of claim 1 to 6, it is characterised in that calculate by weight, institute Stating thermoplastic polyester granule is PBT granule.
8. the preparation technology of a nano-antibacterial bristle, it is characterised in that comprise the steps:
S801, by weight, adds mixer by PBT granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder;Add The nanometer anion powder solution of 30%;Drying, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing;
S802, cuts into chunks according to customization size, utilizes sodium hydroxide to burn a mao peak, then utilize organic acid to clean;
S803, put into dye vat equipment dyeing, add after fixation 30% nanometer anion powder solution and 30% couplant pass through High temperature dye vat is warmed up to 80 to 110 degree insulation 30 minutes;
S804, again cleans, is dehydrated, enters baking box 110 degree baking drying in 100 minutes.
The preparation technology of a kind of nano-antibacterial bristle the most according to claim 8, it is characterised in that comprise the steps:
S801, by weight, by PBT granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder, hyaluronic acid, Chinese herbal medicine Extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent add mixer;The nanometer anion powder of addition 30% is molten Liquid, mixes 40 minutes;Drying 1.5 hours, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing;
S802, cuts into chunks according to customization size, utilizes sodium hydroxide to burn a mao peak, then utilize organic acid to clean, then with swashing Light subtracts material process equipment and repairs a mao peak further;
S803, put into dye vat equipment dyeing, add after fixation 30% nanometer anion powder solution and 30% couplant pass through High temperature dye vat is warmed up to 80 to 110 degree insulation 30 minutes;
S804, again cleans, is dehydrated, enters baking box 110 degree baking drying in 100 minutes.
CN201610766111.2A 2016-08-31 2016-08-31 A kind of nano-negative ion bristle and preparation process Active CN106165965B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106859016A (en) * 2017-03-15 2017-06-20 安徽省潜山县鑫烨塑刷有限公司 A kind of magnetic brush filament and its production technology
CN107557899A (en) * 2017-09-26 2018-01-09 枣庄正和制刷有限公司 A kind of preparation technology of nylon flush for rolling brush
WO2018112811A1 (en) * 2016-12-22 2018-06-28 东莞市正和日用制品有限公司 Negative-ion nanobristle formula and preparation process
CN110338555A (en) * 2019-07-29 2019-10-18 上海晓邦家居用品有限公司 A kind of preparation method of double end brush filament
CN110863262A (en) * 2019-11-25 2020-03-06 安徽三和刷业有限公司 Nanometer negative ion brush hair for brush and preparation method thereof
CN112120393A (en) * 2020-09-24 2020-12-25 孙国涛 Imitative ecological quick-drying anion silk cosmetic brush

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009285445A (en) * 2008-04-28 2009-12-10 Fuji Chemical Kk Anti-bacterial make-up brush and method of manufacturing brush bristle
CN201767325U (en) * 2010-06-18 2011-03-23 骆敬华 Nanometer negative ion antibacterial health-care toothbrush
CN102462151A (en) * 2010-11-05 2012-05-23 Hct亚洲有限公司 Brush with magnetic filaments

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009285445A (en) * 2008-04-28 2009-12-10 Fuji Chemical Kk Anti-bacterial make-up brush and method of manufacturing brush bristle
CN201767325U (en) * 2010-06-18 2011-03-23 骆敬华 Nanometer negative ion antibacterial health-care toothbrush
CN102462151A (en) * 2010-11-05 2012-05-23 Hct亚洲有限公司 Brush with magnetic filaments

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018112811A1 (en) * 2016-12-22 2018-06-28 东莞市正和日用制品有限公司 Negative-ion nanobristle formula and preparation process
CN106859016A (en) * 2017-03-15 2017-06-20 安徽省潜山县鑫烨塑刷有限公司 A kind of magnetic brush filament and its production technology
CN107557899A (en) * 2017-09-26 2018-01-09 枣庄正和制刷有限公司 A kind of preparation technology of nylon flush for rolling brush
CN110338555A (en) * 2019-07-29 2019-10-18 上海晓邦家居用品有限公司 A kind of preparation method of double end brush filament
CN110863262A (en) * 2019-11-25 2020-03-06 安徽三和刷业有限公司 Nanometer negative ion brush hair for brush and preparation method thereof
CN112120393A (en) * 2020-09-24 2020-12-25 孙国涛 Imitative ecological quick-drying anion silk cosmetic brush

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